data_nl-5_p_01 _diffrn_source_target Cu _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 1.540598 _diffrn_radiation_type 'Cu K\a~1+2~' _pd_instr_cons_illum_flag yes _pd_instr_var_illum_len 10.000 _pd_meas_2theta_range_min 10.02000000 _pd_meas_2theta_range_max 90.00000000 _pd_meas_2theta_range_inc 0.02000000 _pd_proc_2theta_range_min 10.02000000 _pd_proc_2theta_range_max 90.00000000 _pd_proc_2theta_range_inc 0.02000000 loop_ _pd_meas_intensity_total 166.4100 163.8400 156.2500 166.4100 161.2900 174.2400 171.6100 153.7600 171.6100 174.2400 163.8400 148.8400 176.8900 190.4400 198.8100 166.4100 144.0000 148.8400 134.5600 136.8900 171.6100 161.2900 174.2400 166.4100 148.8400 171.6100 169.0000 156.2500 153.7600 169.0000 179.5600 182.2500 146.4100 141.6100 176.8900 163.8400 136.8900 169.0000 182.2500 151.2900 184.9600 144.0000 161.2900 161.2900 148.8400 184.9600 184.9600 176.8900 171.6100 169.0000 176.8900 166.4100 163.8400 144.0000 169.0000 151.2900 166.4100 158.7600 161.2900 174.2400 156.2500 132.2500 163.8400 161.2900 193.2100 169.0000 184.9600 171.6100 190.4400 187.6900 184.9600 148.8400 163.8400 153.7600 201.6400 179.5600 184.9600 182.2500 198.8100 171.6100 153.7600 176.8900 153.7600 179.5600 182.2500 184.9600 182.2500 179.5600 163.8400 166.4100 187.6900 193.2100 174.2400 163.8400 176.8900 156.2500 158.7600 161.2900 148.8400 151.2900 136.8900 144.0000 129.9600 151.2900 148.8400 139.2400 121.0000 151.2900 151.2900 144.0000 125.4400 134.5600 134.5600 141.6100 161.2900 136.8900 139.2400 139.2400 151.2900 151.2900 156.2500 153.7600 116.6400 129.9600 123.2100 136.8900 151.2900 139.2400 146.4100 136.8900 132.2500 132.2500 141.6100 129.9600 132.2500 116.6400 132.2500 136.8900 121.0000 127.6900 129.9600 134.5600 146.4100 132.2500 136.8900 134.5600 114.4900 136.8900 121.0000 108.1600 136.8900 106.0900 123.2100 123.2100 121.0000 100.0000 121.0000 90.2500 118.8100 144.0000 114.4900 96.0400 125.4400 121.0000 104.0400 102.0100 129.9600 106.0900 127.6900 121.0000 116.6400 121.0000 136.8900 114.4900 125.4400 125.4400 125.4400 112.3600 112.3600 136.8900 136.8900 121.0000 129.9600 129.9600 116.6400 121.0000 127.6900 106.0900 127.6900 125.4400 102.0100 129.9600 112.3600 129.9600 136.8900 141.6100 112.3600 141.6100 100.0000 136.8900 139.2400 156.2500 163.8400 132.2500 134.5600 174.2400 134.5600 179.5600 187.6900 163.8400 193.2100 210.2500 231.0400 256.0000 320.4100 275.5600 268.9600 252.8100 225.0000 187.6900 144.0000 123.2100 144.0000 104.0400 125.4400 129.9600 88.3600 121.0000 108.1600 106.0900 139.2400 121.0000 118.8100 118.8100 121.0000 121.0000 108.1600 123.2100 125.4400 102.0100 123.2100 90.2500 110.2500 121.0000 108.1600 112.3600 106.0900 127.6900 110.2500 114.4900 121.0000 121.0000 104.0400 114.4900 102.0100 110.2500 136.8900 110.2500 106.0900 110.2500 104.0400 106.0900 118.8100 121.0000 129.9600 134.5600 112.3600 100.0000 118.8100 121.0000 112.3600 116.6400 129.9600 90.2500 104.0400 129.9600 104.0400 118.8100 118.8100 104.0400 108.1600 118.8100 114.4900 100.0000 106.0900 134.5600 108.1600 94.0900 108.1600 102.0100 116.6400 100.0000 102.0100 92.1600 104.0400 114.4900 100.0000 98.0100 96.0400 92.1600 98.0100 108.1600 81.0000 112.3600 96.0400 96.0400 114.4900 86.4900 118.8100 102.0100 116.6400 94.0900 114.4900 100.0000 98.0100 106.0900 104.0400 104.0400 104.0400 102.0100 110.2500 108.1600 98.0100 84.6400 94.0900 100.0000 102.0100 102.0100 106.0900 104.0400 98.0100 96.0400 90.2500 114.4900 90.2500 110.2500 112.3600 102.0100 100.0000 92.1600 123.2100 114.4900 100.0000 129.9600 102.0100 94.0900 112.3600 102.0100 106.0900 94.0900 90.2500 96.0400 132.2500 104.0400 102.0100 102.0100 118.8100 125.4400 121.0000 116.6400 127.6900 125.4400 125.4400 148.8400 139.2400 139.2400 171.6100 187.6900 161.2900 166.4100 184.9600 163.8400 156.2500 129.9600 146.4100 123.2100 129.9600 132.2500 102.0100 123.2100 112.3600 110.2500 112.3600 112.3600 94.0900 129.9600 148.8400 118.8100 144.0000 158.7600 144.0000 184.9600 163.8400 169.0000 166.4100 210.2500 193.2100 243.3600 246.4900 306.2500 331.2400 388.0900 479.6100 561.6900 681.2100 846.8100 1089.0000 1354.2400 1616.0400 1764.0000 1648.3600 1296.0000 1024.0000 655.3600 449.4400 292.4100 198.8100 163.8400 127.6900 127.6900 118.8100 92.1600 116.6400 110.2500 106.0900 104.0400 132.2500 110.2500 114.4900 106.0900 106.0900 104.0400 90.2500 90.2500 116.6400 98.0100 98.0100 84.6400 90.2500 98.0100 112.3600 92.1600 102.0100 102.0100 92.1600 108.1600 98.0100 106.0900 110.2500 104.0400 114.4900 121.0000 121.0000 121.0000 125.4400 116.6400 116.6400 86.4900 98.0100 102.0100 108.1600 90.2500 75.6900 90.2500 110.2500 106.0900 98.0100 94.0900 88.3600 84.6400 84.6400 77.4400 98.0100 86.4900 86.4900 110.2500 94.0900 94.0900 94.0900 84.6400 88.3600 102.0100 92.1600 96.0400 90.2500 92.1600 94.0900 86.4900 100.0000 92.1600 96.0400 86.4900 112.3600 116.6400 92.1600 127.6900 98.0100 110.2500 123.2100 104.0400 118.8100 129.9600 127.6900 118.8100 125.4400 156.2500 144.0000 121.0000 146.4100 136.8900 127.6900 118.8100 132.2500 136.8900 114.4900 110.2500 118.8100 108.1600 118.8100 100.0000 110.2500 114.4900 116.6400 82.8100 98.0100 108.1600 94.0900 92.1600 96.0400 94.0900 108.1600 116.6400 90.2500 127.6900 129.9600 127.6900 153.7600 136.8900 106.0900 129.9600 156.2500 123.2100 123.2100 127.6900 163.8400 201.6400 210.2500 196.0000 225.0000 243.3600 265.6900 252.8100 231.0400 234.0900 219.0400 196.0000 198.8100 201.6400 163.8400 148.8400 153.7600 132.2500 121.0000 118.8100 106.0900 129.9600 104.0400 104.0400 100.0000 108.1600 102.0100 106.0900 108.1600 102.0100 100.0000 98.0100 102.0100 123.2100 102.0100 125.4400 90.2500 102.0100 108.1600 90.2500 121.0000 114.4900 114.4900 123.2100 156.2500 125.4400 139.2400 158.7600 141.6100 184.9600 219.0400 228.0100 201.6400 216.0900 249.6400 259.2100 292.4100 262.4400 275.5600 309.7600 282.2400 309.7600 324.0000 380.2500 441.0000 484.0000 556.9600 576.0000 625.0000 547.5600 497.2900 470.8900 392.0400 316.8400 246.4900 201.6400 176.8900 153.7600 146.4100 116.6400 127.6900 141.6100 141.6100 139.2400 114.4900 127.6900 121.0000 118.8100 132.2500 141.6100 121.0000 146.4100 121.0000 129.9600 112.3600 132.2500 127.6900 116.6400 129.9600 102.0100 110.2500 127.6900 114.4900 127.6900 106.0900 123.2100 110.2500 102.0100 121.0000 136.8900 116.6400 96.0400 121.0000 114.4900 104.0400 112.3600 118.8100 144.0000 121.0000 136.8900 127.6900 129.9600 136.8900 127.6900 161.2900 169.0000 153.7600 198.8100 196.0000 252.8100 262.4400 265.6900 275.5600 306.2500 324.0000 285.6100 240.2500 262.4400 207.3600 179.5600 148.8400 141.6100 110.2500 94.0900 108.1600 110.2500 106.0900 92.1600 129.9600 94.0900 106.0900 108.1600 102.0100 114.4900 118.8100 94.0900 123.2100 123.2100 86.4900 102.0100 110.2500 98.0100 96.0400 102.0100 127.6900 121.0000 108.1600 139.2400 134.5600 144.0000 144.0000 139.2400 153.7600 156.2500 153.7600 144.0000 125.4400 123.2100 127.6900 114.4900 102.0100 104.0400 121.0000 88.3600 90.2500 104.0400 106.0900 104.0400 123.2100 108.1600 134.5600 156.2500 129.9600 118.8100 163.8400 151.2900 182.2500 210.2500 256.0000 240.2500 278.8900 316.8400 282.2400 278.8900 272.2500 231.0400 201.6400 190.4400 182.2500 169.0000 161.2900 118.8100 141.6100 136.8900 161.2900 190.4400 171.6100 219.0400 246.4900 225.0000 240.2500 240.2500 256.0000 246.4900 231.0400 207.3600 190.4400 182.2500 134.5600 139.2400 106.0900 88.3600 127.6900 104.0400 98.0100 94.0900 96.0400 94.0900 108.1600 108.1600 121.0000 108.1600 104.0400 94.0900 106.0900 86.4900 98.0100 86.4900 92.1600 82.8100 92.1600 104.0400 102.0100 100.0000 110.2500 114.4900 98.0100 104.0400 94.0900 110.2500 90.2500 112.3600 92.1600 112.3600 98.0100 106.0900 100.0000 86.4900 94.0900 92.1600 88.3600 110.2500 96.0400 106.0900 98.0100 116.6400 116.6400 106.0900 102.0100 94.0900 108.1600 123.2100 104.0400 96.0400 88.3600 132.2500 108.1600 129.9600 132.2500 132.2500 146.4100 132.2500 136.8900 112.3600 127.6900 134.5600 141.6100 123.2100 132.2500 98.0100 110.2500 112.3600 110.2500 112.3600 102.0100 92.1600 118.8100 92.1600 98.0100 98.0100 116.6400 104.0400 106.0900 116.6400 96.0400 94.0900 106.0900 104.0400 112.3600 112.3600 112.3600 132.2500 112.3600 125.4400 139.2400 129.9600 121.0000 121.0000 123.2100 129.9600 127.6900 134.5600 118.8100 100.0000 121.0000 116.6400 102.0100 121.0000 123.2100 123.2100 125.4400 144.0000 163.8400 184.9600 196.0000 246.4900 252.8100 334.8900 432.6400 547.5600 665.6400 778.4100 876.1600 961.0000 1024.0000 924.1600 882.0900 823.6900 745.2900 707.5600 712.8900 772.8400 729.0000 761.7600 894.0100 954.8100 1069.2900 1036.8400 1082.4100 985.9600 912.0400 846.8100 707.5600 630.0100 556.9600 479.6100 345.9600 316.8400 278.8900 278.8900 285.6100 262.4400 275.5600 275.5600 265.6900 309.7600 331.2400 338.5600 408.0400 428.4900 556.9600 615.0400 729.0000 882.0900 973.4400 1176.4900 1346.8900 1489.9600 1444.0000 1576.0900 1466.8900 1391.2900 1169.6400 1122.2500 888.0400 712.8900 585.6400 479.6100 380.2500 285.6100 282.2400 243.3600 196.0000 196.0000 187.6900 182.2500 158.7600 144.0000 153.7600 176.8900 129.9600 129.9600 136.8900 127.6900 146.4100 136.8900 125.4400 118.8100 125.4400 114.4900 144.0000 132.2500 116.6400 139.2400 108.1600 132.2500 132.2500 136.8900 144.0000 146.4100 174.2400 153.7600 179.5600 216.0900 246.4900 282.2400 349.6900 376.3600 466.5600 600.2500 645.1600 750.7600 745.2900 756.2500 712.8900 630.0100 547.5600 462.2500 445.2100 338.5600 285.6100 228.0100 174.2400 153.7600 166.4100 136.8900 127.6900 123.2100 134.5600 114.4900 134.5600 127.6900 104.0400 98.0100 125.4400 123.2100 108.1600 121.0000 125.4400 116.6400 121.0000 108.1600 125.4400 116.6400 106.0900 104.0400 118.8100 134.5600 136.8900 102.0100 132.2500 112.3600 139.2400 123.2100 112.3600 129.9600 158.7600 158.7600 161.2900 174.2400 184.9600 198.8100 193.2100 184.9600 184.9600 210.2500 216.0900 207.3600 210.2500 201.6400 187.6900 198.8100 193.2100 176.8900 179.5600 174.2400 153.7600 166.4100 169.0000 148.8400 132.2500 146.4100 134.5600 136.8900 139.2400 118.8100 132.2500 106.0900 110.2500 121.0000 139.2400 106.0900 110.2500 129.9600 127.6900 108.1600 121.0000 132.2500 127.6900 121.0000 102.0100 127.6900 129.9600 139.2400 125.4400 110.2500 112.3600 114.4900 144.0000 144.0000 146.4100 129.9600 153.7600 182.2500 176.8900 184.9600 182.2500 213.1600 201.6400 210.2500 196.0000 231.0400 222.0100 198.8100 198.8100 207.3600 201.6400 161.2900 171.6100 161.2900 176.8900 163.8400 144.0000 148.8400 163.8400 127.6900 156.2500 151.2900 156.2500 163.8400 176.8900 184.9600 176.8900 204.4900 193.2100 179.5600 187.6900 163.8400 184.9600 184.9600 174.2400 153.7600 174.2400 182.2500 171.6100 156.2500 163.8400 169.0000 163.8400 156.2500 158.7600 174.2400 187.6900 174.2400 184.9600 196.0000 201.6400 198.8100 228.0100 219.0400 237.1600 265.6900 272.2500 306.2500 342.2500 420.2500 492.8400 585.6400 691.6900 876.1600 1069.2900 1176.4900 1339.5600 1544.4900 1772.4100 2034.0100 2275.2900 2490.0100 2704.0000 2959.3600 3249.0000 3422.2500 3516.4900 3492.8100 3375.6100 3192.2500 2787.8400 2490.0100 2116.0000 1806.2500 1560.2500 1324.9600 1122.2500 882.0900 734.4100 620.0100 492.8400 420.2500 357.2100 289.0000 259.2100 222.0100 204.4900 171.6100 169.0000 153.7600 148.8400 151.2900 161.2900 129.9600 134.5600 146.4100 136.8900 146.4100 141.6100 169.0000 139.2400 176.8900 146.4100 182.2500 207.3600 213.1600 234.0900 275.5600 256.0000 272.2500 275.5600 282.2400 292.4100 292.4100 324.0000 306.2500 306.2500 357.2100 372.4900 364.8100 457.9600 492.8400 510.7600 552.2500 524.4100 552.2500 497.2900 470.8900 441.0000 361.0000 342.2500 306.2500 272.2500 240.2500 190.4400 190.4400 190.4400 163.8400 174.2400 146.4100 134.5600 182.2500 153.7600 141.6100 198.8100 184.9600 234.0900 249.6400 278.8900 338.5600 428.4900 441.0000 441.0000 470.8900 441.0000 428.4900 349.6900 331.2400 299.2900 256.0000 198.8100 198.8100 158.7600 169.0000 161.2900 141.6100 134.5600 136.8900 144.0000 129.9600 153.7600 169.0000 146.4100 163.8400 187.6900 219.0400 198.8100 237.1600 240.2500 246.4900 265.6900 262.4400 237.1600 249.6400 243.3600 213.1600 237.1600 210.2500 216.0900 225.0000 228.0100 176.8900 184.9600 148.8400 156.2500 121.0000 141.6100 129.9600 134.5600 121.0000 121.0000 121.0000 108.1600 110.2500 104.0400 123.2100 96.0400 118.8100 116.6400 106.0900 112.3600 110.2500 123.2100 125.4400 116.6400 121.0000 125.4400 144.0000 161.2900 166.4100 179.5600 176.8900 187.6900 201.6400 231.0400 256.0000 342.2500 376.3600 462.2500 524.4100 670.8100 795.2400 870.2500 942.4900 876.1600 829.4400 756.2500 676.0000 600.2500 501.7600 412.0900 338.5600 259.2100 225.0000 193.2100 158.7600 127.6900 132.2500 136.8900 139.2400 141.6100 134.5600 148.8400 127.6900 156.2500 141.6100 146.4100 121.0000 114.4900 125.4400 132.2500 121.0000 121.0000 100.0000 116.6400 98.0100 88.3600 98.0100 98.0100 108.1600 106.0900 96.0400 81.0000 102.0100 73.9600 82.8100 82.8100 81.0000 90.2500 82.8100 94.0900 88.3600 79.2100 90.2500 68.8900 108.1600 92.1600 81.0000 72.2500 79.2100 96.0400 96.0400 98.0100 98.0100 102.0100 88.3600 112.3600 82.8100 110.2500 116.6400 86.4900 121.0000 144.0000 166.4100 148.8400 231.0400 222.0100 285.6100 353.4400 372.4900 400.0000 462.2500 497.2900 492.8400 533.6100 501.7600 538.2400 479.6100 400.0000 392.0400 384.1600 372.4900 316.8400 278.8900 282.2400 234.0900 213.1600 225.0000 207.3600 228.0100 240.2500 272.2500 234.0900 219.0400 282.2400 249.6400 249.6400 234.0900 219.0400 201.6400 184.9600 163.8400 169.0000 148.8400 136.8900 125.4400 118.8100 136.8900 77.4400 86.4900 94.0900 110.2500 129.9600 98.0100 106.0900 114.4900 112.3600 108.1600 106.0900 134.5600 146.4100 144.0000 136.8900 166.4100 146.4100 144.0000 153.7600 148.8400 161.2900 156.2500 156.2500 134.5600 148.8400 127.6900 125.4400 127.6900 121.0000 114.4900 92.1600 121.0000 102.0100 114.4900 102.0100 98.0100 114.4900 114.4900 100.0000 77.4400 86.4900 92.1600 116.6400 102.0100 88.3600 108.1600 102.0100 96.0400 100.0000 104.0400 102.0100 94.0900 104.0400 94.0900 81.0000 121.0000 92.1600 98.0100 96.0400 116.6400 100.0000 102.0100 104.0400 92.1600 77.4400 100.0000 98.0100 98.0100 104.0400 102.0100 86.4900 112.3600 102.0100 106.0900 110.2500 92.1600 110.2500 90.2500 100.0000 96.0400 108.1600 84.6400 104.0400 104.0400 88.3600 94.0900 96.0400 104.0400 73.9600 98.0100 98.0100 110.2500 104.0400 125.4400 104.0400 125.4400 132.2500 108.1600 88.3600 129.9600 127.6900 123.2100 158.7600 169.0000 182.2500 213.1600 240.2500 268.9600 388.0900 462.2500 524.4100 561.6900 620.0100 625.0000 635.0400 580.8100 566.4400 506.2500 479.6100 380.2500 327.6100 313.2900 252.8100 234.0900 193.2100 196.0000 139.2400 151.2900 132.2500 148.8400 132.2500 108.1600 110.2500 121.0000 112.3600 110.2500 125.4400 112.3600 125.4400 121.0000 114.4900 141.6100 139.2400 161.2900 196.0000 207.3600 198.8100 249.6400 299.2900 249.6400 316.8400 299.2900 302.7600 327.6100 324.0000 320.4100 313.2900 275.5600 265.6900 265.6900 228.0100 252.8100 228.0100 187.6900 198.8100 198.8100 141.6100 153.7600 144.0000 114.4900 112.3600 110.2500 104.0400 90.2500 104.0400 84.6400 104.0400 86.4900 94.0900 88.3600 77.4400 96.0400 90.2500 73.9600 67.2400 84.6400 96.0400 79.2100 92.1600 96.0400 86.4900 90.2500 92.1600 79.2100 94.0900 86.4900 84.6400 88.3600 77.4400 100.0000 84.6400 104.0400 81.0000 100.0000 77.4400 92.1600 77.4400 82.8100 68.8900 92.1600 75.6900 88.3600 96.0400 86.4900 75.6900 90.2500 86.4900 82.8100 82.8100 98.0100 98.0100 86.4900 94.0900 82.8100 77.4400 88.3600 82.8100 94.0900 90.2500 90.2500 102.0100 90.2500 98.0100 125.4400 96.0400 123.2100 106.0900 104.0400 106.0900 100.0000 110.2500 146.4100 148.8400 136.8900 136.8900 163.8400 139.2400 146.4100 204.4900 225.0000 243.3600 243.3600 256.0000 225.0000 265.6900 246.4900 234.0900 190.4400 196.0000 207.3600 174.2400 207.3600 174.2400 176.8900 158.7600 161.2900 187.6900 179.5600 213.1600 193.2100 262.4400 309.7600 334.8900 353.4400 384.1600 488.4100 519.8400 566.4400 595.3600 681.2100 702.2500 734.4100 723.6100 734.4100 756.2500 789.6100 789.6100 745.2900 745.2900 696.9600 712.8900 696.9600 605.1600 585.6400 552.2500 470.8900 416.1600 376.3600 345.9600 272.2500 228.0100 219.0400 184.9600 156.2500 141.6100 129.9600 146.4100 106.0900 108.1600 106.0900 108.1600 110.2500 108.1600 102.0100 96.0400 104.0400 96.0400 108.1600 132.2500 102.0100 98.0100 112.3600 94.0900 94.0900 88.3600 114.4900 92.1600 104.0400 100.0000 100.0000 96.0400 104.0400 108.1600 82.8100 108.1600 73.9600 106.0900 102.0100 106.0900 112.3600 110.2500 108.1600 98.0100 90.2500 98.0100 110.2500 118.8100 90.2500 112.3600 82.8100 110.2500 90.2500 90.2500 108.1600 106.0900 102.0100 88.3600 106.0900 90.2500 96.0400 98.0100 88.3600 110.2500 127.6900 125.4400 112.3600 123.2100 153.7600 134.5600 158.7600 158.7600 174.2400 196.0000 219.0400 246.4900 295.8400 313.2900 324.0000 380.2500 462.2500 501.7600 561.6900 718.2400 729.0000 858.4900 918.0900 961.0000 1036.8400 1122.2500 1149.2100 1082.4100 1082.4100 1056.2500 973.4400 906.0100 900.0000 756.2500 712.8900 676.0000 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