data_nl-3_p_01 _diffrn_source_target Cu _diffrn_radiation_probe x-ray _diffrn_radiation_wavelength 1.540598 _diffrn_radiation_type 'Cu K\a~1+2~' _pd_instr_cons_illum_flag yes _pd_instr_var_illum_len 10.000 _pd_meas_2theta_range_min 10.02000000 _pd_meas_2theta_range_max 90.00000000 _pd_meas_2theta_range_inc 0.02000000 _pd_proc_2theta_range_min 10.02000000 _pd_proc_2theta_range_max 90.00000000 _pd_proc_2theta_range_inc 0.02000000 loop_ _pd_meas_intensity_total 163.8400 129.9600 156.2500 156.2500 156.2500 129.9600 151.2900 139.2400 156.2500 148.8400 161.2900 176.8900 153.7600 121.0000 144.0000 141.6100 144.0000 161.2900 146.4100 169.0000 129.9600 163.8400 158.7600 158.7600 132.2500 146.4100 156.2500 153.7600 139.2400 146.4100 148.8400 136.8900 148.8400 161.2900 144.0000 161.2900 171.6100 153.7600 153.7600 148.8400 127.6900 144.0000 148.8400 156.2500 144.0000 156.2500 182.2500 169.0000 141.6100 161.2900 163.8400 161.2900 163.8400 161.2900 169.0000 161.2900 144.0000 146.4100 144.0000 116.6400 144.0000 158.7600 151.2900 136.8900 169.0000 161.2900 163.8400 158.7600 136.8900 144.0000 146.4100 158.7600 136.8900 141.6100 166.4100 148.8400 153.7600 148.8400 161.2900 148.8400 169.0000 163.8400 144.0000 146.4100 151.2900 148.8400 146.4100 169.0000 153.7600 146.4100 146.4100 144.0000 161.2900 139.2400 144.0000 158.7600 151.2900 144.0000 136.8900 139.2400 127.6900 129.9600 127.6900 129.9600 151.2900 148.8400 144.0000 158.7600 127.6900 141.6100 158.7600 129.9600 129.9600 132.2500 121.0000 141.6100 139.2400 139.2400 139.2400 125.4400 136.8900 141.6100 132.2500 127.6900 134.5600 136.8900 121.0000 139.2400 139.2400 102.0100 125.4400 112.3600 129.9600 121.0000 127.6900 125.4400 134.5600 106.0900 139.2400 108.1600 123.2100 129.9600 136.8900 129.9600 118.8100 118.8100 134.5600 118.8100 116.6400 110.2500 106.0900 129.9600 125.4400 127.6900 121.0000 114.4900 125.4400 121.0000 127.6900 121.0000 112.3600 118.8100 118.8100 118.8100 118.8100 106.0900 112.3600 139.2400 121.0000 96.0400 102.0100 125.4400 127.6900 125.4400 112.3600 121.0000 114.4900 123.2100 110.2500 123.2100 114.4900 104.0400 106.0900 110.2500 127.6900 110.2500 123.2100 123.2100 112.3600 146.4100 112.3600 98.0100 134.5600 121.0000 96.0400 112.3600 114.4900 106.0900 116.6400 98.0100 123.2100 127.6900 116.6400 123.2100 134.5600 96.0400 116.6400 114.4900 112.3600 123.2100 129.9600 146.4100 121.0000 123.2100 108.1600 134.5600 153.7600 127.6900 127.6900 129.9600 151.2900 141.6100 129.9600 118.8100 127.6900 102.0100 144.0000 114.4900 121.0000 116.6400 121.0000 110.2500 92.1600 123.2100 123.2100 125.4400 116.6400 121.0000 110.2500 104.0400 102.0100 121.0000 104.0400 118.8100 106.0900 110.2500 114.4900 96.0400 118.8100 118.8100 110.2500 104.0400 110.2500 116.6400 108.1600 118.8100 98.0100 123.2100 106.0900 132.2500 118.8100 96.0400 114.4900 123.2100 94.0900 96.0400 118.8100 118.8100 92.1600 134.5600 102.0100 114.4900 112.3600 92.1600 108.1600 125.4400 114.4900 118.8100 118.8100 96.0400 92.1600 104.0400 112.3600 96.0400 114.4900 106.0900 92.1600 116.6400 106.0900 112.3600 92.1600 121.0000 108.1600 108.1600 121.0000 98.0100 108.1600 129.9600 102.0100 98.0100 116.6400 98.0100 108.1600 104.0400 104.0400 112.3600 96.0400 123.2100 96.0400 121.0000 123.2100 104.0400 123.2100 116.6400 112.3600 110.2500 112.3600 104.0400 112.3600 108.1600 92.1600 106.0900 88.3600 121.0000 106.0900 90.2500 118.8100 88.3600 100.0000 118.8100 92.1600 116.6400 102.0100 98.0100 102.0100 106.0900 86.4900 92.1600 102.0100 102.0100 102.0100 104.0400 121.0000 79.2100 102.0100 121.0000 121.0000 114.4900 102.0100 96.0400 112.3600 92.1600 114.4900 118.8100 139.2400 102.0100 106.0900 116.6400 125.4400 121.0000 118.8100 108.1600 127.6900 139.2400 148.8400 148.8400 169.0000 139.2400 190.4400 190.4400 184.9600 246.4900 243.3600 204.4900 225.0000 148.8400 156.2500 158.7600 158.7600 141.6100 123.2100 127.6900 116.6400 129.9600 121.0000 125.4400 106.0900 104.0400 90.2500 114.4900 98.0100 102.0100 114.4900 110.2500 118.8100 110.2500 123.2100 112.3600 125.4400 132.2500 106.0900 123.2100 134.5600 118.8100 121.0000 102.0100 104.0400 110.2500 108.1600 121.0000 156.2500 118.8100 102.0100 125.4400 129.9600 144.0000 136.8900 136.8900 121.0000 127.6900 121.0000 121.0000 123.2100 100.0000 112.3600 136.8900 110.2500 96.0400 116.6400 127.6900 100.0000 102.0100 108.1600 129.9600 106.0900 102.0100 90.2500 125.4400 110.2500 110.2500 108.1600 114.4900 98.0100 110.2500 110.2500 123.2100 106.0900 104.0400 118.8100 114.4900 127.6900 121.0000 106.0900 118.8100 112.3600 100.0000 129.9600 100.0000 127.6900 106.0900 84.6400 94.0900 112.3600 102.0100 98.0100 106.0900 116.6400 96.0400 106.0900 94.0900 102.0100 116.6400 112.3600 108.1600 102.0100 108.1600 114.4900 114.4900 100.0000 118.8100 84.6400 112.3600 102.0100 121.0000 106.0900 110.2500 100.0000 114.4900 121.0000 127.6900 116.6400 110.2500 104.0400 118.8100 112.3600 123.2100 100.0000 121.0000 123.2100 118.8100 110.2500 141.6100 141.6100 139.2400 148.8400 139.2400 153.7600 158.7600 190.4400 161.2900 158.7600 163.8400 134.5600 136.8900 136.8900 144.0000 151.2900 151.2900 153.7600 134.5600 144.0000 153.7600 146.4100 134.5600 132.2500 112.3600 121.0000 136.8900 116.6400 129.9600 100.0000 136.8900 132.2500 139.2400 112.3600 127.6900 104.0400 116.6400 98.0100 139.2400 125.4400 118.8100 132.2500 112.3600 110.2500 129.9600 129.9600 148.8400 163.8400 158.7600 127.6900 141.6100 151.2900 139.2400 144.0000 127.6900 136.8900 141.6100 123.2100 134.5600 127.6900 125.4400 127.6900 136.8900 114.4900 127.6900 114.4900 121.0000 114.4900 106.0900 116.6400 129.9600 123.2100 121.0000 114.4900 108.1600 125.4400 125.4400 129.9600 123.2100 132.2500 144.0000 127.6900 116.6400 141.6100 136.8900 116.6400 132.2500 134.5600 114.4900 118.8100 139.2400 136.8900 146.4100 144.0000 148.8400 146.4100 176.8900 127.6900 161.2900 161.2900 123.2100 146.4100 144.0000 136.8900 158.7600 121.0000 132.2500 144.0000 179.5600 127.6900 153.7600 153.7600 163.8400 163.8400 169.0000 166.4100 148.8400 158.7600 169.0000 163.8400 121.0000 139.2400 156.2500 129.9600 125.4400 125.4400 125.4400 132.2500 148.8400 121.0000 129.9600 151.2900 146.4100 139.2400 148.8400 139.2400 161.2900 139.2400 123.2100 127.6900 148.8400 139.2400 153.7600 129.9600 132.2500 127.6900 129.9600 146.4100 144.0000 148.8400 146.4100 144.0000 127.6900 153.7600 144.0000 153.7600 166.4100 144.0000 129.9600 125.4400 153.7600 151.2900 132.2500 148.8400 134.5600 171.6100 146.4100 141.6100 136.8900 146.4100 163.8400 132.2500 146.4100 134.5600 144.0000 136.8900 136.8900 146.4100 148.8400 144.0000 148.8400 132.2500 166.4100 148.8400 153.7600 156.2500 153.7600 158.7600 153.7600 161.2900 187.6900 184.9600 187.6900 196.0000 219.0400 243.3600 198.8100 210.2500 193.2100 219.0400 184.9600 201.6400 174.2400 163.8400 158.7600 151.2900 148.8400 156.2500 144.0000 151.2900 148.8400 136.8900 163.8400 136.8900 146.4100 134.5600 163.8400 144.0000 153.7600 146.4100 148.8400 171.6100 158.7600 163.8400 151.2900 158.7600 163.8400 161.2900 144.0000 144.0000 158.7600 158.7600 161.2900 136.8900 141.6100 179.5600 158.7600 166.4100 174.2400 153.7600 174.2400 198.8100 176.8900 193.2100 184.9600 219.0400 196.0000 213.1600 176.8900 201.6400 216.0900 225.0000 210.2500 182.2500 184.9600 182.2500 184.9600 179.5600 198.8100 163.8400 187.6900 182.2500 182.2500 204.4900 198.8100 179.5600 216.0900 190.4400 190.4400 193.2100 196.0000 190.4400 184.9600 184.9600 174.2400 153.7600 169.0000 169.0000 176.8900 182.2500 166.4100 174.2400 201.6400 193.2100 184.9600 171.6100 146.4100 179.5600 207.3600 196.0000 187.6900 184.9600 179.5600 169.0000 182.2500 176.8900 161.2900 171.6100 179.5600 182.2500 158.7600 196.0000 204.4900 193.2100 179.5600 179.5600 171.6100 207.3600 184.9600 151.2900 182.2500 198.8100 166.4100 163.8400 193.2100 190.4400 163.8400 182.2500 207.3600 201.6400 196.0000 174.2400 187.6900 179.5600 179.5600 196.0000 187.6900 193.2100 198.8100 184.9600 222.0100 216.0900 204.4900 243.3600 225.0000 252.8100 225.0000 243.3600 249.6400 252.8100 249.6400 228.0100 216.0900 237.1600 179.5600 243.3600 234.0900 201.6400 198.8100 207.3600 198.8100 190.4400 234.0900 219.0400 182.2500 210.2500 210.2500 225.0000 216.0900 213.1600 246.4900 213.1600 204.4900 222.0100 222.0100 237.1600 204.4900 246.4900 213.1600 234.0900 243.3600 225.0000 228.0100 190.4400 187.6900 216.0900 228.0100 237.1600 228.0100 246.4900 256.0000 222.0100 259.2100 231.0400 240.2500 237.1600 256.0000 219.0400 262.4400 246.4900 249.6400 246.4900 272.2500 234.0900 252.8100 259.2100 331.2400 285.6100 278.8900 285.6100 324.0000 282.2400 353.4400 361.0000 380.2500 408.0400 445.2100 497.2900 529.0000 519.8400 650.2500 702.2500 718.2400 761.7600 767.2900 707.5600 676.0000 610.0900 519.8400 492.8400 445.2100 400.0000 380.2500 388.0900 320.4100 353.4400 364.8100 357.2100 396.0100 368.6400 372.4900 396.0100 449.4400 412.0900 412.0900 428.4900 453.6900 432.6400 466.5600 519.8400 515.2900 552.2500 571.2100 630.0100 600.2500 660.4900 640.0900 665.6400 625.0000 576.0000 600.2500 510.7600 492.8400 524.4100 497.2900 470.8900 484.0000 449.4400 457.9600 428.4900 372.4900 380.2500 364.8100 338.5600 320.4100 285.6100 338.5600 309.7600 320.4100 292.4100 327.6100 316.8400 324.0000 302.7600 306.2500 282.2400 313.2900 289.0000 327.6100 306.2500 302.7600 306.2500 306.2500 259.2100 309.7600 295.8400 302.7600 320.4100 295.8400 275.5600 302.7600 324.0000 324.0000 313.2900 278.8900 342.2500 295.8400 295.8400 320.4100 345.9600 306.2500 309.7600 342.2500 338.5600 313.2900 302.7600 316.8400 285.6100 299.2900 309.7600 331.2400 316.8400 313.2900 320.4100 309.7600 320.4100 320.4100 320.4100 353.4400 324.0000 353.4400 357.2100 334.8900 285.6100 327.6100 353.4400 349.6900 313.2900 327.6100 331.2400 320.4100 313.2900 313.2900 309.7600 324.0000 331.2400 316.8400 282.2400 320.4100 324.0000 320.4100 334.8900 345.9600 364.8100 361.0000 338.5600 361.0000 368.6400 349.6900 380.2500 388.0900 388.0900 380.2500 392.0400 416.1600 466.5600 441.0000 506.2500 501.7600 542.8900 595.3600 640.0900 712.8900 767.2900 795.2400 739.8400 670.8100 707.5600 635.0400 595.3600 561.6900 497.2900 479.6100 445.2100 408.0400 380.2500 396.0100 334.8900 338.5600 368.6400 313.2900 349.6900 334.8900 357.2100 342.2500 349.6900 338.5600 353.4400 306.2500 361.0000 306.2500 342.2500 342.2500 331.2400 372.4900 324.0000 331.2400 338.5600 380.2500 392.0400 380.2500 408.0400 408.0400 416.1600 384.1600 441.0000 420.2500 392.0400 420.2500 400.0000 428.4900 384.1600 396.0100 368.6400 412.0900 353.4400 380.2500 338.5600 331.2400 345.9600 313.2900 338.5600 349.6900 349.6900 331.2400 384.1600 349.6900 380.2500 376.3600 342.2500 349.6900 384.1600 357.2100 338.5600 342.2500 357.2100 368.6400 364.8100 380.2500 361.0000 331.2400 327.6100 368.6400 338.5600 306.2500 324.0000 357.2100 331.2400 313.2900 285.6100 349.6900 313.2900 338.5600 327.6100 338.5600 320.4100 376.3600 372.4900 392.0400 432.6400 412.0900 368.6400 404.0100 457.9600 519.8400 542.8900 556.9600 576.0000 655.3600 655.3600 723.6100 729.0000 691.6900 745.2900 745.2900 812.2500 789.6100 772.8400 745.2900 800.8900 723.6100 702.2500 625.0000 620.0100 571.2100 529.0000 462.2500 416.1600 424.3600 361.0000 364.8100 313.2900 309.7600 295.8400 285.6100 309.7600 268.9600 295.8400 237.1600 262.4400 213.1600 275.5600 272.2500 256.0000 306.2500 240.2500 246.4900 246.4900 222.0100 252.8100 210.2500 252.8100 234.0900 249.6400 231.0400 278.8900 246.4900 268.9600 246.4900 265.6900 299.2900 262.4400 275.5600 243.3600 289.0000 282.2400 259.2100 262.4400 268.9600 243.3600 262.4400 249.6400 259.2100 252.8100 262.4400 262.4400 259.2100 285.6100 231.0400 243.3600 243.3600 231.0400 216.0900 256.0000 219.0400 219.0400 190.4400 225.0000 182.2500 222.0100 204.4900 196.0000 213.1600 198.8100 219.0400 198.8100 198.8100 207.3600 210.2500 213.1600 240.2500 222.0100 187.6900 213.1600 222.0100 196.0000 216.0900 207.3600 225.0000 228.0100 216.0900 187.6900 201.6400 225.0000 210.2500 198.8100 207.3600 196.0000 219.0400 193.2100 187.6900 196.0000 187.6900 196.0000 204.4900 213.1600 176.8900 210.2500 225.0000 222.0100 240.2500 228.0100 228.0100 252.8100 207.3600 228.0100 207.3600 222.0100 216.0900 222.0100 231.0400 196.0000 198.8100 201.6400 210.2500 210.2500 196.0000 190.4400 166.4100 182.2500 198.8100 187.6900 225.0000 179.5600 187.6900 176.8900 184.9600 193.2100 187.6900 201.6400 193.2100 196.0000 184.9600 182.2500 182.2500 196.0000 184.9600 184.9600 219.0400 222.0100 222.0100 246.4900 285.6100 262.4400 278.8900 302.7600 278.8900 289.0000 285.6100 282.2400 259.2100 268.9600 243.3600 234.0900 272.2500 201.6400 219.0400 213.1600 198.8100 213.1600 171.6100 176.8900 176.8900 184.9600 161.2900 182.2500 184.9600 210.2500 190.4400 198.8100 219.0400 219.0400 243.3600 225.0000 246.4900 259.2100 278.8900 249.6400 306.2500 252.8100 252.8100 246.4900 201.6400 246.4900 207.3600 201.6400 187.6900 198.8100 201.6400 182.2500 184.9600 158.7600 151.2900 174.2400 179.5600 190.4400 176.8900 213.1600 136.8900 174.2400 163.8400 158.7600 158.7600 174.2400 182.2500 174.2400 163.8400 156.2500 158.7600 174.2400 158.7600 182.2500 187.6900 144.0000 174.2400 174.2400 182.2500 193.2100 176.8900 171.6100 171.6100 169.0000 179.5600 174.2400 187.6900 174.2400 166.4100 187.6900 169.0000 213.1600 179.5600 213.1600 213.1600 198.8100 216.0900 228.0100 207.3600 193.2100 222.0100 246.4900 225.0000 204.4900 213.1600 231.0400 198.8100 198.8100 184.9600 201.6400 213.1600 201.6400 201.6400 182.2500 201.6400 210.2500 210.2500 222.0100 184.9600 234.0900 187.6900 219.0400 169.0000 219.0400 234.0900 234.0900 222.0100 219.0400 246.4900 240.2500 222.0100 228.0100 225.0000 249.6400 225.0000 222.0100 210.2500 207.3600 225.0000 219.0400 219.0400 210.2500 225.0000 201.6400 198.8100 219.0400 228.0100 228.0100 252.8100 240.2500 246.4900 243.3600 252.8100 246.4900 225.0000 265.6900 213.1600 231.0400 210.2500 234.0900 204.4900 198.8100 176.8900 201.6400 201.6400 207.3600 174.2400 176.8900 144.0000 156.2500 166.4100 166.4100 158.7600 176.8900 169.0000 171.6100 166.4100 174.2400 153.7600 187.6900 196.0000 201.6400 163.8400 182.2500 163.8400 184.9600 171.6100 187.6900 182.2500 169.0000 169.0000 179.5600 179.5600 193.2100 151.2900 179.5600 161.2900 182.2500 156.2500 179.5600 148.8400 169.0000 187.6900 161.2900 174.2400 187.6900 174.2400 176.8900 193.2100 193.2100 198.8100 174.2400 174.2400 171.6100 169.0000 166.4100 222.0100 187.6900 166.4100 198.8100 210.2500 207.3600 176.8900 179.5600 166.4100 190.4400 176.8900 171.6100 174.2400 196.0000 187.6900 210.2500 163.8400 163.8400 193.2100 190.4400 174.2400 163.8400 182.2500 156.2500 174.2400 163.8400 169.0000 174.2400 193.2100 156.2500 161.2900 161.2900 171.6100 171.6100 166.4100 176.8900 171.6100 184.9600 166.4100 179.5600 171.6100 169.0000 171.6100 187.6900 166.4100 163.8400 176.8900 163.8400 193.2100 163.8400 179.5600 166.4100 184.9600 153.7600 144.0000 187.6900 174.2400 201.6400 179.5600 151.2900 213.1600 187.6900 196.0000 201.6400 222.0100 225.0000 207.3600 225.0000 219.0400 222.0100 228.0100 187.6900 234.0900 234.0900 213.1600 204.4900 222.0100 193.2100 196.0000 193.2100 182.2500 174.2400 184.9600 190.4400 174.2400 190.4400 163.8400 169.0000 196.0000 158.7600 158.7600 166.4100 151.2900 179.5600 146.4100 148.8400 158.7600 153.7600 161.2900 169.0000 166.4100 141.6100 174.2400 139.2400 158.7600 153.7600 171.6100 151.2900 148.8400 153.7600 169.0000 158.7600 163.8400 163.8400 166.4100 187.6900 171.6100 163.8400 176.8900 161.2900 151.2900 158.7600 176.8900 153.7600 179.5600 166.4100 166.4100 153.7600 163.8400 174.2400 161.2900 153.7600 176.8900 166.4100 156.2500 166.4100 163.8400 174.2400 193.2100 169.0000 169.0000 163.8400 161.2900 166.4100 163.8400 179.5600 193.2100 171.6100 190.4400 171.6100 158.7600 207.3600 193.2100 193.2100 176.8900 182.2500 190.4400 166.4100 198.8100 207.3600 222.0100 207.3600 190.4400 176.8900 184.9600 225.0000 240.2500 246.4900 213.1600 259.2100 234.0900 210.2500 237.1600 240.2500 234.0900 216.0900 240.2500 225.0000 210.2500 246.4900 210.2500 225.0000 219.0400 262.4400 237.1600 272.2500 295.8400 275.5600 299.2900 320.4100 361.0000 384.1600 396.0100 357.2100 364.8100 457.9600 432.6400 449.4400 424.3600 457.9600 453.6900 416.1600 424.3600 441.0000 384.1600 357.2100 353.4400 338.5600 316.8400 320.4100 289.0000 246.4900 243.3600 231.0400 243.3600 196.0000 210.2500 193.2100 187.6900 166.4100 210.2500 182.2500 184.9600 182.2500 169.0000 182.2500 169.0000 169.0000 187.6900 184.9600 179.5600 169.0000 158.7600 184.9600 187.6900 153.7600 158.7600 166.4100 166.4100 210.2500 184.9600 184.9600 193.2100 198.8100 163.8400 176.8900 182.2500 158.7600 182.2500 190.4400 169.0000 179.5600 182.2500 179.5600 201.6400 174.2400 169.0000 187.6900 171.6100 176.8900 166.4100 163.8400 176.8900 169.0000 169.0000 139.2400 163.8400 144.0000 174.2400 179.5600 176.8900 176.8900 174.2400 176.8900 163.8400 179.5600 153.7600 158.7600 171.6100 171.6100 171.6100 166.4100 169.0000 174.2400 237.1600 222.0100 187.6900 225.0000 228.0100 213.1600 225.0000 272.2500 249.6400 306.2500 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