 
data_argentopolybasite
 
_audit_creation_method            SHELXL-97
_chemical_name_systematic
;
 ?
;
_chemical_name_common             'argentopolybasite'
_chemical_melting_point           ?
_chemical_formula_moiety          
 'Ag32 S22 Sb4'
_chemical_formula_sum
 'Ag32 S22 Sb4'
_chemical_formula_weight          4644.20
 
loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'Ag'  'Ag'  -0.8971   1.1015
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Cu'  'Cu'   0.3201   1.2651
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'S'  'S'   0.1246   0.1234
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Sb'  'Sb'  -0.5866   1.5461
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_symmetry_cell_setting            'monoclinic'
_symmetry_space_group_name_H-M    'C 2/c'
 
loop_
 _symmetry_equiv_pos_as_xyz
 'x, y, z'
 '-x, y, -z+1/2'
 'x+1/2, y+1/2, z'
 '-x+1/2, y+1/2, -z+1/2'
 '-x, -y, -z'
 'x, -y, z-1/2'
 '-x+1/2, -y+1/2, -z'
 'x+1/2, -y+1/2, z-1/2'
 
_cell_length_a                    26.384(2)
_cell_length_b                    15.2320(10)
_cell_length_c                    24.148(2)
_cell_angle_alpha                 90.00
_cell_angle_beta                  90.030(10)
_cell_angle_gamma                 90.00
_cell_volume                      9704.6(13)
_cell_formula_units_Z             8
_cell_measurement_temperature     298(2)
_cell_measurement_reflns_used     1568
_cell_measurement_theta_min       10.4
_cell_measurement_theta_max       27.3
 
_exptl_crystal_description        block
_exptl_crystal_colour             black
_exptl_crystal_size_max           0.055
_exptl_crystal_size_mid           0.040
_exptl_crystal_size_min           0.032
_exptl_crystal_density_meas       ?
_exptl_crystal_density_diffrn     6.357
_exptl_crystal_density_method     'not measured'
_exptl_crystal_F_000              16480
_exptl_absorpt_coefficient_mu     15.704
_exptl_absorpt_correction_type    'gaussian'
_exptl_absorpt_correction_T_min   0.502
_exptl_absorpt_correction_T_max   0.615
_exptl_absorpt_process_details    
'(ABSPACK; Oxford Diffraction, 2006)'
 
_exptl_special_details
;
 ?
;
 
_diffrn_ambient_temperature       298(2)
_diffrn_radiation_wavelength      0.71069
_diffrn_radiation_type            MoK\a
_diffrn_radiation_source          'fine-focus sealed tube'
_diffrn_radiation_monochromator   graphite
_diffrn_measurement_device_type   'Oxford Xcalibur 3'
_diffrn_measurement_method        'ω scans'
_diffrn_detector_area_resol_mean  ?
_diffrn_standards_number          ?
_diffrn_standards_interval_count  .
_diffrn_standards_interval_time   .
_diffrn_standards_decay_%         ?
_diffrn_reflns_number             88756
_diffrn_reflns_av_R_equivalents   0.0412
_diffrn_reflns_av_sigmaI/netI     0.0389
_diffrn_reflns_limit_h_min        -41
_diffrn_reflns_limit_h_max        41
_diffrn_reflns_limit_k_min        -23
_diffrn_reflns_limit_k_max        23
_diffrn_reflns_limit_l_min        -38
_diffrn_reflns_limit_l_max        38
_diffrn_reflns_theta_min          3.99
_diffrn_reflns_theta_max          34.72
_reflns_number_total              18461
_reflns_number_gt                 11867
_reflns_threshold_expression      >2sigma(I)
 
_computing_data_collection        'CrysAlis (Oxford Diffraction, 2006)'
_computing_cell_refinement        'CrysAlis (Oxford Diffraction, 2006)'
_computing_data_reduction         'CrysAlis (Oxford Diffraction, 2006)'
_computing_structure_solution     'SHELXS-97 (Sheldrick, 2008)'
_computing_structure_refinement   'SHELXL-97 (Sheldrick, 2008)'
_computing_molecular_graphics     'DIAMOND (Brandenburg, 2001)'
_computing_publication_material   'SHELXL-97 (Sheldrick, 2008)'
 
_refine_special_details
;
 Refinement of F² against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F², conventional R-factors R are based
 on F, with F set to zero for negative F². The threshold expression of
 F² > 2sigma(F²) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F² are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;
 
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
 'calc w=1/[σ²(Fo²)+(0.1000P)²+0.0000P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      'known structure'
_atom_sites_solution_secondary    'known structure'
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     .
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        ?
_refine_ls_number_reflns          18461
_refine_ls_number_parameters      524
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0380
_refine_ls_R_factor_gt            0.0334
_refine_ls_wR_factor_ref          0.0945
_refine_ls_wR_factor_gt           0.0915
_refine_ls_goodness_of_fit_ref    0.976
_refine_ls_restrained_S_all       0.976
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_symmetry_multiplicity
 _atom_site_calc_flag
 _atom_site_refinement_flags
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Sb1 Sb 0.16691(2) 0.24568(4) 0.04551(3) 0.02390(13) Uani 1 1 d . . .
Sb2 Sb 0.16614(2) 0.75682(4) 0.04760(3) 0.02314(12) Uani 1 1 d . . .
Sb3 Sb 0.42097(3) -0.00615(4) 0.04548(3) 0.02750(14) Uani 1 1 d . . .
Sb4 Sb 0.41115(3) 0.50121(4) 0.04669(3) 0.02540(13) Uani 1 1 d . . .
Ag1 Ag 0.03321(3) 0.14641(5) 0.05461(3) 0.02381(14) Uani 1 1 d . . .
Ag2 Ag 0.04441(3) 0.36053(5) 0.06740(3) 0.02963(16) Uani 1 1 d . . .
Ag3 Ag 0.04226(3) 0.63239(5) 0.06980(3) 0.03086(16) Uani 1 1 d . . .
Ag4 Ag 0.03024(3) 0.86014(6) 0.05619(4) 0.03431(17) Uani 1 1 d . . .
Ag5 Ag 0.16431(3) 0.00340(4) 0.07375(3) 0.02338(14) Uani 1 1 d . . .
Ag6 Ag 0.18510(3) 0.50140(4) 0.05036(3) 0.02526(15) Uani 1 1 d . . .
Ag7 Ag 0.28764(3) 0.10215(5) 0.05251(3) 0.02563(14) Uani 1 1 d . . .
Ag8 Ag 0.28426(3) 0.37816(5) 0.06410(3) 0.02702(15) Uani 1 1 d . . .
Ag9 Ag 0.28844(3) 0.62838(5) 0.06431(3) 0.02505(14) Uani 1 1 d . . .
Ag10 Ag 0.28740(3) 0.89928(5) 0.05731(3) 0.02605(14) Uani 1 1 d . . .
Ag11 Ag 0.43054(3) 0.25110(5) 0.05747(4) 0.02999(16) Uani 1 1 d . . .
Ag12 Ag 0.41695(3) 0.74575(4) 0.06320(3) 0.02297(14) Uani 1 1 d . . .
Ag13 Ag 0.16010(3) 0.00619(4) 0.19916(3) 0.02222(14) Uani 1 1 d . . .
Ag14 Ag 0.34440(3) 0.03098(4) 0.18214(3) 0.02314(14) Uani 1 1 d . . .
Ag15 Ag 0.46083(3) 0.01073(4) 0.19471(3) 0.02405(14) Uani 1 1 d . . .
Ag16 Ag 0.09771(3) 0.19267(5) 0.19881(3) 0.02802(15) Uani 1 1 d . . .
Ag17 Ag 0.22637(3) 0.17237(5) 0.19512(3) 0.02740(15) Uani 1 1 d . . .
Ag18 Ag 0.41216(3) 0.20899(5) 0.18777(3) 0.02554(14) Uani 1 1 d . . .
Ag19 Ag 0.05187(2) 0.37819(4) 0.19633(3) 0.02187(13) Uani 1 1 d . . .
Ag20 Ag 0.17394(2) 0.37676(4) 0.19206(3) 0.02311(13) Uani 1 1 d . . .
Ag21 Ag 0.29034(3) 0.36017(4) 0.19443(3) 0.02379(14) Uani 1 1 d . . .
Ag22 Ag 0.40171(3) 0.41655(4) 0.19273(3) 0.02481(14) Uani 1 1 d . . .
Ag23 Ag 0.06024(3) 0.63446(5) 0.19426(3) 0.02585(14) Uani 1 1 d . . .
Ag24 Ag 0.18806(3) 0.62956(5) 0.18622(3) 0.02689(15) Uani 1 1 d . . .
Ag25 Ag 0.31385(3) 0.60678(5) 0.19050(3) 0.02585(14) Uani 1 1 d . . .
Ag26 Ag 0.46801(2) 0.59315(4) 0.18471(3) 0.02055(13) Uani 1 1 d . . .
Ag27 Ag 0.02232(2) 0.90310(4) 0.18660(3) 0.02034(13) Uani 1 1 d . . .
Ag28 Ag 0.13268(3) 0.80878(5) 0.19468(3) 0.02781(15) Uani 1 1 d . . .
Ag29 Ag 0.26177(3) 0.84456(5) 0.19285(3) 0.02928(16) Uani 1 1 d . . .
Ag30 Ag 0.41352(3) 0.80102(5) 0.18812(3) 0.02606(14) Uani 1 1 d . . .
B1 Ag 0.0000 0.24475(11) 0.2500 0.0256(3) Uani 1 2 d S . .
B2 Ag 0.0000 0.74655(11) 0.2500 0.0298(4) Uani 1 2 d S . .
B3 Ag 0.24338(5) 0.50483(8) 0.24935(6) 0.0311(3) Uani 1 1 d . . .
S1 S 0.11902(11) 0.14149(18) 0.09743(12) 0.0348(6) Uani 1 1 d . . .
S2 S 0.13475(11) 0.37550(18) 0.09219(12) 0.0344(6) Uani 1 1 d . . .
S3 S 0.24675(12) 0.2345(2) 0.09678(14) 0.0403(6) Uani 1 1 d . . .
S4 S 0.13464(10) 0.62891(17) 0.09323(11) 0.0297(5) Uani 1 1 d . . .
S5 S 0.11974(10) 0.86334(18) 0.10389(12) 0.0323(5) Uani 1 1 d . . .
S6 S 0.24578(11) 0.75742(18) 0.09717(13) 0.0350(6) Uani 1 1 d . . .
S7 S 0.49696(11) -0.00545(17) 0.10375(13) 0.0340(6) Uani 1 1 d . . .
S8 S 0.37820(10) 0.11673(18) 0.08883(12) 0.0343(6) Uani 1 1 d . . .
S9 S 0.37899(10) 0.37537(19) 0.09527(13) 0.0356(6) Uani 1 1 d . . .
S10 S 0.49500(13) 0.50201(18) 0.08751(15) 0.0383(7) Uani 1 1 d . . .
S11 S 0.37774(10) 0.6146(2) 0.10800(13) 0.0370(6) Uani 1 1 d . . .
S12 S 0.37495(10) 0.88612(18) 0.09878(12) 0.0316(5) Uani 1 1 d . . .
S13 S 0.22948(11) -0.00524(16) -0.00027(13) 0.0339(6) Uani 1 1 d . . .
S14 S 0.49126(10) 0.77315(19) 0.00101(11) 0.0334(5) Uani 1 1 d . . .
S15 S 0.07471(12) 0.0171(2) 0.23208(14) 0.0402(6) Uani 1 1 d . . .
S16 S 0.24825(12) 0.00408(18) 0.15216(15) 0.0399(7) Uani 1 1 d . . .
S17 S 0.01688(10) 0.25707(17) 0.15271(12) 0.0295(5) Uani 1 1 d . . .
S18 S 0.32914(11) 0.22636(18) 0.23173(12) 0.0344(5) Uani 1 1 d . . .
S19 S 0.10120(11) 0.50514(17) 0.23299(14) 0.0357(6) Uani 1 1 d . . .
S20 S 0.24730(12) 0.49353(17) 0.15005(14) 0.0364(6) Uani 1 1 d . . .
S21 S 0.01109(12) 0.74163(19) 0.15147(14) 0.0391(6) Uani 1 1 d . . .
S22 S 0.33200(13) 0.7524(2) 0.23559(15) 0.0417(7) Uani 1 1 d . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Sb1 S1 2.385(3) . ?
Sb1 S2 2.429(3) . ?
Sb1 S3 2.449(3) . ?
Sb2 S4 2.388(3) . ?
Sb2 S6 2.418(3) . ?
Sb2 S5 2.445(3) . ?
Sb3 S12 2.413(3) 1_545 ?
Sb3 S8 2.424(3) . ?
Sb3 S7 2.449(3) . ?
Sb4 S9 2.402(3) . ?
Sb4 S10 2.421(3) . ?
Sb4 S11 2.440(3) . ?
Ag1 S1 2.490(3) . ?
Ag1 S10 2.547(3) 3_445 ?
Ag1 S14 2.574(3) 3_445 ?
Ag1 S17 2.939(3) . ?
Ag1 Ag4 3.1570(13) 5_565 ?
Ag1 Ag11 3.2681(11) 7 ?
Ag1 Ag2 3.2893(11) . ?
Ag2 S2 2.468(3) . ?
Ag2 S14 2.511(3) 3_445 ?
Ag2 S7 2.551(3) 3_455 ?
Ag2 S17 2.694(3) . ?
Ag2 Ag19 3.1312(11) . ?
Ag3 S14 2.403(3) 7_565 ?
Ag3 S4 2.503(3) . ?
Ag3 S7 2.552(3) 3_455 ?
Ag3 S21 2.709(3) . ?
Ag3 Ag23 3.0428(12) . ?
Ag4 S10 2.471(3) 3_455 ?
Ag4 S14 2.520(3) 7_565 ?
Ag4 S5 2.627(3) . ?
Ag4 S21 2.968(3) . ?
Ag4 Ag11 3.1110(12) 3_455 ?
Ag4 Ag1 3.1570(13) 5_565 ?
Ag4 Ag27 3.2233(11) . ?
Ag5 S13 2.484(3) . ?
Ag5 S1 2.486(3) . ?
Ag5 S5 2.543(3) 1_545 ?
Ag5 S16 2.913(4) . ?
Ag5 Ag13 3.0306(11) . ?
Ag6 S2 2.542(3) . ?
Ag6 S13 2.559(3) 7 ?
Ag6 S4 2.572(3) . ?
Ag6 S20 2.915(3) . ?
Ag6 Ag7 3.0294(11) 7 ?
Ag6 Ag10 3.0948(11) 7_565 ?
Ag6 Ag8 3.2370(10) . ?
Ag6 Ag9 3.3597(10) . ?
Ag7 S3 2.525(3) . ?
Ag7 S8 2.554(3) . ?
Ag7 S13 2.579(3) . ?
Ag7 Ag6 3.0294(11) 7 ?
Ag7 Ag10 3.0923(11) 1_545 ?
Ag8 S13 2.501(3) 7 ?
Ag8 S3 2.528(3) . ?
Ag8 S9 2.610(3) . ?
Ag8 S20 2.890(3) . ?
Ag8 Ag21 3.1631(11) . ?
Ag9 S6 2.400(3) . ?
Ag9 S13 2.476(3) 7 ?
Ag9 S11 2.590(3) . ?
Ag9 Ag25 3.1372(11) . ?
Ag10 S12 2.525(3) . ?
Ag10 S13 2.526(3) 1_565 ?
Ag10 S6 2.608(3) . ?
Ag10 Ag7 3.0923(11) 1_565 ?
Ag10 Ag6 3.0948(11) 7_565 ?
Ag11 S9 2.503(3) . ?
Ag11 S14 2.528(3) 5_665 ?
Ag11 S8 2.583(3) . ?
Ag11 Ag4 3.1110(12) 3_545 ?
Ag11 Ag18 3.2479(12) . ?
Ag11 Ag1 3.2681(11) 7 ?
Ag12 S11 2.496(3) . ?
Ag12 S14 2.505(3) . ?
Ag12 S12 2.557(3) . ?
Ag12 Ag30 3.1333(11) . ?
Ag13 S15 2.395(3) . ?
Ag13 S16 2.589(3) . ?
Ag13 B3 2.8334(16) 4_545 ?
Ag13 Ag17 3.0780(10) . ?
Ag13 Ag28 3.0946(10) 1_545 ?
Ag13 Ag25 3.1492(11) 4_545 ?
Ag13 Ag16 3.2830(10) . ?
Ag13 Ag22 3.3680(10) 4_545 ?
Ag14 S19 2.532(3) 4_545 ?
Ag14 S16 2.669(3) . ?
Ag14 S8 2.753(3) . ?
Ag14 B3 2.8747(16) 4_545 ?
Ag14 Ag15 3.1021(10) . ?
Ag14 Ag18 3.2505(10) . ?
Ag15 S19 2.395(3) 4_545 ?
Ag15 S7 2.408(3) . ?
Ag15 Ag19 3.1379(10) 3_545 ?
Ag15 Ag23 3.2296(10) 3_545 ?
Ag15 Ag18 3.2859(10) . ?
Ag15 Ag23 3.3241(11) 4_545 ?
Ag15 Ag19 3.3334(10) 4_545 ?
Ag15 Ag15 3.3757(16) 2_655 ?
Ag16 S17 2.597(3) . ?
Ag16 S22 2.603(4) 4_545 ?
Ag16 S1 2.630(3) . ?
Ag16 S15 2.858(3) . ?
Ag16 B1 2.9676(9) . ?
Ag16 Ag19 3.0744(10) . ?
Ag16 Ag30 3.2043(11) 4_545 ?
Ag17 S22 2.581(3) 4_545 ?
Ag17 S3 2.613(3) . ?
Ag17 S16 2.825(3) . ?
Ag17 S18 2.968(3) . ?
Ag17 B3 2.9910(15) 4_545 ?
Ag17 Ag25 3.1234(11) 4_545 ?
Ag17 Ag21 3.3215(10) . ?
Ag18 S18 2.449(3) . ?
Ag18 S21 2.798(3) 3_545 ?
Ag18 B2 2.8201(9) 3_545 ?
Ag18 S8 2.913(3) . ?
Ag18 Ag23 3.1514(11) 4_545 ?
Ag18 Ag22 3.1758(10) . ?
Ag19 S17 2.316(3) . ?
Ag19 S19 2.493(3) . ?
Ag19 B1 2.7723(14) . ?
Ag19 Ag15 3.1379(10) 3_455 ?
Ag19 Ag30 3.1619(11) 4_545 ?
Ag19 Ag20 3.2224(9) . ?
Ag19 Ag15 3.3334(10) 4 ?
Ag20 S22 2.582(3) 4_545 ?
Ag20 S2 2.623(3) . ?
Ag20 S20 2.818(3) . ?
Ag20 S19 2.913(3) . ?
Ag20 B3 3.0122(15) . ?
Ag20 Ag21 3.0820(10) . ?
Ag20 Ag29 3.2920(11) 4_545 ?
Ag21 S18 2.452(3) . ?
Ag21 S20 2.562(3) . ?
Ag21 B3 2.8551(15) . ?
Ag21 Ag29 3.0594(11) 4_545 ?
Ag21 Ag22 3.0616(10) . ?
Ag22 S15 2.455(3) 4 ?
Ag22 S9 2.508(3) . ?
Ag22 Ag27 3.1924(9) 3_545 ?
Ag22 Ag26 3.2147(9) . ?
Ag22 Ag28 3.3033(11) 4_545 ?
Ag22 Ag13 3.3680(10) 4 ?
Ag23 S21 2.327(3) . ?
Ag23 S19 2.433(3) . ?
Ag23 B2 2.6935(13) . ?
Ag23 Ag18 3.1514(11) 4 ?
Ag23 Ag15 3.2296(10) 3_455 ?
Ag23 Ag28 3.2717(10) . ?
Ag23 Ag15 3.3241(11) 4 ?
Ag23 Ag24 3.3789(10) . ?
Ag24 S18 2.511(3) 4 ?
Ag24 S4 2.651(3) . ?
Ag24 S20 2.739(3) . ?
Ag24 B3 2.8392(16) . ?
Ag24 Ag28 3.1031(10) . ?
Ag24 Ag25 3.3385(10) . ?
Ag25 S22 2.517(3) . ?
Ag25 S11 2.613(3) . ?
Ag25 S20 2.648(3) . ?
Ag25 B3 2.8090(15) . ?
Ag25 Ag17 3.1234(11) 4 ?
Ag25 Ag13 3.1492(11) 4 ?
Ag26 S15 2.579(3) 4 ?
Ag26 S10 2.819(3) . ?
Ag26 S17 2.914(3) 3 ?
Ag26 B1 2.9205(15) 3 ?
Ag26 Ag27 3.2304(9) 3_545 ?
Ag27 S15 2.476(3) 1_565 ?
Ag27 S21 2.618(3) . ?
Ag27 B2 2.8944(16) . ?
Ag27 S10 2.918(3) 3_455 ?
Ag27 Ag22 3.1924(9) 3_455 ?
Ag27 Ag26 3.2304(9) 3_455 ?
Ag27 Ag28 3.2526(10) . ?
Ag27 Ag27 3.2812(14) 2 ?
Ag28 S5 2.369(3) . ?
Ag28 S18 2.397(3) 4 ?
Ag28 Ag13 3.0946(10) 1_565 ?
Ag28 Ag22 3.3033(11) 4 ?
Ag29 S22 2.543(3) . ?
Ag29 S16 2.645(3) 1_565 ?
Ag29 S6 2.698(3) . ?
Ag29 B3 2.8155(15) 4 ?
Ag29 Ag21 3.0594(11) 4 ?
Ag29 Ag20 3.2920(11) 4 ?
Ag30 S22 2.548(3) . ?
Ag30 S12 2.715(3) . ?
Ag30 B1 2.8583(9) 3 ?
Ag30 S17 2.936(3) 3 ?
Ag30 Ag19 3.1619(11) 4 ?
Ag30 Ag16 3.2043(11) 4 ?
B1 S17 2.399(3) . ?
B1 S17 2.399(3) 2 ?
B1 Ag19 2.7723(14) 2 ?
B1 Ag30 2.8583(9) 4_545 ?
B1 Ag30 2.8583(9) 3_445 ?
B1 Ag26 2.9205(14) 3_445 ?
B1 Ag26 2.9205(14) 4_545 ?
B1 Ag16 2.9676(9) 2 ?
B2 S21 2.398(3) . ?
B2 S21 2.398(3) 2 ?
B2 Ag23 2.6935(13) 2 ?
B2 Ag18 2.8201(9) 3_455 ?
B2 Ag18 2.8201(9) 4 ?
B2 Ag27 2.8944(16) 2 ?
B3 S16 2.388(4) 4 ?
B3 S20 2.406(4) . ?
B3 Ag29 2.8155(15) 4_545 ?
B3 Ag13 2.8334(16) 4 ?
B3 Ag14 2.8747(16) 4 ?
B3 Ag17 2.9910(15) 4 ?
S5 Ag5 2.543(3) 1_565 ?
S7 Ag2 2.551(3) 3_545 ?
S7 Ag3 2.552(3) 3_545 ?
S10 Ag4 2.471(3) 3_545 ?
S10 Ag1 2.547(3) 3 ?
S10 Ag27 2.918(3) 3_545 ?
S12 Sb3 2.413(3) 1_565 ?
S13 Ag9 2.476(3) 7 ?
S13 Ag8 2.501(3) 7 ?
S13 Ag10 2.526(3) 1_545 ?
S13 Ag6 2.559(3) 7 ?
S14 Ag3 2.403(3) 7_565 ?
S14 Ag2 2.511(3) 3 ?
S14 Ag4 2.520(3) 7_565 ?
S14 Ag11 2.528(3) 5_665 ?
S14 Ag1 2.574(3) 3 ?
S15 Ag22 2.455(3) 4_545 ?
S15 Ag27 2.476(3) 1_545 ?
S15 Ag26 2.579(3) 4_545 ?
S16 B3 2.388(4) 4_545 ?
S16 Ag29 2.645(3) 1_545 ?
S17 Ag26 2.914(3) 3_445 ?
S17 Ag30 2.936(3) 3_445 ?
S18 Ag28 2.397(3) 4_545 ?
S18 Ag24 2.511(3) 4_545 ?
S19 Ag15 2.395(3) 4 ?
S19 Ag14 2.532(3) 4 ?
S21 Ag18 2.798(3) 3_455 ?
S22 Ag17 2.581(3) 4 ?
S22 Ag20 2.582(3) 4 ?
S22 Ag16 2.603(4) 4 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
S1 Sb1 S2 96.46(10) . . ?
S1 Sb1 S3 98.27(10) . . ?
S2 Sb1 S3 97.03(10) . . ?
S4 Sb2 S6 94.42(10) . . ?
S4 Sb2 S5 96.34(9) . . ?
S6 Sb2 S5 99.06(10) . . ?
S12 Sb3 S8 93.45(10) 1_545 . ?
S12 Sb3 S7 96.23(10) 1_545 . ?
S8 Sb3 S7 97.45(10) . . ?
S9 Sb4 S10 97.36(10) . . ?
S9 Sb4 S11 98.10(11) . . ?
S10 Sb4 S11 94.57(10) . . ?
S1 Ag1 S10 101.80(10) . 3_445 ?
S1 Ag1 S14 128.47(9) . 3_445 ?
S10 Ag1 S14 129.38(10) 3_445 3_445 ?
S1 Ag1 S17 79.41(9) . . ?
S10 Ag1 S17 100.70(9) 3_445 . ?
S14 Ag1 S17 84.95(8) 3_445 . ?
S1 Ag1 Ag4 146.37(7) . 5_565 ?
S10 Ag1 Ag4 91.56(8) 3_445 5_565 ?
S14 Ag1 Ag4 50.94(7) 3_445 5_565 ?
S17 Ag1 Ag4 128.56(6) . 5_565 ?
S1 Ag1 Ag11 95.27(7) . 7 ?
S10 Ag1 Ag11 141.90(8) 3_445 7 ?
S14 Ag1 Ag11 49.55(6) 3_445 7 ?
S17 Ag1 Ag11 115.89(6) . 7 ?
Ag4 Ag1 Ag11 57.89(3) 5_565 7 ?
S1 Ag1 Ag2 84.79(7) . . ?
S10 Ag1 Ag2 149.61(8) 3_445 . ?
S14 Ag1 Ag2 48.86(7) 3_445 . ?
S17 Ag1 Ag2 50.87(5) . . ?
Ag4 Ag1 Ag2 99.12(3) 5_565 . ?
Ag11 Ag1 Ag2 65.03(2) 7 . ?
S2 Ag2 S14 137.97(10) . 3_445 ?
S2 Ag2 S7 108.47(10) . 3_455 ?
S14 Ag2 S7 111.71(10) 3_445 3_455 ?
S2 Ag2 S17 97.43(9) . . ?
S14 Ag2 S17 91.57(9) 3_445 . ?
S7 Ag2 S17 94.16(9) 3_455 . ?
S2 Ag2 Ag19 71.98(7) . . ?
S14 Ag2 Ag19 135.66(7) 3_445 . ?
S7 Ag2 Ag19 67.65(7) 3_455 . ?
S17 Ag2 Ag19 46.11(6) . . ?
S2 Ag2 Ag1 101.60(7) . . ?
S14 Ag2 Ag1 50.54(7) 3_445 . ?
S7 Ag2 Ag1 141.42(7) 3_455 . ?
S17 Ag2 Ag1 57.82(6) . . ?
Ag19 Ag2 Ag1 100.61(3) . . ?
S14 Ag3 S4 122.11(10) 7_565 . ?
S14 Ag3 S7 123.30(10) 7_565 3_455 ?
S4 Ag3 S7 111.48(9) . 3_455 ?
S14 Ag3 S21 92.21(10) 7_565 . ?
S4 Ag3 S21 98.31(9) . . ?
S7 Ag3 S21 97.42(10) 3_455 . ?
S14 Ag3 Ag23 138.92(8) 7_565 . ?
S4 Ag3 Ag23 68.01(7) . . ?
S7 Ag3 Ag23 76.35(8) 3_455 . ?
S21 Ag3 Ag23 47.28(7) . . ?
S10 Ag4 S14 141.96(11) 3_455 7_565 ?
S10 Ag4 S5 100.83(10) 3_455 . ?
S14 Ag4 S5 117.21(9) 7_565 . ?
S10 Ag4 S21 103.32(10) 3_455 . ?
S14 Ag4 S21 84.06(9) 7_565 . ?
S5 Ag4 S21 79.91(9) . . ?
S10 Ag4 Ag11 98.37(8) 3_455 3_455 ?
S14 Ag4 Ag11 52.07(7) 7_565 3_455 ?
S5 Ag4 Ag11 139.94(7) . 3_455 ?
S21 Ag4 Ag11 61.53(7) . 3_455 ?
S10 Ag4 Ag1 95.03(9) 3_455 5_565 ?
S14 Ag4 Ag1 52.48(7) 7_565 5_565 ?
S5 Ag4 Ag1 148.01(7) . 5_565 ?
S21 Ag4 Ag1 123.19(7) . 5_565 ?
Ag11 Ag4 Ag1 62.85(3) 3_455 5_565 ?
S10 Ag4 Ag27 59.93(8) 3_455 . ?
S14 Ag4 Ag27 133.19(7) 7_565 . ?
S5 Ag4 Ag27 68.07(7) . . ?
S21 Ag4 Ag27 49.83(6) . . ?
Ag11 Ag4 Ag27 92.49(3) 3_455 . ?
Ag1 Ag4 Ag27 143.12(3) 5_565 . ?
S13 Ag5 S1 122.90(9) . . ?
S13 Ag5 S5 118.81(9) . 1_545 ?
S1 Ag5 S5 114.95(10) . 1_545 ?
S13 Ag5 S16 86.65(10) . . ?
S1 Ag5 S16 102.29(9) . . ?
S5 Ag5 S16 99.70(9) 1_545 . ?
S13 Ag5 Ag13 138.19(8) . . ?
S1 Ag5 Ag13 74.96(7) . . ?
S5 Ag5 Ag13 73.06(7) 1_545 . ?
S16 Ag5 Ag13 51.59(7) . . ?
S2 Ag6 S13 131.72(9) . 7 ?
S2 Ag6 S4 97.99(10) . . ?
S13 Ag6 S4 128.98(8) 7 . ?
S2 Ag6 S20 86.27(9) . . ?
S13 Ag6 S20 84.01(10) 7 . ?
S4 Ag6 S20 89.42(9) . . ?
S2 Ag6 Ag7 93.29(7) . 7 ?
S13 Ag6 Ag7 54.18(7) 7 7 ?
S4 Ag6 Ag7 147.80(7) . 7 ?
S20 Ag6 Ag7 121.46(6) . 7 ?
S2 Ag6 Ag10 145.62(8) . 7_565 ?
S13 Ag6 Ag10 52.03(7) 7 7_565 ?
S4 Ag6 Ag10 95.20(6) . 7_565 ?
S20 Ag6 Ag10 125.57(7) . 7_565 ?
Ag7 Ag6 Ag10 60.64(3) 7 7_565 ?
S2 Ag6 Ag8 86.81(7) . . ?
S13 Ag6 Ag8 49.44(7) 7 . ?
S4 Ag6 Ag8 144.59(7) . . ?
S20 Ag6 Ag8 55.73(6) . . ?
Ag7 Ag6 Ag8 65.79(3) 7 . ?
Ag10 Ag6 Ag8 100.36(3) 7_565 . ?
S2 Ag6 Ag9 144.94(7) . . ?
S13 Ag6 Ag9 47.10(7) 7 . ?
S4 Ag6 Ag9 86.85(6) . . ?
S20 Ag6 Ag9 58.96(6) . . ?
Ag7 Ag6 Ag9 100.89(3) 7 . ?
Ag10 Ag6 Ag9 67.18(2) 7_565 . ?
Ag8 Ag6 Ag9 70.59(2) . . ?
S3 Ag7 S8 100.66(10) . . ?
S3 Ag7 S13 117.49(10) . . ?
S8 Ag7 S13 141.35(9) . . ?
S3 Ag7 Ag6 149.85(8) . 7 ?
S8 Ag7 Ag6 95.99(7) . 7 ?
S13 Ag7 Ag6 53.57(7) . 7 ?
S3 Ag7 Ag10 141.38(8) . 1_545 ?
S8 Ag7 Ag10 94.36(7) . 1_545 ?
S13 Ag7 Ag10 51.94(6) . 1_545 ?
Ag6 Ag7 Ag10 60.73(2) 7 1_545 ?
S13 Ag8 S3 143.69(10) 7 . ?
S13 Ag8 S9 109.20(10) 7 . ?
S3 Ag8 S9 105.71(10) . . ?
S13 Ag8 S20 85.59(9) 7 . ?
S3 Ag8 S20 99.77(10) . . ?
S9 Ag8 S20 97.25(9) . . ?
S13 Ag8 Ag21 133.44(7) 7 . ?
S3 Ag8 Ag21 68.53(8) . . ?
S9 Ag8 Ag21 70.34(7) . . ?
S20 Ag8 Ag21 49.83(6) . . ?
S13 Ag8 Ag6 51.03(7) 7 . ?
S3 Ag8 Ag6 102.56(8) . . ?
S9 Ag8 Ag6 144.37(7) . . ?
S20 Ag8 Ag6 56.49(7) . . ?
Ag21 Ag8 Ag6 101.12(3) . . ?
S6 Ag9 S13 137.51(10) . 7 ?
S6 Ag9 S11 110.99(10) . . ?
S13 Ag9 S11 111.50(10) 7 . ?
S6 Ag9 Ag25 82.23(8) . . ?
S13 Ag9 Ag25 124.60(7) 7 . ?
S11 Ag9 Ag25 53.26(7) . . ?
S6 Ag9 Ag6 97.12(7) . . ?
S13 Ag9 Ag6 49.21(7) 7 . ?
S11 Ag9 Ag6 137.09(7) . . ?
Ag25 Ag9 Ag6 102.13(3) . . ?
S12 Ag10 S13 144.78(9) . 1_565 ?
S12 Ag10 S6 99.97(9) . . ?
S13 Ag10 S6 115.18(9) 1_565 . ?
S12 Ag10 Ag7 95.30(7) . 1_565 ?
S13 Ag10 Ag7 53.51(6) 1_565 1_565 ?
S6 Ag10 Ag7 147.42(7) . 1_565 ?
S12 Ag10 Ag6 99.04(7) . 7_565 ?
S13 Ag10 Ag6 53.00(7) 1_565 7_565 ?
S6 Ag10 Ag6 144.49(7) . 7_565 ?
Ag7 Ag10 Ag6 58.63(2) 1_565 7_565 ?
S9 Ag11 S14 139.28(10) . 5_665 ?
S9 Ag11 S8 101.63(10) . . ?
S14 Ag11 S8 118.99(9) 5_665 . ?
S9 Ag11 Ag4 93.41(7) . 3_545 ?
S14 Ag11 Ag4 51.84(7) 5_665 3_545 ?
S8 Ag11 Ag4 151.43(7) . 3_545 ?
S9 Ag11 Ag18 73.42(7) . . ?
S14 Ag11 Ag18 129.40(7) 5_665 . ?
S8 Ag11 Ag18 58.62(7) . . ?
Ag4 Ag11 Ag18 103.99(3) 3_545 . ?
S9 Ag11 Ag1 95.74(7) . 7 ?
S14 Ag11 Ag1 50.79(7) 5_665 7 ?
S8 Ag11 Ag1 141.09(7) . 7 ?
Ag4 Ag11 Ag1 59.27(3) 3_545 7 ?
Ag18 Ag11 Ag1 160.15(3) . 7 ?
S11 Ag12 S14 135.87(10) . . ?
S11 Ag12 S12 110.10(10) . . ?
S14 Ag12 S12 113.67(9) . . ?
S11 Ag12 Ag30 77.62(7) . . ?
S14 Ag12 Ag30 123.74(7) . . ?
S12 Ag12 Ag30 55.88(7) . . ?
S15 Ag13 S16 172.68(12) . . ?
S15 Ag13 B3 134.44(9) . 4_545 ?
S16 Ag13 B3 52.03(9) . 4_545 ?
S15 Ag13 Ag5 111.57(9) . . ?
S16 Ag13 Ag5 61.86(8) . . ?
B3 Ag13 Ag5 113.89(4) 4_545 . ?
S15 Ag13 Ag17 119.21(8) . . ?
S16 Ag13 Ag17 59.06(7) . . ?
B3 Ag13 Ag17 60.62(3) 4_545 . ?
Ag5 Ag13 Ag17 87.64(3) . . ?
S15 Ag13 Ag28 81.89(8) . 1_545 ?
S16 Ag13 Ag28 100.53(7) . 1_545 ?
B3 Ag13 Ag28 102.61(3) 4_545 1_545 ?
Ag5 Ag13 Ag28 87.72(3) . 1_545 ?
Ag17 Ag13 Ag28 158.55(3) . 1_545 ?
S15 Ag13 Ag25 83.71(8) . 4_545 ?
S16 Ag13 Ag25 100.44(8) . 4_545 ?
B3 Ag13 Ag25 55.70(3) 4_545 4_545 ?
Ag5 Ag13 Ag25 147.58(3) . 4_545 ?
Ag17 Ag13 Ag25 60.20(2) . 4_545 ?
Ag28 Ag13 Ag25 123.59(3) 1_545 4_545 ?
S15 Ag13 Ag16 57.95(8) . . ?
S16 Ag13 Ag16 117.40(7) . . ?
B3 Ag13 Ag16 117.26(3) 4_545 . ?
Ag5 Ag13 Ag16 91.62(3) . . ?
Ag17 Ag13 Ag16 64.74(2) . . ?
Ag28 Ag13 Ag16 136.34(3) 1_545 . ?
Ag25 Ag13 Ag16 71.97(2) 4_545 . ?
S15 Ag13 Ag22 46.75(8) . 4_545 ?
S16 Ag13 Ag22 140.38(8) . 4_545 ?
B3 Ag13 Ag22 95.30(4) 4_545 4_545 ?
Ag5 Ag13 Ag22 141.89(3) . 4_545 ?
Ag17 Ag13 Ag22 129.29(3) . 4_545 ?
Ag28 Ag13 Ag22 61.31(2) 1_545 4_545 ?
Ag25 Ag13 Ag22 69.33(2) 4_545 4_545 ?
Ag16 Ag13 Ag22 96.30(3) . 4_545 ?
S19 Ag14 S16 137.20(10) 4_545 . ?
S19 Ag14 S8 123.54(9) 4_545 . ?
S16 Ag14 S8 99.15(10) . . ?
S19 Ag14 B3 88.23(8) 4_545 4_545 ?
S16 Ag14 B3 50.87(8) . 4_545 ?
S8 Ag14 B3 142.95(7) . 4_545 ?
S19 Ag14 Ag15 49.04(7) 4_545 . ?
S16 Ag14 Ag15 162.22(7) . . ?
S8 Ag14 Ag15 78.82(6) . . ?
B3 Ag14 Ag15 136.72(4) 4_545 . ?
S19 Ag14 Ag18 77.54(6) 4_545 . ?
S16 Ag14 Ag18 131.45(7) . . ?
S8 Ag14 Ag18 57.33(6) . . ?
B3 Ag14 Ag18 122.32(4) 4_545 . ?
Ag15 Ag14 Ag18 62.24(2) . . ?
S19 Ag15 S7 158.80(11) 4_545 . ?
S19 Ag15 Ag14 52.98(8) 4_545 . ?
S7 Ag15 Ag14 108.26(8) . . ?
S19 Ag15 Ag19 119.43(8) 4_545 3_545 ?
S7 Ag15 Ag19 69.03(7) . 3_545 ?
Ag14 Ag15 Ag19 145.40(3) . 3_545 ?
S19 Ag15 Ag23 125.34(8) 4_545 3_545 ?
S7 Ag15 Ag23 74.62(7) . 3_545 ?
Ag14 Ag15 Ag23 138.23(3) . 3_545 ?
Ag19 Ag15 Ag23 75.75(2) 3_545 3_545 ?
S19 Ag15 Ag18 78.62(7) 4_545 . ?
S7 Ag15 Ag18 101.68(7) . . ?
Ag14 Ag15 Ag18 61.09(2) . . ?
Ag19 Ag15 Ag18 153.01(3) 3_545 . ?
Ag23 Ag15 Ag18 77.35(2) 3_545 . ?
S19 Ag15 Ag23 46.97(7) 4_545 4_545 ?
S7 Ag15 Ag23 149.36(7) . 4_545 ?
Ag14 Ag15 Ag23 81.75(3) . 4_545 ?
Ag19 Ag15 Ag23 118.88(3) 3_545 4_545 ?
Ag23 Ag15 Ag23 78.93(3) 3_545 4_545 ?
Ag18 Ag15 Ag23 56.94(2) . 4_545 ?
S19 Ag15 Ag19 48.25(7) 4_545 4_545 ?
S7 Ag15 Ag19 134.28(7) . 4_545 ?
Ag14 Ag15 Ag19 92.15(3) . 4_545 ?
Ag19 Ag15 Ag19 71.20(3) 3_545 4_545 ?
Ag23 Ag15 Ag19 115.98(3) 3_545 4_545 ?
Ag18 Ag15 Ag19 123.88(3) . 4_545 ?
Ag23 Ag15 Ag19 71.93(2) 4_545 4_545 ?
S19 Ag15 Ag15 80.89(8) 4_545 2_655 ?
S7 Ag15 Ag15 118.63(8) . 2_655 ?
Ag14 Ag15 Ag15 133.10(4) . 2_655 ?
Ag19 Ag15 Ag15 61.43(2) 3_545 2_655 ?
Ag23 Ag15 Ag15 60.38(2) 3_545 2_655 ?
Ag18 Ag15 Ag15 106.23(2) . 2_655 ?
Ag23 Ag15 Ag15 57.63(2) 4_545 2_655 ?
Ag19 Ag15 Ag15 55.77(2) 4_545 2_655 ?
S17 Ag16 S22 135.52(9) . 4_545 ?
S17 Ag16 S1 83.62(9) . . ?
S22 Ag16 S1 121.16(10) 4_545 . ?
S17 Ag16 S15 107.43(9) . . ?
S22 Ag16 S15 107.90(10) 4_545 . ?
S1 Ag16 S15 91.71(10) . . ?
S17 Ag16 B1 50.53(6) . . ?
S22 Ag16 B1 105.78(8) 4_545 . ?
S1 Ag16 B1 130.78(7) . . ?
S15 Ag16 B1 87.05(7) . . ?
S17 Ag16 Ag19 47.29(6) . . ?
S22 Ag16 Ag19 88.32(7) 4_545 . ?
S1 Ag16 Ag19 109.79(7) . . ?
S15 Ag16 Ag19 141.46(7) . . ?
B1 Ag16 Ag19 54.59(3) . . ?
S17 Ag16 Ag30 95.42(7) . 4_545 ?
S22 Ag16 Ag30 50.76(8) 4_545 4_545 ?
S1 Ag16 Ag30 164.93(7) . 4_545 ?
S15 Ag16 Ag30 102.87(7) . 4_545 ?
B1 Ag16 Ag30 55.02(2) . 4_545 ?
Ag19 Ag16 Ag30 60.43(2) . 4_545 ?
S17 Ag16 Ag13 137.68(7) . . ?
S22 Ag16 Ag13 86.78(7) 4_545 . ?
S1 Ag16 Ag13 68.81(7) . . ?
S15 Ag16 Ag13 45.26(7) . . ?
B1 Ag16 Ag13 131.75(4) . . ?
Ag19 Ag16 Ag13 173.01(3) . . ?
Ag30 Ag16 Ag13 119.35(3) 4_545 . ?
S22 Ag17 S3 122.77(10) 4_545 . ?
S22 Ag17 S16 142.08(10) 4_545 . ?
S3 Ag17 S16 87.30(10) . . ?
S22 Ag17 S18 102.80(10) 4_545 . ?
S3 Ag17 S18 88.96(9) . . ?
S16 Ag17 S18 100.02(9) . . ?
S22 Ag17 B3 105.76(8) 4_545 4_545 ?
S3 Ag17 B3 131.42(8) . 4_545 ?
S16 Ag17 B3 48.39(8) . 4_545 ?
S18 Ag17 B3 81.91(6) . 4_545 ?
S22 Ag17 Ag13 91.65(7) 4_545 . ?
S3 Ag17 Ag13 116.36(8) . . ?
S16 Ag17 Ag13 51.80(7) . . ?
S18 Ag17 Ag13 137.51(6) . . ?
B3 Ag17 Ag13 55.64(3) 4_545 . ?
S22 Ag17 Ag25 51.29(7) 4_545 4_545 ?
S3 Ag17 Ag25 171.83(8) . 4_545 ?
S16 Ag17 Ag25 95.97(7) . 4_545 ?
S18 Ag17 Ag25 97.82(6) . 4_545 ?
B3 Ag17 Ag25 54.65(3) 4_545 4_545 ?
Ag13 Ag17 Ag25 61.03(2) . 4_545 ?
S22 Ag17 Ag21 84.25(7) 4_545 . ?
S3 Ag17 Ag21 65.07(7) . . ?
S16 Ag17 Ag21 132.50(7) . . ?
S18 Ag17 Ag21 45.46(6) . . ?
B3 Ag17 Ag21 126.98(4) 4_545 . ?
Ag13 Ag17 Ag21 175.64(3) . . ?
Ag25 Ag17 Ag21 116.93(3) 4_545 . ?
S18 Ag18 S21 162.03(10) . 3_545 ?
S18 Ag18 B2 118.83(8) . 3_545 ?
S21 Ag18 B2 50.54(7) 3_545 3_545 ?
S18 Ag18 S8 97.63(9) . . ?
S21 Ag18 S8 96.62(9) 3_545 . ?
B2 Ag18 S8 141.93(6) 3_545 . ?
S18 Ag18 Ag23 81.58(7) . 4_545 ?
S21 Ag18 Ag23 97.58(7) 3_545 4_545 ?
B2 Ag18 Ag23 53.27(3) 3_545 4_545 ?
S8 Ag18 Ag23 129.68(6) . 4_545 ?
S18 Ag18 Ag22 78.37(7) . . ?
S21 Ag18 Ag22 85.18(6) 3_545 . ?
B2 Ag18 Ag22 81.33(4) 3_545 . ?
S8 Ag18 Ag22 118.99(6) . . ?
Ag23 Ag18 Ag22 110.16(3) 4_545 . ?
S18 Ag18 Ag11 122.18(8) . . ?
S21 Ag18 Ag11 61.42(7) 3_545 . ?
B2 Ag18 Ag11 110.67(3) 3_545 . ?
S8 Ag18 Ag11 49.20(6) . . ?
Ag23 Ag18 Ag11 155.82(3) 4_545 . ?
Ag22 Ag18 Ag11 81.55(3) . . ?
S18 Ag18 Ag14 67.43(7) . . ?
S21 Ag18 Ag14 130.40(7) 3_545 . ?
B2 Ag18 Ag14 130.04(4) 3_545 . ?
S8 Ag18 Ag14 52.72(6) . . ?
Ag23 Ag18 Ag14 82.19(3) 4_545 . ?
Ag22 Ag18 Ag14 141.65(3) . . ?
Ag11 Ag18 Ag14 101.92(3) . . ?
S18 Ag18 Ag15 115.27(7) . . ?
S21 Ag18 Ag15 79.32(6) 3_545 . ?
B2 Ag18 Ag15 80.69(4) 3_545 . ?
S8 Ag18 Ag15 73.65(6) . . ?
Ag23 Ag18 Ag15 62.14(2) 4_545 . ?
Ag22 Ag18 Ag15 161.25(3) . . ?
Ag11 Ag18 Ag15 99.92(3) . . ?
Ag14 Ag18 Ag15 56.66(2) . . ?
S17 Ag19 S19 170.81(10) . . ?
S17 Ag19 B1 55.38(7) . . ?
S19 Ag19 B1 131.33(8) . . ?
S17 Ag19 Ag16 55.48(7) . . ?
S19 Ag19 Ag16 120.05(7) . . ?
B1 Ag19 Ag16 60.74(3) . . ?
S17 Ag19 Ag2 56.94(7) . . ?
S19 Ag19 Ag2 116.89(8) . . ?
B1 Ag19 Ag2 111.78(3) . . ?
Ag16 Ag19 Ag2 87.99(3) . . ?
S17 Ag19 Ag15 101.65(7) . 3_455 ?
S19 Ag19 Ag15 84.54(7) . 3_455 ?
B1 Ag19 Ag15 95.71(3) . 3_455 ?
Ag16 Ag19 Ag15 153.22(3) . 3_455 ?
Ag2 Ag19 Ag15 89.72(3) . 3_455 ?
S17 Ag19 Ag30 102.71(7) . 4_545 ?
S19 Ag19 Ag30 79.90(8) . 4_545 ?
B1 Ag19 Ag30 57.136(19) . 4_545 ?
Ag16 Ag19 Ag30 61.82(2) . 4_545 ?
Ag2 Ag19 Ag30 149.71(3) . 4_545 ?
Ag15 Ag19 Ag30 118.09(3) 3_455 4_545 ?
S17 Ag19 Ag20 112.22(7) . . ?
S19 Ag19 Ag20 59.67(7) . . ?
B1 Ag19 Ag20 120.24(3) . . ?
Ag16 Ag19 Ag20 66.50(2) . . ?
Ag2 Ag19 Ag20 91.71(3) . . ?
Ag15 Ag19 Ag20 140.26(3) 3_455 . ?
Ag30 Ag19 Ag20 74.79(2) 4_545 . ?
S17 Ag19 Ag15 143.24(7) . 4 ?
S19 Ag19 Ag15 45.79(7) . 4 ?
B1 Ag19 Ag15 91.44(3) . 4 ?
Ag16 Ag19 Ag15 125.53(3) . 4 ?
Ag2 Ag19 Ag15 146.16(3) . 4 ?
Ag15 Ag19 Ag15 62.80(3) 3_455 4 ?
Ag30 Ag19 Ag15 63.75(2) 4_545 4 ?
Ag20 Ag19 Ag15 97.49(3) . 4 ?
S22 Ag20 S2 126.34(10) 4_545 . ?
S22 Ag20 S20 138.48(10) 4_545 . ?
S2 Ag20 S20 86.80(9) . . ?
S22 Ag20 S19 102.87(10) 4_545 . ?
S2 Ag20 S19 93.29(9) . . ?
S20 Ag20 S19 98.70(8) . . ?
S22 Ag20 B3 101.62(8) 4_545 . ?
S2 Ag20 B3 131.78(7) . . ?
S20 Ag20 B3 48.61(7) . . ?
S19 Ag20 B3 79.05(7) . . ?
S22 Ag20 Ag21 89.32(8) 4_545 . ?
S2 Ag20 Ag21 114.12(7) . . ?
S20 Ag20 Ag21 51.23(6) . . ?
S19 Ag20 Ag21 134.86(7) . . ?
B3 Ag20 Ag21 55.86(3) . . ?
S22 Ag20 Ag19 85.54(8) 4_545 . ?
S2 Ag20 Ag19 68.66(7) . . ?
S20 Ag20 Ag19 133.94(7) . . ?
S19 Ag20 Ag19 47.62(6) . . ?
B3 Ag20 Ag19 126.06(4) . . ?
Ag21 Ag20 Ag19 174.80(3) . . ?
S22 Ag20 Ag29 49.52(8) 4_545 4_545 ?
S2 Ag20 Ag29 167.86(7) . 4_545 ?
S20 Ag20 Ag29 92.54(7) . 4_545 ?
S19 Ag20 Ag29 98.79(7) . 4_545 ?
B3 Ag20 Ag29 52.82(3) . 4_545 ?
Ag21 Ag20 Ag29 57.25(2) . 4_545 ?
Ag19 Ag20 Ag29 119.24(3) . 4_545 ?
S18 Ag21 S20 176.06(10) . . ?
S18 Ag21 B3 130.70(8) . . ?
S20 Ag21 B3 52.41(8) . . ?
S18 Ag21 Ag29 78.25(7) . 4_545 ?
S20 Ag21 Ag29 103.56(8) . 4_545 ?
B3 Ag21 Ag29 56.73(3) . 4_545 ?
S18 Ag21 Ag22 80.65(7) . . ?
S20 Ag21 Ag22 101.38(7) . . ?
B3 Ag21 Ag22 101.91(4) . . ?
Ag29 Ag21 Ag22 117.74(3) 4_545 . ?
S18 Ag21 Ag20 119.39(7) . . ?
S20 Ag21 Ag20 59.05(7) . . ?
B3 Ag21 Ag20 60.83(3) . . ?
Ag29 Ag21 Ag20 64.83(3) 4_545 . ?
Ag22 Ag21 Ag20 158.93(3) . . ?
S18 Ag21 Ag8 117.28(7) . . ?
S20 Ag21 Ag8 59.53(8) . . ?
B3 Ag21 Ag8 111.93(4) . . ?
Ag29 Ag21 Ag8 150.39(3) 4_545 . ?
Ag22 Ag21 Ag8 90.61(3) . . ?
Ag20 Ag21 Ag8 85.66(3) . . ?
S18 Ag21 Ag17 59.62(7) . . ?
S20 Ag21 Ag17 117.38(7) . . ?
B3 Ag21 Ag17 116.21(4) . . ?
Ag29 Ag21 Ag17 72.54(2) 4_545 . ?
Ag22 Ag21 Ag17 136.83(3) . . ?
Ag20 Ag21 Ag17 64.17(2) . . ?
Ag8 Ag21 Ag17 93.10(3) . . ?
S15 Ag22 S9 155.55(11) 4 . ?
S15 Ag22 Ag21 114.07(8) 4 . ?
S9 Ag22 Ag21 73.35(7) . . ?
S15 Ag22 Ag18 128.82(8) 4 . ?
S9 Ag22 Ag18 74.71(7) . . ?
Ag21 Ag22 Ag18 78.73(2) . . ?
S15 Ag22 Ag27 79.75(8) 4 3_545 ?
S9 Ag22 Ag27 100.26(7) . 3_545 ?
Ag21 Ag22 Ag27 159.94(3) . 3_545 ?
Ag18 Ag22 Ag27 81.25(2) . 3_545 ?
S15 Ag22 Ag26 52.05(8) 4 . ?
S9 Ag22 Ag26 106.41(7) . . ?
Ag21 Ag22 Ag26 139.27(3) . . ?
Ag18 Ag22 Ag26 141.58(3) . . ?
Ag27 Ag22 Ag26 60.55(2) 3_545 . ?
S15 Ag22 Ag28 76.75(8) 4 4_545 ?
S9 Ag22 Ag28 125.62(7) . 4_545 ?
Ag21 Ag22 Ag28 65.52(2) . 4_545 ?
Ag18 Ag22 Ag28 63.91(2) . 4_545 ?
Ag27 Ag22 Ag28 106.29(3) 3_545 4_545 ?
Ag26 Ag22 Ag28 127.97(3) . 4_545 ?
S15 Ag22 Ag13 45.29(8) 4 4 ?
S9 Ag22 Ag13 135.49(7) . 4 ?
Ag21 Ag22 Ag13 68.79(2) . 4 ?
Ag18 Ag22 Ag13 118.35(3) . 4 ?
Ag27 Ag22 Ag13 123.03(3) 3_545 4 ?
Ag26 Ag22 Ag13 88.35(2) . 4 ?
Ag28 Ag22 Ag13 55.26(2) 4_545 4 ?
S21 Ag23 S19 170.40(11) . . ?
S21 Ag23 B2 56.51(8) . . ?
S19 Ag23 B2 125.67(8) . . ?
S21 Ag23 Ag3 58.80(8) . . ?
S19 Ag23 Ag3 116.12(8) . . ?
B2 Ag23 Ag3 114.10(3) . . ?
S21 Ag23 Ag18 106.09(8) . 4 ?
S19 Ag23 Ag18 80.90(8) . 4 ?
B2 Ag23 Ag18 57.05(2) . 4 ?
Ag3 Ag23 Ag18 158.82(3) . 4 ?
S21 Ag23 Ag15 87.62(8) . 3_455 ?
S19 Ag23 Ag15 83.50(7) . 3_455 ?
B2 Ag23 Ag15 83.62(3) . 3_455 ?
Ag3 Ag23 Ag15 82.59(3) . 3_455 ?
Ag18 Ag23 Ag15 113.23(3) 4 3_455 ?
S21 Ag23 Ag28 75.96(8) . . ?
S19 Ag23 Ag28 113.36(8) . . ?
B2 Ag23 Ag28 80.15(3) . . ?
Ag3 Ag23 Ag28 95.87(3) . . ?
Ag18 Ag23 Ag28 64.54(2) 4 . ?
Ag15 Ag23 Ag28 161.44(3) 3_455 . ?
S21 Ag23 Ag15 131.49(8) . 4 ?
S19 Ag23 Ag15 46.02(8) . 4 ?
B2 Ag23 Ag15 81.80(3) . 4 ?
Ag3 Ag23 Ag15 139.89(3) . 4 ?
Ag18 Ag23 Ag15 60.92(2) 4 4 ?
Ag15 Ag23 Ag15 61.99(3) 3_455 4 ?
Ag28 Ag23 Ag15 123.75(3) . 4 ?
S21 Ag23 Ag24 123.10(8) . . ?
S19 Ag23 Ag24 63.97(7) . . ?
B2 Ag23 Ag24 129.19(3) . . ?
Ag3 Ag23 Ag24 95.63(3) . . ?
Ag18 Ag23 Ag24 80.20(3) 4 . ?
Ag15 Ag23 Ag24 142.93(3) 3_455 . ?
Ag28 Ag23 Ag24 55.60(2) . . ?
Ag15 Ag23 Ag24 101.61(3) 4 . ?
S18 Ag24 S4 125.06(9) 4 . ?
S18 Ag24 S20 143.05(10) 4 . ?
S4 Ag24 S20 91.74(9) . . ?
S18 Ag24 B3 93.57(8) 4 . ?
S4 Ag24 B3 136.50(7) . . ?
S20 Ag24 B3 51.07(8) . . ?
S18 Ag24 Ag28 49.18(7) 4 . ?
S4 Ag24 Ag28 78.98(6) . . ?
S20 Ag24 Ag28 162.82(7) . . ?
B3 Ag24 Ag28 142.68(4) . . ?
S18 Ag24 Ag25 102.51(7) 4 . ?
S4 Ag24 Ag25 123.64(6) . . ?
S20 Ag24 Ag25 50.49(7) . . ?
B3 Ag24 Ag25 53.35(3) . . ?
Ag28 Ag24 Ag25 123.88(3) . . ?
S18 Ag24 Ag23 76.17(7) 4 . ?
S4 Ag24 Ag23 61.22(6) . . ?
S20 Ag24 Ag23 127.21(7) . . ?
B3 Ag24 Ag23 119.78(4) . . ?
Ag28 Ag24 Ag23 60.45(2) . . ?
Ag25 Ag24 Ag23 173.09(3) . . ?
S22 Ag25 S11 99.60(10) . . ?
S22 Ag25 S20 149.28(10) . . ?
S11 Ag25 S20 100.17(10) . . ?
S22 Ag25 B3 113.21(9) . . ?
S11 Ag25 B3 146.98(8) . . ?
S20 Ag25 B3 52.23(8) . . ?
S22 Ag25 Ag17 53.14(8) . 4 ?
S11 Ag25 Ag17 151.54(7) . 4 ?
S20 Ag25 Ag17 108.00(8) . 4 ?
B3 Ag25 Ag17 60.28(3) . 4 ?
S22 Ag25 Ag9 111.61(8) . . ?
S11 Ag25 Ag9 52.57(7) . . ?
S20 Ag25 Ag9 64.45(7) . . ?
B3 Ag25 Ag9 114.09(4) . . ?
Ag17 Ag25 Ag9 138.84(3) 4 . ?
S22 Ag25 Ag13 91.22(8) . 4 ?
S11 Ag25 Ag13 121.79(7) . 4 ?
S20 Ag25 Ag13 98.02(7) . 4 ?
B3 Ag25 Ag13 56.44(4) . 4 ?
Ag17 Ag25 Ag13 58.77(2) 4 4 ?
Ag9 Ag25 Ag13 156.83(3) . 4 ?
S22 Ag25 Ag24 96.36(8) . . ?
S11 Ag25 Ag24 127.83(7) . . ?
S20 Ag25 Ag24 52.93(7) . . ?
B3 Ag25 Ag24 54.19(3) . . ?
Ag17 Ag25 Ag24 69.88(3) 4 . ?
Ag9 Ag25 Ag24 75.35(3) . . ?
Ag13 Ag25 Ag24 107.05(3) 4 . ?
S15 Ag26 S10 122.55(10) 4 . ?
S15 Ag26 S17 141.72(10) 4 3 ?
S10 Ag26 S17 95.12(8) . 3 ?
S15 Ag26 B1 93.50(8) 4 3 ?
S10 Ag26 B1 139.99(7) . 3 ?
S17 Ag26 B1 48.55(6) 3 3 ?
S15 Ag26 Ag22 48.62(7) 4 . ?
S10 Ag26 Ag22 77.04(7) . . ?
S17 Ag26 Ag22 166.82(6) 3 . ?
B1 Ag26 Ag22 141.83(3) 3 . ?
S15 Ag26 Ag27 77.31(7) 4 3_545 ?
S10 Ag26 Ag27 57.19(7) . 3_545 ?
S17 Ag26 Ag27 125.11(6) 3 3_545 ?
B1 Ag26 Ag27 124.95(3) 3 3_545 ?
Ag22 Ag26 Ag27 59.38(2) . 3_545 ?
S15 Ag27 S21 149.94(10) 1_565 . ?
S15 Ag27 B2 117.18(8) 1_565 . ?
S21 Ag27 B2 51.28(8) . . ?
S15 Ag27 S10 98.02(10) 1_565 3_455 ?
S21 Ag27 S10 101.03(10) . 3_455 ?
B2 Ag27 S10 143.99(7) . 3_455 ?
S15 Ag27 Ag22 119.39(8) 1_565 3_455 ?
S21 Ag27 Ag22 87.86(7) . 3_455 ?
B2 Ag27 Ag22 79.93(2) . 3_455 ?
S10 Ag27 Ag22 76.05(7) 3_455 3_455 ?
S15 Ag27 Ag4 122.64(8) 1_565 . ?
S21 Ag27 Ag4 60.01(8) . . ?
B2 Ag27 Ag4 111.27(3) . . ?
S10 Ag27 Ag4 47.13(6) 3_455 . ?
Ag22 Ag27 Ag4 97.09(3) 3_455 . ?
S15 Ag27 Ag26 68.00(8) 1_565 3_455 ?
S21 Ag27 Ag26 141.90(7) . 3_455 ?
B2 Ag27 Ag26 130.95(3) . 3_455 ?
S10 Ag27 Ag26 54.29(6) 3_455 3_455 ?
Ag22 Ag27 Ag26 60.06(2) 3_455 3_455 ?
Ag4 Ag27 Ag26 101.36(3) . 3_455 ?
S15 Ag27 Ag28 77.50(8) 1_565 . ?
S21 Ag27 Ag28 72.89(7) . . ?
B2 Ag27 Ag28 77.69(2) . . ?
S10 Ag27 Ag28 119.87(7) 3_455 . ?
Ag22 Ag27 Ag28 156.62(3) 3_455 . ?
Ag4 Ag27 Ag28 84.86(3) . . ?
Ag26 Ag27 Ag28 142.54(3) 3_455 . ?
S15 Ag27 Ag27 77.68(8) 1_565 2 ?
S21 Ag27 Ag27 105.17(7) . 2 ?
B2 Ag27 Ag27 55.47(2) . 2 ?
S10 Ag27 Ag27 132.58(7) 3_455 2 ?
Ag22 Ag27 Ag27 66.32(3) 3_455 2 ?
Ag4 Ag27 Ag27 159.25(3) . 2 ?
Ag26 Ag27 Ag27 81.591(19) 3_455 2 ?
Ag28 Ag27 Ag27 105.42(3) . 2 ?
S5 Ag28 S18 158.43(10) . 4 ?
S5 Ag28 Ag13 74.04(7) . 1_565 ?
S18 Ag28 Ag13 112.63(8) 4 1_565 ?
S5 Ag28 Ag24 108.38(7) . . ?
S18 Ag28 Ag24 52.44(7) 4 . ?
Ag13 Ag28 Ag24 138.33(3) 1_565 . ?
S5 Ag28 Ag27 70.19(7) . . ?
S18 Ag28 Ag27 130.66(7) 4 . ?
Ag13 Ag28 Ag27 77.42(2) 1_565 . ?
Ag24 Ag28 Ag27 143.72(3) . . ?
S5 Ag28 Ag23 101.42(7) . . ?
S18 Ag28 Ag23 79.77(7) 4 . ?
Ag13 Ag28 Ag23 157.71(3) 1_565 . ?
Ag24 Ag28 Ag23 63.95(2) . . ?
Ag27 Ag28 Ag23 80.52(2) . . ?
S5 Ag28 Ag22 123.21(7) . 4 ?
S18 Ag28 Ag22 76.45(7) 4 4 ?
Ag13 Ag28 Ag22 63.43(2) 1_565 4 ?
Ag24 Ag28 Ag22 128.38(3) . 4 ?
Ag27 Ag28 Ag22 65.39(2) . 4 ?
Ag23 Ag28 Ag22 104.19(3) . 4 ?
S22 Ag29 S16 139.10(11) . 1_565 ?
S22 Ag29 S6 100.93(10) . . ?
S16 Ag29 S6 96.48(10) 1_565 . ?
S22 Ag29 B3 108.23(8) . 4 ?
S16 Ag29 B3 51.76(8) 1_565 4 ?
S6 Ag29 B3 147.53(7) . 4 ?
S22 Ag29 Ag21 90.55(8) . 4 ?
S16 Ag29 Ag21 101.45(8) 1_565 4 ?
S6 Ag29 Ag21 136.90(7) . 4 ?
B3 Ag29 Ag21 57.98(3) 4 4 ?
S22 Ag29 Ag20 50.55(8) . 4 ?
S16 Ag29 Ag20 104.24(8) 1_565 4 ?
S6 Ag29 Ag20 151.25(7) . 4 ?
B3 Ag29 Ag20 58.48(3) 4 4 ?
Ag21 Ag29 Ag20 57.92(2) 4 4 ?
S22 Ag30 S12 100.38(10) . . ?
S22 Ag30 B1 110.58(8) . 3 ?
S12 Ag30 B1 149.04(6) . 3 ?
S22 Ag30 S17 148.13(9) . 3 ?
S12 Ag30 S17 103.02(8) . 3 ?
B1 Ag30 S17 48.89(6) 3 3 ?
S22 Ag30 Ag12 112.33(8) . . ?
S12 Ag30 Ag12 51.25(6) . . ?
B1 Ag30 Ag12 113.53(3) 3 . ?
S17 Ag30 Ag12 68.34(6) 3 . ?
S22 Ag30 Ag19 87.39(8) . 4 ?
S12 Ag30 Ag19 129.19(6) . 4 ?
B1 Ag30 Ag19 54.56(3) 3 4 ?
S17 Ag30 Ag19 94.24(6) 3 4 ?
Ag12 Ag30 Ag19 160.22(3) . 4 ?
S22 Ag30 Ag16 52.30(8) . 4 ?
S12 Ag30 Ag16 152.68(6) . 4 ?
B1 Ag30 Ag16 58.28(2) 3 4 ?
S17 Ag30 Ag16 102.53(6) 3 4 ?
Ag12 Ag30 Ag16 133.21(3) . 4 ?
Ag19 Ag30 Ag16 57.75(2) 4 4 ?
S17 B1 S17 171.03(14) . 2 ?
S17 B1 Ag19 52.62(7) . . ?
S17 B1 Ag19 119.50(8) 2 . ?
S17 B1 Ag19 119.50(8) . 2 ?
S17 B1 Ag19 52.62(7) 2 2 ?
Ag19 B1 Ag19 85.69(5) . 2 ?
S17 B1 Ag30 109.88(7) . 4_545 ?
S17 B1 Ag30 67.24(6) 2 4_545 ?
Ag19 B1 Ag30 68.31(3) . 4_545 ?
Ag19 B1 Ag30 85.98(4) 2 4_545 ?
S17 B1 Ag30 67.24(6) . 3_445 ?
S17 B1 Ag30 109.88(7) 2 3_445 ?
Ag19 B1 Ag30 85.98(4) . 3_445 ?
Ag19 B1 Ag30 68.31(3) 2 3_445 ?
Ag30 B1 Ag30 145.10(7) 4_545 3_445 ?
S17 B1 Ag26 65.59(7) . 3_445 ?
S17 B1 Ag26 122.47(8) 2 3_445 ?
Ag19 B1 Ag26 118.03(2) . 3_445 ?
Ag19 B1 Ag26 133.591(19) 2 3_445 ?
Ag30 B1 Ag26 138.57(5) 4_545 3_445 ?
Ag30 B1 Ag26 74.01(2) 3_445 3_445 ?
S17 B1 Ag26 122.47(8) . 4_545 ?
S17 B1 Ag26 65.59(7) 2 4_545 ?
Ag19 B1 Ag26 133.591(19) . 4_545 ?
Ag19 B1 Ag26 118.03(2) 2 4_545 ?
Ag30 B1 Ag26 74.01(2) 4_545 4_545 ?
Ag30 B1 Ag26 138.57(5) 3_445 4_545 ?
Ag26 B1 Ag26 75.50(5) 3_445 4_545 ?
S17 B1 Ag16 56.71(6) . . ?
S17 B1 Ag16 126.20(7) 2 . ?
Ag19 B1 Ag16 64.67(2) . . ?
Ag19 B1 Ag16 145.07(5) 2 . ?
Ag30 B1 Ag16 66.71(2) 4_545 . ?
Ag30 B1 Ag16 123.77(2) 3_445 . ?
Ag26 B1 Ag16 79.31(3) 3_445 . ?
Ag26 B1 Ag16 76.27(3) 4_545 . ?
S17 B1 Ag16 126.20(7) . 2 ?
S17 B1 Ag16 56.71(6) 2 2 ?
Ag19 B1 Ag16 145.07(5) . 2 ?
Ag19 B1 Ag16 64.67(2) 2 2 ?
Ag30 B1 Ag16 123.77(2) 4_545 2 ?
Ag30 B1 Ag16 66.70(2) 3_445 2 ?
Ag26 B1 Ag16 76.27(3) 3_445 2 ?
Ag26 B1 Ag16 79.31(3) 4_545 2 ?
Ag16 B1 Ag16 148.99(7) . 2 ?
S21 B2 S21 176.42(16) . 2 ?
S21 B2 Ag23 54.00(8) . . ?
S21 B2 Ag23 123.24(9) 2 . ?
S21 B2 Ag23 123.24(9) . 2 ?
S21 B2 Ag23 54.00(8) 2 2 ?
Ag23 B2 Ag23 101.32(7) . 2 ?
S21 B2 Ag18 64.26(8) . 3_455 ?
S21 B2 Ag18 114.93(8) 2 3_455 ?
Ag23 B2 Ag18 95.17(4) . 3_455 ?
Ag23 B2 Ag18 69.67(3) 2 3_455 ?
S21 B2 Ag18 114.93(8) . 4 ?
S21 B2 Ag18 64.26(8) 2 4 ?
Ag23 B2 Ag18 69.67(3) . 4 ?
Ag23 B2 Ag18 95.17(4) 2 4 ?
Ag18 B2 Ag18 156.59(7) 3_455 4 ?
S21 B2 Ag27 58.41(8) . . ?
S21 B2 Ag27 125.13(9) 2 . ?
Ag23 B2 Ag27 97.91(2) . . ?
Ag23 B2 Ag27 155.07(4) 2 . ?
Ag18 B2 Ag27 93.02(3) 3_455 . ?
Ag18 B2 Ag27 106.35(4) 4 . ?
S21 B2 Ag27 125.13(9) . 2 ?
S21 B2 Ag27 58.41(8) 2 2 ?
Ag23 B2 Ag27 155.07(4) . 2 ?
Ag23 B2 Ag27 97.91(2) 2 2 ?
Ag18 B2 Ag27 106.35(4) 3_455 2 ?
Ag18 B2 Ag27 93.02(3) 4 2 ?
Ag27 B2 Ag27 69.06(5) . 2 ?
S16 B3 S20 171.08(12) 4 . ?
S16 B3 Ag25 116.46(9) 4 . ?
S20 B3 Ag25 60.44(8) . . ?
S16 B3 Ag29 60.44(8) 4 4_545 ?
S20 B3 Ag29 115.72(8) . 4_545 ?
Ag25 B3 Ag29 139.66(6) . 4_545 ?
S16 B3 Ag13 58.70(9) 4 4 ?
S20 B3 Ag13 113.50(9) . 4 ?
Ag25 B3 Ag13 67.85(4) . 4 ?
Ag29 B3 Ag13 80.35(4) 4_545 4 ?
S16 B3 Ag24 125.81(9) 4 . ?
S20 B3 Ag24 62.30(8) . . ?
Ag25 B3 Ag24 72.46(4) . . ?
Ag29 B3 Ag24 145.23(6) 4_545 . ?
Ag13 B3 Ag24 133.82(5) 4 . ?
S16 B3 Ag21 114.77(9) 4 . ?
S20 B3 Ag21 57.52(7) . . ?
Ag25 B3 Ag21 84.50(4) . . ?
Ag29 B3 Ag21 65.30(3) 4_545 . ?
Ag13 B3 Ag21 79.59(4) 4 . ?
Ag24 B3 Ag21 119.35(6) . . ?
S16 B3 Ag14 60.11(9) 4 4 ?
S20 B3 Ag14 128.20(9) . 4 ?
Ag25 B3 Ag14 138.44(5) . 4 ?
Ag29 B3 Ag14 78.21(4) 4_545 4 ?
Ag13 B3 Ag14 118.07(5) 4 4 ?
Ag24 B3 Ag14 78.59(4) . 4 ?
Ag21 B3 Ag14 136.40(5) . 4 ?
S16 B3 Ag17 62.17(8) 4 4 ?
S20 B3 Ag17 119.75(8) . 4 ?
Ag25 B3 Ag17 65.08(3) . 4 ?
Ag29 B3 Ag17 122.04(6) 4_545 4 ?
Ag13 B3 Ag17 63.73(3) 4 4 ?
Ag24 B3 Ag17 78.86(4) . 4 ?
Ag21 B3 Ag17 138.67(5) . 4 ?
Ag14 B3 Ag17 80.72(4) 4 4 ?
S16 B3 Ag20 120.67(9) 4 . ?
S20 B3 Ag20 61.47(8) . . ?
Ag25 B3 Ag20 121.89(5) . . ?
Ag29 B3 Ag20 68.69(3) 4_545 . ?
Ag13 B3 Ag20 138.81(5) 4 . ?
Ag24 B3 Ag20 82.78(4) . . ?
Ag21 B3 Ag20 63.31(3) . . ?
Ag14 B3 Ag20 82.19(4) 4 . ?
Ag17 B3 Ag20 157.01(5) 4 . ?
Sb1 S1 Ag5 100.80(10) . . ?
Sb1 S1 Ag1 104.10(11) . . ?
Ag5 S1 Ag1 111.53(11) . . ?
Sb1 S1 Ag16 113.93(11) . . ?
Ag5 S1 Ag16 124.60(12) . . ?
Ag1 S1 Ag16 100.53(10) . . ?
Sb1 S2 Ag2 98.61(10) . . ?
Sb1 S2 Ag6 104.30(11) . . ?
Ag2 S2 Ag6 118.56(12) . . ?
Sb1 S2 Ag20 107.15(11) . . ?
Ag2 S2 Ag20 127.14(12) . . ?
Ag6 S2 Ag20 98.86(10) . . ?
Sb1 S3 Ag7 102.06(12) . . ?
Sb1 S3 Ag8 96.83(11) . . ?
Ag7 S3 Ag8 113.06(13) . . ?
Sb1 S3 Ag17 107.89(12) . . ?
Ag7 S3 Ag17 100.59(11) . . ?
Ag8 S3 Ag17 132.71(13) . . ?
Sb2 S4 Ag3 102.56(10) . . ?
Sb2 S4 Ag6 104.48(10) . . ?
Ag3 S4 Ag6 115.42(10) . . ?
Sb2 S4 Ag24 101.71(10) . . ?
Ag3 S4 Ag24 135.14(11) . . ?
Ag6 S4 Ag24 93.94(9) . . ?
Ag28 S5 Sb2 102.11(11) . . ?
Ag28 S5 Ag5 119.52(12) . 1_565 ?
Sb2 S5 Ag5 99.55(10) . 1_565 ?
Ag28 S5 Ag4 121.88(11) . . ?
Sb2 S5 Ag4 101.19(10) . . ?
Ag5 S5 Ag4 107.81(10) 1_565 . ?
Ag9 S6 Sb2 103.93(11) . . ?
Ag9 S6 Ag10 111.03(11) . . ?
Sb2 S6 Ag10 100.74(11) . . ?
Ag9 S6 Ag29 127.80(12) . . ?
Sb2 S6 Ag29 124.15(12) . . ?
Ag10 S6 Ag29 80.96(8) . . ?
Ag15 S7 Sb3 101.56(11) . . ?
Ag15 S7 Ag2 126.19(12) . 3_545 ?
Sb3 S7 Ag2 101.58(11) . 3_545 ?
Ag15 S7 Ag3 113.24(11) . 3_545 ?
Sb3 S7 Ag3 101.68(11) . 3_545 ?
Ag2 S7 Ag3 108.54(11) 3_545 3_545 ?
Sb3 S8 Ag7 102.72(11) . . ?
Sb3 S8 Ag11 103.66(10) . . ?
Ag7 S8 Ag11 117.93(11) . . ?
Sb3 S8 Ag14 97.95(10) . . ?
Ag7 S8 Ag14 86.36(9) . . ?
Ag11 S8 Ag14 142.13(12) . . ?
Sb3 S8 Ag18 125.72(11) . . ?
Ag7 S8 Ag18 127.65(11) . . ?
Ag11 S8 Ag18 72.17(7) . . ?
Ag14 S8 Ag18 69.95(7) . . ?
Sb4 S9 Ag11 103.49(11) . . ?
Sb4 S9 Ag22 100.04(11) . . ?
Ag11 S9 Ag22 113.68(11) . . ?
Sb4 S9 Ag8 100.64(11) . . ?
Ag11 S9 Ag8 115.31(12) . . ?
Ag22 S9 Ag8 119.66(11) . . ?
Sb4 S10 Ag4 102.41(12) . 3_545 ?
Sb4 S10 Ag1 103.83(12) . 3 ?
Ag4 S10 Ag1 120.71(14) 3_545 3 ?
Sb4 S10 Ag26 96.33(11) . . ?
Ag4 S10 Ag26 141.33(14) 3_545 . ?
Ag1 S10 Ag26 86.25(9) 3 . ?
Sb4 S10 Ag27 123.82(13) . 3_545 ?
Ag4 S10 Ag27 72.94(8) 3_545 3_545 ?
Ag1 S10 Ag27 127.16(13) 3 3_545 ?
Ag26 S10 Ag27 68.52(8) . 3_545 ?
Sb4 S11 Ag12 98.84(11) . . ?
Sb4 S11 Ag9 97.99(11) . . ?
Ag12 S11 Ag9 97.81(11) . . ?
Sb4 S11 Ag25 131.57(13) . . ?
Ag12 S11 Ag25 129.40(12) . . ?
Ag9 S11 Ag25 74.17(8) . . ?
Sb3 S12 Ag10 101.24(10) 1_565 . ?
Sb3 S12 Ag12 99.85(10) 1_565 . ?
Ag10 S12 Ag12 109.25(10) . . ?
Sb3 S12 Ag30 124.06(11) 1_565 . ?
Ag10 S12 Ag30 134.07(11) . . ?
Ag12 S12 Ag30 72.87(7) . . ?
Ag9 S13 Ag5 110.94(11) 7 . ?
Ag9 S13 Ag8 100.01(12) 7 7 ?
Ag5 S13 Ag8 107.60(11) . 7 ?
Ag9 S13 Ag10 91.31(9) 7 1_545 ?
Ag5 S13 Ag10 93.05(11) . 1_545 ?
Ag8 S13 Ag10 150.73(13) 7 1_545 ?
Ag9 S13 Ag6 83.69(9) 7 7 ?
Ag5 S13 Ag6 161.61(14) . 7 ?
Ag8 S13 Ag6 79.54(9) 7 7 ?
Ag10 S13 Ag6 74.97(8) 1_545 7 ?
Ag9 S13 Ag7 154.45(13) 7 . ?
Ag5 S13 Ag7 91.30(10) . . ?
Ag8 S13 Ag7 84.24(8) 7 . ?
Ag10 S13 Ag7 74.55(9) 1_545 . ?
Ag6 S13 Ag7 72.25(8) 7 . ?
Ag3 S14 Ag12 103.80(10) 7_565 . ?
Ag3 S14 Ag2 110.01(12) 7_565 3 ?
Ag12 S14 Ag2 98.19(10) . 3 ?
Ag3 S14 Ag4 90.56(9) 7_565 7_565 ?
Ag12 S14 Ag4 91.05(10) . 7_565 ?
Ag2 S14 Ag4 154.47(12) 3 7_565 ?
Ag3 S14 Ag11 89.43(9) 7_565 5_665 ?
Ag12 S14 Ag11 161.75(13) . 5_665 ?
Ag2 S14 Ag11 88.76(9) 3 5_665 ?
Ag4 S14 Ag11 76.09(8) 7_565 5_665 ?
Ag3 S14 Ag1 164.77(13) 7_565 3 ?
Ag12 S14 Ag1 84.84(9) . 3 ?
Ag2 S14 Ag1 80.60(8) 3 3 ?
Ag4 S14 Ag1 76.59(9) 7_565 3 ?
Ag11 S14 Ag1 79.66(8) 5_665 3 ?
Ag13 S15 Ag22 87.96(11) . 4_545 ?
Ag13 S15 Ag27 109.23(13) . 1_545 ?
Ag22 S15 Ag27 91.83(11) 4_545 1_545 ?
Ag13 S15 Ag26 134.52(14) . 4_545 ?
Ag22 S15 Ag26 79.33(10) 4_545 4_545 ?
Ag27 S15 Ag26 114.62(12) 1_545 4_545 ?
Ag13 S15 Ag16 76.79(9) . . ?
Ag22 S15 Ag16 137.55(14) 4_545 . ?
Ag27 S15 Ag16 130.55(14) 1_545 . ?
Ag26 S15 Ag16 83.77(9) 4_545 . ?
B3 S16 Ag13 69.27(10) 4_545 . ?
B3 S16 Ag29 67.80(9) 4_545 1_545 ?
Ag13 S16 Ag29 88.26(10) . 1_545 ?
B3 S16 Ag14 69.02(10) 4_545 . ?
Ag13 S16 Ag14 137.15(15) . . ?
Ag29 S16 Ag14 84.97(10) 1_545 . ?
B3 S16 Ag17 69.44(9) 4_545 . ?
Ag13 S16 Ag17 69.14(8) . . ?
Ag29 S16 Ag17 136.44(14) 1_545 . ?
Ag14 S16 Ag17 87.45(9) . . ?
B3 S16 Ag5 135.82(14) 4_545 . ?
Ag13 S16 Ag5 66.55(8) . . ?
Ag29 S16 Ag5 109.91(10) 1_545 . ?
Ag14 S16 Ag5 154.01(14) . . ?
Ag17 S16 Ag5 94.96(9) . . ?
Ag19 S17 B1 72.00(9) . . ?
Ag19 S17 Ag16 77.23(8) . . ?
B1 S17 Ag16 72.75(8) . . ?
Ag19 S17 Ag2 76.95(8) . . ?
B1 S17 Ag2 147.67(12) . . ?
Ag16 S17 Ag2 109.09(9) . . ?
Ag19 S17 Ag26 137.57(12) . 3_445 ?
B1 S17 Ag26 65.86(7) . 3_445 ?
Ag16 S17 Ag26 85.76(8) . 3_445 ?
Ag2 S17 Ag26 145.43(11) . 3_445 ?
Ag19 S17 Ag30 93.21(9) . 3_445 ?
B1 S17 Ag30 63.87(6) . 3_445 ?
Ag16 S17 Ag30 136.37(11) . 3_445 ?
Ag2 S17 Ag30 109.89(9) . 3_445 ?
Ag26 S17 Ag30 72.97(6) 3_445 3_445 ?
Ag19 S17 Ag1 139.89(11) . . ?
B1 S17 Ag1 140.52(11) . . ?
Ag16 S17 Ag1 90.47(8) . . ?
Ag2 S17 Ag1 71.30(7) . . ?
Ag26 S17 Ag1 77.73(7) 3_445 . ?
Ag30 S17 Ag1 120.14(9) 3_445 . ?
Ag28 S18 Ag18 90.13(10) 4_545 . ?
Ag28 S18 Ag21 90.70(10) 4_545 . ?
Ag18 S18 Ag21 107.70(11) . . ?
Ag28 S18 Ag24 78.38(9) 4_545 4_545 ?
Ag18 S18 Ag24 116.14(12) . 4_545 ?
Ag21 S18 Ag24 134.61(12) . 4_545 ?
Ag28 S18 Ag17 138.53(12) 4_545 . ?
Ag18 S18 Ag17 131.17(12) . . ?
Ag21 S18 Ag17 74.91(8) . . ?
Ag24 S18 Ag17 84.65(8) 4_545 . ?
Ag15 S19 Ag23 87.01(10) 4 . ?
Ag15 S19 Ag19 85.96(10) 4 . ?
Ag23 S19 Ag19 105.05(12) . . ?
Ag15 S19 Ag14 77.98(10) 4 4 ?
Ag23 S19 Ag14 115.89(11) . 4 ?
Ag19 S19 Ag14 134.71(12) . 4 ?
Ag15 S19 Ag20 136.20(12) 4 . ?
Ag23 S19 Ag20 134.87(13) . . ?
Ag19 S19 Ag20 72.71(7) . . ?
Ag14 S19 Ag20 90.33(9) 4 . ?
B3 S20 Ag21 70.07(9) . . ?
B3 S20 Ag25 67.33(9) . . ?
Ag21 S20 Ag25 93.93(11) . . ?
B3 S20 Ag24 66.63(8) . . ?
Ag21 S20 Ag24 136.01(14) . . ?
Ag25 S20 Ag24 76.58(8) . . ?
B3 S20 Ag20 69.92(9) . . ?
Ag21 S20 Ag20 69.72(7) . . ?
Ag25 S20 Ag20 137.21(13) . . ?
Ag24 S20 Ag20 88.31(9) . . ?
B3 S20 Ag8 140.71(12) . . ?
Ag21 S20 Ag8 70.64(7) . . ?
Ag25 S20 Ag8 115.92(11) . . ?
Ag24 S20 Ag8 151.89(13) . . ?
Ag20 S20 Ag8 96.13(9) . . ?
B3 S20 Ag6 142.70(13) . . ?
Ag21 S20 Ag6 128.85(11) . . ?
Ag25 S20 Ag6 130.60(11) . . ?
Ag24 S20 Ag6 84.90(9) . . ?
Ag20 S20 Ag6 86.37(9) . . ?
Ag8 S20 Ag6 67.78(8) . . ?
Ag23 S21 B2 69.49(10) . . ?
Ag23 S21 Ag27 116.88(13) . . ?
B2 S21 Ag27 70.31(9) . . ?
Ag23 S21 Ag3 73.92(9) . . ?
B2 S21 Ag3 141.15(14) . . ?
Ag27 S21 Ag3 141.13(13) . . ?
Ag23 S21 Ag18 104.83(11) . 3_455 ?
B2 S21 Ag18 65.20(8) . 3_455 ?
Ag27 S21 Ag18 99.84(10) . 3_455 ?
Ag3 S21 Ag18 113.74(11) . 3_455 ?
Ag23 S21 Ag4 132.53(13) . . ?
B2 S21 Ag4 140.43(13) . . ?
Ag27 S21 Ag4 70.16(8) . . ?
Ag3 S21 Ag4 75.95(9) . . ?
Ag18 S21 Ag4 120.67(11) 3_455 . ?
Ag25 S22 Ag29 99.93(12) . . ?
Ag25 S22 Ag30 102.83(12) . . ?
Ag29 S22 Ag30 105.79(12) . . ?
Ag25 S22 Ag17 75.56(9) . 4 ?
Ag29 S22 Ag17 95.10(11) . 4 ?
Ag30 S22 Ag17 158.94(15) . 4 ?
Ag25 S22 Ag20 158.09(15) . 4 ?
Ag29 S22 Ag20 79.93(9) . 4 ?
Ag30 S22 Ag20 98.21(11) . 4 ?
Ag17 S22 Ag20 82.61(10) 4 4 ?
Ag25 S22 Ag16 95.20(11) . 4 ?
Ag29 S22 Ag16 163.50(14) . 4 ?
Ag30 S22 Ag16 76.94(10) . 4 ?
Ag17 S22 Ag16 82.27(10) 4 4 ?
Ag20 S22 Ag16 83.58(11) 4 4 ?
 
_diffrn_measured_fraction_theta_max    0.991
_diffrn_reflns_theta_full              34.72
_diffrn_measured_fraction_theta_full   0.991
_refine_diff_density_max    1.424
_refine_diff_density_min   -1.485
_refine_diff_density_rms    0.949
