 
data_pohlite
 
_audit_creation_method            'SHELXL-2016/6'
_shelx_SHELXL_version_number      '2016/6'
_chemical_name_mineral            'pohlite'
_chemical_compound_source         'La Compania mine, Sierra Gorda, Chile'
_chemical_formula_sum
 'Cl9 H4 I O7 Pb7' 
_chemical_formula_weight          2012.31

loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'Cl'  'Cl'   0.1484   0.1585
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'I'  'I'  -0.4742   1.8119
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'O'  'O'   0.0106   0.0060
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Pb'  'Pb'  -3.3944  10.1111
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'H'  'H'   0.0000   0.0000
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_space_group_crystal_system       triclinic
_space_group_IT_number            2
_space_group_name_H-M_alt         'P -1'
_space_group_name_Hall            '-P 1'
 
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
 
loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 '-x, -y, -z'
 
_cell_length_a                    7.3366(5)
_cell_length_b                    9.5130(9)
_cell_length_c                    16.2434(15)
_cell_angle_alpha                 81.592(7)
_cell_angle_beta                  84.955(7)
_cell_angle_gamma                 89.565(6)
_cell_volume                      1117.13(17)
_cell_formula_units_Z             2
_cell_measurement_temperature     293(2)
_cell_measurement_reflns_used     13815
_cell_measurement_theta_min       3.1
_cell_measurement_theta_max       27.5
 
_exptl_crystal_description        'block'
_exptl_crystal_colour             'colourless'
_exptl_crystal_density_diffrn     5.982          
_exptl_crystal_F_000              1680
_exptl_crystal_size_max           0.080
_exptl_crystal_size_mid           0.080
_exptl_crystal_size_min           0.080
_exptl_absorpt_coefficient_mu     55.027
_shelx_estimated_absorpt_T_min    0.096
_shelx_estimated_absorpt_T_max    0.096
_exptl_absorpt_correction_type    'Multi-scan'
_exptl_absorpt_correction_T_max   1.000
_exptl_absorpt_correction_T_min   0.603
_exptl_absorpt_process_details    'Higashi2001'
_diffrn_ambient_temperature       293(2)
_diffrn_radiation_wavelength      0.71075
_diffrn_radiation_type            MoK\a
_diffrn_source                    'Sealed Tube'
_diffrn_radiation_monochromator   'Graphite Monochromator'
_diffrn_measurement_device_type   'Rigaku R-axis RAPID II'
_diffrn_measurement_method        'profile data from ω-scans'
_diffrn_reflns_number             15819
_diffrn_reflns_av_unetI/netI      0.0533
_diffrn_reflns_av_R_equivalents   0.0716
_diffrn_reflns_limit_h_min        -8
_diffrn_reflns_limit_h_max        7
_diffrn_reflns_limit_k_min        -11
_diffrn_reflns_limit_k_max        11
_diffrn_reflns_limit_l_min        -19
_diffrn_reflns_limit_l_max        19
_diffrn_reflns_theta_min          3.091
_diffrn_reflns_theta_max          25.028
_diffrn_reflns_theta_full         25.028
_diffrn_measured_fraction_theta_max   0.997
_diffrn_measured_fraction_theta_full  0.997
_diffrn_reflns_Laue_measured_fraction_max    0.997
_diffrn_reflns_Laue_measured_fraction_full   0.997
_diffrn_reflns_point_group_measured_fraction_max   0.997
_diffrn_reflns_point_group_measured_fraction_full  0.997
_reflns_number_total              3941
_reflns_number_gt                 3394
_reflns_threshold_expression      'I > 2σ(I)'
_reflns_Friedel_coverage          0.000
_reflns_Friedel_fraction_max      .
_reflns_Friedel_fraction_full     .
 
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
 
_computing_structure_solution     'SHELXT 2014/5 (Sheldrick, 2014)'
_computing_structure_refinement   'SHELXL-2016/6 (Sheldrick, 2016)'
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0163P)²+8.7538P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_hydrogens    difmap
_refine_ls_hydrogen_treatment     refxyz
_refine_ls_extinction_method      'SHELXL-2016/6 (Sheldrick 2016)'
_refine_ls_extinction_coef        0.00056(4)
_refine_ls_extinction_expression
 'Fc^*^=kFc[1+0.001xFc²λ³/sin(2θ)]^-1/4^'
_refine_ls_number_reflns          3941
_refine_ls_number_parameters      221
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0414
_refine_ls_R_factor_gt            0.0328
_refine_ls_wR_factor_ref          0.0709
_refine_ls_wR_factor_gt           0.0671
_refine_ls_goodness_of_fit_ref    1.107
_refine_ls_restrained_S_all       1.107
_refine_ls_shift/su_max           0.001
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_site_symmetry_order  
 _atom_site_calc_flag
 _atom_site_refinement_flags_posn
 _atom_site_refinement_flags_adp
 _atom_site_refinement_flags_occupancy
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Pb1 Pb 0.74291(7) 0.42581(6) 0.91662(3) 0.01969(14) Uani 1 1 d . . . . .
Pb2 Pb 0.79848(7) 0.69909(6) 0.70735(3) 0.02094(14) Uani 1 1 d . . . . .
Pb3 Pb 0.74834(7) 0.85567(6) 0.92106(3) 0.02249(15) Uani 1 1 d . . . . .
Pb4 Pb 0.61383(6) 0.20810(6) 0.67053(3) 0.01864(14) Uani 1 1 d . . . . .
Pb5 Pb 0.19352(6) 0.16830(5) 0.82207(3) 0.01608(14) Uani 1 1 d . . . . .
Pb6 Pb 0.23058(7) 0.44608(6) 0.59329(3) 0.01986(14) Uani 1 1 d . . . . .
Pb7 Pb 0.23103(7) 0.01186(6) 0.59162(3) 0.02008(14) Uani 1 1 d . . . . .
I I 0.38916(10) 0.66590(8) 0.85039(4) 0.01114(18) Uani 1 1 d . . . . .
O1 O 0.5276(11) 0.5352(9) 0.8022(5) 0.017(2) Uani 1 1 d . . . . .
O2 O 0.5285(11) 0.8199(10) 0.8036(5) 0.021(2) Uani 1 1 d . . . . .
O3 O 0.4981(11) 0.6392(9) 0.9484(5) 0.0148(19) Uani 1 1 d . . . . .
OH4 O 0.8560(11) 0.6642(9) 0.8533(5) 0.0155(19) Uani 1 1 d . . . . .
OH5 O 0.3457(11) 0.0515(9) 0.7218(5) 0.0160(19) Uani 1 1 d . . . . .
OH6 O 0.3504(11) 0.3377(9) 0.7234(5) 0.0148(19) Uani 1 1 d . . . . .
OH7 O 0.3884(11) 0.2329(9) 0.5715(5) 0.0127(19) Uani 1 1 d . . . . .
H7 H 0.400(17) 0.265(14) 0.517(8) 0.019 Uiso 1 1 d . U . . .
Cl1 Cl 0.9059(4) 0.3903(3) 0.74684(18) 0.0185(7) Uani 1 1 d . . . . .
Cl2 Cl 0.1639(4) 0.4151(4) 0.93651(18) 0.0201(7) Uani 1 1 d . . . . .
Cl3 Cl 0.6132(4) 0.5275(4) 0.58762(17) 0.0198(7) Uani 1 1 d . . . . .
Cl4 Cl 0.9589(4) 0.2437(4) 0.5241(2) 0.0270(8) Uani 1 1 d . . . . .
Cl5 Cl 0.6159(4) 0.9301(4) 0.58706(18) 0.0213(7) Uani 1 1 d . . . . .
Cl6 Cl 0.8999(4) 0.9852(4) 0.75465(19) 0.0213(7) Uani 1 1 d . . . . .
Cl7 Cl 0.2034(4) 0.7044(3) 0.69307(18) 0.0197(7) Uani 1 1 d . . . . .
Cl8 Cl 0.1417(5) 0.8610(4) 0.9469(2) 0.0270(8) Uani 1 1 d . . . . .
Cl9 Cl 0.5343(4) 0.1516(4) 0.8882(2) 0.0258(8) Uani 1 1 d . . . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Pb1 OH4 2.467(8) . ?
Pb1 O1 2.637(8) . ?
Pb1 O3 2.693(8) 2_667 ?
Pb1 O3 2.775(9) . ?
Pb1 Cl1 2.973(3) . ?
Pb1 Cl2 3.132(3) 2_667 ?
Pb1 Cl2 3.133(3) 1_655 ?
Pb1 Cl9 3.146(3) . ?
Pb1 Cl8 3.406(4) 2_667 ?
Pb1 I 3.5766(10) . ?
Pb2 OH4 2.419(8) . ?
Pb2 O1 2.750(8) . ?
Pb2 O2 2.762(9) . ?
Pb2 Cl7 2.959(3) 1_655 ?
Pb2 Cl1 3.027(3) . ?
Pb2 Cl6 3.049(3) . ?
Pb2 Cl5 3.098(3) . ?
Pb2 Cl3 3.118(3) . ?
Pb2 I 3.6179(9) . ?
Pb3 OH4 2.360(9) . ?
Pb3 O2 2.664(8) . ?
Pb3 O3 2.731(8) . ?
Pb3 Cl6 2.929(3) . ?
Pb3 Cl8 2.954(3) 1_655 ?
Pb3 Cl9 3.212(4) 1_565 ?
Pb3 Cl2 3.301(3) 2_667 ?
Pb3 Cl9 3.566(3) 2_667 ?
Pb3 I 3.5681(9) . ?
Pb3 Cl8 3.813(4) 2_677 ?
Pb4 OH7 2.393(8) . ?
Pb4 OH6 2.444(8) . ?
Pb4 OH5 2.485(8) . ?
Pb4 Cl3 3.139(3) . ?
Pb4 Cl5 3.143(3) 1_545 ?
Pb4 Cl1 3.207(3) . ?
Pb4 Cl6 3.218(3) 1_545 ?
Pb4 Cl4 3.301(3) . ?
Pb4 Cl9 3.495(3) . ?
Pb4 Pb5 3.7578(7) . ?
Pb5 OH5 2.307(8) . ?
Pb5 OH6 2.332(8) . ?
Pb5 Cl9 2.801(3) . ?
Pb5 Cl6 3.147(3) 1_445 ?
Pb5 Cl1 3.168(3) 1_455 ?
Pb5 Cl2 3.195(3) . ?
Pb5 Cl8 3.309(4) 1_545 ?
Pb5 O2 4.142(9) 1_545 ?
Pb5 OH7 4.153(8) . ?
Pb6 OH7 2.384(8) . ?
Pb6 OH6 2.444(8) . ?
Pb6 Cl3 2.908(3) . ?
Pb6 Cl3 3.035(3) 2_666 ?
Pb6 Cl7 3.131(3) . ?
Pb6 Cl4 3.167(3) 1_455 ?
Pb6 Cl1 3.281(3) 1_455 ?
Pb6 Cl4 3.610(4) 2_666 ?
Pb6 Pb7 4.1348(8) . ?
Pb7 OH7 2.373(8) . ?
Pb7 OH5 2.424(8) . ?
Pb7 Cl5 2.921(3) 1_545 ?
Pb7 Cl5 2.993(3) 2_666 ?
Pb7 Cl4 3.109(4) 1_455 ?
Pb7 Cl7 3.139(3) 1_545 ?
Pb7 Cl6 3.415(3) 1_445 ?
Pb7 Cl4 3.637(4) 2_656 ?
I O1 1.820(8) . ?
I O2 1.825(9) . ?
I O3 1.828(7) . ?
I Cl7 2.976(3) . ?
I Cl2 3.010(3) . ?
I Cl8 3.082(4) . ?
I OH4 3.429(8) . ?
O1 OH6 2.811(12) . ?
OH4 Cl8 3.416(8) 1_655 ?
OH4 Cl7 3.460(8) 1_655 ?
OH7 H7 0.90(12) . ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
OH4 Pb1 O1 70.5(3) . . ?
OH4 Pb1 O3 127.2(3) . 2_667 ?
O1 Pb1 O3 101.7(2) . 2_667 ?
OH4 Pb1 O3 67.4(3) . . ?
O1 Pb1 O3 59.6(2) . . ?
O3 Pb1 O3 64.6(3) 2_667 . ?
OH4 Pb1 Cl1 74.89(19) . . ?
O1 Pb1 Cl1 69.42(18) . . ?
O3 Pb1 Cl1 153.31(18) 2_667 . ?
O3 Pb1 Cl1 123.79(17) . . ?
OH4 Pb1 Cl2 73.14(19) . 2_667 ?
O1 Pb1 Cl2 122.52(19) . 2_667 ?
O3 Pb1 Cl2 68.50(17) 2_667 2_667 ?
O3 Pb1 Cl2 65.94(16) . 2_667 ?
Cl1 Pb1 Cl2 137.86(8) . 2_667 ?
OH4 Pb1 Cl2 75.6(2) . 1_655 ?
O1 Pb1 Cl2 136.89(18) . 1_655 ?
O3 Pb1 Cl2 120.00(17) 2_667 1_655 ?
O3 Pb1 Cl2 128.08(17) . 1_655 ?
Cl1 Pb1 Cl2 76.73(8) . 1_655 ?
Cl2 Pb1 Cl2 69.31(10) 2_667 1_655 ?
OH4 Pb1 Cl9 145.66(19) . . ?
O1 Pb1 Cl9 79.4(2) . . ?
O3 Pb1 Cl9 74.03(18) 2_667 . ?
O3 Pb1 Cl9 110.82(17) . . ?
Cl1 Pb1 Cl9 79.52(9) . . ?
Cl2 Pb1 Cl9 139.47(8) 2_667 . ?
Cl2 Pb1 Cl9 120.18(9) 1_655 . ?
OH4 Pb1 Cl8 141.09(19) . 2_667 ?
O1 Pb1 Cl8 148.1(2) . 2_667 ?
O3 Pb1 Cl8 65.35(19) 2_667 2_667 ?
O3 Pb1 Cl8 127.27(17) . 2_667 ?
Cl1 Pb1 Cl8 108.36(9) . 2_667 ?
Cl2 Pb1 Cl8 81.47(8) 2_667 2_667 ?
Cl2 Pb1 Cl8 67.93(8) 1_655 2_667 ?
Cl9 Pb1 Cl8 69.12(8) . 2_667 ?
OH4 Pb1 I 66.22(19) . . ?
O1 Pb1 I 29.41(17) . . ?
O3 Pb1 I 82.27(18) 2_667 . ?
O3 Pb1 I 30.22(15) . . ?
Cl1 Pb1 I 96.65(6) . . ?
Cl2 Pb1 I 94.88(6) 2_667 . ?
Cl2 Pb1 I 141.62(6) 1_655 . ?
Cl9 Pb1 I 94.89(6) . . ?
Cl8 Pb1 I 146.53(6) 2_667 . ?
OH4 Pb2 O1 69.2(2) . . ?
OH4 Pb2 O2 68.4(3) . . ?
O1 Pb2 O2 58.9(3) . . ?
OH4 Pb2 Cl7 79.38(19) . 1_655 ?
O1 Pb2 Cl7 136.15(19) . 1_655 ?
O2 Pb2 Cl7 134.61(18) . 1_655 ?
OH4 Pb2 Cl1 74.5(2) . . ?
O1 Pb2 Cl1 67.22(19) . . ?
O2 Pb2 Cl1 122.15(19) . . ?
Cl7 Pb2 Cl1 75.56(9) 1_655 . ?
OH4 Pb2 Cl6 71.6(2) . . ?
O1 Pb2 Cl6 119.93(18) . . ?
O2 Pb2 Cl6 65.15(19) . . ?
Cl7 Pb2 Cl6 75.04(9) 1_655 . ?
Cl1 Pb2 Cl6 138.34(8) . . ?
OH4 Pb2 Cl5 136.2(2) . . ?
O1 Pb2 Cl5 108.42(19) . . ?
O2 Pb2 Cl5 73.65(19) . . ?
Cl7 Pb2 Cl5 115.43(9) 1_655 . ?
Cl1 Pb2 Cl5 147.23(8) . . ?
Cl6 Pb2 Cl5 73.27(9) . . ?
OH4 Pb2 Cl3 136.5(2) . . ?
O1 Pb2 Cl3 72.91(17) . . ?
O2 Pb2 Cl3 108.67(18) . . ?
Cl7 Pb2 Cl3 116.70(9) 1_655 . ?
Cl1 Pb2 Cl3 71.68(9) . . ?
Cl6 Pb2 Cl3 149.17(9) . . ?
Cl5 Pb2 Cl3 76.03(9) . . ?
OH4 Pb2 I 65.79(18) . . ?
O1 Pb2 I 29.39(18) . . ?
O2 Pb2 I 29.54(18) . . ?
Cl7 Pb2 I 145.16(6) 1_655 . ?
Cl1 Pb2 I 94.82(6) . . ?
Cl6 Pb2 I 92.78(6) . . ?
Cl5 Pb2 I 90.92(6) . . ?
Cl3 Pb2 I 90.56(6) . . ?
OH4 Pb2 Pb1 36.3(2) . . ?
O1 Pb2 Pb1 41.62(17) . . ?
O2 Pb2 Pb1 76.80(18) . . ?
Cl7 Pb2 Pb1 95.78(6) 1_655 . ?
Cl1 Pb2 Pb1 48.13(6) . . ?
Cl6 Pb2 Pb1 107.03(6) . . ?
Cl5 Pb2 Pb1 146.99(6) . . ?
Cl3 Pb2 Pb1 100.22(6) . . ?
I Pb2 Pb1 56.123(17) . . ?
OH4 Pb3 O2 70.9(3) . . ?
OH4 Pb3 O3 69.6(3) . . ?
O2 Pb3 O3 60.0(2) . . ?
OH4 Pb3 Cl6 74.7(2) . . ?
O2 Pb3 Cl6 68.06(19) . . ?
O3 Pb3 Cl6 123.73(16) . . ?
OH4 Pb3 Cl8 79.1(2) . 1_655 ?
O2 Pb3 Cl8 140.3(2) . 1_655 ?
O3 Pb3 Cl8 131.46(19) . 1_655 ?
Cl6 Pb3 Cl8 79.51(9) . 1_655 ?
OH4 Pb3 Cl9 141.6(2) . 1_565 ?
O2 Pb3 Cl9 75.5(2) . 1_565 ?
O3 Pb3 Cl9 108.60(19) . 1_565 ?
Cl6 Pb3 Cl9 75.93(9) . 1_565 ?
Cl8 Pb3 Cl9 118.83(9) 1_655 1_565 ?
OH4 Pb3 Cl2 71.1(2) . 2_667 ?
O2 Pb3 Cl2 119.9(2) . 2_667 ?
O3 Pb3 Cl2 63.92(17) . 2_667 ?
Cl6 Pb3 Cl2 138.30(9) . 2_667 ?
Cl8 Pb3 Cl2 71.39(9) 1_655 2_667 ?
Cl9 Pb3 Cl2 144.67(8) 1_565 2_667 ?
OH4 Pb3 Cl9 129.0(2) . 2_667 ?
O2 Pb3 Cl9 106.93(19) . 2_667 ?
O3 Pb3 Cl9 66.77(17) . 2_667 ?
Cl6 Pb3 Cl9 154.21(9) . 2_667 ?
Cl8 Pb3 Cl9 112.09(8) 1_655 2_667 ?
Cl9 Pb3 Cl9 78.34(9) 1_565 2_667 ?
Cl2 Pb3 Cl9 66.92(8) 2_667 2_667 ?
OH4 Pb3 I 67.15(19) . . ?
O2 Pb3 I 29.80(18) . . ?
O3 Pb3 I 30.17(15) . . ?
Cl6 Pb3 I 95.88(6) . . ?
Cl8 Pb3 I 145.88(7) 1_655 . ?
Cl9 Pb3 I 92.08(6) 1_565 . ?
Cl2 Pb3 I 92.14(6) 2_667 . ?
Cl9 Pb3 I 86.63(5) 2_667 . ?
OH4 Pb3 Cl8 147.2(2) . 2_677 ?
O2 Pb3 Cl8 138.8(2) . 2_677 ?
O3 Pb3 Cl8 131.61(17) . 2_677 ?
Cl6 Pb3 Cl8 101.41(8) . 2_677 ?
Cl8 Pb3 Cl8 68.22(11) 1_655 2_677 ?
Cl9 Pb3 Cl8 63.33(8) 1_565 2_677 ?
Cl2 Pb3 Cl8 94.89(8) 2_667 2_677 ?
Cl9 Pb3 Cl8 64.88(7) 2_667 2_677 ?
I Pb3 Cl8 144.78(6) . 2_677 ?
OH7 Pb4 OH6 70.3(3) . . ?
OH7 Pb4 OH5 69.2(3) . . ?
OH6 Pb4 OH5 67.2(3) . . ?
OH7 Pb4 Cl3 72.3(2) . . ?
OH6 Pb4 Cl3 67.62(19) . . ?
OH5 Pb4 Cl3 127.9(2) . . ?
OH7 Pb4 Cl5 71.9(2) . 1_545 ?
OH6 Pb4 Cl5 128.3(2) . 1_545 ?
OH5 Pb4 Cl5 67.2(2) . 1_545 ?
Cl3 Pb4 Cl5 129.64(8) . 1_545 ?
OH7 Pb4 Cl1 141.3(2) . . ?
OH6 Pb4 Cl1 94.1(2) . . ?
OH5 Pb4 Cl1 138.09(18) . . ?
Cl3 Pb4 Cl1 69.09(8) . . ?
Cl5 Pb4 Cl1 136.83(8) 1_545 . ?
OH7 Pb4 Cl6 142.2(2) . 1_545 ?
OH6 Pb4 Cl6 134.79(19) . 1_545 ?
OH5 Pb4 Cl6 93.3(2) . 1_545 ?
Cl3 Pb4 Cl6 137.68(8) . 1_545 ?
Cl5 Pb4 Cl6 70.42(8) 1_545 1_545 ?
Cl1 Pb4 Cl6 73.35(8) . 1_545 ?
OH7 Pb4 Cl4 93.29(19) . . ?
OH6 Pb4 Cl4 141.21(19) . . ?
OH5 Pb4 Cl4 140.6(2) . . ?
Cl3 Pb4 Cl4 74.00(9) . . ?
Cl5 Pb4 Cl4 73.97(9) 1_545 . ?
Cl1 Pb4 Cl4 76.97(8) . . ?
Cl6 Pb4 Cl4 79.26(8) 1_545 . ?
OH7 Pb4 Cl9 126.94(19) . . ?
OH6 Pb4 Cl9 66.36(19) . . ?
OH5 Pb4 Cl9 66.82(18) . . ?
Cl3 Pb4 Cl9 115.15(8) . . ?
Cl5 Pb4 Cl9 114.50(8) 1_545 . ?
Cl1 Pb4 Cl9 71.35(8) . . ?
Cl6 Pb4 Cl9 68.48(8) 1_545 . ?
Cl4 Pb4 Cl9 139.77(8) . . ?
OH7 Pb4 Pb5 81.68(18) . . ?
OH6 Pb4 Pb5 37.07(18) . . ?
OH5 Pb4 Pb5 36.70(19) . . ?
Cl3 Pb4 Pb5 104.68(6) . . ?
Cl5 Pb4 Pb5 103.85(6) 1_545 . ?
Cl1 Pb4 Pb5 107.27(5) . . ?
Cl6 Pb4 Pb5 104.45(6) 1_545 . ?
Cl4 Pb4 Pb5 174.94(6) . . ?
Cl9 Pb4 Pb5 45.26(5) . . ?
OH5 Pb5 OH6 72.0(3) . . ?
OH5 Pb5 Cl9 82.8(2) . . ?
OH6 Pb5 Cl9 81.4(2) . . ?
OH5 Pb5 Cl6 73.1(2) . 1_445 ?
OH6 Pb5 Cl6 116.1(2) . 1_445 ?
Cl9 Pb5 Cl6 142.65(10) . 1_445 ?
OH5 Pb5 Cl1 112.5(2) . 1_455 ?
OH6 Pb5 Cl1 71.7(2) . 1_455 ?
Cl9 Pb5 Cl1 141.96(9) . 1_455 ?
Cl6 Pb5 Cl1 74.85(8) 1_445 1_455 ?
OH5 Pb5 Cl2 151.9(2) . . ?
OH6 Pb5 Cl2 84.8(2) . . ?
Cl9 Pb5 Cl2 78.15(9) . . ?
Cl6 Pb5 Cl2 133.11(8) 1_445 . ?
Cl1 Pb5 Cl2 73.13(8) 1_455 . ?
OH5 Pb5 Cl8 89.1(2) . 1_545 ?
OH6 Pb5 Cl8 155.2(2) . 1_545 ?
Cl9 Pb5 Cl8 80.43(9) . 1_545 ?
Cl6 Pb5 Cl8 71.25(8) 1_445 1_545 ?
Cl1 Pb5 Cl8 131.86(8) 1_455 1_545 ?
Cl2 Pb5 Cl8 107.68(8) . 1_545 ?
OH5 Pb5 Pb4 40.1(2) . . ?
OH6 Pb5 Pb4 39.2(2) . . ?
Cl9 Pb5 Pb4 62.40(7) . . ?
Cl6 Pb5 Pb4 109.35(6) 1_445 . ?
Cl1 Pb5 Pb4 106.38(6) 1_455 . ?
Cl2 Pb5 Pb4 111.98(6) . . ?
Cl8 Pb5 Pb4 116.48(6) 1_545 . ?
OH5 Pb5 O2 40.0(2) . 1_545 ?
OH6 Pb5 O2 100.1(2) . 1_545 ?
Cl9 Pb5 O2 59.22(13) . 1_545 ?
Cl6 Pb5 O2 84.47(13) 1_445 1_545 ?
Cl1 Pb5 O2 150.63(13) 1_455 1_545 ?
Cl2 Pb5 O2 135.39(13) . 1_545 ?
Cl8 Pb5 O2 55.85(13) 1_545 1_545 ?
Pb4 Pb5 O2 60.95(11) . 1_545 ?
OH5 Pb5 OH7 39.0(2) . . ?
OH6 Pb5 OH7 39.5(2) . . ?
Cl9 Pb5 OH7 97.17(13) . . ?
Cl6 Pb5 OH7 81.87(12) 1_445 . ?
Cl1 Pb5 OH7 79.04(13) 1_455 . ?
Cl2 Pb5 OH7 123.52(13) . . ?
Cl8 Pb5 OH7 127.23(13) 1_545 . ?
Pb4 Pb5 OH7 34.77(11) . . ?
O2 Pb5 OH7 77.56(16) 1_545 . ?
OH7 Pb6 OH6 70.4(3) . . ?
OH7 Pb6 Cl3 76.9(2) . . ?
OH6 Pb6 Cl3 71.8(2) . . ?
OH7 Pb6 Cl3 70.9(2) . 2_666 ?
OH6 Pb6 Cl3 132.0(2) . 2_666 ?
Cl3 Pb6 Cl3 72.70(9) . 2_666 ?
OH7 Pb6 Cl7 146.17(19) . . ?
OH6 Pb6 Cl7 80.0(2) . . ?
Cl3 Pb6 Cl7 78.62(9) . . ?
Cl3 Pb6 Cl7 122.71(9) 2_666 . ?
OH7 Pb6 Cl4 71.6(2) . 1_455 ?
OH6 Pb6 Cl4 113.0(2) . 1_455 ?
Cl3 Pb6 Cl4 143.46(9) . 1_455 ?
Cl3 Pb6 Cl4 79.80(8) 2_666 1_455 ?
Cl7 Pb6 Cl4 137.52(9) . 1_455 ?
OH7 Pb6 Cl1 111.9(2) . 1_455 ?
OH6 Pb6 Cl1 68.4(2) . 1_455 ?
Cl3 Pb6 Cl1 132.36(8) . 1_455 ?
Cl3 Pb6 Cl1 154.90(8) 2_666 1_455 ?
Cl7 Pb6 Cl1 69.73(8) . 1_455 ?
Cl4 Pb6 Cl1 77.82(8) 1_455 1_455 ?
OH7 Pb6 Cl4 140.2(2) . 2_666 ?
OH6 Pb6 Cl4 147.8(2) . 2_666 ?
Cl3 Pb6 Cl4 101.54(8) . 2_666 ?
Cl3 Pb6 Cl4 70.80(9) 2_666 2_666 ?
Cl7 Pb6 Cl4 67.87(8) . 2_666 ?
Cl4 Pb6 Cl4 91.35(9) 1_455 2_666 ?
Cl1 Pb6 Cl4 98.44(8) 1_455 2_666 ?
OH7 Pb6 Pb4 37.76(19) . . ?
OH6 Pb6 Pb4 39.32(19) . . ?
Cl3 Pb6 Pb4 54.07(7) . . ?
Cl3 Pb6 Pb4 93.14(7) 2_666 . ?
Cl7 Pb6 Pb4 108.42(6) . . ?
Cl4 Pb6 Pb4 105.21(7) 1_455 . ?
Cl1 Pb6 Pb4 103.55(6) 1_455 . ?
Cl4 Pb6 Pb4 154.74(5) 2_666 . ?
OH7 Pb6 Pb7 29.56(19) . . ?
OH6 Pb6 Pb7 73.30(19) . . ?
Cl3 Pb6 Pb7 105.59(7) . . ?
Cl3 Pb6 Pb7 86.43(6) 2_666 . ?
Cl7 Pb6 Pb7 149.68(6) . . ?
Cl4 Pb6 Pb7 48.19(7) 1_455 . ?
Cl1 Pb6 Pb7 87.08(6) 1_455 . ?
Cl4 Pb6 Pb7 137.22(6) 2_666 . ?
Pb4 Pb6 Pb7 57.139(14) . . ?
OH7 Pb7 OH5 70.6(3) . . ?
OH7 Pb7 Cl5 76.5(2) . 1_545 ?
OH5 Pb7 Cl5 71.9(2) . 1_545 ?
OH7 Pb7 Cl5 72.10(19) . 2_666 ?
OH5 Pb7 Cl5 133.3(2) . 2_666 ?
Cl5 Pb7 Cl5 73.00(10) 1_545 2_666 ?
OH7 Pb7 Cl4 72.8(2) . 1_455 ?
OH5 Pb7 Cl4 113.4(2) . 1_455 ?
Cl5 Pb7 Cl4 144.28(9) 1_545 1_455 ?
Cl5 Pb7 Cl4 80.42(9) 2_666 1_455 ?
OH7 Pb7 Cl7 145.4(2) . 1_545 ?
OH5 Pb7 Cl7 78.9(2) . 1_545 ?
Cl5 Pb7 Cl7 78.85(9) 1_545 1_545 ?
Cl5 Pb7 Cl7 122.62(9) 2_666 1_545 ?
Cl4 Pb7 Cl7 136.52(9) 1_455 1_545 ?
OH7 Pb7 Cl6 112.34(19) . 1_445 ?
OH5 Pb7 Cl6 66.8(2) . 1_445 ?
Cl5 Pb7 Cl6 130.48(8) 1_545 1_445 ?
Cl5 Pb7 Cl6 156.37(8) 2_666 1_445 ?
Cl4 Pb7 Cl6 79.06(8) 1_455 1_445 ?
Cl7 Pb7 Cl6 67.74(8) 1_545 1_445 ?
OH7 Pb7 Cl4 141.58(19) . 2_656 ?
OH5 Pb7 Cl4 146.3(2) . 2_656 ?
Cl5 Pb7 Cl4 101.76(8) 1_545 2_656 ?
Cl5 Pb7 Cl4 70.85(8) 2_666 2_656 ?
Cl4 Pb7 Cl4 91.30(9) 1_455 2_656 ?
Cl7 Pb7 Cl4 67.44(8) 1_545 2_656 ?
Cl6 Pb7 Cl4 97.97(8) 1_445 2_656 ?
OH7 Pb7 Pb4 37.3(2) . . ?
OH5 Pb7 Pb4 39.90(18) . . ?
Cl5 Pb7 Pb4 53.87(7) 1_545 . ?
Cl5 Pb7 Pb4 93.97(7) 2_666 . ?
Cl4 Pb7 Pb4 106.03(7) 1_455 . ?
Cl7 Pb7 Pb4 108.07(6) 1_545 . ?
Cl6 Pb7 Pb4 102.86(5) 1_445 . ?
Cl4 Pb7 Pb4 155.00(5) 2_656 . ?
OH7 Pb7 Pb6 29.7(2) . . ?
OH5 Pb7 Pb6 73.1(2) . . ?
Cl5 Pb7 Pb6 105.25(7) 1_545 . ?
Cl5 Pb7 Pb6 87.75(7) 2_666 . ?
Cl4 Pb7 Pb6 49.40(7) 1_455 . ?
Cl7 Pb7 Pb6 148.45(6) 1_545 . ?
Cl6 Pb7 Pb6 87.77(6) 1_445 . ?
Cl4 Pb7 Pb6 138.59(6) 2_656 . ?
Pb4 Pb7 Pb6 56.743(14) . . ?
O1 I O2 96.1(4) . . ?
O1 I O3 95.2(4) . . ?
O2 I O3 95.2(4) . . ?
O1 I Cl7 85.1(3) . . ?
O2 I Cl7 86.3(3) . . ?
O3 I Cl7 178.4(3) . . ?
O1 I Cl2 85.3(3) . . ?
O2 I Cl2 177.0(3) . . ?
O3 I Cl2 82.1(3) . . ?
Cl7 I Cl2 96.44(9) . . ?
O1 I Cl8 173.9(3) . . ?
O2 I Cl8 89.4(3) . . ?
O3 I Cl8 81.6(3) . . ?
Cl7 I Cl8 97.93(9) . . ?
Cl2 I Cl8 89.04(9) . . ?
O1 I OH4 59.2(3) . . ?
O2 I OH4 58.5(3) . . ?
O3 I OH4 58.4(3) . . ?
Cl7 I OH4 122.95(14) . . ?
Cl2 I OH4 120.40(16) . . ?
Cl8 I OH4 122.34(16) . . ?
O1 I Pb3 98.6(3) . . ?
O2 I Pb3 46.5(3) . . ?
O3 I Pb3 48.7(3) . . ?
Cl7 I Pb3 132.84(7) . . ?
Cl2 I Pb3 130.69(6) . . ?
Cl8 I Pb3 83.29(7) . . ?
OH4 I Pb3 39.35(14) . . ?
O1 I Pb1 45.4(3) . . ?
O2 I Pb1 99.6(3) . . ?
O3 I Pb1 49.8(3) . . ?
Cl7 I Pb1 130.37(7) . . ?
Cl2 I Pb1 79.47(7) . . ?
Cl8 I Pb1 131.08(7) . . ?
OH4 I Pb1 41.16(14) . . ?
Pb3 I Pb1 70.059(19) . . ?
O1 I Pb2 47.8(3) . . ?
O2 I Pb2 48.3(3) . . ?
O3 I Pb2 98.4(3) . . ?
Cl7 I Pb2 82.92(6) . . ?
Cl2 I Pb2 133.12(7) . . ?
Cl8 I Pb2 137.67(7) . . ?
OH4 I Pb2 40.03(13) . . ?
Pb3 I Pb2 66.883(18) . . ?
Pb1 I Pb2 66.756(18) . . ?
I O1 Pb1 105.2(3) . . ?
I O1 Pb2 102.8(4) . . ?
Pb1 O1 Pb2 94.6(3) . . ?
I O1 OH6 118.5(4) . . ?
Pb1 O1 OH6 115.5(4) . . ?
Pb2 O1 OH6 116.9(3) . . ?
I O1 Pb4 154.9(4) . . ?
Pb1 O1 Pb4 92.6(2) . . ?
Pb2 O1 Pb4 93.0(2) . . ?
OH6 O1 Pb4 36.5(2) . . ?
I O2 Pb3 103.7(3) . . ?
I O2 Pb2 102.2(4) . . ?
Pb3 O2 Pb2 93.7(3) . . ?
I O2 Pb4 154.5(4) . 1_565 ?
Pb3 O2 Pb4 95.8(2) . 1_565 ?
Pb2 O2 Pb4 92.7(2) . 1_565 ?
I O2 Pb5 105.3(3) . 1_565 ?
Pb3 O2 Pb5 98.6(2) . 1_565 ?
Pb2 O2 Pb5 146.1(3) . 1_565 ?
Pb4 O2 Pb5 54.80(12) 1_565 1_565 ?
I O3 Pb1 112.9(3) . 2_667 ?
I O3 Pb3 101.2(3) . . ?
Pb1 O3 Pb3 126.8(3) 2_667 . ?
I O3 Pb1 99.9(3) . . ?
Pb1 O3 Pb1 115.4(3) 2_667 . ?
Pb3 O3 Pb1 96.3(2) . . ?
Pb3 OH4 Pb2 112.0(3) . . ?
Pb3 OH4 Pb1 116.3(3) . . ?
Pb2 OH4 Pb1 108.2(3) . . ?
Pb3 OH4 Cl8 58.15(18) . 1_655 ?
Pb2 OH4 Cl8 126.7(3) . 1_655 ?
Pb1 OH4 Cl8 123.2(3) . 1_655 ?
Pb3 OH4 I 73.5(2) . . ?
Pb2 OH4 I 74.18(19) . . ?
Pb1 OH4 I 72.62(18) . . ?
Cl8 OH4 I 131.4(3) 1_655 . ?
Pb3 OH4 Cl7 122.2(3) . 1_655 ?
Pb2 OH4 Cl7 57.22(16) . 1_655 ?
Pb1 OH4 Cl7 120.8(3) . 1_655 ?
Cl8 OH4 Cl7 83.31(18) 1_655 1_655 ?
I OH4 Cl7 131.4(2) . 1_655 ?
Pb3 OH4 I 106.9(2) . 1_655 ?
Pb2 OH4 I 104.4(2) . 1_655 ?
Pb1 OH4 I 108.3(3) . 1_655 ?
Cl8 OH4 I 49.21(12) 1_655 1_655 ?
I OH4 I 178.5(2) . 1_655 ?
Cl7 OH4 I 47.16(11) 1_655 1_655 ?
Pb5 OH5 Pb7 125.8(4) . . ?
Pb5 OH5 Pb4 103.2(3) . . ?
Pb7 OH5 Pb4 101.4(3) . . ?
Pb5 OH5 O2 108.1(3) . 1_545 ?
Pb7 OH5 O2 114.7(4) . 1_545 ?
Pb4 OH5 O2 98.9(3) . 1_545 ?
Pb5 OH5 I 100.6(2) . 1_545 ?
Pb7 OH5 I 104.9(3) . 1_545 ?
Pb4 OH5 I 123.1(3) . 1_545 ?
O2 OH5 I 24.19(18) 1_545 1_545 ?
Pb5 OH5 Pb6 76.0(2) . . ?
Pb7 OH5 Pb6 72.87(19) . . ?
Pb4 OH5 Pb6 64.03(17) . . ?
O2 OH5 Pb6 162.8(3) 1_545 . ?
I OH5 Pb6 172.9(2) 1_545 . ?
Pb5 OH6 Pb4 103.8(3) . . ?
Pb5 OH6 Pb6 124.2(3) . . ?
Pb4 OH6 Pb6 101.3(3) . . ?
Pb5 OH6 O1 110.6(3) . . ?
Pb4 OH6 O1 100.4(3) . . ?
Pb6 OH6 O1 112.6(3) . . ?
Pb5 OH6 I 102.4(2) . . ?
Pb4 OH6 I 123.8(3) . . ?
Pb6 OH6 I 103.4(3) . . ?
O1 OH6 I 23.51(19) . . ?
Pb5 OH6 Pb7 75.2(2) . . ?
Pb4 OH6 Pb7 64.30(18) . . ?
Pb6 OH6 Pb7 72.40(19) . . ?
O1 OH6 Pb7 164.7(3) . . ?
I OH6 Pb7 171.8(2) . . ?
Pb7 OH7 Pb6 120.7(3) . . ?
Pb7 OH7 Pb4 105.7(3) . . ?
Pb6 OH7 Pb4 104.7(3) . . ?
Pb7 OH7 Pb5 74.91(19) . . ?
Pb6 OH7 Pb5 75.07(19) . . ?
Pb4 OH7 Pb5 63.55(17) . . ?
Pb7 OH7 H7 108(8) . . ?
Pb6 OH7 H7 88(9) . . ?
Pb4 OH7 H7 130(8) . . ?
Pb5 OH7 H7 162(8) . . ?
Pb1 Cl1 Pb2 82.56(8) . . ?
Pb1 Cl1 Pb5 91.52(8) . 1_655 ?
Pb2 Cl1 Pb5 147.32(11) . 1_655 ?
Pb1 Cl1 Pb4 105.70(9) . . ?
Pb2 Cl1 Pb4 106.81(9) . . ?
Pb5 Cl1 Pb4 105.73(9) 1_655 . ?
Pb1 Cl1 Pb6 152.07(11) . 1_655 ?
Pb2 Cl1 Pb6 88.57(8) . 1_655 ?
Pb5 Cl1 Pb6 81.78(7) 1_655 1_655 ?
Pb4 Cl1 Pb6 102.21(8) . 1_655 ?
I Cl2 Pb1 76.37(8) . 2_667 ?
I Cl2 Pb1 116.89(11) . 1_455 ?
Pb1 Cl2 Pb1 110.69(10) 2_667 1_455 ?
I Cl2 Pb5 109.01(9) . . ?
Pb1 Cl2 Pb5 156.04(12) 2_667 . ?
Pb1 Cl2 Pb5 88.14(8) 1_455 . ?
I Cl2 Pb3 132.78(11) . 2_667 ?
Pb1 Cl2 Pb3 79.17(7) 2_667 2_667 ?
Pb1 Cl2 Pb3 109.37(9) 1_455 2_667 ?
Pb5 Cl2 Pb3 80.64(8) . 2_667 ?
I Cl2 Pb1 56.17(5) . . ?
Pb1 Cl2 Pb1 76.14(6) 2_667 . ?
Pb1 Cl2 Pb1 169.70(9) 1_455 . ?
Pb5 Cl2 Pb1 87.49(7) . . ?
Pb3 Cl2 Pb1 79.09(7) 2_667 . ?
Pb6 Cl3 Pb6 107.30(9) . 2_666 ?
Pb6 Cl3 Pb2 128.24(11) . . ?
Pb6 Cl3 Pb2 118.51(10) 2_666 . ?
Pb6 Cl3 Pb4 77.32(7) . . ?
Pb6 Cl3 Pb4 109.97(10) 2_666 . ?
Pb2 Cl3 Pb4 106.30(9) . . ?
Pb7 Cl4 Pb6 82.42(8) 1_655 1_655 ?
Pb7 Cl4 Pb4 103.00(10) 1_655 . ?
Pb6 Cl4 Pb4 102.62(10) 1_655 . ?
Pb7 Cl4 Pb6 162.22(11) 1_655 2_666 ?
Pb6 Cl4 Pb6 88.65(9) 1_655 2_666 ?
Pb4 Cl4 Pb6 93.92(8) . 2_666 ?
Pb7 Cl4 Pb7 88.70(9) 1_655 2_656 ?
Pb6 Cl4 Pb7 163.12(11) 1_655 2_656 ?
Pb4 Cl4 Pb7 93.32(8) . 2_656 ?
Pb6 Cl4 Pb7 95.82(8) 2_666 2_656 ?
Pb7 Cl4 Pb2 94.54(8) 1_655 2_766 ?
Pb6 Cl4 Pb2 94.76(8) 1_655 2_766 ?
Pb4 Cl4 Pb2 156.67(10) . 2_766 ?
Pb6 Cl4 Pb2 70.82(6) 2_666 2_766 ?
Pb7 Cl4 Pb2 71.57(6) 2_656 2_766 ?
Pb7 Cl5 Pb7 107.00(10) 1_565 2_666 ?
Pb7 Cl5 Pb2 127.99(11) 1_565 . ?
Pb7 Cl5 Pb2 118.70(11) 2_666 . ?
Pb7 Cl5 Pb4 77.48(8) 1_565 1_565 ?
Pb7 Cl5 Pb4 110.83(10) 2_666 1_565 ?
Pb2 Cl5 Pb4 105.97(9) . 1_565 ?
Pb3 Cl6 Pb2 82.95(8) . . ?
Pb3 Cl6 Pb5 94.48(9) . 1_665 ?
Pb2 Cl6 Pb5 147.46(12) . 1_665 ?
Pb3 Cl6 Pb4 110.18(10) . 1_565 ?
Pb2 Cl6 Pb4 105.32(9) . 1_565 ?
Pb5 Cl6 Pb4 105.97(10) 1_665 1_565 ?
Pb3 Cl6 Pb7 151.42(12) . 1_665 ?
Pb2 Cl6 Pb7 87.14(8) . 1_665 ?
Pb5 Cl6 Pb7 79.77(7) 1_665 1_665 ?
Pb4 Cl6 Pb7 98.28(8) 1_565 1_665 ?
Pb2 Cl7 I 117.76(10) 1_455 . ?
Pb2 Cl7 Pb6 92.68(8) 1_455 . ?
I Cl7 Pb6 115.26(11) . . ?
Pb2 Cl7 Pb7 94.03(9) 1_455 1_565 ?
I Cl7 Pb7 115.00(10) . 1_565 ?
Pb6 Cl7 Pb7 118.13(9) . 1_565 ?
Pb2 Cl7 Pb2 172.57(10) 1_455 . ?
I Cl7 Pb2 54.83(5) . . ?
Pb6 Cl7 Pb2 90.63(7) . . ?
Pb7 Cl7 Pb2 90.27(7) 1_565 . ?
Pb3 Cl8 I 115.99(11) 1_455 . ?
Pb3 Cl8 Pb5 90.72(9) 1_455 1_565 ?
I Cl8 Pb5 101.41(9) . 1_565 ?
Pb3 Cl8 Pb1 111.07(10) 1_455 2_667 ?
I Cl8 Pb1 71.45(8) . 2_667 ?
Pb5 Cl8 Pb1 158.12(11) 1_565 2_667 ?
Pb3 Cl8 Pb3 111.78(11) 1_455 2_677 ?
I Cl8 Pb3 131.86(10) . 2_677 ?
Pb5 Cl8 Pb3 71.96(7) 1_565 2_677 ?
Pb1 Cl8 Pb3 96.99(8) 2_667 2_677 ?
Pb3 Cl8 Pb5 68.30(7) 1_455 2_567 ?
I Cl8 Pb5 138.13(11) . 2_567 ?
Pb5 Cl8 Pb5 120.42(10) 1_565 2_567 ?
Pb1 Cl8 Pb5 68.84(6) 2_667 2_567 ?
Pb3 Cl8 Pb5 66.69(5) 2_677 2_567 ?
Pb3 Cl8 Pb3 166.12(11) 1_455 . ?
I Cl8 Pb3 53.05(5) . . ?
Pb5 Cl8 Pb3 84.05(7) 1_565 . ?
Pb1 Cl8 Pb3 75.15(6) 2_667 . ?
Pb3 Cl8 Pb3 78.84(6) 2_677 . ?
Pb5 Cl8 Pb3 125.33(8) 2_567 . ?
Pb5 Cl9 Pb1 121.46(12) . . ?
Pb5 Cl9 Pb3 121.52(11) . 1_545 ?
Pb1 Cl9 Pb3 116.74(10) . 1_545 ?
Pb5 Cl9 Pb4 72.34(7) . . ?
Pb1 Cl9 Pb4 95.66(9) . . ?
Pb3 Cl9 Pb4 97.45(9) 1_545 . ?
Pb5 Cl9 Pb3 81.70(8) . 2_667 ?
Pb1 Cl9 Pb3 92.32(8) . 2_667 ?
Pb3 Cl9 Pb3 101.66(9) 1_545 2_667 ?
Pb4 Cl9 Pb3 153.23(10) . 2_667 ?
 
loop_
 _geom_hbond_atom_site_label_D 
 _geom_hbond_atom_site_label_H 
 _geom_hbond_atom_site_label_A 
 _geom_hbond_distance_DH 
 _geom_hbond_distance_HA 
 _geom_hbond_distance_DA 
 _geom_hbond_angle_DHA 
 _geom_hbond_site_symmetry_A 
OH7 H7 Cl3  0.90(12) 2.41(13) 3.187(9) 145(11) 2_666
 
_refine_diff_density_max    1.699
_refine_diff_density_min   -1.765
_refine_diff_density_rms    0.423



