 
data_arsenopal_a
 
_audit_creation_method            'SHELXL-2014/7'
_shelx_SHELXL_version_number      '2014/7'
_chemical_name_systematic         ?
_chemical_name_common             ?
_chemical_melting_point           ?
_chemical_formula_moiety          ?
_chemical_formula_sum
 'As5 Pd16 Sb' 
_chemical_formula_weight          2198.75

loop_
 _atom_type_symbol
 _atom_type_description
 _atom_type_scat_dispersion_real
 _atom_type_scat_dispersion_imag
 _atom_type_scat_source
 'As'  'As'   0.0499   2.0058
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Pd'  'Pd'  -0.9988   1.0072
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 'Sb'  'Sb'  -0.5866   1.5461
 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
 
_space_group_crystal_system       triclinic
_space_group_IT_number            2
_space_group_name_H-M_alt         'P -1'
_space_group_name_Hall            '-P 1'
 
_shelx_space_group_comment
;
The symmetry employed for this shelxl refinement is uniquely defined
by the following loop, which should always be used as a source of
symmetry information in preference to the above space-group names.
They are only intended as comments.
;
 
loop_
 _space_group_symop_operation_xyz
 'x, y, z'
 '-x, -y, -z'
 
_cell_length_a                    7.3344(7)
_cell_length_b                    7.3870(8)
_cell_length_c                    7.5255(7)
_cell_angle_alpha                 98.869(8)
_cell_angle_beta                  102.566(8)
_cell_angle_gamma                 119.096(11)
_cell_volume                      331.19(7)
_cell_formula_units_Z             1
_cell_measurement_temperature     296(1) 
_cell_measurement_reflns_used     2462
_cell_measurement_theta_min       3.1950
_cell_measurement_theta_max       28.5930
 
_exptl_crystal_description        'block'
_exptl_crystal_colour             ?
_exptl_crystal_density_meas       ?
_exptl_crystal_density_method     ?
_exptl_crystal_density_diffrn     11.024         
_exptl_crystal_F_000              952
_exptl_transmission_factor_min    ?
_exptl_transmission_factor_max    ?
_exptl_crystal_size_max           0.250
_exptl_crystal_size_mid           0.230
_exptl_crystal_size_min           0.150
_exptl_absorpt_coefficient_mu     35.472
_shelx_estimated_absorpt_T_min    ?
_shelx_estimated_absorpt_T_max    ?
_exptl_absorpt_correction_T_min   0.12564
_exptl_absorpt_correction_T_max   1.00000
_exptl_absorpt_correction_type    'multi-scan'
_exptl_absorpt_process_details
;
CrysAlisPro, Agilent Technologies,
Version 1.171.36.32 (release 02-08-2013 CrysAlis171 .NET)
(compiled Aug  2 2013,16:46:58)
Empirical absorption correction using spherical harmonics,
 implemented in SCALE3 ABSPACK scaling algorithm.
;
_diffrn_ambient_temperature       296(1) 
_diffrn_radiation_wavelength      0.7107
_diffrn_radiation_type            'Mo K\a'
_diffrn_radiation_source          'Enhance (Mo) X-ray Source'
_diffrn_radiation_monochromator   'graphite'
_diffrn_measurement_device_type   'Xcalibur, Eos'
_diffrn_detector_area_resol_mean  16.2096
_diffrn_reflns_number             4130
_diffrn_reflns_av_unetI/netI      0.0478
_diffrn_reflns_av_R_equivalents   0.0545
_diffrn_reflns_limit_h_min        -9
_diffrn_reflns_limit_h_max        9
_diffrn_reflns_limit_k_min        -9
_diffrn_reflns_limit_k_max        9
_diffrn_reflns_limit_l_min        -9
_diffrn_reflns_limit_l_max        9
_diffrn_reflns_theta_min          2.912
_diffrn_reflns_theta_max          25.997
_diffrn_reflns_theta_full         25.242
_diffrn_measured_fraction_theta_max   1.000
_diffrn_measured_fraction_theta_full  1.000
_diffrn_reflns_Laue_measured_fraction_max    1.000
_diffrn_reflns_Laue_measured_fraction_full   1.000
_diffrn_reflns_point_group_measured_fraction_max   1.000
_diffrn_reflns_point_group_measured_fraction_full  1.000
_reflns_number_total              1299
_reflns_number_gt                 1224
_reflns_threshold_expression      'I > 2σ(I)'
_reflns_Friedel_coverage          0.000
_reflns_Friedel_fraction_max      .
_reflns_Friedel_fraction_full     .
 
_reflns_special_details
;
 Reflections were merged by SHELXL according to the crystal
 class for the calculation of statistics and refinement.
 
 _reflns_Friedel_fraction is defined as the number of unique
 Friedel pairs measured divided by the number that would be
 possible theoretically, ignoring centric projections and
 systematic absences.
;
 
_computing_data_collection        ?
_computing_cell_refinement        ?
_computing_data_reduction         ?
_computing_structure_solution     ?
_computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)'
_computing_molecular_graphics     ?
_computing_publication_material   ?
_refine_special_details           ?
_refine_ls_structure_factor_coef  Fsqd
_refine_ls_matrix_type            full
_refine_ls_weighting_scheme       calc
_refine_ls_weighting_details
'w=1/[σ²(Fo²)+(0.0675P)²+6.2603P] where P=(Fo²+2Fc²)/3'
_atom_sites_solution_primary      ?
_atom_sites_solution_secondary    ?
_atom_sites_solution_hydrogens    .
_refine_ls_hydrogen_treatment     undef
_refine_ls_extinction_method      none
_refine_ls_extinction_coef        .
_refine_ls_number_reflns          1299
_refine_ls_number_parameters      103
_refine_ls_number_restraints      0
_refine_ls_R_factor_all           0.0479
_refine_ls_R_factor_gt            0.0451
_refine_ls_wR_factor_ref          0.1241
_refine_ls_wR_factor_gt           0.1216
_refine_ls_goodness_of_fit_ref    1.117
_refine_ls_restrained_S_all       1.117
_refine_ls_shift/su_max           0.000
_refine_ls_shift/su_mean          0.000
 
loop_
 _atom_site_label
 _atom_site_type_symbol
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_U_iso_or_equiv
 _atom_site_adp_type
 _atom_site_occupancy
 _atom_site_site_symmetry_order  
 _atom_site_calc_flag
 _atom_site_refinement_flags_posn
 _atom_site_refinement_flags_adp
 _atom_site_refinement_flags_occupancy
 _atom_site_disorder_assembly
 _atom_site_disorder_group
Sb1 Sb 0.0000 0.0000 0.0000 0.0098(3) Uani 1 2 d S . P . .
Pd1 Pd 0.4357(2) 0.05665(19) 0.15926(18) 0.0170(3) Uani 1 1 d . . . . .
Pd2 Pd 0.1814(2) 0.12257(19) 0.39072(18) 0.0165(3) Uani 1 1 d . . . . .
Pd3 Pd 0.7896(2) 0.5003(2) 0.3932(2) 0.0212(4) Uani 1 1 d . . . . .
Pd4 Pd 0.3778(2) 0.4168(2) 0.15203(19) 0.0252(4) Uani 1 1 d . . . . .
Pd5 Pd 0.0506(2) 0.7101(2) -0.20324(19) 0.0225(4) Uani 1 1 d . . . . .
Pd6 Pd -0.0135(2) 0.3095(2) -0.15586(19) 0.0226(4) Uani 1 1 d . . . . .
Pd7 Pd 0.7230(2) 0.8474(2) 0.20667(19) 0.0236(4) Uani 1 1 d . . . . .
Pd8 Pd 0.4092(2) 0.7740(3) 0.3954(2) 0.0247(4) Uani 1 1 d . . . . .
As1 As 0.5000 0.5000 0.5000 0.0124(5) Uani 1 2 d S . P . .
As2 As 0.1677(3) 0.8345(3) -0.4739(2) 0.0141(4) Uani 1 1 d . . . . .
As3 As 0.3345(2) 0.6753(2) 0.0015(2) 0.0137(4) Uani 1 1 d . . . . .
 
 
_geom_special_details
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;
 
loop_
 _geom_bond_atom_site_label_1
 _geom_bond_atom_site_label_2
 _geom_bond_distance
 _geom_bond_site_symmetry_2
 _geom_bond_publ_flag
Sb1 Pd5 2.6594(13) 2_565 ?
Sb1 Pd5 2.6594(13) 1_545 ?
Sb1 Pd7 2.7397(13) 2_665 ?
Sb1 Pd7 2.7397(13) 1_445 ?
Sb1 Pd2 2.7460(13) . ?
Sb1 Pd2 2.7460(13) 2 ?
Sb1 Pd6 2.7584(13) 2 ?
Sb1 Pd6 2.7584(13) . ?
Sb1 Pd4 2.7755(14) . ?
Sb1 Pd4 2.7755(14) 2 ?
Sb1 Pd1 2.9498(13) 2 ?
Sb1 Pd1 2.9498(13) . ?
Pd1 As3 2.5394(19) 1_545 ?
Pd1 As3 2.5700(19) 2_665 ?
Pd1 Pd4 2.8971(19) . ?
Pd1 Pd8 2.9080(19) 1_545 ?
Pd1 Pd1 2.910(3) 2_655 ?
Pd1 Pd3 2.9220(19) . ?
Pd1 Pd6 2.9502(18) 2 ?
Pd1 Pd2 2.9641(18) . ?
Pd1 As2 2.976(2) 2_665 ?
Pd1 Pd5 3.0714(19) 1_545 ?
Pd1 Pd7 3.074(2) 2_665 ?
Pd2 As1 2.4558(13) . ?
Pd2 As2 2.466(2) 1_546 ?
Pd2 Pd8 2.7344(18) 2_666 ?
Pd2 Pd7 2.7952(17) 1_445 ?
Pd2 Pd5 2.8197(18) 2_565 ?
Pd2 Pd6 2.8841(19) 2 ?
Pd2 Pd3 2.8851(18) 2_666 ?
Pd2 Pd7 2.9049(19) 2_666 ?
Pd2 As2 2.910(2) 2_565 ?
Pd2 Pd4 3.0512(19) . ?
Pd3 As1 2.4280(13) . ?
Pd3 As2 2.482(2) 1_656 ?
Pd3 Pd5 2.7660(18) 2_665 ?
Pd3 Pd6 2.7691(19) 2_665 ?
Pd3 As2 2.778(2) 2_665 ?
Pd3 As3 2.797(2) 2_665 ?
Pd3 Pd8 2.8091(19) 2_666 ?
Pd3 Pd4 2.873(2) . ?
Pd3 Pd2 2.8851(18) 2_666 ?
Pd3 Pd5 2.902(2) 1_656 ?
Pd3 Pd3 3.157(3) 2_766 ?
Pd4 As1 2.4464(14) . ?
Pd4 As3 2.4761(19) . ?
Pd4 Pd7 2.783(2) 2_665 ?
Pd4 Pd7 2.8301(19) . ?
Pd4 Pd8 2.847(2) . ?
Pd4 As3 2.909(2) 2_665 ?
Pd4 Pd6 2.926(2) . ?
Pd4 Pd5 2.945(2) 2_565 ?
Pd5 As3 2.454(2) . ?
Pd5 As2 2.510(2) . ?
Pd5 Sb1 2.6594(13) 1_565 ?
Pd5 Pd3 2.7660(18) 2_665 ?
Pd5 Pd6 2.7930(19) 2_565 ?
Pd5 Pd2 2.8197(18) 2_565 ?
Pd5 Pd6 2.8552(19) . ?
Pd5 Pd7 2.865(2) 2_675 ?
Pd5 Pd3 2.902(2) 1_454 ?
Pd5 Pd4 2.945(2) 2_565 ?
Pd5 Pd1 3.0714(19) 1_565 ?
Pd5 Pd1 3.2001(19) 2_665 ?
Pd6 As3 2.4920(19) . ?
Pd6 As2 2.592(2) 2_564 ?
Pd6 Pd3 2.7692(18) 2_665 ?
Pd6 Pd8 2.7739(19) 2_565 ?
Pd6 Pd5 2.7930(19) 2_565 ?
Pd6 As3 2.883(2) 2_565 ?
Pd6 Pd2 2.8841(19) 2 ?
Pd6 Pd7 2.941(2) 2_665 ?
Pd6 Pd1 2.9502(18) 2 ?
Pd7 As3 2.465(2) . ?
Pd7 As2 2.493(2) 2_675 ?
Pd7 Sb1 2.7397(13) 1_665 ?
Pd7 Pd4 2.783(2) 2_665 ?
Pd7 Pd2 2.7952(17) 1_665 ?
Pd7 Pd8 2.8379(18) . ?
Pd7 Pd5 2.865(2) 2_675 ?
Pd7 Pd2 2.9049(19) 2_666 ?
Pd7 Pd6 2.941(2) 2_665 ?
Pd7 Pd1 3.074(2) 2_665 ?
Pd7 Pd1 3.157(2) 1_565 ?
Pd8 As2 2.387(2) 1_556 ?
Pd8 As1 2.5948(14) . ?
Pd8 Pd2 2.7345(18) 2_666 ?
Pd8 Pd6 2.7739(19) 2_565 ?
Pd8 As3 2.803(2) . ?
Pd8 Pd3 2.8091(19) 2_666 ?
Pd8 As2 2.879(2) 2_675 ?
Pd8 Pd1 2.9080(19) 1_565 ?
Pd8 Pd8 2.923(3) 2_676 ?
Pd8 Pd1 3.1231(19) 2_666 ?
As1 Pd3 2.4280(13) 2_666 ?
As1 Pd4 2.4464(14) 2_666 ?
As1 Pd2 2.4558(13) 2_666 ?
As1 Pd8 2.5948(14) 2_666 ?
As2 Pd8 2.387(2) 1_554 ?
As2 Pd2 2.466(2) 1_564 ?
As2 Pd3 2.482(2) 1_454 ?
As2 Pd7 2.493(2) 2_675 ?
As2 Pd6 2.592(2) 2_564 ?
As2 Pd3 2.778(2) 2_665 ?
As2 Pd8 2.879(2) 2_675 ?
As2 Pd2 2.910(2) 2_565 ?
As2 Pd1 2.976(2) 2_665 ?
As3 Pd1 2.5394(19) 1_565 ?
As3 Pd1 2.5700(19) 2_665 ?
As3 Pd3 2.797(2) 2_665 ?
As3 Pd6 2.883(2) 2_565 ?
As3 Pd4 2.909(2) 2_665 ?
 
loop_
 _geom_angle_atom_site_label_1
 _geom_angle_atom_site_label_2
 _geom_angle_atom_site_label_3
 _geom_angle
 _geom_angle_site_symmetry_1
 _geom_angle_site_symmetry_3
 _geom_angle_publ_flag
Pd5 Sb1 Pd5 180.00(6) 2_565 1_545 ?
Pd5 Sb1 Pd7 115.93(5) 2_565 2_665 ?
Pd5 Sb1 Pd7 64.07(5) 1_545 2_665 ?
Pd5 Sb1 Pd7 64.07(5) 2_565 1_445 ?
Pd5 Sb1 Pd7 115.93(5) 1_545 1_445 ?
Pd7 Sb1 Pd7 180.00(7) 2_665 1_445 ?
Pd5 Sb1 Pd2 62.86(4) 2_565 . ?
Pd5 Sb1 Pd2 117.14(4) 1_545 . ?
Pd7 Sb1 Pd2 118.73(4) 2_665 . ?
Pd7 Sb1 Pd2 61.27(4) 1_445 . ?
Pd5 Sb1 Pd2 117.14(4) 2_565 2 ?
Pd5 Sb1 Pd2 62.86(4) 1_545 2 ?
Pd7 Sb1 Pd2 61.27(4) 2_665 2 ?
Pd7 Sb1 Pd2 118.73(4) 1_445 2 ?
Pd2 Sb1 Pd2 180.0 . 2 ?
Pd5 Sb1 Pd6 117.97(4) 2_565 2 ?
Pd5 Sb1 Pd6 62.03(4) 1_545 2 ?
Pd7 Sb1 Pd6 115.32(5) 2_665 2 ?
Pd7 Sb1 Pd6 64.68(5) 1_445 2 ?
Pd2 Sb1 Pd6 63.20(4) . 2 ?
Pd2 Sb1 Pd6 116.80(4) 2 2 ?
Pd5 Sb1 Pd6 62.03(4) 2_565 . ?
Pd5 Sb1 Pd6 117.97(4) 1_545 . ?
Pd7 Sb1 Pd6 64.68(5) 2_665 . ?
Pd7 Sb1 Pd6 115.32(5) 1_445 . ?
Pd2 Sb1 Pd6 116.80(4) . . ?
Pd2 Sb1 Pd6 63.20(4) 2 . ?
Pd6 Sb1 Pd6 180.0 2 . ?
Pd5 Sb1 Pd4 65.59(5) 2_565 . ?
Pd5 Sb1 Pd4 114.41(5) 1_545 . ?
Pd7 Sb1 Pd4 60.61(4) 2_665 . ?
Pd7 Sb1 Pd4 119.39(4) 1_445 . ?
Pd2 Sb1 Pd4 67.09(4) . . ?
Pd2 Sb1 Pd4 112.91(4) 2 . ?
Pd6 Sb1 Pd4 116.16(4) 2 . ?
Pd6 Sb1 Pd4 63.84(4) . . ?
Pd5 Sb1 Pd4 114.41(5) 2_565 2 ?
Pd5 Sb1 Pd4 65.59(5) 1_545 2 ?
Pd7 Sb1 Pd4 119.39(4) 2_665 2 ?
Pd7 Sb1 Pd4 60.61(4) 1_445 2 ?
Pd2 Sb1 Pd4 112.91(4) . 2 ?
Pd2 Sb1 Pd4 67.09(4) 2 2 ?
Pd6 Sb1 Pd4 63.84(4) 2 2 ?
Pd6 Sb1 Pd4 116.16(4) . 2 ?
Pd4 Sb1 Pd4 180.0 . 2 ?
Pd5 Sb1 Pd1 66.17(4) 2_565 2 ?
Pd5 Sb1 Pd1 113.83(4) 1_545 2 ?
Pd7 Sb1 Pd1 114.72(4) 2_665 2 ?
Pd7 Sb1 Pd1 65.28(4) 1_445 2 ?
Pd2 Sb1 Pd1 117.40(4) . 2 ?
Pd2 Sb1 Pd1 62.60(4) 2 2 ?
Pd6 Sb1 Pd1 117.87(4) 2 2 ?
Pd6 Sb1 Pd1 62.13(4) . 2 ?
Pd4 Sb1 Pd1 119.29(4) . 2 ?
Pd4 Sb1 Pd1 60.71(4) 2 2 ?
Pd5 Sb1 Pd1 113.83(4) 2_565 . ?
Pd5 Sb1 Pd1 66.17(4) 1_545 . ?
Pd7 Sb1 Pd1 65.28(4) 2_665 . ?
Pd7 Sb1 Pd1 114.72(4) 1_445 . ?
Pd2 Sb1 Pd1 62.60(4) . . ?
Pd2 Sb1 Pd1 117.40(4) 2 . ?
Pd6 Sb1 Pd1 62.13(4) 2 . ?
Pd6 Sb1 Pd1 117.87(4) . . ?
Pd4 Sb1 Pd1 60.71(4) . . ?
Pd4 Sb1 Pd1 119.29(4) 2 . ?
Pd1 Sb1 Pd1 180.0 2 . ?
As3 Pd1 As3 110.56(6) 1_545 2_665 ?
As3 Pd1 Pd4 150.32(7) 1_545 . ?
As3 Pd1 Pd4 63.97(6) 2_665 . ?
As3 Pd1 Pd8 61.50(5) 1_545 1_545 ?
As3 Pd1 Pd8 148.16(7) 2_665 1_545 ?
Pd4 Pd1 Pd8 138.74(6) . 1_545 ?
As3 Pd1 Pd1 55.78(5) 1_545 2_655 ?
As3 Pd1 Pd1 54.79(5) 2_665 2_655 ?
Pd4 Pd1 Pd1 111.75(7) . 2_655 ?
Pd8 Pd1 Pd1 109.50(7) 1_545 2_655 ?
As3 Pd1 Pd3 146.56(7) 1_545 . ?
As3 Pd1 Pd3 60.83(5) 2_665 . ?
Pd4 Pd1 Pd3 59.17(5) . . ?
Pd8 Pd1 Pd3 107.34(6) 1_545 . ?
Pd1 Pd1 Pd3 107.32(6) 2_655 . ?
As3 Pd1 Sb1 99.00(5) 1_545 . ?
As3 Pd1 Sb1 101.09(5) 2_665 . ?
Pd4 Pd1 Sb1 56.67(4) . . ?
Pd8 Pd1 Sb1 110.51(5) 1_545 . ?
Pd1 Pd1 Sb1 107.84(6) 2_655 . ?
Pd3 Pd1 Sb1 114.22(5) . . ?
As3 Pd1 Pd6 62.85(5) 1_545 2 ?
As3 Pd1 Pd6 151.25(7) 2_665 2 ?
Pd4 Pd1 Pd6 106.89(6) . 2 ?
Pd8 Pd1 Pd6 56.52(4) 1_545 2 ?
Pd1 Pd1 Pd6 112.09(7) 2_655 2 ?
Pd3 Pd1 Pd6 140.49(6) . 2 ?
Sb1 Pd1 Pd6 55.75(4) . 2 ?
As3 Pd1 Pd2 120.24(6) 1_545 . ?
As3 Pd1 Pd2 125.84(6) 2_665 . ?
Pd4 Pd1 Pd2 62.73(5) . . ?
Pd8 Pd1 Pd2 77.84(5) 1_545 . ?
Pd1 Pd1 Pd2 163.03(8) 2_655 . ?
Pd3 Pd1 Pd2 84.05(5) . . ?
Sb1 Pd1 Pd2 55.33(3) . . ?
Pd6 Pd1 Pd2 58.37(5) 2 . ?
As3 Pd1 As2 94.93(6) 1_545 2_665 ?
As3 Pd1 As2 93.79(6) 2_665 2_665 ?
Pd4 Pd1 As2 114.20(6) . 2_665 ?
Pd8 Pd1 As2 58.58(5) 1_545 2_665 ?
Pd1 Pd1 As2 97.66(7) 2_655 2_665 ?
Pd3 Pd1 As2 56.20(5) . 2_665 ?
Sb1 Pd1 As2 154.50(6) . 2_665 ?
Pd6 Pd1 As2 114.24(6) 2 2_665 ?
Pd2 Pd1 As2 99.17(6) . 2_665 ?
As3 Pd1 Pd5 50.80(5) 1_545 1_545 ?
As3 Pd1 Pd5 98.00(6) 2_665 1_545 ?
Pd4 Pd1 Pd5 99.87(5) . 1_545 ?
Pd8 Pd1 Pd5 98.14(5) 1_545 1_545 ?
Pd1 Pd1 Pd5 64.62(5) 2_655 1_545 ?
Pd3 Pd1 Pd5 154.43(6) . 1_545 ?
Sb1 Pd1 Pd5 52.37(3) . 1_545 ?
Pd6 Pd1 Pd5 55.22(4) 2 1_545 ?
Pd2 Pd1 Pd5 99.66(5) . 1_545 ?
As2 Pd1 Pd5 145.73(6) 2_665 1_545 ?
As3 Pd1 Pd7 97.46(6) 1_545 2_665 ?
As3 Pd1 Pd7 50.83(5) 2_665 2_665 ?
Pd4 Pd1 Pd7 55.47(5) . 2_665 ?
Pd8 Pd1 Pd7 153.64(6) 1_545 2_665 ?
Pd1 Pd1 Pd7 63.61(5) 2_655 2_665 ?
Pd3 Pd1 Pd7 98.88(5) . 2_665 ?
Sb1 Pd1 Pd7 54.06(3) . 2_665 ?
Pd6 Pd1 Pd7 100.89(5) 2 2_665 ?
Pd2 Pd1 Pd7 102.83(5) . 2_665 ?
As2 Pd1 Pd7 144.62(6) 2_665 2_665 ?
Pd5 Pd1 Pd7 55.57(4) 1_545 2_665 ?
As1 Pd2 As2 124.65(6) . 1_546 ?
As1 Pd2 Pd8 59.70(4) . 2_666 ?
As2 Pd2 Pd8 67.00(6) 1_546 2_666 ?
As1 Pd2 Sb1 108.21(5) . . ?
As2 Pd2 Sb1 115.81(6) 1_546 . ?
Pd8 Pd2 Sb1 128.20(6) 2_666 . ?
As1 Pd2 Pd7 145.19(6) . 1_445 ?
As2 Pd2 Pd7 87.90(6) 1_546 1_445 ?
Pd8 Pd2 Pd7 154.72(6) 2_666 1_445 ?
Sb1 Pd2 Pd7 59.26(4) . 1_445 ?
As1 Pd2 Pd5 84.34(5) . 2_565 ?
As2 Pd2 Pd5 148.16(7) 1_546 2_565 ?
Pd8 Pd2 Pd5 143.91(6) 2_666 2_565 ?
Sb1 Pd2 Pd5 57.07(4) . 2_565 ?
Pd7 Pd2 Pd5 61.35(5) 1_445 2_565 ?
As1 Pd2 Pd6 142.91(6) . 2 ?
As2 Pd2 Pd6 57.32(5) 1_546 2 ?
Pd8 Pd2 Pd6 99.31(6) 2_666 2 ?
Sb1 Pd2 Pd6 58.61(4) . 2 ?
Pd7 Pd2 Pd6 62.36(5) 1_445 2 ?
Pd5 Pd2 Pd6 108.99(6) 2_565 2 ?
As1 Pd2 Pd3 53.34(4) . 2_666 ?
As2 Pd2 Pd3 122.77(7) 1_546 2_666 ?
Pd8 Pd2 Pd3 95.69(6) 2_666 2_666 ?
Sb1 Pd2 Pd3 116.97(5) . 2_666 ?
Pd7 Pd2 Pd3 100.77(6) 1_445 2_666 ?
Pd5 Pd2 Pd3 61.14(5) 2_565 2_666 ?
Pd6 Pd2 Pd3 162.86(6) 2 2_666 ?
As1 Pd2 Pd7 85.58(5) . 2_666 ?
As2 Pd2 Pd7 54.57(5) 1_546 2_666 ?
Pd8 Pd2 Pd7 60.34(5) 2_666 2_666 ?
Sb1 Pd2 Pd7 166.04(5) . 2_666 ?
Pd7 Pd2 Pd7 108.12(5) 1_445 2_666 ?
Pd5 Pd2 Pd7 124.38(6) 2_565 2_666 ?
Pd6 Pd2 Pd7 111.51(6) 2 2_666 ?
Pd3 Pd2 Pd7 69.22(5) 2_666 2_666 ?
As1 Pd2 As2 103.29(5) . 2_565 ?
As2 Pd2 As2 103.50(6) 1_546 2_565 ?
Pd8 Pd2 As2 134.87(7) 2_666 2_565 ?
Sb1 Pd2 As2 96.24(5) . 2_565 ?
Pd7 Pd2 As2 51.77(5) 1_445 2_565 ?
Pd5 Pd2 As2 51.93(5) 2_565 2_565 ?
Pd6 Pd2 As2 112.20(6) 2 2_565 ?
Pd3 Pd2 As2 50.70(5) 2_666 2_565 ?
Pd7 Pd2 As2 77.98(5) 2_666 2_565 ?
As1 Pd2 Pd1 82.46(4) . . ?
As2 Pd2 Pd1 89.74(6) 1_546 . ?
Pd8 Pd2 Pd1 66.32(5) 2_666 . ?
Sb1 Pd2 Pd1 62.07(4) . . ?
Pd7 Pd2 Pd1 112.60(6) 1_445 . ?
Pd5 Pd2 Pd1 108.76(6) 2_565 . ?
Pd6 Pd2 Pd1 60.57(5) 2 . ?
Pd3 Pd2 Pd1 134.33(6) 2_666 . ?
Pd7 Pd2 Pd1 123.79(6) 2_666 . ?
As2 Pd2 Pd1 158.12(6) 2_565 . ?
As1 Pd2 Pd4 51.37(3) . . ?
As2 Pd2 Pd4 146.74(7) 1_546 . ?
Pd8 Pd2 Pd4 91.86(5) 2_666 . ?
Sb1 Pd2 Pd4 56.92(4) . . ?
Pd7 Pd2 Pd4 108.99(5) 1_445 . ?
Pd5 Pd2 Pd4 60.07(5) 2_565 . ?
Pd6 Pd2 Pd4 104.59(5) 2 . ?
Pd3 Pd2 Pd4 83.06(5) 2_666 . ?
Pd7 Pd2 Pd4 136.94(6) 2_666 . ?
As2 Pd2 Pd4 109.46(6) 2_565 . ?
Pd1 Pd2 Pd4 57.56(4) . . ?
As1 Pd3 As2 118.42(6) . 1_656 ?
As1 Pd3 Pd5 151.68(6) . 2_665 ?
As2 Pd3 Pd5 89.48(6) 1_656 2_665 ?
As1 Pd3 Pd6 135.08(7) . 2_665 ?
As2 Pd3 Pd6 58.86(5) 1_656 2_665 ?
Pd5 Pd3 Pd6 62.11(5) 2_665 2_665 ?
As1 Pd3 As2 108.98(6) . 2_665 ?
As2 Pd3 As2 106.48(7) 1_656 2_665 ?
Pd5 Pd3 As2 53.83(5) 2_665 2_665 ?
Pd6 Pd3 As2 114.50(7) 2_665 2_665 ?
As1 Pd3 As3 114.76(6) . 2_665 ?
As2 Pd3 As3 111.42(7) 1_656 2_665 ?
Pd5 Pd3 As3 52.36(5) 2_665 2_665 ?
Pd6 Pd3 As3 53.19(5) 2_665 2_665 ?
As2 Pd3 As3 93.43(6) 2_665 2_665 ?
As1 Pd3 Pd8 58.86(4) . 2_666 ?
As2 Pd3 Pd8 124.10(8) 1_656 2_666 ?
Pd5 Pd3 Pd8 102.67(6) 2_665 2_666 ?
Pd6 Pd3 Pd8 164.77(7) 2_665 2_666 ?
As2 Pd3 Pd8 50.58(5) 2_665 2_666 ?
As3 Pd3 Pd8 119.11(6) 2_665 2_666 ?
As1 Pd3 Pd4 54.18(4) . . ?
As2 Pd3 Pd4 131.43(7) 1_656 . ?
Pd5 Pd3 Pd4 111.90(6) 2_665 . ?
Pd6 Pd3 Pd4 92.38(6) 2_665 . ?
As2 Pd3 Pd4 121.51(6) 2_665 . ?
As3 Pd3 Pd4 61.72(6) 2_665 . ?
Pd8 Pd3 Pd4 94.21(5) 2_666 . ?
As1 Pd3 Pd2 54.24(4) . 2_666 ?
As2 Pd3 Pd2 65.17(5) 1_656 2_666 ?
Pd5 Pd3 Pd2 154.07(6) 2_665 2_666 ?
Pd6 Pd3 Pd2 97.87(6) 2_665 2_666 ?
As2 Pd3 Pd2 136.20(7) 2_665 2_666 ?
As3 Pd3 Pd2 130.21(7) 2_665 2_666 ?
Pd8 Pd3 Pd2 96.50(6) 2_666 2_666 ?
Pd4 Pd3 Pd2 83.57(5) . 2_666 ?
As1 Pd3 Pd5 83.07(5) . 1_656 ?
As2 Pd3 Pd5 54.91(5) 1_656 1_656 ?
Pd5 Pd3 Pd5 112.36(6) 2_665 1_656 ?
Pd6 Pd3 Pd5 113.63(6) 2_665 1_656 ?
As2 Pd3 Pd5 81.24(6) 2_665 1_656 ?
As3 Pd3 Pd5 162.12(6) 2_665 1_656 ?
Pd8 Pd3 Pd5 70.27(6) 2_666 1_656 ?
Pd4 Pd3 Pd5 135.30(6) . 1_656 ?
Pd2 Pd3 Pd5 58.32(4) 2_666 1_656 ?
As1 Pd3 Pd1 83.82(4) . . ?
As2 Pd3 Pd1 157.76(7) 1_656 . ?
Pd5 Pd3 Pd1 68.41(5) 2_665 . ?
Pd6 Pd3 Pd1 106.01(6) 2_665 . ?
As2 Pd3 Pd1 62.88(5) 2_665 . ?
As3 Pd3 Pd1 53.35(5) 2_665 . ?
Pd8 Pd3 Pd1 66.01(5) 2_666 . ?
Pd4 Pd3 Pd1 59.98(5) . . ?
Pd2 Pd3 Pd1 136.47(6) 2_666 . ?
Pd5 Pd3 Pd1 134.90(6) 1_656 . ?
As1 Pd3 Pd3 131.33(8) . 2_766 ?
As2 Pd3 Pd3 57.56(5) 1_656 2_766 ?
Pd5 Pd3 Pd3 58.23(5) 2_665 2_766 ?
Pd6 Pd3 Pd3 87.62(6) 2_665 2_766 ?
As2 Pd3 Pd3 48.92(5) 2_665 2_766 ?
As3 Pd3 Pd3 109.86(7) 2_665 2_766 ?
Pd8 Pd3 Pd3 83.22(7) 2_666 2_766 ?
Pd4 Pd3 Pd3 168.56(7) . 2_766 ?
Pd2 Pd3 Pd3 107.77(7) 2_666 2_766 ?
Pd5 Pd3 Pd3 54.13(5) 1_656 2_766 ?
Pd1 Pd3 Pd3 109.05(7) . 2_766 ?
As1 Pd4 As3 120.52(7) . . ?
As1 Pd4 Sb1 107.56(5) . . ?
As3 Pd4 Sb1 111.95(6) . . ?
As1 Pd4 Pd7 149.52(7) . 2_665 ?
As3 Pd4 Pd7 89.70(6) . 2_665 ?
Sb1 Pd4 Pd7 59.06(4) . 2_665 ?
As1 Pd4 Pd7 87.41(5) . . ?
As3 Pd4 Pd7 54.86(5) . . ?
Sb1 Pd4 Pd7 164.48(6) . . ?
Pd7 Pd4 Pd7 109.61(6) 2_665 . ?
As1 Pd4 Pd8 58.12(4) . . ?
As3 Pd4 Pd8 63.10(6) . . ?
Sb1 Pd4 Pd8 124.37(7) . . ?
Pd7 Pd4 Pd8 152.34(7) 2_665 . ?
Pd7 Pd4 Pd8 59.98(5) . . ?
As1 Pd4 Pd3 53.59(4) . . ?
As3 Pd4 Pd3 125.22(7) . . ?
Sb1 Pd4 Pd3 121.58(5) . . ?
Pd7 Pd4 Pd3 107.32(7) 2_665 . ?
Pd7 Pd4 Pd3 70.42(5) . . ?
Pd8 Pd4 Pd3 93.52(5) . . ?
As1 Pd4 Pd1 84.04(5) . . ?
As3 Pd4 Pd1 154.11(8) . . ?
Sb1 Pd4 Pd1 62.62(4) . . ?
Pd7 Pd4 Pd1 65.49(5) 2_665 . ?
Pd7 Pd4 Pd1 124.75(7) . . ?
Pd8 Pd4 Pd1 142.14(6) . . ?
Pd3 Pd4 Pd1 60.85(5) . . ?
As1 Pd4 As3 110.39(6) . 2_665 ?
As3 Pd4 As3 106.64(7) . 2_665 ?
Sb1 Pd4 As3 97.32(5) . 2_665 ?
Pd7 Pd4 As3 51.26(5) 2_665 2_665 ?
Pd7 Pd4 As3 80.68(6) . 2_665 ?
Pd8 Pd4 As3 138.22(7) . 2_665 ?
Pd3 Pd4 As3 57.85(5) . 2_665 ?
Pd1 Pd4 As3 52.54(5) . 2_665 ?
As1 Pd4 Pd6 137.73(7) . . ?
As3 Pd4 Pd6 54.17(5) . . ?
Sb1 Pd4 Pd6 57.80(4) . . ?
Pd7 Pd4 Pd6 61.96(5) 2_665 . ?
Pd7 Pd4 Pd6 108.33(6) . . ?
Pd8 Pd4 Pd6 95.50(6) . . ?
Pd3 Pd4 Pd6 168.57(8) . . ?
Pd1 Pd4 Pd6 114.24(6) . . ?
As3 Pd4 Pd6 110.76(6) 2_665 . ?
As1 Pd4 Pd5 81.85(5) . 2_565 ?
As3 Pd4 Pd5 85.92(7) . 2_565 ?
Sb1 Pd4 Pd5 55.31(4) . 2_565 ?
Pd7 Pd4 Pd5 106.04(6) 2_665 2_565 ?
Pd7 Pd4 Pd5 125.37(7) . 2_565 ?
Pd8 Pd4 Pd5 69.14(5) . 2_565 ?
Pd3 Pd4 Pd5 133.61(6) . 2_565 ?
Pd1 Pd4 Pd5 107.20(6) . 2_565 ?
As3 Pd4 Pd5 152.62(6) 2_665 2_565 ?
Pd6 Pd4 Pd5 56.81(5) . 2_565 ?
As1 Pd4 Pd2 51.65(4) . . ?
As3 Pd4 Pd2 140.92(8) . . ?
Sb1 Pd4 Pd2 55.99(3) . . ?
Pd7 Pd4 Pd2 107.91(5) 2_665 . ?
Pd7 Pd4 Pd2 139.05(6) . . ?
Pd8 Pd4 Pd2 92.09(6) . . ?
Pd3 Pd4 Pd2 83.33(5) . . ?
Pd1 Pd4 Pd2 59.71(4) . . ?
As3 Pd4 Pd2 111.61(6) 2_665 . ?
Pd6 Pd4 Pd2 103.30(6) . . ?
Pd5 Pd4 Pd2 56.06(4) 2_565 . ?
As3 Pd5 As2 109.68(8) . . ?
As3 Pd5 Sb1 109.69(6) . 1_565 ?
As2 Pd5 Sb1 109.14(6) . 1_565 ?
As3 Pd5 Pd3 64.47(6) . 2_665 ?
As2 Pd5 Pd3 63.34(6) . 2_665 ?
Sb1 Pd5 Pd3 165.42(7) 1_565 2_665 ?
As3 Pd5 Pd6 66.30(6) . 2_565 ?
As2 Pd5 Pd6 164.11(7) . 2_565 ?
Sb1 Pd5 Pd6 60.72(4) 1_565 2_565 ?
Pd3 Pd5 Pd6 123.28(6) 2_665 2_565 ?
As3 Pd5 Pd2 163.61(7) . 2_565 ?
As2 Pd5 Pd2 65.90(6) . 2_565 ?
Sb1 Pd5 Pd2 60.07(4) 1_565 2_565 ?
Pd3 Pd5 Pd2 121.92(6) 2_665 2_565 ?
Pd6 Pd5 Pd2 113.29(6) 2_565 2_565 ?
As3 Pd5 Pd6 55.36(5) . . ?
As2 Pd5 Pd6 120.70(7) . . ?
Sb1 Pd5 Pd6 130.15(6) 1_565 . ?
Pd3 Pd5 Pd6 59.00(5) 2_665 . ?
Pd6 Pd5 Pd6 70.71(6) 2_565 . ?
Pd2 Pd5 Pd6 140.93(6) 2_565 . ?
As3 Pd5 Pd7 105.23(7) . 2_675 ?
As2 Pd5 Pd7 54.79(5) . 2_675 ?
Sb1 Pd5 Pd7 59.33(4) 1_565 2_675 ?
Pd3 Pd5 Pd7 108.15(6) 2_665 2_675 ?
Pd6 Pd5 Pd7 110.38(6) 2_565 2_675 ?
Pd2 Pd5 Pd7 58.90(5) 2_565 2_675 ?
Pd6 Pd5 Pd7 159.25(7) . 2_675 ?
As3 Pd5 Pd3 130.99(7) . 1_454 ?
As2 Pd5 Pd3 54.00(5) . 1_454 ?
Sb1 Pd5 Pd3 119.32(5) 1_565 1_454 ?
Pd3 Pd5 Pd3 67.64(6) 2_665 1_454 ?
Pd6 Pd5 Pd3 140.75(7) 2_565 1_454 ?
Pd2 Pd5 Pd3 60.54(5) 2_565 1_454 ?
Pd6 Pd5 Pd3 91.16(6) . 1_454 ?
Pd7 Pd5 Pd3 98.73(6) 2_675 1_454 ?
As3 Pd5 Pd4 123.93(7) . 2_565 ?
As2 Pd5 Pd4 126.16(7) . 2_565 ?
Sb1 Pd5 Pd4 59.10(4) 1_565 2_565 ?
Pd3 Pd5 Pd4 135.47(6) 2_665 2_565 ?
Pd6 Pd5 Pd4 61.25(5) 2_565 2_565 ?
Pd2 Pd5 Pd4 63.87(5) 2_565 2_565 ?
Pd6 Pd5 Pd4 88.88(6) . 2_565 ?
Pd7 Pd5 Pd4 110.07(6) 2_675 2_565 ?
Pd3 Pd5 Pd4 84.66(5) 1_454 2_565 ?
As3 Pd5 Pd1 53.31(5) . 1_565 ?
As2 Pd5 Pd1 104.66(7) . 1_565 ?
Sb1 Pd5 Pd1 61.46(4) 1_565 1_565 ?
Pd3 Pd5 Pd1 107.07(6) 2_665 1_565 ?
Pd6 Pd5 Pd1 60.18(4) 2_565 1_565 ?
Pd2 Pd5 Pd1 111.38(5) 2_565 1_565 ?
Pd6 Pd5 Pd1 103.97(5) . 1_565 ?
Pd7 Pd5 Pd1 62.26(5) 2_675 1_565 ?
Pd3 Pd5 Pd1 158.51(6) 1_454 1_565 ?
Pd4 Pd5 Pd1 110.40(5) 2_565 1_565 ?
As3 Pd5 Pd1 52.05(5) . 2_665 ?
As2 Pd5 Pd1 61.42(5) . 2_665 ?
Sb1 Pd5 Pd1 107.49(5) 1_565 2_665 ?
Pd3 Pd5 Pd1 58.11(4) 2_665 2_665 ?
Pd6 Pd5 Pd1 108.21(6) 2_565 2_665 ?
Pd2 Pd5 Pd1 116.29(6) 2_565 2_665 ?
Pd6 Pd5 Pd1 97.16(5) . 2_665 ?
Pd7 Pd5 Pd1 62.45(5) 2_675 2_665 ?
Pd3 Pd5 Pd1 108.40(6) 1_454 2_665 ?
Pd4 Pd5 Pd1 165.39(6) 2_565 2_665 ?
Pd1 Pd5 Pd1 55.25(5) 1_565 2_665 ?
As3 Pd6 As2 118.28(7) . 2_564 ?
As3 Pd6 Sb1 112.01(6) . . ?
As2 Pd6 Sb1 111.28(6) 2_564 . ?
As3 Pd6 Pd3 63.98(5) . 2_665 ?
As2 Pd6 Pd3 55.02(5) 2_564 2_665 ?
Sb1 Pd6 Pd3 127.51(7) . 2_665 ?
As3 Pd6 Pd8 125.54(7) . 2_565 ?
As2 Pd6 Pd8 52.70(5) 2_564 2_565 ?
Sb1 Pd6 Pd8 120.94(5) . 2_565 ?
Pd3 Pd6 Pd8 91.49(6) 2_665 2_565 ?
As3 Pd6 Pd5 89.00(6) . 2_565 ?
As2 Pd6 Pd5 152.26(7) 2_564 2_565 ?
Sb1 Pd6 Pd5 57.24(4) . 2_565 ?
Pd3 Pd6 Pd5 152.71(6) 2_665 2_565 ?
Pd8 Pd6 Pd5 108.53(6) 2_565 2_565 ?
As3 Pd6 Pd5 54.13(5) . . ?
As2 Pd6 Pd5 85.40(6) 2_564 . ?
Sb1 Pd6 Pd5 162.98(6) . . ?
Pd3 Pd6 Pd5 58.89(5) 2_665 . ?
Pd8 Pd6 Pd5 71.46(5) 2_565 . ?
Pd5 Pd6 Pd5 109.29(6) 2_565 . ?
As3 Pd6 As3 105.50(7) . 2_565 ?
As2 Pd6 As3 111.61(7) 2_564 2_565 ?
Sb1 Pd6 As3 95.67(5) . 2_565 ?
Pd3 Pd6 As3 136.75(7) 2_665 2_565 ?
Pd8 Pd6 As3 59.37(5) 2_565 2_565 ?
Pd5 Pd6 As3 51.21(5) 2_565 2_565 ?
Pd5 Pd6 As3 80.57(6) . 2_565 ?
As3 Pd6 Pd2 141.99(8) . 2 ?
As2 Pd6 Pd2 53.20(5) 2_564 2 ?
Sb1 Pd6 Pd2 58.19(4) . 2 ?
Pd3 Pd6 Pd2 92.17(6) 2_665 2 ?
Pd8 Pd6 Pd2 81.37(5) 2_565 2 ?
Pd5 Pd6 Pd2 108.67(5) 2_565 2 ?
Pd5 Pd6 Pd2 138.60(6) . 2 ?
As3 Pd6 Pd2 111.83(6) 2_565 2 ?
As3 Pd6 Pd4 53.66(5) . . ?
As2 Pd6 Pd4 137.52(8) 2_564 . ?
Sb1 Pd6 Pd4 58.36(4) . . ?
Pd3 Pd6 Pd4 96.39(6) 2_665 . ?
Pd8 Pd6 Pd4 169.77(7) 2_565 . ?
Pd5 Pd6 Pd4 61.94(5) 2_565 . ?
Pd5 Pd6 Pd4 107.20(5) . . ?
As3 Pd6 Pd4 110.45(6) 2_565 . ?
Pd2 Pd6 Pd4 104.75(6) 2 . ?
As3 Pd6 Pd7 85.87(6) . 2_665 ?
As2 Pd6 Pd7 82.53(6) 2_564 2_665 ?
Sb1 Pd6 Pd7 57.35(4) . 2_665 ?
Pd3 Pd6 Pd7 70.25(5) 2_665 2_665 ?
Pd8 Pd6 Pd7 132.78(7) 2_565 2_665 ?
Pd5 Pd6 Pd7 105.89(6) 2_565 2_665 ?
Pd5 Pd6 Pd7 124.68(6) . 2_665 ?
As3 Pd6 Pd7 153.00(6) 2_565 2_665 ?
Pd2 Pd6 Pd7 57.34(5) 2 2_665 ?
Pd4 Pd6 Pd7 56.64(5) . 2_665 ?
As3 Pd6 Pd1 152.16(8) . 2 ?
As2 Pd6 Pd1 87.67(6) 2_564 2 ?
Sb1 Pd6 Pd1 62.12(4) . 2 ?
Pd3 Pd6 Pd1 142.69(6) 2_665 2 ?
Pd8 Pd6 Pd1 60.97(5) 2_565 2 ?
Pd5 Pd6 Pd1 64.59(5) 2_565 2 ?
Pd5 Pd6 Pd1 124.34(7) . 2 ?
As3 Pd6 Pd1 51.60(5) 2_565 2 ?
Pd2 Pd6 Pd1 61.06(4) 2 2 ?
Pd4 Pd6 Pd1 114.47(6) . 2 ?
Pd7 Pd6 Pd1 108.87(6) 2_665 2 ?
As3 Pd7 As2 110.55(8) . 2_675 ?
As3 Pd7 Sb1 110.10(6) . 1_665 ?
As2 Pd7 Sb1 107.15(6) 2_675 1_665 ?
As3 Pd7 Pd4 67.01(6) . 2_665 ?
As2 Pd7 Pd4 162.66(8) 2_675 2_665 ?
Sb1 Pd7 Pd4 60.33(4) 1_665 2_665 ?
As3 Pd7 Pd2 165.29(7) . 1_665 ?
As2 Pd7 Pd2 66.50(6) 2_675 1_665 ?
Sb1 Pd7 Pd2 59.48(4) 1_665 1_665 ?
Pd4 Pd7 Pd2 111.17(6) 2_665 1_665 ?
As3 Pd7 Pd4 55.24(5) . . ?
As2 Pd7 Pd4 123.40(7) 2_675 . ?
Sb1 Pd7 Pd4 129.44(6) 1_665 . ?
Pd4 Pd7 Pd4 70.39(6) 2_665 . ?
Pd2 Pd7 Pd4 139.02(7) 1_665 . ?
As3 Pd7 Pd8 63.37(6) . . ?
As2 Pd7 Pd8 65.00(6) 2_675 . ?
Sb1 Pd7 Pd8 164.24(7) 1_665 . ?
Pd4 Pd7 Pd8 123.64(6) 2_665 . ?
Pd2 Pd7 Pd8 123.56(6) 1_665 . ?
Pd4 Pd7 Pd8 60.31(5) . . ?
As3 Pd7 Pd5 106.26(7) . 2_675 ?
As2 Pd7 Pd5 55.35(5) 2_675 2_675 ?
Sb1 Pd7 Pd5 56.60(4) 1_665 2_675 ?
Pd4 Pd7 Pd5 107.99(6) 2_665 2_675 ?
Pd2 Pd7 Pd5 59.75(5) 1_665 2_675 ?
Pd4 Pd7 Pd5 161.08(7) . 2_675 ?
Pd8 Pd7 Pd5 109.99(7) . 2_675 ?
As3 Pd7 Pd2 118.88(7) . 2_666 ?
As2 Pd7 Pd2 53.71(5) 2_675 2_666 ?
Sb1 Pd7 Pd2 130.95(5) 1_665 2_666 ?
Pd4 Pd7 Pd2 143.29(7) 2_665 2_666 ?
Pd2 Pd7 Pd2 71.88(5) 1_665 2_666 ?
Pd4 Pd7 Pd2 83.98(5) . 2_666 ?
Pd8 Pd7 Pd2 56.86(5) . 2_666 ?
Pd5 Pd7 Pd2 104.61(6) 2_675 2_666 ?
As3 Pd7 Pd6 125.09(7) . 2_665 ?
As2 Pd7 Pd6 124.31(7) 2_675 2_665 ?
Sb1 Pd7 Pd6 57.97(4) 1_665 2_665 ?
Pd4 Pd7 Pd6 61.41(5) 2_665 2_665 ?
Pd2 Pd7 Pd6 60.31(5) 1_665 2_665 ?
Pd4 Pd7 Pd6 89.73(6) . 2_665 ?
Pd8 Pd7 Pd6 137.78(7) . 2_665 ?
Pd5 Pd7 Pd6 106.21(5) 2_675 2_665 ?
Pd2 Pd7 Pd6 93.66(6) 2_666 2_665 ?
As3 Pd7 Pd1 53.94(5) . 2_665 ?
As2 Pd7 Pd1 105.02(7) 2_675 2_665 ?
Sb1 Pd7 Pd1 60.66(4) 1_665 2_665 ?
Pd4 Pd7 Pd1 59.04(5) 2_665 2_665 ?
Pd2 Pd7 Pd1 112.00(6) 1_665 2_665 ?
Pd4 Pd7 Pd1 103.50(5) . 2_665 ?
Pd8 Pd7 Pd1 106.91(6) . 2_665 ?
Pd5 Pd7 Pd1 62.17(5) 2_675 2_665 ?
Pd2 Pd7 Pd1 156.18(7) 2_666 2_665 ?
Pd6 Pd7 Pd1 108.77(6) 2_665 2_665 ?
As3 Pd7 Pd1 51.95(5) . 1_565 ?
As2 Pd7 Pd1 62.27(6) 2_675 1_565 ?
Sb1 Pd7 Pd1 106.66(5) 1_665 1_565 ?
Pd4 Pd7 Pd1 107.89(6) 2_665 1_565 ?
Pd2 Pd7 Pd1 118.45(6) 1_665 1_565 ?
Pd4 Pd7 Pd1 98.07(5) . 1_565 ?
Pd8 Pd7 Pd1 57.74(5) . 1_565 ?
Pd5 Pd7 Pd1 63.99(5) 2_675 1_565 ?
Pd2 Pd7 Pd1 101.22(5) 2_666 1_565 ?
Pd6 Pd7 Pd1 163.81(6) 2_665 1_565 ?
Pd1 Pd7 Pd1 55.67(5) 2_665 1_565 ?
As2 Pd8 As1 116.73(6) 1_556 . ?
As2 Pd8 Pd2 123.88(7) 1_556 2_666 ?
As1 Pd8 Pd2 54.80(4) . 2_666 ?
As2 Pd8 Pd6 59.74(6) 1_556 2_565 ?
As1 Pd8 Pd6 128.59(7) . 2_565 ?
Pd2 Pd8 Pd6 174.47(6) 2_666 2_565 ?
As2 Pd8 As3 121.44(7) 1_556 . ?
As1 Pd8 As3 104.64(6) . . ?
Pd2 Pd8 As3 113.41(6) 2_666 . ?
Pd6 Pd8 As3 62.26(5) 2_565 . ?
As2 Pd8 Pd3 64.04(5) 1_556 2_666 ?
As1 Pd8 Pd3 53.22(4) . 2_666 ?
Pd2 Pd8 Pd3 90.60(6) 2_666 2_666 ?
Pd6 Pd8 Pd3 94.87(6) 2_565 2_666 ?
As3 Pd8 Pd3 129.35(7) . 2_666 ?
As2 Pd8 Pd7 158.17(8) 1_556 . ?
As1 Pd8 Pd7 84.48(5) . . ?
Pd2 Pd8 Pd7 62.81(5) 2_666 . ?
Pd6 Pd8 Pd7 112.21(6) 2_565 . ?
As3 Pd8 Pd7 51.81(5) . . ?
Pd3 Pd8 Pd7 137.58(7) 2_666 . ?
As2 Pd8 Pd4 136.46(8) 1_556 . ?
As1 Pd8 Pd4 53.18(4) . . ?
Pd2 Pd8 Pd4 86.83(6) 2_666 . ?
Pd6 Pd8 Pd4 92.54(6) 2_565 . ?
As3 Pd8 Pd4 51.97(5) . . ?
Pd3 Pd8 Pd4 88.24(6) 2_666 . ?
Pd7 Pd8 Pd4 59.71(5) . . ?
As2 Pd8 As2 113.34(7) 1_556 2_675 ?
As1 Pd8 As2 105.43(6) . 2_675 ?
Pd2 Pd8 As2 52.04(5) 2_666 2_675 ?
Pd6 Pd8 As2 123.37(6) 2_565 2_675 ?
As3 Pd8 As2 91.62(6) . 2_675 ?
Pd3 Pd8 As2 135.30(7) 2_666 2_675 ?
Pd7 Pd8 As2 51.70(5) . 2_675 ?
Pd4 Pd8 As2 109.96(6) . 2_675 ?
As2 Pd8 Pd1 92.66(6) 1_556 1_565 ?
As1 Pd8 Pd1 150.45(6) . 1_565 ?
Pd2 Pd8 Pd1 112.31(6) 2_666 1_565 ?
Pd6 Pd8 Pd1 62.51(5) 2_565 1_565 ?
As3 Pd8 Pd1 52.76(5) . 1_565 ?
Pd3 Pd8 Pd1 154.41(6) 2_666 1_565 ?
Pd7 Pd8 Pd1 66.64(5) . 1_565 ?
Pd4 Pd8 Pd1 103.70(6) . 1_565 ?
As2 Pd8 Pd1 61.89(5) 2_675 1_565 ?
As2 Pd8 Pd8 64.76(6) 1_556 2_676 ?
As1 Pd8 Pd8 129.01(8) . 2_676 ?
Pd2 Pd8 Pd8 81.34(7) 2_666 2_676 ?
Pd6 Pd8 Pd8 97.48(7) 2_565 2_676 ?
As3 Pd8 Pd8 116.99(7) . 2_676 ?
Pd3 Pd8 Pd8 110.04(7) 2_666 2_676 ?
Pd7 Pd8 Pd8 98.49(7) . 2_676 ?
Pd4 Pd8 Pd8 158.17(8) . 2_676 ?
As2 Pd8 Pd8 48.59(5) 2_675 2_676 ?
Pd1 Pd8 Pd8 64.77(5) 1_565 2_676 ?
As2 Pd8 Pd1 63.75(5) 1_556 2_666 ?
As1 Pd8 Pd1 77.23(4) . 2_666 ?
Pd2 Pd8 Pd1 60.37(5) 2_666 2_666 ?
Pd6 Pd8 Pd1 123.48(6) 2_565 2_666 ?
As3 Pd8 Pd1 171.19(7) . 2_666 ?
Pd3 Pd8 Pd1 58.73(5) 2_666 2_666 ?
Pd7 Pd8 Pd1 120.49(6) . 2_666 ?
Pd4 Pd8 Pd1 130.41(6) . 2_666 ?
As2 Pd8 Pd1 79.61(6) 2_675 2_666 ?
Pd1 Pd8 Pd1 122.16(6) 1_565 2_666 ?
Pd8 Pd8 Pd1 57.39(5) 2_676 2_666 ?
Pd3 As1 Pd3 180.0 2_666 . ?
Pd3 As1 Pd4 72.23(5) 2_666 2_666 ?
Pd3 As1 Pd4 107.77(5) . 2_666 ?
Pd3 As1 Pd4 107.77(5) 2_666 . ?
Pd3 As1 Pd4 72.23(5) . . ?
Pd4 As1 Pd4 180.0 2_666 . ?
Pd3 As1 Pd2 72.42(4) 2_666 . ?
Pd3 As1 Pd2 107.58(4) . . ?
Pd4 As1 Pd2 103.01(4) 2_666 . ?
Pd4 As1 Pd2 76.98(4) . . ?
Pd3 As1 Pd2 107.58(4) 2_666 2_666 ?
Pd3 As1 Pd2 72.42(4) . 2_666 ?
Pd4 As1 Pd2 76.99(5) 2_666 2_666 ?
Pd4 As1 Pd2 103.01(4) . 2_666 ?
Pd2 As1 Pd2 180.0 . 2_666 ?
Pd3 As1 Pd8 112.08(5) 2_666 2_666 ?
Pd3 As1 Pd8 67.92(4) . 2_666 ?
Pd4 As1 Pd8 68.70(5) 2_666 2_666 ?
Pd4 As1 Pd8 111.30(5) . 2_666 ?
Pd2 As1 Pd8 65.49(4) . 2_666 ?
Pd2 As1 Pd8 114.51(4) 2_666 2_666 ?
Pd3 As1 Pd8 67.92(4) 2_666 . ?
Pd3 As1 Pd8 112.08(5) . . ?
Pd4 As1 Pd8 111.30(5) 2_666 . ?
Pd4 As1 Pd8 68.70(5) . . ?
Pd2 As1 Pd8 114.51(4) . . ?
Pd2 As1 Pd8 65.49(4) 2_666 . ?
Pd8 As1 Pd8 180.0 2_666 . ?
Pd8 As2 Pd2 98.95(7) 1_554 1_564 ?
Pd8 As2 Pd3 109.24(8) 1_554 1_454 ?
Pd2 As2 Pd3 110.82(8) 1_564 1_454 ?
Pd8 As2 Pd7 126.80(8) 1_554 2_675 ?
Pd2 As2 Pd7 71.72(6) 1_564 2_675 ?
Pd3 As2 Pd7 123.22(8) 1_454 2_675 ?
Pd8 As2 Pd5 125.45(8) 1_554 . ?
Pd2 As2 Pd5 133.13(8) 1_564 . ?
Pd3 As2 Pd5 71.09(6) 1_454 . ?
Pd7 As2 Pd5 69.86(6) 2_675 . ?
Pd8 As2 Pd6 67.56(6) 1_554 2_564 ?
Pd2 As2 Pd6 69.47(6) 1_564 2_564 ?
Pd3 As2 Pd6 66.11(6) 1_454 2_564 ?
Pd7 As2 Pd6 140.45(8) 2_675 2_564 ?
Pd5 As2 Pd6 136.97(8) . 2_564 ?
Pd8 As2 Pd3 65.37(6) 1_554 2_665 ?
Pd2 As2 Pd3 163.97(8) 1_564 2_665 ?
Pd3 As2 Pd3 73.52(7) 1_454 2_665 ?
Pd7 As2 Pd3 119.67(8) 2_675 2_665 ?
Pd5 As2 Pd3 62.83(6) . 2_665 ?
Pd6 As2 Pd3 99.87(7) 2_564 2_665 ?
Pd8 As2 Pd8 66.66(7) 1_554 2_675 ?
Pd2 As2 Pd8 60.96(5) 1_564 2_675 ?
Pd3 As2 Pd8 168.76(8) 1_454 2_675 ?
Pd7 As2 Pd8 63.30(6) 2_675 2_675 ?
Pd5 As2 Pd8 120.01(8) . 2_675 ?
Pd6 As2 Pd8 102.92(7) 2_564 2_675 ?
Pd3 As2 Pd8 112.22(7) 2_665 2_675 ?
Pd8 As2 Pd2 168.99(8) 1_554 2_565 ?
Pd2 As2 Pd2 76.50(6) 1_564 2_565 ?
Pd3 As2 Pd2 64.12(5) 1_454 2_565 ?
Pd7 As2 Pd2 61.73(5) 2_675 2_565 ?
Pd5 As2 Pd2 62.18(5) . 2_565 ?
Pd6 As2 Pd2 101.43(7) 2_564 2_565 ?
Pd3 As2 Pd2 118.27(7) 2_665 2_565 ?
Pd8 As2 Pd2 118.04(7) 2_675 2_565 ?
Pd8 As2 Pd1 70.25(6) 1_554 2_665 ?
Pd2 As2 Pd1 118.63(7) 1_564 2_665 ?
Pd3 As2 Pd1 130.09(8) 1_454 2_665 ?
Pd7 As2 Pd1 69.87(6) 2_675 2_665 ?
Pd5 As2 Pd1 70.79(6) . 2_665 ?
Pd6 As2 Pd1 137.80(8) 2_564 2_665 ?
Pd3 As2 Pd1 60.92(5) 2_665 2_665 ?
Pd8 As2 Pd1 59.53(5) 2_675 2_665 ?
Pd2 As2 Pd1 120.76(7) 2_565 2_665 ?
Pd5 As3 Pd7 148.50(8) . . ?
Pd5 As3 Pd4 141.41(8) . . ?
Pd7 As3 Pd4 69.89(6) . . ?
Pd5 As3 Pd6 70.51(6) . . ?
Pd7 As3 Pd6 140.63(8) . . ?
Pd4 As3 Pd6 72.17(6) . . ?
Pd5 As3 Pd1 75.89(6) . 1_565 ?
Pd7 As3 Pd1 78.21(6) . 1_565 ?
Pd4 As3 Pd1 128.95(8) . 1_565 ?
Pd6 As3 Pd1 136.38(8) . 1_565 ?
Pd5 As3 Pd1 79.09(6) . 2_665 ?
Pd7 As3 Pd1 75.23(6) . 2_665 ?
Pd4 As3 Pd1 133.64(8) . 2_665 ?
Pd6 As3 Pd1 127.83(8) . 2_665 ?
Pd1 As3 Pd1 69.44(6) 1_565 2_665 ?
Pd5 As3 Pd3 63.17(6) . 2_665 ?
Pd7 As3 Pd3 119.85(7) . 2_665 ?
Pd4 As3 Pd3 107.13(7) . 2_665 ?
Pd6 As3 Pd3 62.83(5) . 2_665 ?
Pd1 As3 Pd3 123.30(7) 1_565 2_665 ?
Pd1 As3 Pd3 65.82(6) 2_665 2_665 ?
Pd5 As3 Pd8 118.36(7) . . ?
Pd7 As3 Pd8 64.82(6) . . ?
Pd4 As3 Pd8 64.93(6) . . ?
Pd6 As3 Pd8 107.48(7) . . ?
Pd1 As3 Pd8 65.74(6) 1_565 . ?
Pd1 As3 Pd8 124.27(7) 2_665 . ?
Pd3 As3 Pd8 169.72(7) 2_665 . ?
Pd5 As3 Pd6 62.49(5) . 2_565 ?
Pd7 As3 Pd6 120.95(7) . 2_565 ?
Pd4 As3 Pd6 98.27(7) . 2_565 ?
Pd6 As3 Pd6 74.50(7) . 2_565 ?
Pd1 As3 Pd6 65.56(5) 1_565 2_565 ?
Pd1 As3 Pd6 126.00(7) 2_665 2_565 ?
Pd3 As3 Pd6 118.89(7) 2_665 2_565 ?
Pd8 As3 Pd6 58.37(5) . 2_565 ?
Pd5 As3 Pd4 120.96(7) . 2_665 ?
Pd7 As3 Pd4 61.73(5) . 2_665 ?
Pd4 As3 Pd4 73.36(7) . 2_665 ?
Pd6 As3 Pd4 97.57(7) . 2_665 ?
Pd1 As3 Pd4 123.70(7) 1_565 2_665 ?
Pd1 As3 Pd4 63.49(5) 2_665 2_665 ?
Pd3 As3 Pd4 60.43(5) 2_665 2_665 ?
Pd8 As3 Pd4 120.30(7) . 2_665 ?
Pd6 As3 Pd4 170.13(7) 2_565 2_665 ?
 
_refine_diff_density_max    2.804
_refine_diff_density_min   -2.890
_refine_diff_density_rms    0.633



