data_magnesioleydetite _audit_creation_method 'SHELXL-2016/6' _chemical_name_mineral 'magnesioleydetite' _chemical_compound_source 'Markey mine, Utah' _chemical_formula_sum 'Fe0.26 H22 Mg0.56 O21 S2 U Zn0.18' _chemical_formula_weight 700.23 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mg' 'Mg' 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'U' 'U' -9.6767 9.6646 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3463 0.8444 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Zn' 'Zn' 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 15 _space_group_name_H-M_alt 'C 2/c' _space_group_name_Hall '-C 2yc' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z+1/2' '-x, -y, -z' 'x, -y, z-1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z-1/2' _cell_length_a 11.3513(3) _cell_length_b 7.7310(2) _cell_length_c 21.7957(15) _cell_angle_alpha 90 _cell_angle_beta 102.387(7) _cell_angle_gamma 90 _cell_volume 1868.19(16) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _exptl_crystal_density_diffrn 2.490 _exptl_crystal_F_000 1332 _exptl_crystal_size_max 0.160 _exptl_crystal_size_mid 0.070 _exptl_crystal_size_min 0.040 _exptl_absorpt_coefficient_mu 9.445 _shelx_estimated_absorpt_T_min 0.313 _shelx_estimated_absorpt_T_max 0.704 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details Higashi2001 _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71075 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_reflns_number 8487 _diffrn_reflns_av_unetI/netI 0.0220 _diffrn_reflns_av_R_equivalents 0.0261 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -10 _diffrn_reflns_limit_k_max 10 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 28 _diffrn_reflns_theta_min 3.532 _diffrn_reflns_theta_max 27.481 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measured_fraction_theta_full 0.988 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_Laue_measured_fraction_full 0.988 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_point_group_measured_fraction_full 0.988 _reflns_number_total 2110 _reflns_number_gt 2040 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2016/6 (Sheldrick, 2016)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ? _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0154P)^2^+1.9286P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens difmap _refine_ls_hydrogen_treatment refxyz _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 2110 _refine_ls_number_parameters 149 _refine_ls_number_restraints 11 _refine_ls_R_factor_all 0.0169 _refine_ls_R_factor_gt 0.0161 _refine_ls_wR_factor_ref 0.0350 _refine_ls_wR_factor_gt 0.0348 _refine_ls_goodness_of_fit_ref 1.114 _refine_ls_restrained_S_all 1.116 _refine_ls_shift/su_max 0.002 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group U U 0.000000 0.20592(2) 0.250000 0.01424(5) Uani 1 2 d S T P . . S S 0.30824(6) 0.36607(8) 0.28936(3) 0.01860(13) Uani 1 1 d . . . . . Mg Mg 0.000000 0.500000 0.000000 0.02634(17) Uani 0.56 2 d S . P . . Fe Fe 0.000000 0.500000 0.000000 0.02634(17) Uani 0.26 2 d S . P . . Zn Zn 0.000000 0.500000 0.000000 0.02634(17) Uani 0.18 2 d S . P . . O1 O 0.2857(2) 0.4801(3) 0.33826(10) 0.0334(5) Uani 1 1 d . . . . . O2 O 0.3775(2) 0.2150(3) 0.31627(10) 0.0331(5) Uani 1 1 d . . . . . O3 O 0.19402(18) 0.3113(3) 0.24741(10) 0.0282(4) Uani 1 1 d . . . . . O4 O 0.37668(17) 0.4576(2) 0.24769(9) 0.0230(4) Uani 1 1 d . . . . . O5 O 0.03506(18) 0.2037(3) 0.33310(9) 0.0268(4) Uani 1 1 d . . . . . OW6 O 0.000000 0.5167(4) 0.250000 0.0413(9) Uani 1 2 d DS T P . . H6 H -0.036(3) 0.583(4) 0.2668(18) 0.050 Uiso 1 1 d D U . . . OW7 O 0.0764(3) 0.7268(3) 0.47353(12) 0.0399(6) Uani 1 1 d D . . . . H7A H 0.100(4) 0.808(4) 0.4981(17) 0.048 Uiso 1 1 d D U . . . H7B H 0.098(4) 0.736(5) 0.4408(15) 0.048 Uiso 1 1 d D U . . . OW8 O 0.1094(2) 0.3485(3) 0.45511(11) 0.0385(5) Uani 1 1 d D . . . . H8A H 0.084(4) 0.312(5) 0.4197(13) 0.046 Uiso 1 1 d D U . . . H8B H 0.181(2) 0.378(5) 0.4583(18) 0.046 Uiso 1 1 d D U . . . OW9 O 0.3673(2) 0.0139(3) 0.41863(11) 0.0419(6) Uani 1 1 d D . . . . H9A H 0.379(4) 0.074(5) 0.3920(16) 0.050 Uiso 1 1 d D U . . . H9B H 0.320(3) -0.055(5) 0.4058(18) 0.050 Uiso 1 1 d D U . . . OW10 O 0.1823(2) 0.7789(3) 0.37316(11) 0.0356(5) Uani 1 1 d D . . . . H10A H 0.208(4) 0.705(4) 0.3576(18) 0.043 Uiso 1 1 d D U . . . H10B H 0.151(3) 0.836(5) 0.3443(15) 0.043 Uiso 1 1 d D U . . . OW11 O 0.3430(3) 0.4680(3) 0.46503(12) 0.0436(6) Uani 1 1 d D . . . . H11A H 0.345(4) 0.473(6) 0.4310(13) 0.052 Uiso 1 1 d D U . . . H11B H 0.371(4) 0.383(4) 0.4820(18) 0.052 Uiso 1 1 d D U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 U 0.01144(7) 0.01318(7) 0.01856(7) 0.000 0.00424(4) 0.000 S 0.0173(3) 0.0155(3) 0.0245(3) -0.0011(2) 0.0079(2) -0.0020(3) Mg 0.0335(4) 0.0236(4) 0.0221(4) 0.0006(3) 0.0064(3) 0.0021(3) Fe 0.0335(4) 0.0236(4) 0.0221(4) 0.0006(3) 0.0064(3) 0.0021(3) Zn 0.0335(4) 0.0236(4) 0.0221(4) 0.0006(3) 0.0064(3) 0.0021(3) O1 0.0417(13) 0.0282(11) 0.0340(12) -0.0084(9) 0.0162(9) -0.0008(10) O2 0.0396(13) 0.0275(11) 0.0343(12) 0.0088(9) 0.0129(10) 0.0120(10) O3 0.0200(10) 0.0286(11) 0.0377(12) -0.0060(9) 0.0097(8) -0.0067(9) O4 0.0197(9) 0.0212(9) 0.0306(10) -0.0008(8) 0.0107(8) -0.0075(8) O5 0.0249(10) 0.0309(11) 0.0247(10) -0.0038(8) 0.0053(8) -0.0037(9) OW6 0.041(2) 0.0154(15) 0.078(3) 0.000 0.0371(18) 0.000 OW7 0.0575(16) 0.0323(12) 0.0343(13) -0.0031(10) 0.0193(12) -0.0136(12) OW8 0.0408(13) 0.0481(14) 0.0273(11) -0.0116(10) 0.0089(10) -0.0015(12) OW9 0.0510(16) 0.0432(15) 0.0265(12) 0.0080(10) -0.0024(10) -0.0159(12) OW10 0.0463(15) 0.0341(13) 0.0263(12) 0.0002(10) 0.0073(10) 0.0069(11) OW11 0.0535(16) 0.0365(13) 0.0375(13) -0.0005(12) 0.0023(12) 0.0087(12) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag U O5 1.769(2) . ? U O5 1.769(2) 2 ? U O3 2.3603(19) 2 ? U O3 2.360(2) . ? U O4 2.3700(18) 3_445 ? U O4 2.3700(18) 4_545 ? U OW6 2.403(3) . ? S O1 1.447(2) . ? S O2 1.459(2) . ? S O3 1.479(2) . ? S O4 1.4940(19) . ? Mg OW9 2.068(2) 8_455 ? Mg OW9 2.068(2) 4 ? Mg OW7 2.091(2) 2 ? Mg OW7 2.091(2) 6_565 ? Mg OW8 2.096(2) 2 ? Mg OW8 2.096(2) 6_565 ? OW6 H6 0.79(2) . ? OW6 H6 0.79(2) 2 ? OW7 H7A 0.83(3) . ? OW7 H7B 0.81(3) . ? OW8 H8A 0.81(3) . ? OW8 H8B 0.84(3) . ? OW9 H9A 0.78(3) . ? OW9 H9B 0.77(3) . ? OW10 H10A 0.75(2) . ? OW10 H10B 0.79(2) . ? OW11 H11A 0.75(3) . ? OW11 H11B 0.79(3) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O5 U O5 178.88(13) . 2 ? O5 U O3 89.14(8) . 2 ? O5 U O3 91.24(8) 2 2 ? O5 U O3 91.24(8) . . ? O5 U O3 89.14(8) 2 . ? O3 U O3 139.61(10) 2 . ? O5 U O4 90.91(8) . 3_445 ? O5 U O4 88.18(8) 2 3_445 ? O3 U O4 74.35(7) 2 3_445 ? O3 U O4 146.00(7) . 3_445 ? O5 U O4 88.18(8) . 4_545 ? O5 U O4 90.91(8) 2 4_545 ? O3 U O4 146.00(7) 2 4_545 ? O3 U O4 74.35(7) . 4_545 ? O4 U O4 71.82(9) 3_445 4_545 ? O5 U OW6 90.56(7) . . ? O5 U OW6 90.56(7) 2 . ? O3 U OW6 69.80(5) 2 . ? O3 U OW6 69.80(5) . . ? O4 U OW6 144.09(5) 3_445 . ? O4 U OW6 144.09(5) 4_545 . ? O1 S O2 110.90(13) . . ? O1 S O3 111.09(13) . . ? O2 S O3 110.18(13) . . ? O1 S O4 110.85(12) . . ? O2 S O4 108.52(12) . . ? O3 S O4 105.13(12) . . ? OW9 Mg OW9 180.00(18) 8_455 4 ? OW9 Mg OW7 90.64(10) 8_455 2 ? OW9 Mg OW7 89.36(10) 4 2 ? OW9 Mg OW7 89.36(10) 8_455 6_565 ? OW9 Mg OW7 90.64(10) 4 6_565 ? OW7 Mg OW7 180.00(13) 2 6_565 ? OW9 Mg OW8 88.63(10) 8_455 2 ? OW9 Mg OW8 91.37(10) 4 2 ? OW7 Mg OW8 90.98(10) 2 2 ? OW7 Mg OW8 89.02(10) 6_565 2 ? OW9 Mg OW8 91.37(10) 8_455 6_565 ? OW9 Mg OW8 88.63(10) 4 6_565 ? OW7 Mg OW8 89.02(10) 2 6_565 ? OW7 Mg OW8 90.98(10) 6_565 6_565 ? OW8 Mg OW8 180.00(15) 2 6_565 ? S O3 U 141.51(13) . . ? S O4 U 138.82(11) . 3 ? U OW6 H6 130(3) . . ? U OW6 H6 130(3) . 2 ? H6 OW6 H6 99(6) . 2 ? Mg OW7 H7A 123(3) 2 . ? Mg OW7 H7B 123(3) 2 . ? H7A OW7 H7B 113(4) . . ? Mg OW8 H8A 120(3) 2 . ? Mg OW8 H8B 118(3) 2 . ? H8A OW8 H8B 108(4) . . ? Mg OW9 H9A 118(3) 4_545 . ? Mg OW9 H9B 127(3) 4_545 . ? H9A OW9 H9B 111(4) . . ? H10A OW10 H10B 102(4) . . ? H11A OW11 H11B 114(5) . . ? loop_ _geom_hbond_atom_site_label_D _geom_hbond_atom_site_label_H _geom_hbond_atom_site_label_A _geom_hbond_distance_DH _geom_hbond_distance_HA _geom_hbond_distance_DA _geom_hbond_angle_DHA _geom_hbond_site_symmetry_A OW6 H6 O2 0.79(2) 1.91(2) 2.689(3) 171(4) 3_455 OW7 H7A OW11 0.83(3) 1.96(3) 2.770(4) 165(4) 7_566 OW7 H7B OW10 0.81(3) 1.95(3) 2.742(3) 168(4) . OW8 H8A O5 0.81(3) 2.03(3) 2.842(3) 174(4) . OW8 H8B OW11 0.84(3) 1.94(3) 2.772(4) 175(4) . OW9 H9A O2 0.78(3) 1.98(3) 2.742(3) 170(4) . OW9 H9B OW10 0.77(3) 2.03(3) 2.793(4) 174(4) 1_545 OW10 H10A O1 0.75(2) 2.04(3) 2.771(3) 165(4) . OW10 H10B O4 0.79(2) 2.18(3) 2.922(3) 159(4) 4 OW11 H11A O1 0.75(3) 1.99(3) 2.701(3) 159(5) . OW11 H11B OW8 0.79(3) 2.23(3) 2.984(4) 159(4) 7_556 _refine_diff_density_max 0.913 _refine_diff_density_min -0.671 _refine_diff_density_rms 0.106 _shelx_res_file ; TITL JM-13157 13157.res created by SHELXL-2016/6 at 15:23:46 on 28-May-2017 CELL 0.71075 11.35130 7.73096 21.79570 90.00000 102.38700 90.00000 ZERR 4 0.00026 0.00021 0.00153 0.00000 0.00720 0.00000 LATT 7 SYMM -X, +Y, 1/2-Z SFAC H MG O S U FE ZN UNIT 88 2.24 84 8 4 1.04 0.72 L.S. 10 omit -8 0 8 omit 0 0 4 omit 3 1 2 omit -1 1 3 omit -1 1 1 omit -1 1 5 omit -4 0 2 omit 3 1 1 omit 2 0 4 omit -3 1 1 omit -2 0 4 omit -1 1 4 omit 1 1 0 omit 1 1 2 omit -2 2 2 omit 0 2 2 omit 1 1 1 omit -3 1 3 omit -1 1 7 omit 2 0 0 EXYZ MG FE ZN EADP MG FE ZN FMAP 2 PLAN 8 ACTA BOND $H DFIX 0.82 0.03 OW6 H6 OW7 H7a OW7 H7b OW8 H8a OW8 H8b DFIX 0.82 0.03 OW9 H9a OW9 H9b OW10 H10a OW10 H10b OW11 H11a OW11 H11b EQIV $1 x-1/2, y+1/2, z HTAB OW6 O2_$1 EQIV $2 -x+1/2, -y+3/2, -z+1 HTAB OW7 OW11_$2 HTAB OW7 OW10 HTAB OW8 O5 HTAB OW8 OW11 HTAB OW9 O2 EQIV $3 x, y-1, z HTAB OW9 OW10_$3 HTAB OW10 O1 EQIV $4 -x+1/2, y+1/2, -z+1/2 HTAB OW10 O4_$4 HTAB OW11 O1 EQIV $5 -x+1/2, -y+1/2, -z+1 HTAB OW11 OW8_$5 SIZE 0.160 0.070 0.040 WGHT 0.015400 1.928600 FVAR 0.28509 U 5 0.000000 0.205919 0.250000 10.50000 0.01144 0.01318 = 0.01856 0.00000 0.00424 0.00000 S 4 0.308239 0.366073 0.289363 11.00000 0.01728 0.01553 = 0.02453 -0.00112 0.00791 -0.00202 MG 2 0.000000 0.500000 0.000000 10.28000 0.03352 0.02360 = 0.02208 0.00057 0.00641 0.00210 FE 6 0.000000 0.500000 0.000000 10.13000 0.03352 0.02360 = 0.02208 0.00057 0.00641 0.00210 ZN 7 0.000000 0.500000 0.000000 10.09000 0.03352 0.02360 = 0.02208 0.00057 0.00641 0.00210 O1 3 0.285745 0.480125 0.338259 11.00000 0.04168 0.02821 = 0.03401 -0.00842 0.01622 -0.00081 O2 3 0.377547 0.215012 0.316267 11.00000 0.03962 0.02748 = 0.03430 0.00884 0.01286 0.01198 O3 3 0.194025 0.311316 0.247415 11.00000 0.01997 0.02856 = 0.03765 -0.00598 0.00971 -0.00669 O4 3 0.376679 0.457615 0.247694 11.00000 0.01971 0.02118 = 0.03057 -0.00076 0.01066 -0.00753 O5 3 0.035056 0.203683 0.333104 11.00000 0.02487 0.03090 = 0.02468 -0.00377 0.00527 -0.00375 OW6 3 0.000000 0.516697 0.250000 10.50000 0.04114 0.01541 = 0.07831 0.00000 0.03714 0.00000 H6 1 -0.035543 0.582786 0.266757 11.00000 -1.20000 OW7 3 0.076441 0.726761 0.473528 11.00000 0.05747 0.03228 = 0.03428 -0.00309 0.01927 -0.01364 H7A 1 0.100173 0.807854 0.498063 11.00000 -1.20000 H7B 1 0.098171 0.735979 0.440791 11.00000 -1.20000 OW8 3 0.109417 0.348535 0.455110 11.00000 0.04084 0.04806 = 0.02730 -0.01162 0.00886 -0.00148 H8A 1 0.083765 0.312412 0.419723 11.00000 -1.20000 H8B 1 0.181288 0.377854 0.458296 11.00000 -1.20000 OW9 3 0.367345 0.013857 0.418634 11.00000 0.05102 0.04320 = 0.02655 0.00796 -0.00236 -0.01592 H9A 1 0.378608 0.073948 0.391984 11.00000 -1.20000 H9B 1 0.319856 -0.055465 0.405807 11.00000 -1.20000 OW10 3 0.182282 0.778896 0.373163 11.00000 0.04627 0.03410 = 0.02626 0.00022 0.00729 0.00693 H10A 1 0.207509 0.704739 0.357645 11.00000 -1.20000 H10B 1 0.151354 0.835822 0.344265 11.00000 -1.20000 OW11 3 0.343007 0.468000 0.465030 11.00000 0.05352 0.03654 = 0.03747 -0.00049 0.00233 0.00872 H11A 1 0.345324 0.473176 0.431021 11.00000 -1.20000 H11B 1 0.370794 0.382618 0.481980 11.00000 -1.20000 HKLF 4 REM JM-13157 REM R1 = 0.0161 for 2040 Fo > 4sig(Fo) and 0.0169 for all 2110 data REM 149 parameters refined using 11 restraints END WGHT 0.0153 1.8979 REM Highest difference peak 0.913, deepest hole -0.671, 1-sigma level 0.106 Q1 1 0.0172 0.2084 0.2926 11.00000 0.05 0.91 Q2 1 0.0564 0.1349 0.2578 11.00000 0.05 0.55 Q3 1 0.2959 0.4502 0.3116 11.00000 0.05 0.47 Q4 1 -0.0568 0.2795 0.2494 11.00000 0.05 0.45 Q5 1 0.2027 0.2255 0.2393 11.00000 0.05 0.38 Q6 1 0.5000 0.3461 0.2500 10.50000 0.05 0.37 Q7 1 0.0824 0.2522 0.3261 11.00000 0.05 0.37 Q8 1 0.2409 0.2780 0.2742 11.00000 0.05 0.35 ; _shelx_res_checksum 87393 _shelx_hkl_file ; 1 -1 0 76.18 2.63 -1 -1 0 76.76 3.11 -1 1 0 92.68 3.83 1 1 0 80.60 2.96 -1 1 0 81.64 2.66 -1 -1 1 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18 22.50 17.49 1 -1 18 3.83 11.60 -5 -3 16 1418.96 40.40 -5 3 16 1425.98 48.57 5 -3 -16 1414.47 42.84 -4 6 -3 1833.74 51.45 4 -6 3 1746.09 57.04 4 6 3 1773.30 57.10 -1 5 13 18.42 12.22 -1 -5 13 35.64 14.70 -1 -5 13 17.14 3.96 1 5 -13 18.96 9.58 1 -5 -13 20.81 17.62 8 -4 -1 3064.12 93.90 8 4 -1 3165.60 95.68 -8 4 1 3227.96 117.28 -10 0 4 5238.56 106.01 10 0 -4 5175.57 147.60 9 -1 4 14.82 7.09 -9 -1 -4 34.75 5.87 -9 1 -4 14.84 7.46 9 -1 4 20.46 12.02 9 1 4 35.73 12.36 9 1 4 16.85 4.88 -7 -1 16 378.38 17.33 -7 1 16 399.28 19.24 7 -1 -16 362.82 14.67 7 1 -16 390.64 10.14 10 0 -5 14.36 10.12 -8 0 -8 2325.87 62.20 8 0 8 2229.74 59.20 8 0 8 2299.87 73.59 10 0 -3 26.96 16.02 -10 0 3 10.15 4.13 -9 3 4 3119.79 78.77 9 -3 -4 3186.05 95.43 9 3 -4 3146.33 88.43 -9 3 4 3184.82 97.48 5 -1 14 160.11 18.65 5 1 14 159.98 16.97 5 -1 14 162.63 14.80 -5 1 -14 164.69 18.33 5 1 14 178.45 17.76 9 -3 -3 1926.26 64.96 -9 3 3 2044.74 88.39 9 3 -3 1992.45 61.47 8 4 -6 309.77 17.65 -8 4 6 318.53 24.05 8 -4 -6 294.57 22.65 5 3 12 372.95 26.15 5 -3 12 327.08 27.61 -5 3 -12 335.81 24.05 5 -3 12 323.75 24.54 5 3 12 380.06 19.52 -2 -6 9 2300.63 57.92 2 -6 -9 2310.07 74.70 2 6 -9 2335.51 53.61 2 6 -9 2322.81 61.13 -2 -6 9 2311.75 53.84 -2 6 9 2425.70 74.38 0 6 9 725.37 34.75 0 6 -9 660.76 17.08 0 -6 -9 613.97 48.51 0 -6 9 669.38 23.41 0 -6 9 630.22 26.33 0 6 -9 618.82 38.05 4 -2 -18 2292.18 70.34 -4 2 18 2392.90 67.75 -4 -2 18 2315.11 68.88 0 2 18 1636.47 58.52 0 -2 18 1748.19 81.44 0 2 -18 1760.11 61.82 0 -2 18 1674.75 35.98 0 2 18 1748.06 52.10 0 -2 18 1677.72 31.59 9 3 -5 1966.39 56.69 -9 3 5 2082.40 68.50 9 -3 -5 2003.89 64.82 -3 -1 19 1352.11 62.19 -3 -1 19 1318.37 27.46 -3 1 19 1223.10 46.60 -3 1 19 1415.65 48.97 3 -1 -19 1326.29 32.97 -2 4 -14 94.93 24.16 2 4 14 92.30 16.93 2 -4 14 97.73 8.38 2 -4 14 106.26 16.57 10 0 -6 3261.18 92.15 -10 0 6 3299.49 68.16 4 4 -15 1554.25 45.84 -4 -4 15 1509.73 42.79 4 -4 -15 1516.89 48.78 -4 4 15 1570.62 70.39 -9 3 2 918.54 38.43 9 -3 -2 886.67 53.61 9 3 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26.89 10 0 -7 2.37 9.32 -10 0 7 14.12 3.76 8 4 -7 2440.11 62.36 8 -4 -7 2410.40 74.49 -8 4 7 2428.66 76.41 8 4 -7 2331.35 58.15 -9 3 1 1552.37 56.01 9 -3 -1 1487.10 54.56 0 0 19 3.83 7.38 0 0 19 -11.92 14.93 4 6 4 30.09 11.10 -4 6 -4 7.13 8.58 4 -6 4 13.16 10.16 9 -1 -12 271.95 16.03 -9 1 12 193.22 29.12 9 1 -12 278.56 13.05 -9 -1 12 284.10 14.25 -8 2 -7 674.31 28.27 8 -2 7 726.36 49.04 8 -2 7 703.42 39.61 8 2 7 721.64 28.58 10 0 -1 13.97 10.18 -10 0 1 2.62 4.39 -7 5 3 171.84 18.31 7 5 -3 102.68 14.58 7 -5 -3 136.62 28.36 2 -2 17 793.73 21.53 2 -2 17 837.20 57.33 2 -2 17 794.86 22.17 -2 2 -17 806.08 39.14 2 2 17 792.16 35.86 2 2 17 794.85 44.70 -8 0 15 18.65 6.54 -8 0 15 12.34 6.86 8 0 -15 -1.55 5.35 -7 5 2 3541.52 127.37 7 -5 -2 3531.94 105.69 7 5 -2 3535.65 100.13 7 5 -4 3054.42 82.25 7 -5 -4 3016.69 93.92 -7 5 4 3081.64 91.96 -3 3 -15 1515.79 57.70 3 3 15 1547.36 55.67 3 -3 15 1471.15 38.42 3 -3 15 1453.33 55.27 3 3 15 1515.01 49.93 -4 2 -15 528.39 29.46 4 -2 15 479.31 20.97 4 2 15 521.58 28.69 4 -2 15 479.79 30.17 4 2 15 558.80 26.91 4 -4 12 924.59 31.05 4 4 12 1018.61 45.02 4 -4 12 986.97 41.74 -4 4 -12 962.96 42.03 4 4 12 938.63 32.86 9 3 -7 1872.56 50.84 -9 3 7 2006.16 52.68 9 -3 -7 1926.53 82.35 -9 3 7 1898.55 64.47 7 3 -14 1236.28 23.97 -7 3 14 1270.64 45.37 7 3 -14 1232.46 19.37 -7 -3 14 1273.81 29.64 7 -3 -14 1293.07 53.70 -8 4 -1 2717.22 82.58 8 -4 1 2790.27 86.58 8 4 1 2871.08 90.97 -2 6 -8 329.53 21.34 2 6 8 316.71 26.52 2 -6 8 321.56 19.45 2 -6 8 432.42 24.30 -2 6 -8 376.27 24.01 -2 -6 -8 304.95 27.50 7 -5 -1 12.57 10.88 7 5 -1 7.02 2.09 7 5 -1 13.33 14.29 -7 5 1 6.97 10.21 7 5 -1 7.74 2.40 -2 4 16 130.68 18.25 2 -4 -16 186.59 25.45 2 4 -16 182.00 16.77 -2 -4 16 180.08 16.32 -6 0 -13 9.07 9.27 6 0 13 10.58 9.07 6 0 13 0.41 9.55 6 -2 12 1153.86 53.60 6 2 12 1169.75 38.28 6 -2 12 1056.43 59.79 6 2 12 1224.22 48.63 -6 2 -12 1051.62 42.02 -7 5 5 71.43 14.65 7 -5 -5 56.93 15.22 7 5 -5 44.27 10.26 10 0 -8 3984.96 107.00 -10 0 8 3915.33 75.84 -9 3 0 1089.85 34.06 -9 3 0 1131.66 45.51 9 -3 0 1042.92 44.51 4 0 16 2442.13 70.64 4 0 16 2399.08 76.00 -6 0 18 3062.20 84.25 6 0 -18 3177.42 72.41 -6 0 18 3154.76 72.09 6 -2 -17 282.06 14.83 -6 2 17 293.23 19.17 -6 -2 17 311.30 24.58 9 1 5 2861.64 71.62 -9 1 -5 2775.18 72.45 -9 -1 -5 2851.04 67.15 9 1 5 2869.04 116.54 9 -1 5 2941.10 114.71 9 -1 5 2847.23 84.40 2 0 18 767.81 26.63 2 0 18 786.29 55.21 -8 4 8 283.67 22.81 8 4 -8 265.44 21.86 8 -4 -8 279.03 21.26 8 4 -8 268.40 13.66 -10 0 0 5003.69 119.92 10 0 0 5014.22 177.80 4 6 -8 299.78 14.99 4 -6 -8 322.75 26.10 4 6 -8 348.36 11.93 -4 6 8 361.03 25.09 8 -2 -14 1616.16 46.34 8 2 -14 1662.22 33.22 -8 2 14 1760.56 71.36 -8 -2 14 1655.45 37.36 7 -5 0 1657.94 78.02 7 5 0 1573.67 27.77 7 5 0 1588.23 22.77 -7 5 0 1687.07 54.63 7 5 0 1723.92 71.96 3 -5 11 570.34 46.24 -3 5 -11 536.42 29.38 -3 5 -11 535.54 17.99 3 -5 11 559.93 22.87 3 5 11 552.57 33.93 2 -6 -10 49.61 19.55 -2 6 10 22.94 13.62 2 6 -10 28.65 4.34 -2 -6 10 35.28 8.99 -2 -6 10 24.04 8.92 2 6 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61.92 -1 -7 0 2273.01 74.02 1 7 0 2368.27 81.91 -9 3 -1 747.78 35.25 9 -3 1 683.84 51.82 -9 3 -1 696.41 27.14 1 -7 -1 403.21 28.24 -1 7 1 443.49 35.05 1 7 -1 460.69 22.33 1 7 -1 528.36 21.58 -1 -7 1 446.04 28.18 -10 0 9 2.90 5.75 10 0 -9 12.22 7.90 -8 0 -9 -6.03 11.46 8 0 9 2.03 10.77 8 0 9 -5.85 9.93 5 5 -12 1618.94 27.25 5 5 -12 1633.91 26.59 5 5 -12 1623.37 40.35 -5 -5 12 1686.50 38.10 5 -5 -12 1677.55 56.35 -5 5 12 1631.25 58.75 7 5 1 7.44 3.98 7 5 1 2.39 3.18 7 5 1 2.65 14.81 7 -5 1 -3.53 10.26 -7 5 -1 1.42 9.28 -1 -7 -1 96.19 15.68 -1 7 -1 87.97 18.99 1 -7 1 87.20 22.73 1 7 1 75.21 13.38 0 4 -16 1130.61 44.75 0 -4 16 1067.95 17.59 0 -4 16 1074.01 45.64 0 -4 16 1133.53 18.45 0 4 16 1184.54 45.03 0 -4 -16 1073.47 42.98 1 7 -2 1876.53 52.98 -1 -7 2 1900.17 63.39 -1 7 2 1941.76 57.94 1 -7 -2 1883.36 65.21 -1 -5 14 1895.96 29.39 -1 -5 14 1952.68 59.76 1 5 -14 2013.09 77.02 1 -5 -14 1950.37 65.35 -1 5 14 2079.62 68.35 10 0 1 11.38 10.01 -10 0 -1 -3.47 7.14 5 5 8 1418.28 56.47 -5 5 -8 1360.41 49.11 -5 5 -8 1392.47 40.09 5 -5 8 1404.25 51.71 5 -5 8 1339.82 61.70 9 -1 -13 1251.46 48.37 9 1 -13 1219.61 31.74 -9 1 13 1204.24 43.82 -9 -1 13 1285.38 29.46 -7 5 7 15.51 10.89 7 -5 -7 7.63 11.45 7 5 -7 4.23 9.75 8 4 -9 1436.72 37.78 8 4 -9 1433.66 35.50 8 -4 -9 1422.23 51.40 -8 4 9 1509.79 53.59 -7 -1 17 743.19 25.98 7 1 -17 708.24 18.68 -7 1 17 680.92 27.20 7 -1 -17 664.64 28.67 -5 3 17 516.13 27.21 5 -3 -17 450.27 31.49 -5 -3 17 510.11 22.61 6 4 9 1700.96 56.09 6 -4 9 1736.93 55.53 6 -4 9 1668.86 58.30 -6 4 -9 1692.04 57.89 6 4 9 1765.46 68.31 -6 4 14 242.15 20.36 -6 -4 14 208.98 11.10 6 -4 -14 224.84 18.39 -1 -7 -2 486.87 41.81 1 7 2 457.92 24.89 1 -7 2 457.52 26.36 -1 7 -2 485.85 22.00 3 -3 -18 563.25 35.54 -3 3 18 625.97 28.96 -3 -3 18 650.16 29.02 -1 3 18 856.55 35.49 -1 -3 18 875.31 38.94 1 3 -18 883.20 39.47 1 -3 -18 871.70 32.98 -1 3 18 815.46 42.08 -9 3 9 1821.56 62.54 9 3 -9 1788.76 46.12 9 -3 -9 1734.85 76.91 -1 -7 3 106.25 15.63 1 7 -3 90.20 12.06 -1 7 3 146.12 15.80 1 -7 -3 116.44 17.97 7 -3 9 1950.53 63.69 7 -3 9 1976.62 63.50 -7 3 -9 1954.17 63.15 7 3 9 1923.83 50.43 7 3 9 2156.03 76.31 -2 0 20 2290.45 96.10 -2 0 20 2276.56 55.64 -10 2 4 1540.44 58.26 10 -2 -4 1492.34 53.56 10 2 -4 1527.26 49.93 5 -1 -19 1549.81 45.69 5 1 -19 1540.29 23.77 -5 -1 19 1525.64 49.88 -5 1 19 1531.81 56.15 -5 1 19 1500.78 49.34 -5 -1 19 1520.13 27.95 10 2 -5 101.88 21.81 10 -2 -5 95.46 17.19 -10 2 5 133.19 18.69 5 -3 13 718.30 36.26 -5 3 -13 723.36 35.44 5 -3 13 684.94 38.64 5 3 13 751.72 38.00 5 3 13 713.49 42.05 8 -2 8 425.88 27.00 -8 2 -8 411.76 23.10 8 2 8 418.24 17.05 8 -2 8 431.70 22.22 10 -2 -3 214.58 21.90 -10 2 3 230.32 23.40 10 2 -3 215.19 19.29 4 6 -9 3756.19 87.98 4 -6 -9 3834.26 118.24 4 6 -9 3881.64 105.94 -4 6 9 3993.66 144.61 -2 -6 -9 4480.64 141.11 -2 6 -9 4318.37 102.16 -2 6 -9 4501.16 125.86 2 -6 9 4419.99 138.66 2 6 9 4587.58 140.36 2 -6 9 4392.03 149.05 4 -4 -16 1142.35 41.37 -4 -4 16 1179.55 50.42 4 4 -16 1196.50 51.10 -4 4 16 1169.47 62.33 -3 5 14 2507.13 104.30 3 -5 -14 2533.99 99.60 -3 -5 14 2396.28 65.65 3 5 -14 2474.13 70.11 10 2 -6 2398.04 69.81 -10 2 6 2423.59 100.92 -10 2 6 2387.93 56.80 10 -2 -6 2484.48 94.89 9 -3 2 351.49 25.74 -9 3 -2 296.30 25.75 -9 3 -2 387.90 28.72 7 5 2 2096.69 39.53 7 -5 2 2242.15 72.10 7 5 2 2241.83 95.21 -7 5 -2 2184.73 67.74 2 4 15 1483.44 51.84 2 -4 15 1524.46 36.45 -2 4 -15 1445.45 54.84 2 -4 15 1443.99 56.90 2 4 15 1545.67 57.36 -8 4 -3 2054.01 61.57 8 4 3 2194.65 99.12 8 4 3 2005.87 34.62 8 -4 3 2059.07 68.81 -8 4 -3 2035.64 65.44 -10 0 10 1867.15 42.80 10 0 -10 1886.29 54.13 8 0 -16 4329.71 99.98 -8 0 16 4366.56 110.56 -8 0 16 4308.89 109.17 10 2 -2 1942.73 80.83 -10 2 2 1887.33 47.52 10 -2 -2 1922.06 64.77 5 1 15 2181.95 69.22 5 -1 15 2116.24 72.48 -5 1 -15 2192.34 73.59 5 1 15 2213.10 70.09 5 -1 15 2107.09 63.97 9 1 6 113.16 30.50 9 1 6 110.12 9.13 9 -1 6 80.08 12.05 9 -1 6 103.63 18.71 -9 1 -6 93.84 18.44 -9 -1 -6 136.88 10.67 1 7 3 305.99 17.35 -1 -7 -3 323.73 25.12 -1 7 -3 303.51 25.80 1 7 3 275.55 21.31 1 -7 3 304.49 21.75 -7 3 15 1509.08 51.32 7 -3 -15 1367.35 44.85 7 3 -15 1348.51 18.84 -7 -3 15 1445.44 35.25 7 3 -15 1431.13 20.57 4 -2 -19 1442.32 40.41 -4 2 19 1544.07 48.35 -4 -2 19 1491.39 51.06 -4 6 -6 65.77 11.05 4 6 6 81.43 16.12 4 -6 6 76.17 13.32 1 -1 19 2684.50 63.44 1 1 19 2643.88 87.02 1 1 19 2604.64 90.81 1 -1 19 2697.34 112.91 1 7 -4 3415.56 100.93 -1 -7 4 3331.21 101.74 -1 7 4 3377.83 97.99 1 -7 -4 3334.81 129.83 1 7 -4 3424.19 88.78 -7 5 8 1772.36 83.73 7 5 -8 1746.69 43.77 7 -5 -8 1781.83 61.16 10 0 2 3258.63 104.24 -10 0 -2 3239.06 73.42 -10 2 7 281.14 14.06 10 -2 -7 267.70 22.03 -10 2 7 251.40 23.57 10 2 -7 235.43 25.94 2 6 -11 3294.78 107.49 2 6 -11 3359.29 68.67 -2 -6 11 3346.64 70.64 -2 6 11 3357.38 107.27 2 -6 -11 3246.79 103.26 -2 -6 11 3202.89 85.13 0 -2 19 178.37 10.31 0 -2 19 175.39 31.86 0 2 19 133.65 24.69 0 -2 19 174.27 10.06 0 2 19 185.94 21.97 0 2 -19 217.83 22.76 -3 1 20 38.19 13.13 -3 -1 20 44.07 13.06 -3 1 20 45.91 13.87 -3 -1 20 31.40 5.73 3 -1 -20 53.88 11.01 -8 4 10 30.69 20.39 8 -4 -10 37.84 18.57 8 4 -10 27.72 5.83 8 4 -10 24.75 6.73 10 -2 -1 34.19 15.32 10 2 -1 35.13 13.99 -10 2 1 57.78 8.58 -4 4 -13 1168.69 47.45 4 -4 13 1145.42 36.78 4 4 13 1181.09 39.75 4 4 13 1201.75 50.21 4 -4 13 1180.57 48.44 8 2 -15 301.01 13.19 -8 -2 15 337.25 19.57 8 -2 -15 341.17 26.17 -8 2 15 297.88 22.18 -9 3 10 932.11 40.67 9 -3 -10 926.74 37.57 9 3 -10 910.75 26.11 4 0 -20 1284.81 27.75 -4 0 20 1319.33 33.89 -4 0 20 1196.40 46.52 0 -6 11 863.73 33.99 0 -6 11 915.47 35.74 0 -6 -11 905.09 41.66 0 6 11 894.95 44.27 0 6 -11 877.07 34.38 0 6 -11 843.38 19.45 1 7 4 892.55 51.64 1 -7 4 799.53 35.28 -1 7 -4 852.83 32.28 -1 7 -4 844.38 28.27 -1 -7 -4 814.10 39.75 -1 -1 20 209.14 35.41 -1 -1 20 232.53 9.85 -1 1 20 271.79 14.88 -1 1 20 209.81 23.55 1 -7 -5 58.53 16.87 1 7 -5 57.23 9.68 -1 7 5 85.51 14.77 -1 -7 5 84.86 13.49 6 -2 13 691.66 35.38 -6 2 -13 745.90 36.07 6 -2 13 744.25 32.42 6 2 13 812.68 56.10 6 2 13 802.37 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875.58 39.87 -11 -1 8 16.35 2.50 11 1 -8 18.17 15.54 11 -1 -8 16.67 11.44 -11 -1 8 14.87 1.76 0 -4 -18 414.90 26.69 0 -4 18 419.97 29.92 0 4 -18 384.82 29.19 0 4 18 501.82 43.57 -11 -1 1 1690.14 36.16 11 1 -1 1739.62 64.38 11 -1 -1 1745.36 90.28 -11 1 1 1682.39 41.92 1 7 8 1803.65 68.00 -1 -7 -8 1717.23 95.35 -1 7 -8 1714.50 77.34 1 -7 8 1668.84 72.36 -1 7 -8 1724.17 44.86 5 3 15 411.89 33.08 5 -3 15 500.24 33.73 5 3 15 466.93 26.57 5 -3 15 500.09 23.64 -5 3 -15 463.87 33.31 -9 3 -6 244.14 20.61 9 -3 6 301.37 20.74 9 -3 6 262.88 38.60 9 3 6 327.23 29.48 9 3 6 260.65 10.97 2 0 20 1429.22 45.05 2 0 20 1569.19 62.95 10 2 4 1101.43 51.66 -10 2 -4 1082.43 35.86 10 2 4 1022.36 22.26 10 -2 4 1007.56 71.24 5 -5 11 11.68 9.89 5 5 11 8.25 13.17 5 -5 11 17.97 13.03 -5 5 -11 17.68 13.55 5 5 11 9.58 21.78 1 3 19 481.36 32.33 1 -3 19 513.82 19.17 1 -3 19 484.16 13.43 -1 3 -19 516.77 34.72 1 -3 19 576.44 52.11 1 3 19 500.19 29.28 3 -1 19 768.70 27.61 3 1 19 791.84 41.88 3 -1 19 769.56 28.67 3 1 19 796.82 34.46 3 -1 19 821.17 43.40 -1 7 9 35.25 15.91 1 7 -9 40.25 6.85 -1 -7 9 44.77 9.96 1 7 -9 50.97 19.55 1 -7 -9 53.70 16.82 3 7 -8 1061.69 46.20 -3 7 8 1004.11 47.09 3 -7 -8 996.40 49.07 3 7 -8 1053.08 35.93 -3 -7 8 1101.54 34.62 10 0 -14 878.58 28.65 -2 2 21 164.58 23.88 -2 -2 21 231.38 23.05 -2 2 21 187.53 16.99 2 -2 -21 200.25 14.77 -2 -6 -12 131.52 32.50 2 6 12 106.42 21.06 2 -6 12 102.30 13.39 -2 6 -12 108.06 18.20 -2 6 -12 103.42 8.83 2 -6 12 109.12 29.19 3 -3 -20 1111.14 53.35 -3 3 20 1136.28 44.30 -3 -3 20 1111.62 46.70 -8 4 -7 1900.36 63.66 8 -4 7 1897.36 69.31 8 4 7 1864.52 45.66 8 -4 7 1845.53 63.57 8 4 7 1928.15 79.42 2 4 17 1488.05 74.80 2 4 17 1416.38 79.31 2 -4 17 1417.81 35.39 2 -4 17 1410.56 83.68 -2 4 -17 1391.35 58.75 -11 -1 9 1755.58 30.55 -11 -1 9 1706.21 27.35 11 -1 -9 1892.56 77.56 11 1 -9 1807.72 56.00 -3 5 -14 1326.75 56.72 3 -5 14 1469.38 54.53 3 -5 14 1399.07 58.61 3 5 14 1466.65 61.71 -11 1 0 55.81 8.52 11 1 0 53.88 16.31 -11 -1 0 45.97 7.78 11 -1 0 46.36 17.33 9 1 9 2409.20 89.80 9 -1 9 2389.41 86.87 9 1 9 2298.11 63.73 -9 1 -9 2465.42 73.54 9 -1 9 2322.59 87.20 10 0 6 1141.55 33.27 10 0 6 1083.76 54.50 -10 0 -6 1143.87 35.69 -5 1 21 1240.20 53.47 -5 -1 21 1277.65 47.34 5 -1 -21 1212.68 32.57 -5 1 21 1236.33 48.49 4 4 15 625.42 30.90 4 -4 15 624.70 25.64 4 4 15 631.33 56.22 -4 4 -15 659.42 37.99 4 -4 15 645.61 56.44 6 -6 5 1940.93 68.18 6 6 5 1897.05 72.62 -6 6 -5 1955.33 61.14 -6 6 -5 2032.53 69.68 1 3 -20 1312.76 55.52 1 -3 -20 1248.89 44.68 -1 3 20 1309.78 57.01 -1 -3 20 1240.68 54.84 -1 3 20 1311.77 67.42 -3 -7 -6 961.37 70.17 -3 7 -6 959.45 33.09 3 7 6 973.69 46.40 -3 7 -6 986.33 58.77 3 -7 6 956.09 40.58 6 -6 -10 36.34 15.06 6 6 -10 35.53 6.47 6 6 -10 27.63 5.67 -6 6 10 40.00 15.37 -6 4 -12 793.50 58.72 6 -4 12 700.11 47.63 6 4 12 764.43 44.88 6 -4 12 761.97 40.74 6 4 12 743.46 30.40 -4 6 13 1607.10 65.06 4 6 -13 1602.12 47.31 -4 -6 13 1566.29 43.68 4 -6 -13 1594.85 85.46 5 1 17 1488.57 57.25 5 -1 17 1518.68 50.98 5 -1 17 1423.99 59.96 -5 1 -17 1535.80 60.55 5 1 17 1567.47 79.61 5 -1 17 1478.21 49.44 -6 -4 17 870.94 29.88 -6 4 17 941.88 42.99 6 -4 -17 867.65 36.96 8 0 12 3075.54 102.82 -8 0 -12 3077.52 94.45 8 0 12 2978.38 90.12 9 3 -14 397.79 12.81 -9 3 14 460.36 42.29 -9 -3 14 368.51 9.82 9 -3 -14 453.20 24.86 5 -7 -2 493.42 34.60 5 7 -2 518.65 26.35 5 7 -2 562.47 17.15 -5 7 2 561.77 31.76 7 5 7 141.06 22.80 -7 5 -7 110.68 20.36 -7 5 -7 139.35 16.98 7 5 7 140.35 10.30 7 -5 7 87.75 18.74 7 -5 7 113.59 19.93 -8 2 -11 128.21 17.32 8 2 11 162.75 21.25 8 2 11 148.88 23.31 8 -2 11 98.99 17.44 8 -2 11 117.62 19.35 5 -7 -3 662.77 39.33 5 7 -3 686.09 20.10 -5 7 3 703.57 52.16 5 7 -3 674.20 28.53 5 7 -1 422.66 14.91 5 -7 -1 369.35 29.98 -5 7 1 400.74 27.31 5 7 -1 410.66 35.60 2 6 -14 11.24 11.16 2 -6 -14 11.75 14.36 -2 -6 14 22.74 10.92 -2 6 14 43.07 14.94 10 -2 -13 1132.61 40.79 -10 -2 13 1031.21 23.55 10 2 -13 1133.89 31.44 -10 2 13 1181.17 49.36 8 4 -14 28.63 3.93 8 4 -14 30.39 6.22 -8 4 14 43.15 14.23 -8 -4 14 27.90 4.58 8 -4 -14 24.58 19.02 -4 -2 21 605.50 34.18 4 -2 -21 614.50 33.51 -4 2 21 664.24 30.78 -4 2 21 634.97 35.16 7 3 12 2101.42 81.98 7 3 12 1980.81 59.13 7 -3 12 1952.94 88.11 -7 3 -12 1878.51 92.26 7 -3 12 1983.28 94.60 6 2 15 652.38 39.01 -6 2 -15 652.80 37.41 6 -2 15 665.79 31.02 6 -2 15 639.97 37.68 6 2 15 663.82 32.99 -1 5 -16 1300.61 52.15 -1 -5 -16 1234.45 53.67 1 -5 16 1288.01 52.77 1 -5 16 1229.06 30.45 1 5 16 1296.97 57.62 -2 0 22 945.43 45.48 -2 0 22 920.94 37.05 -11 -1 10 7.54 2.16 11 1 -10 10.59 8.55 -11 -1 10 11.21 4.18 11 -1 -10 9.38 9.93 5 7 -4 1278.86 31.02 5 -7 -4 1192.06 77.69 -5 7 4 1295.84 52.08 5 7 -4 1294.82 53.37 -3 7 9 332.56 29.14 -3 -7 9 364.08 16.91 3 -7 -9 366.41 30.01 3 7 -9 322.31 18.43 3 7 -9 308.73 19.53 1 7 9 360.41 32.12 -1 7 -9 472.03 27.97 1 -7 9 399.67 35.35 -1 7 -9 370.70 16.26 -1 -7 -9 438.36 33.82 -5 7 0 1321.38 67.24 5 7 0 1289.80 30.79 5 -7 0 1245.36 75.68 5 7 0 1242.24 47.66 11 -1 1 856.45 45.94 11 1 1 853.63 63.14 -11 1 -1 883.24 26.89 -11 -1 -1 827.66 20.48 6 -2 -20 609.48 23.33 -6 2 20 608.34 30.04 -6 -2 20 620.56 29.57 7 -5 -13 128.17 30.02 7 5 -13 133.35 7.67 7 5 -13 145.25 5.65 -7 5 13 197.21 21.60 -7 -5 13 157.36 11.18 4 -6 10 37.76 20.44 -4 6 -10 31.12 12.27 4 -6 10 0.58 9.68 -4 6 -10 7.09 7.53 4 6 10 18.36 14.48 7 1 14 529.53 29.83 7 1 14 572.66 35.95 -7 1 -14 568.62 32.90 7 -1 14 604.21 32.72 7 -1 14 553.57 31.69 10 2 5 495.47 15.07 10 -2 5 512.11 36.23 10 2 5 522.05 37.96 -10 2 -5 537.82 25.36 10 -2 5 555.76 25.49 2 -4 -19 889.97 39.41 -2 -4 19 874.57 41.26 -2 4 19 913.43 43.07 2 4 -19 946.21 42.53 -1 7 10 1884.08 96.73 1 7 -10 1918.01 59.02 1 7 -10 1821.05 50.22 1 -7 -10 1901.91 74.51 -1 -7 10 1821.62 65.09 9 3 7 828.21 23.33 -9 3 -7 877.37 51.39 9 3 7 1003.35 73.96 9 -3 7 844.83 36.22 9 -3 7 859.30 43.64 6 0 16 1612.89 81.89 6 0 16 1584.71 58.43 6 0 16 1665.68 60.36 -5 7 5 495.26 30.95 5 7 -5 502.70 21.62 5 -7 -5 437.80 34.95 -1 -5 17 82.56 17.00 1 -5 -17 84.54 18.00 1 5 -17 82.40 17.31 -1 5 17 123.74 19.33 5 -7 1 488.38 33.28 -5 7 -1 552.55 29.91 5 7 1 511.19 17.02 5 7 1 526.48 30.35 0 -6 14 11.55 11.30 0 6 14 18.28 13.96 0 6 -14 6.40 17.63 0 -6 -14 11.45 13.64 0 -6 14 12.95 5.11 -7 3 18 953.73 42.30 -7 -3 18 976.37 32.38 7 -3 -18 905.02 35.11 -9 1 17 2003.78 64.88 -9 -1 17 2037.00 55.34 9 -1 -17 2139.58 68.34 9 1 -17 1992.96 53.96 1 -1 21 1499.41 38.86 1 -1 21 1536.75 40.80 1 1 21 1614.14 50.67 1 1 21 1569.70 67.61 1 -1 21 1588.59 66.06 3 5 -17 129.33 16.39 -3 -5 17 89.26 15.74 -3 5 17 116.63 20.29 3 -5 -17 118.80 18.20 3 3 18 586.55 34.43 3 3 18 579.64 34.53 3 -3 18 591.11 21.75 3 -3 18 606.14 39.80 -3 3 -18 573.69 39.93 -6 0 21 -3.39 7.43 6 0 -21 0.36 3.46 -6 0 21 0.59 8.32 10 0 -15 -2.00 9.47 -10 0 15 -1.90 5.70 -3 -1 22 10.91 3.14 -3 1 22 21.23 8.20 -3 -1 22 17.65 12.17 -3 1 22 23.39 12.58 -4 0 22 789.57 33.90 -4 0 22 767.57 38.30 -3 7 -7 36.85 14.73 3 -7 7 50.67 13.37 3 7 7 57.28 16.36 -3 7 -7 40.77 9.94 -3 -7 -7 28.21 17.45 0 -2 21 164.37 7.15 0 2 21 163.08 23.89 0 -2 21 145.61 23.16 0 2 21 151.68 16.89 0 -2 21 161.30 7.52 -6 6 -6 19.29 10.61 6 -6 6 10.53 12.34 6 6 6 16.13 14.56 8 -2 -18 1009.85 43.96 8 2 -18 921.05 16.73 -8 -2 18 1034.24 32.70 -8 2 18 1077.95 42.72 -8 0 19 -6.37 7.67 -8 0 19 -2.36 10.08 8 0 -19 10.38 4.75 5 -5 -16 1175.65 65.90 -5 5 16 1214.27 54.20 -5 -5 16 1265.43 37.85 5 5 -16 1186.22 52.66 6 -6 -11 942.36 44.55 -6 6 11 947.43 67.54 6 6 -11 884.90 21.04 6 6 -11 935.82 33.80 4 2 18 1804.99 87.05 4 -2 18 1632.55 50.37 -4 2 -18 1797.09 74.01 4 2 18 1840.24 65.81 4 -2 18 1721.44 95.72 4 -2 18 1837.80 52.62 -7 1 20 65.74 14.03 7 -1 -20 77.12 8.97 -7 1 20 94.25 13.18 -7 -1 20 102.04 13.12 10 4 -4 161.55 33.06 -10 4 4 231.93 24.75 10 -4 -4 251.50 25.70 10 4 -4 198.67 19.88 10 4 -5 869.33 36.52 10 4 -5 852.60 55.45 10 -4 -5 900.69 45.01 -10 4 5 957.05 45.35 8 -4 8 453.84 31.65 8 4 8 490.75 37.98 -8 4 -8 447.49 30.18 8 4 8 463.86 18.24 8 -4 8 427.60 30.35 10 -4 -3 1156.83 54.02 10 4 -3 1186.55 69.92 -10 4 3 1213.44 74.86 10 4 -3 1123.83 45.81 9 -5 -4 1146.47 52.90 9 5 -4 1078.29 43.05 -9 5 4 1175.83 52.62 -9 5 3 57.66 17.94 9 -5 -3 83.69 27.75 9 5 -3 46.56 22.71 -5 7 6 474.88 48.16 5 -7 -6 492.16 34.97 5 7 -6 474.05 20.11 11 -1 -11 2484.24 93.48 -11 1 11 2540.18 84.73 11 1 -11 2378.48 68.00 -11 1 11 2518.20 56.59 -11 -1 11 2294.19 43.59 -11 -1 11 2288.20 44.46 -5 5 -12 1261.73 54.29 5 -5 12 1193.08 45.07 5 5 12 1224.00 42.26 5 -5 12 1235.82 56.33 5 5 12 1298.17 81.08 10 0 7 13.89 13.54 -10 0 -7 -3.57 12.33 10 0 7 13.30 11.02 -11 1 -2 344.76 16.89 -11 -1 -2 349.57 13.19 11 1 2 287.61 29.90 11 -1 2 341.28 32.18 -5 7 -2 620.27 45.26 5 7 2 650.32 33.31 5 -7 2 576.07 36.16 5 7 2 587.83 18.93 9 -5 -5 269.65 26.52 9 5 -5 196.85 19.60 -9 5 5 263.44 26.84 10 -4 -6 68.02 16.16 10 4 -6 44.53 11.70 10 4 -6 18.78 20.46 -10 4 6 51.18 26.42 -1 -1 22 670.47 19.79 -1 1 22 748.89 42.08 -1 -1 22 728.61 41.00 -1 1 22 758.70 38.47 -9 5 2 2222.37 80.10 9 5 -2 2222.14 99.79 9 -5 -2 2317.47 82.15 -10 4 2 17.08 14.32 10 -4 -2 38.03 15.06 -10 4 2 17.15 10.52 10 4 -2 5.89 21.09 -2 2 -20 434.49 36.67 2 -2 20 405.40 52.12 2 2 20 443.88 39.09 2 -2 20 430.48 17.33 2 -2 20 426.03 16.69 2 2 20 468.91 50.08 -5 -3 20 875.58 36.91 -5 3 20 916.31 41.11 5 -3 -20 838.40 32.45 2 6 13 2615.50 95.65 -2 6 -13 2568.62 86.00 2 -6 13 2621.38 87.31 2 -6 13 2681.94 75.15 -2 6 -13 2455.17 57.84 -2 -6 -13 2607.73 96.18 -4 -4 19 966.35 40.42 -4 4 19 1054.15 46.93 4 -4 -19 983.47 40.73 10 2 -14 1924.59 57.27 10 -2 -14 1875.38 59.32 -10 2 14 2061.72 71.90 -10 -2 14 1821.96 37.58 9 -5 -6 1782.86 94.08 9 5 -6 1733.74 56.13 -9 5 6 1828.93 71.04 3 7 -10 399.36 18.46 3 7 -10 387.18 20.85 3 -7 -10 415.08 32.55 -3 7 10 393.96 48.74 7 5 8 1223.28 35.91 -7 5 -8 1255.45 46.20 -7 5 -8 1291.35 53.21 7 -5 8 1271.45 53.62 7 5 8 1329.11 62.72 7 -5 8 1307.92 51.93 9 1 10 308.03 30.28 9 -1 10 291.53 22.08 -9 1 -10 298.66 32.86 9 1 10 296.04 18.83 9 -1 10 327.19 28.15 -9 3 15 774.73 54.16 9 3 -15 700.66 16.46 -9 -3 15 637.59 17.12 9 -3 -15 723.75 44.97 -10 4 7 1220.68 56.10 -10 4 7 1228.87 42.73 10 4 -7 1144.87 59.58 10 -4 -7 1203.01 73.62 10 4 -7 1162.26 39.51 9 -5 -1 84.87 20.47 9 5 -1 86.74 27.40 -9 5 1 94.27 19.09 -4 -6 14 9.72 11.43 4 6 -14 5.63 8.12 -4 6 14 -1.55 12.80 4 -6 -14 5.74 11.74 5 -3 16 1022.93 70.19 5 3 16 1033.51 48.33 5 3 16 981.25 41.10 -5 3 -16 964.20 49.73 5 -3 16 932.72 35.89 0 4 19 1002.90 44.87 0 4 -19 972.00 47.17 0 -4 -19 907.44 42.38 0 -4 19 859.59 47.36 0 4 19 1007.98 49.09 4 0 19 21.87 14.32 4 0 19 -5.68 12.88 10 4 -1 925.80 67.60 -10 4 1 976.80 47.56 10 -4 -1 954.31 70.84 -8 4 15 1856.65 93.80 8 4 -15 1680.85 31.15 -8 -4 15 1730.10 37.84 8 -4 -15 1842.27 60.81 8 4 -15 1753.00 32.73 1 7 10 1032.42 52.08 1 -7 10 974.99 53.14 -1 7 -10 961.39 36.28 -1 7 -10 1019.12 41.72 -1 -7 -10 965.09 52.50 -5 7 7 367.82 30.32 5 7 -7 343.90 17.01 5 -7 -7 345.67 30.52 0 0 22 1590.71 66.87 0 0 22 1574.24 56.86 10 -2 6 1850.36 72.01 -10 2 -6 1856.56 73.53 10 -2 6 1862.72 73.62 10 2 6 1913.31 75.91 10 2 6 1723.09 41.87 3 5 15 580.53 39.84 3 -5 15 605.45 57.18 3 -5 15 572.49 32.74 -3 5 -15 528.82 36.30 3 5 15 580.37 30.68 -5 7 -3 378.81 24.39 5 -7 3 392.83 29.61 5 7 3 371.24 15.51 5 7 3 389.40 28.63 0 -8 0 48.06 27.49 0 8 0 83.34 21.43 -9 5 7 339.62 29.25 9 -5 -7 284.57 27.13 9 5 -7 245.52 18.70 -7 5 14 1979.46 73.48 -7 -5 14 1756.65 47.41 7 -5 -14 1922.28 67.07 0 8 1 1809.15 61.27 0 -8 -1 1754.94 69.96 0 -8 1 1759.11 92.51 0 8 -1 1779.20 57.11 -1 7 11 61.30 30.82 1 -7 -11 110.92 19.99 1 7 -11 65.58 10.47 1 7 -11 80.43 14.92 -1 -7 11 74.61 14.70 6 4 13 1255.77 60.87 6 4 13 1312.30 61.58 -6 4 -13 1339.31 56.07 6 -4 13 1278.14 57.35 6 -4 13 1295.37 63.88 2 -6 -15 3185.68 106.60 -2 6 15 3157.97 112.29 -2 -6 15 3084.18 115.97 2 6 -15 3213.99 96.92 10 -4 -8 746.26 41.24 10 4 -8 677.61 44.72 -10 4 8 752.06 43.02 10 4 -8 736.41 27.88 9 -5 0 929.00 48.91 -9 5 0 966.44 46.97 9 5 0 975.06 64.76 1 -3 20 661.77 57.92 1 -3 20 569.06 15.03 1 -3 20 578.53 21.01 1 3 20 589.70 32.59 -1 3 -20 624.33 39.91 1 3 20 601.19 37.96 3 -7 8 1602.39 57.80 -3 7 -8 1575.12 59.76 -3 -7 -8 1571.26 70.13 -3 7 -8 1612.68 46.72 3 7 8 1670.79 68.47 -11 1 12 58.68 8.04 -11 1 12 76.26 15.84 -11 -1 12 38.02 6.04 -11 -1 12 43.28 8.06 11 -1 -12 49.42 13.10 11 1 -12 70.18 10.78 4 -4 16 223.01 26.62 4 4 16 198.77 20.30 4 -4 16 188.35 15.22 4 4 16 205.08 25.38 -4 4 -16 201.47 26.17 -6 4 18 46.13 15.43 -6 -4 18 52.54 15.94 6 -4 -18 33.18 12.97 4 -6 11 1264.13 46.24 4 -6 11 1260.39 54.39 4 6 11 1335.69 61.77 -4 6 -11 1271.23 53.23 -4 6 -11 1265.11 49.76 0 -8 -2 695.73 40.23 0 8 2 653.44 34.29 0 -8 2 633.82 37.55 0 8 -2 655.42 30.19 6 6 7 2251.00 58.79 -6 6 -7 2284.08 69.92 6 -6 7 2384.76 80.42 -6 6 -7 2431.66 83.13 6 6 7 2363.92 89.39 8 -2 12 566.95 34.77 8 -2 12 577.38 32.96 8 2 12 607.19 60.96 -8 2 -12 619.87 33.26 8 2 12 568.84 27.25 2 -4 18 160.94 23.79 2 4 18 155.77 21.91 2 4 18 120.56 21.42 2 -4 18 147.29 10.15 -2 4 -18 162.28 22.75 -11 -1 -3 930.93 26.23 -11 1 -3 1073.07 33.10 11 1 3 1076.51 52.36 11 -1 3 1176.49 76.92 10 4 0 203.44 24.85 -10 4 0 182.41 38.63 10 -4 0 217.30 25.96 9 -3 8 1096.48 44.18 9 3 8 1056.16 41.12 -9 3 -8 1091.24 44.49 9 -3 8 1113.17 51.54 9 3 8 1154.79 60.03 3 -1 20 27.34 16.36 3 -1 20 38.31 13.75 3 1 20 32.60 15.80 3 -1 20 30.03 9.22 3 1 20 26.83 11.43 2 0 21 -2.35 6.52 2 0 21 6.23 11.29 -6 6 12 89.82 19.90 6 -6 -12 101.74 29.42 6 6 -12 81.98 8.04 6 6 -12 89.18 9.60 -3 3 21 325.50 24.25 3 -3 -21 311.66 20.52 -3 -3 21 335.15 25.88 -3 3 21 337.28 29.30 8 0 13 -10.11 15.41 8 0 13 -14.54 11.55 -8 0 -13 4.23 10.38 -2 2 22 860.59 35.13 -2 2 22 777.02 43.68 -2 -2 22 845.54 44.01 7 -3 13 628.22 38.51 7 3 13 715.97 30.78 7 3 13 740.25 45.48 7 -3 13 676.03 49.42 -7 3 -13 629.78 38.53 -10 0 16 2071.22 54.55 10 0 -16 2035.93 53.41 9 5 -8 714.83 27.43 9 -5 -8 708.83 40.58 9 5 -8 681.63 26.76 -9 5 8 772.23 63.11 -5 1 22 237.29 25.09 -5 1 22 182.01 34.28 -5 -1 22 156.51 32.86 5 -1 -22 233.84 12.85 11 3 -5 819.98 37.90 11 -3 -5 887.34 44.51 -11 3 5 890.76 70.60 11 -3 -4 1665.35 65.74 -11 3 4 1694.12 71.06 11 3 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19.47 5 -1 18 207.18 18.46 5 1 18 221.39 34.00 0 6 15 775.93 43.13 0 -6 15 643.73 52.54 0 -6 -15 646.82 41.74 0 6 -15 677.50 35.58 0 -6 15 649.53 22.36 6 -2 16 581.37 37.71 6 2 16 623.30 55.58 -6 2 -16 549.73 38.31 6 2 16 589.20 32.98 6 -2 16 603.34 29.85 -8 6 3 1133.39 51.71 8 -6 -3 1118.42 53.89 8 6 -3 1119.80 43.74 3 7 -11 423.41 31.92 3 7 -11 354.85 16.31 -3 7 11 436.58 48.66 3 -7 -11 378.52 32.74 -8 6 4 110.70 21.72 8 6 -4 119.24 15.53 8 -6 -4 123.43 34.72 10 0 8 1588.08 48.19 -10 0 -8 1713.88 52.55 10 0 8 1778.47 71.80 10 4 1 924.14 48.98 -10 4 -1 919.66 48.14 10 -4 1 928.98 49.48 2 -8 -1 686.30 60.70 -2 8 1 758.18 35.72 2 8 -1 747.54 32.99 -2 -8 1 702.05 42.47 7 -1 15 749.11 37.59 7 -1 15 713.06 57.29 7 1 15 748.31 36.92 -7 1 -15 717.10 40.39 7 1 15 778.35 43.34 8 6 -2 75.08 15.75 8 -6 -2 85.36 20.48 -8 6 2 84.26 18.23 11 -3 -7 533.01 34.38 11 3 -7 469.45 26.62 -11 3 7 537.38 23.50 -11 3 7 526.45 36.22 2 8 0 552.72 29.79 -2 -8 0 567.19 38.08 -2 8 0 609.30 44.74 2 -8 0 559.67 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