data_acmonidesite _audit_creation_method 'SHELXL-2017/1' _shelx_SHELXL_version_number '2017/1' _chemical_name_systematic ? _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Cl8 H23.08 Fe4 K1.23 N5.77 Na1.37 O20 Pb0.63 S5' _chemical_formula_weight 1301.98 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0110 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na' 'Na' 0.0360 0.0250 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1250 0.1230 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cl' 'Cl' 0.1480 0.1590 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2010 0.2490 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Fe' 'Fe' 0.3460 0.8440 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'N' 'N' 0.0060 0.0030 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3940 10.1110 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'H' 'H' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system orthorhombic _space_group_IT_number 20 _space_group_name_H-M_alt 'C 2 2 21' _space_group_name_Hall 'C 2c 2' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z+1/2' 'x, -y, -z' '-x, y, -z+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z+1/2' 'x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z+1/2' _cell_length_a 9.8413(14) _cell_length_b 19.448(3) _cell_length_c 17.847(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 3415.7(9) _cell_formula_units_Z 4 _cell_measurement_temperature 294(2) _cell_measurement_reflns_used 8096 _cell_measurement_theta_min 2.28 _cell_measurement_theta_max 30.88 _exptl_crystal_description prism _exptl_crystal_colour brown _exptl_crystal_density_meas 2.56(1) _exptl_crystal_density_method flotation _exptl_crystal_density_diffrn 2.551 _exptl_crystal_F_000 2535 _exptl_transmission_factor_min 0.662 _exptl_transmission_factor_max 1.000 _exptl_crystal_size_max 0.08 _exptl_crystal_size_mid 0.04 _exptl_crystal_size_min 0.03 _exptl_absorpt_coefficient_mu 5.946 _shelx_estimated_absorpt_T_min ? _shelx_estimated_absorpt_T_max ? _exptl_absorpt_correction_type empirical _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details SADABS _exptl_absorpt_special_details ? _diffrn_ambient_temperature 294(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source ? _diffrn_measurement_device_type 'APEX II CCD diffractometer' _diffrn_measurement_method 'omega scan' _diffrn_detector_area_resol_mean ? _diffrn_reflns_number 17663 _diffrn_reflns_av_unetI/netI 0.0424 _diffrn_reflns_av_R_equivalents 0.0501 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_k_max 27 _diffrn_reflns_limit_l_min -26 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_theta_min 2.094 _diffrn_reflns_theta_max 31.515 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.957 _diffrn_measured_fraction_theta_full 0.999 _diffrn_reflns_Laue_measured_fraction_max 0.957 _diffrn_reflns_Laue_measured_fraction_full 0.999 _diffrn_reflns_point_group_measured_fraction_max 0.957 _diffrn_reflns_point_group_measured_fraction_full 1.000 _reflns_number_total 5336 _reflns_number_gt 4614 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.811 _reflns_Friedel_fraction_max 0.957 _reflns_Friedel_fraction_full 1.000 _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2017/1 (Sheldrick, 2017)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refined as a 2-component inversion twin. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0563P)^2^] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_abs_structure_details ; Refined as an inversion twin. ; _refine_ls_abs_structure_Flack 0.228(8) _chemical_absolute_configuration ? _refine_ls_number_reflns 5336 _refine_ls_number_parameters 214 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0476 _refine_ls_R_factor_gt 0.0363 _refine_ls_wR_factor_ref 0.0945 _refine_ls_wR_factor_gt 0.0907 _refine_ls_goodness_of_fit_ref 1.037 _refine_ls_restrained_S_all 1.037 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Fe1 Fe 0.06089(8) 0.09769(4) 0.14882(4) 0.01876(18) Uani 1 1 d . . . . . Fe2 Fe 0.32631(7) 0.15792(4) -0.00614(5) 0.01962(17) Uani 1 1 d . . . . . Na Na 0.07476(6) -0.10348(3) 0.15782(3) 0.0251(2) Uani 0.6832(15) 1 d . . P . . Pb Pb 0.07476(6) -0.10348(3) 0.15782(3) 0.0251(2) Uani 0.3168(15) 1 d . . P . . K1 K -0.1854(4) 0.000000 0.000000 0.0304(14) Uani 0.259(13) 2 d S T P . . N1 N -0.1854(4) 0.000000 0.000000 0.0304(14) Uani 0.741(13) 2 d S T P . . K2 K 0.43348(19) 0.00093(12) -0.13237(11) 0.0288(7) Uani 0.485(9) 1 d . . P . . N2 N 0.43348(19) 0.00093(12) -0.13237(11) 0.0288(7) Uani 0.515(9) 1 d . . P . . N3 N 0.1904(6) 0.3092(3) 0.1455(3) 0.0367(13) Uani 1 1 d . . . . . N4 N -0.3063(6) 0.1870(3) 0.1444(3) 0.0347(12) Uani 1 1 d . . . . . S1 S 0.19697(12) 0.00302(8) 0.28715(7) 0.0218(3) Uani 1 1 d . . . . . S2 S -0.01601(12) 0.18634(6) -0.00283(7) 0.0165(2) Uani 1 1 d . . . . . S3 S 0.16498(15) 0.000000 0.000000 0.0138(3) Uani 1 2 d S T P . . O1 O 0.3439(5) 0.0072(4) 0.2850(3) 0.0652(19) Uani 1 1 d . . . . . O2 O 0.1430(5) 0.0169(2) 0.2111(2) 0.0314(10) Uani 1 1 d . . . . . O3 O 0.1508(6) -0.0668(3) 0.3071(3) 0.0521(15) Uani 1 1 d . . . . . O4 O 0.1425(4) 0.0534(2) 0.3402(2) 0.0309(9) Uani 1 1 d . . . . . O5 O 0.1255(4) 0.2045(3) -0.0185(3) 0.0431(13) Uani 1 1 d . . . . . O6 O -0.1040(5) 0.2458(2) -0.0174(3) 0.0373(11) Uani 1 1 d . . . . . O7 O -0.0601(7) 0.1307(3) -0.0515(3) 0.0499(14) Uani 1 1 d . . . . . O8 O -0.0306(5) 0.1659(3) 0.0756(3) 0.0403(12) Uani 1 1 d . . . . . O9 O 0.2498(5) 0.0580(2) -0.0234(3) 0.0445(14) Uani 1 1 d . . . . . O10 O 0.0781(4) 0.0199(2) 0.0631(2) 0.0266(8) Uani 1 1 d . . . . . Cl1 Cl 0.29077(14) 0.14689(7) 0.13413(8) 0.0259(3) Uani 1 1 d . . . . . Cl2 Cl 0.000000 0.17900(10) 0.250000 0.0295(4) Uani 1 2 d S T P . . Cl3 Cl 0.3433(2) 0.16197(9) -0.14856(9) 0.0399(4) Uani 1 1 d . . . . . Cl4 Cl 0.55827(13) 0.10510(7) 0.00109(9) 0.0299(3) Uani 1 1 d . . . . . Cl5 Cl 0.000000 -0.21271(12) 0.250000 0.0408(5) Uani 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Fe1 0.0211(4) 0.0192(4) 0.0159(3) 0.0004(3) 0.0005(3) 0.0014(3) Fe2 0.0188(3) 0.0135(3) 0.0265(4) 0.0005(3) 0.0002(3) -0.0024(2) Na 0.0262(3) 0.0234(3) 0.0256(3) -0.0053(2) -0.0012(2) 0.0006(2) Pb 0.0262(3) 0.0234(3) 0.0256(3) -0.0053(2) -0.0012(2) 0.0006(2) K1 0.0213(19) 0.033(2) 0.037(2) -0.007(2) 0.000 0.000 N1 0.0213(19) 0.033(2) 0.037(2) -0.007(2) 0.000 0.000 K2 0.0265(10) 0.0298(11) 0.0302(11) -0.0014(9) 0.0049(7) 0.0018(10) N2 0.0265(10) 0.0298(11) 0.0302(11) -0.0014(9) 0.0049(7) 0.0018(10) N3 0.037(3) 0.027(3) 0.046(3) 0.003(2) -0.005(3) 0.002(2) N4 0.039(3) 0.025(3) 0.040(3) -0.006(2) -0.001(2) 0.002(2) S1 0.0175(5) 0.0299(7) 0.0180(5) 0.0047(6) 0.0000(4) 0.0030(6) S2 0.0197(5) 0.0120(5) 0.0179(5) 0.0015(5) -0.0001(5) 0.0030(4) S3 0.0144(6) 0.0115(6) 0.0154(6) -0.0010(7) 0.000 0.000 O1 0.019(2) 0.135(6) 0.041(3) -0.015(4) -0.005(2) 0.002(4) O2 0.043(2) 0.032(2) 0.0191(18) -0.0001(16) -0.0069(17) 0.0071(19) O3 0.058(3) 0.028(3) 0.070(4) 0.016(3) 0.022(3) 0.007(2) O4 0.027(2) 0.040(3) 0.025(2) -0.0069(18) -0.0004(17) 0.0030(19) O5 0.022(2) 0.041(3) 0.066(4) 0.027(2) 0.009(2) 0.0043(19) O6 0.036(2) 0.020(2) 0.057(3) 0.0018(19) -0.007(2) 0.0120(18) O7 0.078(4) 0.025(2) 0.047(3) -0.013(2) -0.021(3) 0.003(3) O8 0.038(2) 0.056(3) 0.027(2) 0.021(2) 0.0080(19) 0.017(2) O9 0.053(3) 0.026(2) 0.055(3) -0.015(2) 0.029(2) -0.025(2) O10 0.029(2) 0.031(2) 0.0197(17) -0.0094(15) 0.0048(16) -0.0067(17) Cl1 0.0251(6) 0.0237(6) 0.0289(7) -0.0002(5) -0.0012(5) -0.0023(5) Cl2 0.0455(12) 0.0206(9) 0.0225(9) 0.000 0.0078(8) 0.000 Cl3 0.0568(11) 0.0327(8) 0.0304(8) 0.0040(6) -0.0020(7) 0.0097(8) Cl4 0.0229(6) 0.0294(7) 0.0375(7) -0.0006(7) -0.0006(6) 0.0043(5) Cl5 0.0432(13) 0.0323(12) 0.0469(13) 0.000 0.0120(10) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Fe1 O8 2.068(4) . ? Fe1 O2 2.086(4) . ? Fe1 O10 2.158(4) . ? Fe1 O4 2.188(4) 4 ? Fe1 Cl1 2.4702(16) . ? Fe1 Cl2 2.4739(15) . ? Fe1 N4 4.010(6) . ? Fe1 K1 4.067(2) . ? Fe1 K2 4.148(2) 3 ? Fe2 O6 2.039(4) 7 ? Fe2 O9 2.107(4) . ? Fe2 O5 2.185(4) . ? Fe2 Cl4 2.5066(14) . ? Fe2 Cl1 2.5368(17) . ? Fe2 Cl3 2.5485(18) . ? Fe2 N2 3.938(2) . ? Fe2 K2 4.095(2) 3 ? Fe2 N4 4.109(6) 7 ? Fe2 N3 4.215(6) . ? Na O7 2.375(6) 3 ? Na O3 2.414(6) 4 ? Na O2 2.615(4) . ? Na Cl5 2.7857(19) . ? Na O3 2.857(6) . ? Na Cl3 2.882(2) 3 ? Na O10 2.935(4) . ? Na O9 3.084(6) 3 ? Na O5 3.207(6) 3 ? Na Na 3.6044(12) 4 ? Na K2 4.080(2) 3 ? Na N3 4.152(6) 5_445 ? K1 O10 2.853(5) 3 ? K1 O10 2.853(5) . ? K1 O7 2.970(6) . ? K1 O7 2.970(6) 3 ? K1 O4 3.064(4) 4 ? K1 O4 3.064(4) 2_554 ? K1 Cl4 3.247(3) 3_455 ? K1 Cl4 3.247(3) 1_455 ? K1 S3 3.448(4) . ? K1 O3 3.696(6) 4 ? K1 O3 3.696(6) 2_554 ? K1 O8 3.814(6) 3 ? N2 O1 2.646(5) 2_654 ? N2 O1 2.868(5) 3 ? N2 O9 2.878(5) . ? N2 Cl1 3.200(3) 3 ? N2 O2 3.204(5) 3 ? N2 Cl3 3.268(3) . ? N2 Cl4 3.354(3) 3 ? N2 Cl4 3.359(3) . ? N2 O9 3.508(6) 3 ? N2 S3 3.545(2) . ? N2 S1 3.613(2) 3 ? N2 O10 3.732(5) 3 ? N3 O3 2.996(8) 8 ? N3 O7 3.195(8) 7 ? N3 O6 3.235(8) 7 ? N3 Cl1 3.313(6) . ? N3 Cl4 3.363(6) 7_455 ? N3 Cl3 3.462(6) 7_455 ? N3 Cl5 3.598(6) 5 ? N3 O5 3.623(8) . ? N3 Cl2 3.661(6) . ? N3 Cl3 3.733(6) 6 ? N3 O8 3.749(8) . ? N4 O8 3.006(7) . ? N4 O4 3.071(7) 4 ? N4 O5 3.153(7) 7_455 ? N4 Cl3 3.286(6) 7_455 ? N4 Cl4 3.294(6) 1_455 ? N4 Cl5 3.315(6) 5_455 ? N4 Cl2 3.559(6) . ? N4 O6 3.688(8) . ? N4 O1 3.736(10) 4 ? S1 O1 1.448(5) . ? S1 O4 1.464(4) . ? S1 O3 1.475(5) . ? S1 O2 1.483(4) . ? S2 O7 1.455(5) . ? S2 O8 1.462(4) . ? S2 O5 1.464(4) . ? S2 O6 1.467(4) . ? S3 O9 1.463(4) . ? S3 O9 1.463(4) 3 ? S3 O10 1.466(4) 3 ? S3 O10 1.466(4) . ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O8 Fe1 O2 171.0(2) . . ? O8 Fe1 O10 92.06(19) . . ? O2 Fe1 O10 79.60(16) . . ? O8 Fe1 O4 84.89(18) . 4 ? O2 Fe1 O4 90.57(18) . 4 ? O10 Fe1 O4 81.89(16) . 4 ? O8 Fe1 Cl1 94.78(15) . . ? O2 Fe1 Cl1 89.62(14) . . ? O10 Fe1 Cl1 97.16(12) . . ? O4 Fe1 Cl1 178.98(13) 4 . ? O8 Fe1 Cl2 86.89(15) . . ? O2 Fe1 Cl2 100.74(12) . . ? O10 Fe1 Cl2 169.88(12) . . ? O4 Fe1 Cl2 87.99(12) 4 . ? Cl1 Fe1 Cl2 92.96(4) . . ? O8 Fe1 N4 46.94(15) . . ? O2 Fe1 N4 133.28(16) . . ? O10 Fe1 N4 111.11(14) . . ? O4 Fe1 N4 49.32(15) 4 . ? Cl1 Fe1 N4 130.95(9) . . ? Cl2 Fe1 N4 61.27(8) . . ? O8 Fe1 K1 68.13(16) . . ? O2 Fe1 K1 103.11(12) . . ? O10 Fe1 K1 41.95(12) . . ? O4 Fe1 K1 47.88(12) 4 . ? Cl1 Fe1 K1 131.11(5) . . ? Cl2 Fe1 K1 129.12(5) . . ? N4 Fe1 K1 69.66(9) . . ? O8 Fe1 K2 129.55(13) . 3 ? O2 Fe1 K2 49.26(13) . 3 ? O10 Fe1 K2 63.67(12) . 3 ? O4 Fe1 K2 129.25(13) 4 3 ? Cl1 Fe1 K2 50.37(5) . 3 ? Cl2 Fe1 K2 124.14(4) . 3 ? N4 Fe1 K2 174.46(9) . 3 ? K1 Fe1 K2 105.34(5) . 3 ? O6 Fe2 O9 176.37(19) 7 . ? O6 Fe2 O5 86.81(18) 7 . ? O9 Fe2 O5 92.6(2) . . ? O6 Fe2 Cl4 93.41(14) 7 . ? O9 Fe2 Cl4 87.40(16) . . ? O5 Fe2 Cl4 177.11(15) . . ? O6 Fe2 Cl1 85.48(15) 7 . ? O9 Fe2 Cl1 90.95(14) . . ? O5 Fe2 Cl1 90.59(14) . . ? Cl4 Fe2 Cl1 92.30(6) . . ? O6 Fe2 Cl3 98.90(15) 7 . ? O9 Fe2 Cl3 84.63(14) . . ? O5 Fe2 Cl3 86.88(14) . . ? Cl4 Fe2 Cl3 90.24(6) . . ? Cl1 Fe2 Cl3 174.80(7) . . ? O6 Fe2 N2 137.73(14) 7 . ? O9 Fe2 N2 45.33(13) . . ? O5 Fe2 N2 120.37(15) . . ? Cl4 Fe2 N2 57.85(5) . . ? Cl1 Fe2 N2 122.40(5) . . ? Cl3 Fe2 N2 55.65(5) . . ? O6 Fe2 K2 118.84(15) 7 3 ? O9 Fe2 K2 58.93(17) . 3 ? O5 Fe2 K2 127.36(12) . 3 ? Cl4 Fe2 K2 54.91(5) . 3 ? Cl1 Fe2 K2 51.39(5) . 3 ? Cl3 Fe2 K2 127.48(5) . 3 ? N2 Fe2 K2 72.03(5) . 3 ? O6 Fe2 N4 63.64(16) 7 7 ? O9 Fe2 N4 118.43(18) . 7 ? O5 Fe2 N4 49.28(14) . 7 ? Cl4 Fe2 N4 128.39(9) . 7 ? Cl1 Fe2 N4 127.64(9) . 7 ? Cl3 Fe2 N4 53.09(9) . 7 ? N2 Fe2 N4 108.10(9) . 7 ? K2 Fe2 N4 176.36(9) 3 7 ? O6 Fe2 N3 48.19(16) 7 . ? O9 Fe2 N3 128.62(15) . . ? O5 Fe2 N3 59.25(17) . . ? Cl4 Fe2 N3 122.82(9) . . ? Cl1 Fe2 N3 51.81(9) . . ? Cl3 Fe2 N3 129.76(9) . . ? N2 Fe2 N3 173.38(9) . . ? K2 Fe2 N3 102.75(9) 3 . ? N4 Fe2 N3 76.84(10) 7 . ? O7 Na O3 76.1(2) 3 4 ? O7 Na O2 129.28(15) 3 . ? O3 Na O2 82.94(16) 4 . ? O7 Na Cl5 98.88(13) 3 . ? O3 Na Cl5 80.16(13) 4 . ? O2 Na Cl5 122.42(9) . . ? O7 Na O3 161.20(19) 3 . ? O3 Na O3 85.7(2) 4 . ? O2 Na O3 50.99(13) . . ? Cl5 Na O3 73.08(11) . . ? O7 Na Cl3 112.26(14) 3 3 ? O3 Na Cl3 167.06(14) 4 3 ? O2 Na Cl3 97.98(11) . 3 ? Cl5 Na Cl3 88.57(4) . 3 ? O3 Na Cl3 84.94(12) . 3 ? O7 Na O10 74.23(15) 3 . ? O3 Na O10 85.31(16) 4 . ? O2 Na O10 58.28(11) . . ? Cl5 Na O10 165.10(9) . . ? O3 Na O10 109.27(12) . . ? Cl3 Na O10 106.23(9) 3 . ? O7 Na O9 75.80(17) 3 3 ? O3 Na O9 129.11(16) 4 3 ? O2 Na O9 83.23(13) . 3 ? Cl5 Na O9 145.69(8) . 3 ? O3 Na O9 120.49(15) . 3 ? Cl3 Na O9 63.67(8) 3 3 ? O10 Na O9 46.45(11) . 3 ? O7 Na O5 48.06(16) 3 3 ? O3 Na O5 121.70(15) 4 3 ? O2 Na O5 142.19(13) . 3 ? Cl5 Na O5 91.83(9) . 3 ? O3 Na O5 146.57(14) . 3 ? Cl3 Na O5 64.60(8) 3 3 ? O10 Na O5 93.01(11) . 3 ? O9 Na O5 59.05(11) 3 3 ? O7 Na Na 120.07(14) 3 4 ? O3 Na Na 52.24(14) 4 4 ? O2 Na Na 76.89(9) . 4 ? Cl5 Na Na 49.69(3) . 4 ? O3 Na Na 41.92(12) . 4 ? Cl3 Na Na 115.26(4) 3 4 ? O10 Na Na 122.02(7) . 4 ? O9 Na Na 159.78(9) 3 4 ? O5 Na Na 140.45(8) 3 4 ? O7 Na K2 120.23(14) 3 3 ? O3 Na K2 132.84(13) 4 3 ? O2 Na K2 51.72(11) . 3 ? Cl5 Na K2 131.84(4) . 3 ? O3 Na K2 75.83(12) . 3 ? Cl3 Na K2 52.63(5) 3 3 ? O10 Na K2 61.75(9) . 3 ? O9 Na K2 44.74(9) 3 3 ? O5 Na K2 94.49(8) 3 3 ? Na Na K2 117.05(3) 4 3 ? O7 Na N3 50.02(16) 3 5_445 ? O3 Na N3 45.33(15) 4 5_445 ? O2 Na N3 128.27(13) . 5_445 ? Cl5 Na N3 58.59(8) . 5_445 ? O3 Na N3 112.96(14) . 5_445 ? Cl3 Na N3 132.14(9) 3 5_445 ? O10 Na N3 108.30(11) . 5_445 ? O9 Na N3 125.81(12) 3 5_445 ? O5 Na N3 81.40(12) 3 5_445 ? Na Na N3 71.12(9) 4 5_445 ? K2 Na N3 169.20(9) 3 5_445 ? O10 K1 O10 49.33(15) 3 . ? O10 K1 O7 67.46(16) 3 . ? O10 K1 O7 68.22(15) . . ? O10 K1 O7 68.22(15) 3 3 ? O10 K1 O7 67.46(16) . 3 ? O7 K1 O7 131.0(3) . 3 ? O10 K1 O4 106.74(14) 3 4 ? O10 K1 O4 57.42(11) . 4 ? O7 K1 O4 86.63(13) . 4 ? O7 K1 O4 86.81(13) 3 4 ? O10 K1 O4 57.42(11) 3 2_554 ? O10 K1 O4 106.74(14) . 2_554 ? O7 K1 O4 86.81(13) . 2_554 ? O7 K1 O4 86.63(13) 3 2_554 ? O4 K1 O4 164.2(2) 4 2_554 ? O10 K1 Cl4 128.20(9) 3 3_455 ? O10 K1 Cl4 142.55(9) . 3_455 ? O7 K1 Cl4 149.22(14) . 3_455 ? O7 K1 Cl4 77.63(13) 3 3_455 ? O4 K1 Cl4 109.02(10) 4 3_455 ? O4 K1 Cl4 83.58(10) 2_554 3_455 ? O10 K1 Cl4 142.55(9) 3 1_455 ? O10 K1 Cl4 128.20(9) . 1_455 ? O7 K1 Cl4 77.63(13) . 1_455 ? O7 K1 Cl4 149.22(14) 3 1_455 ? O4 K1 Cl4 83.58(10) 4 1_455 ? O4 K1 Cl4 109.02(10) 2_554 1_455 ? Cl4 K1 Cl4 78.03(9) 3_455 1_455 ? O10 K1 S3 24.67(8) 3 . ? O10 K1 S3 24.67(8) . . ? O7 K1 S3 65.48(14) . . ? O7 K1 S3 65.48(14) 3 . ? O4 K1 S3 82.08(10) 4 . ? O4 K1 S3 82.08(10) 2_554 . ? Cl4 K1 S3 140.99(5) 3_455 . ? Cl4 K1 S3 140.99(5) 1_455 . ? O10 K1 O3 103.67(14) 3 4 ? O10 K1 O3 66.19(13) . 4 ? O7 K1 O3 123.43(14) . 4 ? O7 K1 O3 51.14(12) 3 4 ? O4 K1 O3 40.47(11) 4 4 ? O4 K1 O3 137.34(11) 2_554 4 ? Cl4 K1 O3 81.71(10) 3_455 4 ? Cl4 K1 O3 106.69(11) 1_455 4 ? S3 K1 O3 84.72(11) . 4 ? O10 K1 O3 66.19(13) 3 2_554 ? O10 K1 O3 103.67(14) . 2_554 ? O7 K1 O3 51.14(12) . 2_554 ? O7 K1 O3 123.43(14) 3 2_554 ? O4 K1 O3 137.34(11) 4 2_554 ? O4 K1 O3 40.47(11) 2_554 2_554 ? Cl4 K1 O3 106.69(11) 3_455 2_554 ? Cl4 K1 O3 81.71(10) 1_455 2_554 ? S3 K1 O3 84.72(11) . 2_554 ? O3 K1 O3 169.4(2) 4 2_554 ? O10 K1 O8 51.89(11) 3 3 ? O10 K1 O8 83.77(12) . 3 ? O7 K1 O8 116.64(15) . 3 ? O7 K1 O8 38.76(11) 3 3 ? O4 K1 O8 124.11(12) 4 3 ? O4 K1 O8 47.88(10) 2_554 3 ? Cl4 K1 O8 77.03(7) 3_455 3 ? Cl4 K1 O8 147.65(10) 1_455 3 ? S3 K1 O8 66.47(8) . 3 ? O3 K1 O8 89.74(10) 4 3 ? O3 K1 O8 86.05(11) 2_554 3 ? O1 N2 O1 73.87(16) 2_654 3 ? O1 N2 O9 156.9(2) 2_654 . ? O1 N2 O9 118.05(17) 3 . ? O1 N2 Cl1 107.73(19) 2_654 3 ? O1 N2 Cl1 78.83(17) 3 3 ? O9 N2 Cl1 94.43(10) . 3 ? O1 N2 O2 119.23(14) 2_654 3 ? O1 N2 O2 45.84(11) 3 3 ? O9 N2 O2 77.16(14) . 3 ? Cl1 N2 O2 60.43(9) 3 3 ? O1 N2 Cl3 103.46(19) 2_654 . ? O1 N2 Cl3 83.41(17) 3 . ? O9 N2 Cl3 61.31(11) . . ? Cl1 N2 Cl3 137.81(8) 3 . ? O2 N2 Cl3 79.80(10) 3 . ? O1 N2 Cl4 92.83(15) 2_654 3 ? O1 N2 Cl4 137.94(18) 3 3 ? O9 N2 Cl4 89.69(13) . 3 ? Cl1 N2 Cl4 67.37(6) 3 3 ? O2 N2 Cl4 124.48(10) 3 3 ? Cl3 N2 Cl4 138.62(8) . 3 ? O1 N2 Cl4 97.37(16) 2_654 . ? O1 N2 Cl4 144.99(18) 3 . ? O9 N2 Cl4 61.17(11) . . ? Cl1 N2 Cl4 135.17(7) 3 . ? O2 N2 Cl4 134.61(10) 3 . ? Cl3 N2 Cl4 65.42(6) . . ? Cl4 N2 Cl4 75.03(6) 3 . ? O1 N2 O9 148.09(18) 2_654 3 ? O1 N2 O9 125.19(15) 3 3 ? O9 N2 O9 42.82(15) . 3 ? Cl1 N2 O9 59.22(9) 3 3 ? O2 N2 O9 81.49(11) 3 3 ? Cl3 N2 O9 104.06(9) . 3 ? Cl4 N2 O9 55.56(8) 3 3 ? Cl4 N2 O9 79.83(9) . 3 ? O1 N2 S3 171.31(14) 2_654 . ? O1 N2 S3 113.80(11) 3 . ? O9 N2 S3 23.53(8) . . ? Cl1 N2 S3 71.02(5) 3 . ? O2 N2 S3 68.06(8) 3 . ? Cl3 N2 S3 82.03(6) . . ? Cl4 N2 S3 78.71(5) 3 . ? Cl4 N2 S3 78.64(5) . . ? O9 N2 S3 23.94(7) 3 . ? O1 N2 S1 96.10(12) 2_654 3 ? O1 N2 S1 22.24(9) 3 3 ? O9 N2 S1 96.92(13) . 3 ? Cl1 N2 S1 71.98(5) 3 3 ? O2 N2 S1 24.19(7) 3 3 ? Cl3 N2 S1 77.16(6) . 3 ? Cl4 N2 S1 139.19(8) 3 3 ? Cl4 N2 S1 142.22(8) . 3 ? O9 N2 S1 105.48(9) 3 3 ? S3 N2 S1 91.67(5) . 3 ? O1 N2 O10 162.63(17) 2_654 3 ? O1 N2 O10 91.17(12) 3 3 ? O9 N2 O10 39.57(11) . 3 ? Cl1 N2 O10 59.62(7) 3 3 ? O2 N2 O10 45.34(9) 3 3 ? Cl3 N2 O10 83.04(9) . 3 ? Cl4 N2 O10 92.58(8) 3 3 ? Cl4 N2 O10 99.97(8) . 3 ? O9 N2 O10 38.65(9) 3 3 ? S3 N2 O10 23.06(6) . 3 ? S1 N2 O10 69.34(7) 3 3 ? O3 N3 O7 56.82(16) 8 7 ? O3 N3 O6 98.0(2) 8 7 ? O7 N3 O6 43.05(14) 7 7 ? O3 N3 Cl1 128.9(2) 8 . ? O7 N3 Cl1 95.02(18) 7 . ? O6 N3 Cl1 57.02(13) 7 . ? O3 N3 Cl4 91.30(19) 8 7_455 ? O7 N3 Cl4 73.00(18) 7 7_455 ? O6 N3 Cl4 81.71(17) 7 7_455 ? Cl1 N3 Cl4 122.67(19) . 7_455 ? O3 N3 Cl3 112.3(2) 8 7_455 ? O7 N3 Cl3 135.0(2) 7 7_455 ? O6 N3 Cl3 133.0(2) 7 7_455 ? Cl1 N3 Cl3 116.71(17) . 7_455 ? Cl4 N3 Cl3 63.30(11) 7_455 7_455 ? O3 N3 Cl5 60.46(17) 8 5 ? O7 N3 Cl5 70.40(16) 7 5 ? O6 N3 Cl5 78.32(16) 7 5 ? Cl1 N3 Cl5 70.52(12) . 5 ? Cl4 N3 Cl5 142.12(19) 7_455 5 ? Cl3 N3 Cl5 147.8(2) 7_455 5 ? O3 N3 O5 140.6(2) 8 . ? O7 N3 O5 85.24(19) 7 . ? O6 N3 O5 49.71(14) 7 . ? Cl1 N3 O5 57.84(12) . . ? Cl4 N3 O5 65.29(13) 7_455 . ? Cl3 N3 O5 85.99(15) 7_455 . ? Cl5 N3 O5 120.11(18) 5 . ? O3 N3 Cl2 132.8(2) 8 . ? O7 N3 Cl2 156.1(2) 7 . ? O6 N3 Cl2 116.87(18) 7 . ? Cl1 N3 Cl2 61.63(10) . . ? Cl4 N3 Cl2 122.76(17) 7_455 . ? Cl3 N3 Cl2 66.35(11) 7_455 . ? Cl5 N3 Cl2 95.02(14) 5 . ? O5 N3 Cl2 86.14(14) . . ? O3 N3 Cl3 69.34(16) 8 6 ? O7 N3 Cl3 122.0(2) 7 6 ? O6 N3 Cl3 143.2(2) 7 6 ? Cl1 N3 Cl3 103.29(15) . 6 ? Cl4 N3 Cl3 131.07(17) 7_455 6 ? Cl3 N3 Cl3 82.67(14) 7_455 6 ? Cl5 N3 Cl3 65.33(11) 5 6 ? O5 N3 Cl3 149.82(19) . 6 ? Cl2 N3 Cl3 63.69(11) . 6 ? O3 N3 O8 174.3(2) 8 . ? O7 N3 O8 122.9(2) 7 . ? O6 N3 O8 83.24(17) 7 . ? Cl1 N3 O8 56.26(11) . . ? Cl4 N3 O8 83.41(15) 7_455 . ? Cl3 N3 O8 63.46(12) 7_455 . ? Cl5 N3 O8 125.16(17) 5 . ? O5 N3 O8 37.91(11) . . ? Cl2 N3 O8 50.09(10) . . ? Cl3 N3 O8 112.82(17) 6 . ? O3 N3 Na 34.97(13) 8 5 ? O7 N3 Na 34.71(12) 7 5 ? O6 N3 Na 66.59(13) 7 5 ? Cl1 N3 Na 96.97(14) . 5 ? Cl4 N3 Na 100.99(14) 7_455 5 ? Cl3 N3 Na 146.28(17) 7_455 5 ? Cl5 N3 Na 41.36(7) 5 5 ? O5 N3 Na 115.67(17) . 5 ? Cl2 N3 Na 136.24(16) . 5 ? Cl3 N3 Na 88.13(12) 6 5 ? O8 N3 Na 148.24(18) . 5 ? O8 N4 O4 56.43(16) . 4 ? O8 N4 O5 89.6(2) . 7_455 ? O4 N4 O5 137.9(2) 4 7_455 ? O8 N4 Cl3 74.16(17) . 7_455 ? O4 N4 Cl3 121.3(2) 4 7_455 ? O5 N4 Cl3 60.89(13) 7_455 7_455 ? O8 N4 Cl4 88.98(17) . 1_455 ? O4 N4 Cl4 82.69(16) 4 1_455 ? O5 N4 Cl4 71.63(16) 7_455 1_455 ? Cl3 N4 Cl4 129.14(19) 7_455 1_455 ? O8 N4 Cl5 146.3(2) . 5_455 ? O4 N4 Cl5 138.5(2) 4 5_455 ? O5 N4 Cl5 83.63(16) 7_455 5_455 ? Cl3 N4 Cl5 73.68(12) 7_455 5_455 ? Cl4 N4 Cl5 119.55(18) 1_455 5_455 ? O8 N4 Cl2 56.34(13) . . ? O4 N4 Cl2 58.04(13) 4 . ? O5 N4 Cl2 125.9(2) 7_455 . ? Cl3 N4 Cl2 69.36(12) 7_455 . ? Cl4 N4 Cl2 137.11(17) 1_455 . ? Cl5 N4 Cl2 102.21(15) 5_455 . ? O8 N4 O6 40.13(13) . . ? O4 N4 O6 92.80(17) 4 . ? O5 N4 O6 49.48(14) 7_455 . ? Cl3 N4 O6 59.94(13) 7_455 . ? Cl4 N4 O6 76.16(14) 1_455 . ? Cl5 N4 O6 124.98(18) 5_455 . ? Cl2 N4 O6 88.33(15) . . ? O8 N4 O1 95.69(19) . 4 ? O4 N4 O1 39.59(13) 4 4 ? O5 N4 O1 147.7(2) 7_455 4 ? Cl3 N4 O1 150.8(2) 7_455 4 ? Cl4 N4 O1 76.65(15) 1_455 4 ? Cl5 N4 O1 107.57(18) 5_455 4 ? Cl2 N4 O1 82.18(14) . 4 ? O6 N4 O1 127.40(19) . 4 ? O8 N4 Fe1 30.18(10) . . ? O4 N4 Fe1 32.70(10) 4 . ? O5 N4 Fe1 119.71(19) 7_455 . ? Cl3 N4 Fe1 89.02(14) 7_455 . ? Cl4 N4 Fe1 99.82(13) 1_455 . ? Cl5 N4 Fe1 139.61(17) 5_455 . ? Cl2 N4 Fe1 37.56(6) . . ? O6 N4 Fe1 70.31(12) . . ? O1 N4 Fe1 71.15(12) 4 . ? O8 N4 Fe2 64.44(14) . 7_455 ? O4 N4 Fe2 120.55(18) 4 7_455 ? O5 N4 Fe2 31.68(9) 7_455 7_455 ? Cl3 N4 Fe2 38.32(7) 7_455 7_455 ? Cl4 N4 Fe2 91.00(14) 1_455 7_455 ? Cl5 N4 Fe2 95.30(13) 5_455 7_455 ? Cl2 N4 Fe2 94.66(13) . 7_455 ? O6 N4 Fe2 29.69(8) . 7_455 ? O1 N4 Fe2 157.08(18) 4 7_455 ? Fe1 N4 Fe2 92.50(12) . 7_455 ? O8 N4 Na 113.77(19) . 5_455 ? O4 N4 Na 162.1(2) 4 5_455 ? O5 N4 Na 48.67(12) 7_455 5_455 ? Cl3 N4 Na 42.66(7) 7_455 5_455 ? Cl4 N4 Na 113.36(15) 1_455 5_455 ? Cl5 N4 Na 40.97(7) 5_455 5_455 ? Cl2 N4 Na 104.22(13) . 5_455 ? O6 N4 Na 84.02(13) . 5_455 ? O1 N4 Na 148.43(18) 4 5_455 ? Fe1 N4 Na 131.52(15) . 5_455 ? Fe2 N4 Na 54.36(7) 7_455 5_455 ? O1 S1 O4 110.2(3) . . ? O1 S1 O3 111.4(4) . . ? O4 S1 O3 110.3(3) . . ? O1 S1 O2 108.9(3) . . ? O4 S1 O2 109.8(3) . . ? O3 S1 O2 106.2(3) . . ? O1 S1 K2 48.6(2) . 3 ? O4 S1 K2 138.1(2) . 3 ? O3 S1 K2 111.3(2) . 3 ? O2 S1 K2 62.26(19) . 3 ? O7 S2 O8 109.9(3) . . ? O7 S2 O5 110.4(3) . . ? O8 S2 O5 110.0(3) . . ? O7 S2 O6 107.7(3) . . ? O8 S2 O6 109.0(3) . . ? O5 S2 O6 109.7(3) . . ? O9 S3 O9 110.4(5) . 3 ? O9 S3 O10 108.5(3) . 3 ? O9 S3 O10 110.4(2) 3 3 ? O9 S3 O10 110.4(2) . . ? O9 S3 O10 108.5(3) 3 . ? O10 S3 O10 108.6(3) 3 . ? O9 S3 K1 124.8(2) . . ? O9 S3 K1 124.8(2) 3 . ? O10 S3 K1 54.31(16) 3 . ? O10 S3 K1 54.31(16) . . ? O9 S3 K2 76.6(2) . 3 ? O9 S3 K2 51.74(19) 3 3 ? O10 S3 K2 161.00(17) 3 3 ? O10 S3 K2 85.66(16) . 3 ? K1 S3 K2 138.20(4) . 3 ? O9 S3 N2 51.74(19) . . ? O9 S3 N2 76.6(2) 3 . ? O10 S3 N2 85.66(16) 3 . ? O10 S3 N2 161.00(17) . . ? K1 S3 N2 138.20(4) . . ? K2 S3 N2 83.60(7) 3 . ? S1 O1 K2 144.0(3) . 2_655 ? S1 O1 K2 109.2(2) . 3 ? K2 O1 K2 105.74(16) 2_655 3 ? S1 O1 N4 86.8(3) . 4 ? K2 O1 N4 87.1(2) 2_655 4 ? K2 O1 N4 113.7(3) 3 4 ? S1 O2 Fe1 139.8(3) . . ? S1 O2 Na 105.1(2) . . ? Fe1 O2 Na 112.41(17) . . ? S1 O2 K2 93.5(2) . 3 ? Fe1 O2 K2 101.18(16) . 3 ? Na O2 K2 88.43(13) . 3 ? S1 O3 Na 128.1(3) . 4 ? S1 O3 Na 94.9(3) . . ? Na O3 Na 85.8(2) 4 . ? S1 O3 N3 130.4(4) . 8_545 ? Na O3 N3 99.7(2) 4 8_545 ? Na O3 N3 101.5(2) . 8_545 ? S1 O3 K1 82.7(2) . 2 ? Na O3 K1 86.94(16) 4 2 ? Na O3 K1 168.6(2) . 2 ? N3 O3 K1 88.37(18) 8_545 2 ? S1 O4 Fe1 131.0(3) . 4 ? S1 O4 K1 109.0(2) . 2 ? Fe1 O4 K1 100.15(16) 4 2 ? S1 O4 N4 115.6(3) . 4 ? Fe1 O4 N4 97.98(19) 4 4 ? K1 O4 N4 97.52(16) 2 4 ? S2 O5 Fe2 137.8(3) . . ? S2 O5 N4 120.0(3) . 7 ? Fe2 O5 N4 99.04(18) . 7 ? S2 O5 Na 81.5(2) . 3 ? Fe2 O5 Na 88.03(17) . 3 ? N4 O5 Na 83.75(16) 7 3 ? S2 O5 N3 98.5(3) . . ? Fe2 O5 N3 89.53(19) . . ? N4 O5 N3 99.31(18) 7 . ? Na O5 N3 176.36(17) 3 . ? S2 O6 Fe2 152.4(3) . 7_455 ? S2 O6 N3 103.5(2) . 7_455 ? Fe2 O6 N3 103.79(19) 7_455 7_455 ? S2 O6 N4 86.4(2) . . ? Fe2 O6 N4 86.67(18) 7_455 . ? N3 O6 N4 96.50(17) 7_455 . ? S2 O7 Na 118.4(4) . 3 ? S2 O7 K1 125.1(3) . . ? Na O7 K1 106.78(17) 3 . ? S2 O7 N3 105.7(3) . 7_455 ? Na O7 N3 95.3(2) 3 7_455 ? K1 O7 N3 99.0(2) . 7_455 ? S2 O8 Fe1 137.4(3) . . ? S2 O8 N4 116.3(3) . . ? Fe1 O8 N4 102.9(2) . . ? S2 O8 N3 93.4(3) . . ? Fe1 O8 N3 90.79(19) . . ? N4 O8 N3 106.6(2) . . ? S2 O8 K1 86.0(2) . . ? Fe1 O8 K1 81.65(17) . . ? N4 O8 K1 84.24(17) . . ? N3 O8 K1 168.00(17) . . ? S3 O9 Fe2 150.8(3) . . ? S3 O9 N2 104.7(2) . . ? Fe2 O9 N2 103.29(17) . . ? S3 O9 Na 97.1(3) . 3 ? Fe2 O9 Na 92.76(19) . 3 ? N2 O9 Na 86.30(14) . 3 ? S3 O9 K2 79.4(2) . 3 ? Fe2 O9 K2 90.09(18) . 3 ? N2 O9 K2 94.95(17) . 3 ? Na O9 K2 176.54(15) 3 3 ? S3 O10 Fe1 140.8(3) . . ? S3 O10 K1 101.03(18) . . ? Fe1 O10 K1 107.68(16) . . ? S3 O10 Na 103.5(2) . . ? Fe1 O10 Na 99.43(13) . . ? K1 O10 Na 96.10(12) . . ? S3 O10 K2 71.28(16) . 3 ? Fe1 O10 K2 85.10(12) . 3 ? K1 O10 K2 165.41(15) . 3 ? Na O10 K2 74.39(10) . 3 ? Fe1 Cl1 Fe2 105.29(6) . . ? Fe1 Cl1 K2 93.15(6) . 3 ? Fe2 Cl1 K2 90.33(6) . 3 ? Fe1 Cl1 N3 95.13(11) . . ? Fe2 Cl1 N3 91.20(11) . . ? K2 Cl1 N3 170.86(12) 3 . ? Fe1 Cl2 Fe1 100.54(8) 4 . ? Fe1 Cl2 N4 102.09(10) 4 . ? Fe1 Cl2 N4 81.17(9) . . ? Fe1 Cl2 N4 81.17(9) 4 4 ? Fe1 Cl2 N4 102.09(10) . 4 ? N4 Cl2 N4 174.98(19) . 4 ? Fe1 Cl2 N3 86.91(10) 4 4 ? Fe1 Cl2 N3 159.72(10) . 4 ? N4 Cl2 N3 78.82(13) . 4 ? N4 Cl2 N3 97.66(14) 4 4 ? Fe1 Cl2 N3 159.72(10) 4 . ? Fe1 Cl2 N3 86.91(10) . . ? N4 Cl2 N3 97.66(14) . . ? N4 Cl2 N3 78.82(13) 4 . ? N3 Cl2 N3 92.48(19) 4 . ? Fe2 Cl3 Na 89.13(6) . 3 ? Fe2 Cl3 N2 84.26(6) . . ? Na Cl3 N2 82.87(6) 3 . ? Fe2 Cl3 N4 88.59(11) . 7 ? Na Cl3 N4 86.74(11) 3 7 ? N2 Cl3 N4 167.46(13) . 7 ? Fe2 Cl3 N3 93.09(11) . 7 ? Na Cl3 N3 165.85(11) 3 7 ? N2 Cl3 N3 83.45(11) . 7 ? N4 Cl3 N3 107.27(15) 7 7 ? Fe2 Cl3 N3 168.77(11) . 6_554 ? Na Cl3 N3 85.49(10) 3 6_554 ? N2 Cl3 N3 104.79(10) . 6_554 ? N4 Cl3 N3 81.28(13) 7 6_554 ? N3 Cl3 N3 94.52(15) 7 6_554 ? Fe2 Cl4 K1 164.86(7) . 1_655 ? Fe2 Cl4 N4 102.13(11) . 1_655 ? K1 Cl4 N4 89.70(11) 1_655 1_655 ? Fe2 Cl4 K2 87.39(5) . 3 ? K1 Cl4 K2 84.36(6) 1_655 3 ? N4 Cl4 K2 84.45(12) 1_655 3 ? Fe2 Cl4 N2 82.98(5) . . ? K1 Cl4 N2 84.27(6) 1_655 . ? N4 Cl4 N2 171.83(12) 1_655 . ? K2 Cl4 N2 89.47(6) 3 . ? Fe2 Cl4 N3 96.25(11) . 7 ? K1 Cl4 N3 90.40(11) 1_655 7 ? N4 Cl4 N3 101.98(14) 1_655 7 ? K2 Cl4 N3 171.71(12) 3 7 ? N2 Cl4 N3 83.61(12) . 7 ? Na Cl5 Na 80.62(7) . 4 ? Na Cl5 N4 159.43(11) . 8_445 ? Na Cl5 N4 87.75(10) 4 8_445 ? Na Cl5 N4 87.75(10) . 5_545 ? Na Cl5 N4 159.43(11) 4 5_545 ? N4 Cl5 N4 107.9(2) 8_445 5_545 ? Na Cl5 N3 89.55(10) . 8_545 ? Na Cl5 N3 80.05(10) 4 8_545 ? N4 Cl5 N3 105.17(14) 8_445 8_545 ? N4 Cl5 N3 82.96(14) 5_545 8_545 ? Na Cl5 N3 80.05(10) . 5_445 ? Na Cl5 N3 89.56(10) 4 5_445 ? N4 Cl5 N3 82.96(14) 8_445 5_445 ? N4 Cl5 N3 105.17(14) 5_545 5_445 ? N3 Cl5 N3 166.4(2) 8_545 5_445 ? _refine_diff_density_max 1.444 _refine_diff_density_min -0.857 _refine_diff_density_rms 0.157 _shelx_res_file ; TITL acmonidesite in C222(1) shelx.res created by SHELXL-2017/1 at 15:14:10 on 06-Feb-2018 CELL 0.71073 9.8413 19.4476 17.8467 90.000 90.000 90.000 ZERR 4.00 0.0014 0.0028 0.0026 0.000 0.000 0.000 LATT -7 SYMM - X, - Y, 1/2 + Z SYMM X, - Y, - Z SYMM - X, Y, 1/2 - Z SFAC O 3.04850 13.27711 2.28680 5.70111 1.54630 0.32390 = 0.86700 32.90894 0.25080 0.011 0.006 32.500 0.850 15.999 SFAC NA 4.76260 3.28500 3.17360 8.84221 1.26740 0.31360 = 1.11280 129.42410 0.67600 0.036 0.025 116.000 1.860 22.990 SFAC S 6.90531 1.46790 5.20341 22.21512 1.43790 0.25360 = 1.58630 56.17207 0.86690 0.125 0.123 532.000 0.750 32.066 SFAC CL 11.46041 0.01040 7.19641 1.16620 6.25561 18.51942 = 1.64550 47.77846 -9.55741 0.148 0.159 678.000 0.990 35.453 SFAC K 8.21861 12.79491 7.43981 0.77480 1.05190 213.18719 = 0.86590 41.68416 1.42280 0.201 0.249 1050.000 2.500 39.098 SFAC FE 11.76951 4.76111 7.35731 0.30720 3.52220 15.35351 = 2.30450 76.88058 1.03690 0.346 0.844 3490.000 1.260 55.845 SFAC N 12.21261 0.00570 3.13220 9.89331 2.01250 28.99754 = 1.16630 0.58260 -11.52901 0.006 0.003 19.600 2.500 14.007 SFAC PB 31.06174 0.69020 13.06371 2.35760 18.44202 8.61801 = 5.96961 47.25795 13.41181 -3.394 10.111 41900.000 1.750 207.200 SFAC H 0.49300 10.51091 0.32291 26.12573 0.14019 3.14236 = 0.04081 57.79977 0.00304 0.000 0.000 0.620 0.320 1.008 UNIT 80 5.47 20 32 4.92 16 23.08 2.53 92.32 MERG 2 TWIN -1 0 0 0 -1 0 0 0 -1 2 EXYZ N2 K2 EADP N2 K2 EXYZ Na Pb EADP Na Pb EXYZ K1 N1 EADP K1 N1 FMAP 2 PLAN 40 BOND ACTA L.S. 1 WGHT 0.056300 BASF 0.22849 FVAR 0.11014 0.48546 0.68324 0.25948 FE1 6 0.060894 0.097692 0.148817 11.00000 0.02111 0.01925 = 0.01593 0.00036 0.00045 0.00143 FE2 6 0.326309 0.157923 -0.006138 11.00000 0.01880 0.01352 = 0.02653 0.00050 0.00020 -0.00240 NA 2 0.074761 -0.103481 0.157817 31.00000 0.02619 0.02342 = 0.02555 -0.00527 -0.00125 0.00061 PB 8 0.074761 -0.103481 0.157817 -31.00000 0.02619 0.02342 = 0.02555 -0.00527 -0.00125 0.00061 K1 5 -0.185361 0.000000 0.000000 40.50000 0.02131 0.03267 = 0.03712 -0.00678 0.00000 0.00000 N1 7 -0.185361 0.000000 0.000000 -40.50000 0.02131 0.03267 = 0.03712 -0.00678 0.00000 0.00000 K2 5 0.433481 0.000927 -0.132374 21.00000 0.02649 0.02977 = 0.03017 -0.00135 0.00490 0.00176 N2 7 0.433481 0.000927 -0.132374 -21.00000 0.02649 0.02977 = 0.03017 -0.00135 0.00490 0.00176 N3 7 0.190394 0.309190 0.145491 11.00000 0.03697 0.02694 = 0.04610 0.00302 -0.00460 0.00163 N4 7 -0.306309 0.187021 0.144359 11.00000 0.03851 0.02531 = 0.04043 -0.00581 -0.00076 0.00198 S1 3 0.196966 0.003021 0.287153 11.00000 0.01748 0.02991 = 0.01797 0.00470 -0.00004 0.00299 S2 3 -0.016013 0.186341 -0.002833 11.00000 0.01970 0.01203 = 0.01787 0.00148 -0.00006 0.00304 S3 3 0.164982 0.000000 0.000000 10.50000 0.01441 0.01147 = 0.01543 -0.00101 0.00000 0.00000 O1 1 0.343852 0.007182 0.285020 11.00000 0.01903 0.13538 = 0.04120 -0.01475 -0.00472 0.00151 O2 1 0.142979 0.016947 0.211051 11.00000 0.04331 0.03172 = 0.01911 -0.00008 -0.00689 0.00713 O3 1 0.150789 -0.066807 0.307057 11.00000 0.05840 0.02769 = 0.07019 0.01642 0.02159 0.00698 O4 1 0.142467 0.053367 0.340204 11.00000 0.02745 0.03986 = 0.02549 -0.00689 -0.00044 0.00303 O5 1 0.125543 0.204484 -0.018537 11.00000 0.02233 0.04146 = 0.06550 0.02710 0.00917 0.00427 O6 1 -0.103970 0.245753 -0.017361 11.00000 0.03578 0.01954 = 0.05674 0.00177 -0.00680 0.01199 O7 1 -0.060092 0.130669 -0.051533 11.00000 0.07834 0.02467 = 0.04669 -0.01311 -0.02148 0.00349 O8 1 -0.030627 0.165902 0.075601 11.00000 0.03781 0.05567 = 0.02743 0.02111 0.00796 0.01733 O9 1 0.249828 0.057954 -0.023360 11.00000 0.05260 0.02580 = 0.05508 -0.01460 0.02894 -0.02515 O10 1 0.078074 0.019897 0.063091 11.00000 0.02881 0.03135 = 0.01971 -0.00940 0.00477 -0.00666 CL1 4 0.290768 0.146892 0.134135 11.00000 0.02513 0.02369 = 0.02893 -0.00019 -0.00125 -0.00234 CL2 4 0.000000 0.178999 0.250000 10.50000 0.04549 0.02056 = 0.02245 0.00000 0.00779 0.00000 CL3 4 0.343302 0.161968 -0.148564 11.00000 0.05679 0.03269 = 0.03037 0.00398 -0.00200 0.00973 CL4 4 0.558268 0.105101 0.001088 11.00000 0.02286 0.02939 = 0.03750 -0.00057 -0.00064 0.00433 CL5 4 0.000000 -0.212707 0.250000 10.50000 0.04324 0.03225 = 0.04692 0.00000 0.01204 0.00000 HKLF 4 REM acmonidesite in C222(1) REM R1 = 0.0363 for 4614 Fo > 4sig(Fo) and 0.0476 for all 5336 data REM 214 parameters refined using 0 restraints END WGHT 0.0563 0.0000 REM Highest difference peak 1.444, deepest hole -0.857, 1-sigma level 0.157 Q1 1 0.2726 0.1452 -0.1441 11.00000 0.05 1.44 Q2 1 0.3570 0.1592 0.1443 11.00000 0.05 0.87 Q3 1 0.0700 -0.1077 0.2036 11.00000 0.05 0.86 Q4 1 0.1621 0.3111 0.1692 11.00000 0.05 0.78 Q5 1 -0.3359 0.1987 0.1700 11.00000 0.05 0.77 Q6 1 -0.3041 0.1860 0.1237 11.00000 0.05 0.74 Q7 1 -0.3156 0.1842 0.1786 11.00000 0.05 0.74 Q8 1 0.0000 -0.1825 0.2500 10.50000 0.05 0.73 Q9 1 0.0732 -0.1005 0.1127 11.00000 0.05 0.73 Q10 1 0.0025 -0.0911 0.1590 11.00000 0.05 0.72 Q11 1 0.1297 0.1087 0.1514 11.00000 0.05 0.70 Q12 1 0.1906 0.3167 0.1284 11.00000 0.05 0.70 Q13 1 0.3257 0.1618 0.0296 11.00000 0.05 0.69 Q14 1 0.0574 -0.0827 0.1549 11.00000 0.05 0.66 Q15 1 0.1421 -0.1006 0.1621 11.00000 0.05 0.66 Q16 1 0.0666 0.1024 0.1131 11.00000 0.05 0.65 Q17 1 0.1768 0.0043 0.2500 11.00000 0.05 0.65 Q18 1 0.0560 0.1014 0.1881 11.00000 0.05 0.64 Q19 1 0.0063 -0.0802 0.1399 11.00000 0.05 0.61 Q20 1 0.2859 0.1430 0.1653 11.00000 0.05 0.59 Q21 1 -0.0126 0.0998 0.1508 11.00000 0.05 0.57 Q22 1 0.5003 -0.0069 -0.1511 11.00000 0.05 0.57 Q23 1 0.4960 0.0059 -0.1377 11.00000 0.05 0.56 Q24 1 -0.0052 -0.2182 0.2167 11.00000 0.05 0.56 Q25 1 0.0760 0.3026 0.1625 11.00000 0.05 0.56 Q26 1 0.1346 0.3304 0.1071 11.00000 0.05 0.51 Q27 1 0.2443 0.3032 0.1424 11.00000 0.05 0.51 Q28 1 0.1333 -0.0757 0.1272 11.00000 0.05 0.50 Q29 1 -0.2233 0.1758 0.1460 11.00000 0.05 0.49 Q30 1 0.0796 0.0567 0.3462 11.00000 0.05 0.49 Q31 1 0.3411 0.0019 0.3214 11.00000 0.05 0.49 Q32 1 -0.1154 0.0000 0.0000 10.50000 0.05 0.48 Q33 1 0.3024 0.1306 -0.1787 11.00000 0.05 0.48 Q34 1 0.3305 0.1615 -0.0517 11.00000 0.05 0.48 Q35 1 0.2794 0.0157 0.2829 11.00000 0.05 0.48 Q36 1 0.2541 0.3623 0.1444 11.00000 0.05 0.47 Q37 1 0.3573 0.1077 0.1710 11.00000 0.05 0.47 Q38 1 0.2232 0.2601 0.1573 11.00000 0.05 0.47 Q39 1 0.0001 0.1756 0.2147 11.00000 0.05 0.47 Q40 1 0.1373 -0.0240 0.2111 11.00000 0.05 0.46 ; _shelx_res_checksum 64849 _shelx_hkl_file ; -1 -1 -26 25.18 6.14 -2 0 -26 29.38 6.26 -1 -3 -25 5.38 5.13 -1 -1 -25 10.55 5.25 -2 0 -25 9.62 5.11 0 0 -25 4.58 5.37 -3 1 -25 1.03 5.16 -1 1 -25 9.19 5.60 -2 2 -25 16.88 5.53 0 2 -25 3.36 5.38 -3 3 -25 2.06 5.53 -1 3 -25 8.32 5.43 1 3 -25 5.39 6.01 -2 4 -25 -3.31 5.40 0 4 -25 4.85 5.82 -1 -11 -24 2.95 4.72 0 -10 -24 16.76 4.81 1 -9 -24 9.80 4.80 3 -9 -24 32.09 5.21 2 -8 -24 35.80 4.91 3 -7 -24 14.07 4.37 4 -6 -24 7.11 4.38 -5 -5 -24 42.24 6.77 5 -5 -24 27.69 4.60 -1 -3 -24 14.61 5.03 -2 -2 -24 71.10 8.01 -1 -1 -24 4.81 4.89 -2 0 -24 -1.42 4.68 0 0 -24 58.88 6.07 -3 1 -24 13.57 5.05 -1 1 -24 0.81 5.02 -4 2 -24 20.80 5.79 -2 2 -24 49.55 5.86 0 2 -24 4.56 5.22 -3 3 -24 51.05 6.08 -1 3 -24 10.29 5.14 1 3 -24 10.66 5.48 -4 4 -24 -2.27 5.17 -2 4 -24 -1.54 5.17 0 4 -24 24.99 5.76 2 4 -24 2.18 5.66 -5 5 -24 21.11 6.03 -3 5 -24 3.46 5.44 -1 5 -24 81.62 8.91 1 5 -24 86.97 9.19 -4 6 -24 3.12 5.72 -2 6 -24 8.84 5.72 0 6 -24 106.94 9.22 2 6 -24 6.14 5.87 -3 7 -24 9.66 6.02 -1 7 -24 9.40 5.78 1 7 -24 3.73 5.82 -2 -12 -23 4.83 4.75 0 -12 -23 13.98 4.94 -1 -11 -23 25.47 5.09 1 -11 -23 28.91 5.24 -2 -10 -23 29.63 4.92 0 -10 -23 13.80 4.72 2 -10 -23 30.02 5.11 -1 -9 -23 23.70 4.74 1 -9 -23 23.70 4.87 3 -9 -23 12.50 4.59 0 -8 -23 106.77 6.96 2 -8 -23 12.98 4.39 4 -8 -23 1.06 4.13 -5 -7 -23 11.09 6.41 1 -7 -23 49.65 5.06 3 -7 -23 27.92 4.44 5 -7 -23 4.41 4.28 2 -6 -23 3.33 4.09 4 -6 -23 27.80 4.68 -5 -5 -23 39.22 6.16 3 -5 -23 123.22 6.62 5 -5 -23 36.12 4.63 -6 -4 -23 2.46 5.62 4 -4 -23 1.12 3.76 6 -4 -23 -3.03 3.95 5 -3 -23 10.59 4.11 -2 -2 -23 15.36 4.66 -3 -1 -23 42.15 5.20 -1 -1 -23 10.53 4.75 -2 0 -23 55.58 5.57 -3 1 -23 47.67 5.38 -1 1 -23 10.07 4.80 -4 2 -23 5.45 4.80 -2 2 -23 10.21 4.70 0 2 -23 3.45 4.90 -3 3 -23 58.95 5.96 -1 3 -23 34.49 5.57 1 3 -23 31.36 5.74 -4 4 -23 1.85 5.02 -2 4 -23 32.73 5.59 0 4 -23 59.74 6.25 -5 5 -23 37.80 6.07 -3 5 -23 144.17 9.02 -1 5 -23 5.61 5.11 1 5 -23 9.92 5.44 -4 6 -23 19.80 5.67 -2 6 -23 5.63 5.37 0 6 -23 35.25 5.91 2 6 -23 6.61 5.53 -5 7 -23 -5.55 5.37 -3 7 -23 24.56 5.86 -1 7 -23 51.89 6.33 1 7 -23 55.20 6.62 3 7 -23 37.01 6.36 -4 8 -23 -2.10 5.75 -2 8 -23 19.61 5.95 0 8 -23 126.39 9.92 2 8 -23 23.32 6.00 -3 9 -23 0.61 5.79 -1 9 -23 22.97 6.33 1 9 -23 32.95 6.39 -2 10 -23 35.82 6.67 0 10 -23 10.60 6.02 -1 -13 -22 4.87 4.72 1 -13 -22 1.02 4.76 0 -12 -22 1.55 4.66 2 -12 -22 -3.82 4.71 -1 -11 -22 20.87 4.70 1 -11 -22 27.08 4.97 3 -11 -22 2.58 4.52 0 -10 -22 15.11 4.54 2 -10 -22 10.30 4.63 4 -10 -22 2.46 4.27 -5 -9 -22 34.58 6.76 -1 -9 -22 40.73 4.85 1 -9 -22 41.45 5.08 3 -9 -22 31.61 4.72 5 -9 -22 32.98 5.08 -6 -8 -22 -0.65 6.08 -2 -8 -22 6.52 4.12 0 -8 -22 1.98 4.06 2 -8 -22 11.34 4.36 4 -8 -22 42.38 4.91 -5 -7 -22 7.18 5.88 -1 -7 -22 17.63 4.27 1 -7 -22 18.55 4.48 3 -7 -22 6.73 4.07 5 -7 -22 4.73 4.25 -6 -6 -22 3.11 5.86 -4 -6 -22 7.80 5.75 0 -6 -22 93.29 6.41 2 -6 -22 7.75 3.84 4 -6 -22 -0.95 3.83 6 -6 -22 1.06 4.05 -5 -5 -22 24.16 5.59 1 -5 -22 64.52 6.17 3 -5 -22 2.39 3.68 5 -5 -22 11.55 3.97 -6 -4 -22 16.93 5.97 -2 -4 -22 24.64 4.46 2 -4 -22 26.82 4.02 4 -4 -22 28.69 4.23 6 -4 -22 15.85 4.20 3 -3 -22 26.08 4.15 5 -3 -22 15.33 3.89 7 -3 -22 1.60 4.18 -2 -2 -22 67.44 6.83 4 -2 -22 -2.23 3.61 6 -2 -22 20.21 4.11 -3 -1 -22 8.88 4.32 -1 -1 -22 104.17 7.37 7 -1 -22 54.56 6.66 -2 0 -22 25.78 4.80 -3 1 -22 11.44 4.45 -1 1 -22 108.38 7.49 -4 2 -22 -2.19 4.42 -2 2 -22 69.04 7.11 0 2 -22 14.41 4.79 -5 3 -22 12.86 5.02 -3 3 -22 29.86 5.18 -1 3 -22 1.10 4.66 -4 4 -22 29.73 5.29 -2 4 -22 30.75 5.17 0 4 -22 11.84 4.87 -5 5 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1 -15 2 332.82 6.38 3 -15 2 8.27 1.70 5 -15 2 27.61 3.57 7 -15 2 19.05 3.43 -12 -14 2 31.69 5.09 -10 -14 2 10.21 4.33 -8 -14 2 34.73 4.49 -6 -14 2 5.40 3.54 -4 -14 2 68.54 5.53 -2 -14 2 97.22 4.98 0 -14 2 8.75 2.78 2 -14 2 98.10 4.63 4 -14 2 51.73 2.58 6 -14 2 7.87 2.91 -11 -13 2 25.02 4.49 -9 -13 2 16.84 4.05 -7 -13 2 30.90 3.87 -5 -13 2 209.86 6.53 -3 -13 2 46.58 4.56 -1 -13 2 40.25 3.89 1 -13 2 38.16 3.90 3 -13 2 64.46 2.40 5 -13 2 165.26 5.37 7 -13 2 42.73 4.65 -12 -12 2 30.85 5.10 -10 -12 2 23.50 4.20 -8 -12 2 8.63 3.54 -6 -12 2 124.93 5.72 -4 -12 2 38.14 3.44 -2 -12 2 14.65 2.65 0 -12 2 21.11 2.61 2 -12 2 8.70 2.45 4 -12 2 26.09 1.65 6 -12 2 136.35 3.12 8 -12 2 7.55 3.08 -11 -11 2 10.59 3.93 -9 -11 2 52.87 5.45 -7 -11 2 217.51 6.30 -5 -11 2 100.95 4.79 -1 -11 2 19.78 2.45 1 -11 2 15.76 2.28 3 -11 2 3.90 1.24 5 -11 2 92.40 2.57 7 -11 2 227.25 3.69 -10 -10 2 17.69 3.72 -8 -10 2 80.34 5.43 -6 -10 2 1.05 2.68 -2 -10 2 86.78 3.77 0 -10 2 409.14 5.09 2 -10 2 90.40 1.90 4 -10 2 16.89 1.38 6 -10 2 0.87 1.62 8 -10 2 78.14 3.30 -11 -9 2 20.71 3.76 -9 -9 2 35.87 3.66 -7 -9 2 223.00 5.86 -3 -9 2 632.85 6.38 -1 -9 2 137.10 3.65 1 -9 2 141.38 3.57 3 -9 2 642.50 13.99 5 -9 2 24.73 1.81 7 -9 2 237.61 3.63 9 -9 2 32.35 3.76 -10 -8 2 60.98 5.25 -8 -8 2 8.49 2.75 -6 -8 2 124.66 2.52 -4 -8 2 79.11 3.64 -2 -8 2 132.33 3.60 0 -8 2 7.31 1.73 2 -8 2 99.18 2.04 4 -8 2 98.65 1.99 6 -8 2 112.25 2.70 8 -8 2 1.55 1.83 10 -8 2 63.39 5.85 -11 -7 2 14.90 3.29 -9 -7 2 78.82 4.71 -7 -7 2 56.00 2.30 -5 -7 2 69.49 1.95 -3 -7 2 229.51 3.99 -1 -7 2 74.75 2.86 1 -7 2 68.56 2.69 3 -7 2 178.77 3.61 5 -7 2 80.82 2.17 7 -7 2 60.48 2.78 9 -7 2 75.68 3.47 11 -7 2 2.69 3.92 -10 -6 2 14.96 3.11 -8 -6 2 112.08 4.77 -6 -6 2 108.77 2.33 -4 -6 2 18.85 1.36 -2 -6 2 78.52 2.83 0 -6 2 191.75 3.15 2 -6 2 58.90 1.67 4 -6 2 22.12 1.58 6 -6 2 117.00 2.63 8 -6 2 100.10 3.27 10 -6 2 9.98 3.64 12 -6 2 93.78 7.58 -9 -5 2 136.86 5.00 -7 -5 2 47.36 2.29 -5 -5 2 230.88 2.46 -3 -5 2 170.34 1.98 -1 -5 2 1117.93 5.71 1 -5 2 1089.09 5.35 3 -5 2 177.67 1.88 5 -5 2 236.10 2.68 7 -5 2 43.71 2.66 9 -5 2 124.49 3.70 11 -5 2 35.95 4.58 13 -5 2 32.42 5.60 -8 -4 2 36.36 2.51 -6 -4 2 322.66 3.07 -4 -4 2 57.42 1.60 -2 -4 2 48.23 1.43 0 -4 2 239.25 2.80 2 -4 2 55.58 1.23 4 -4 2 51.49 1.73 6 -4 2 314.02 3.36 8 -4 2 25.69 2.15 10 -4 2 6.63 3.51 12 -4 2 5.66 4.19 -9 -3 2 226.09 3.51 -7 -3 2 41.28 2.26 -5 -3 2 8.06 1.07 -3 -3 2 104.87 1.63 -1 -3 2 69.48 1.30 1 -3 2 77.57 1.90 3 -3 2 79.48 1.62 5 -3 2 12.50 1.29 7 -3 2 42.50 2.65 9 -3 2 293.92 6.94 11 -3 2 43.94 4.68 13 -3 2 43.41 5.66 -8 -2 2 157.74 2.97 -6 -2 2 53.96 1.97 -4 -2 2 251.65 2.33 -2 -2 2 17.47 1.15 0 -2 2 694.59 2.98 2 -2 2 28.53 1.24 4 -2 2 299.57 2.62 6 -2 2 50.23 2.35 8 -2 2 189.97 5.74 10 -2 2 15.18 3.80 12 -2 2 16.92 4.83 14 -2 2 8.01 5.11 -9 -1 2 39.32 2.61 -7 -1 2 123.72 2.63 -5 -1 2 53.17 1.79 -3 -1 2 136.34 1.74 -1 -1 2 370.45 2.38 1 -1 2 335.33 2.56 3 -1 2 134.11 1.93 5 -1 2 56.52 2.11 7 -1 2 127.76 4.83 9 -1 2 33.69 3.80 13 -1 2 18.75 5.12 -10 0 2 24.14 2.88 -8 0 2 6.57 1.53 -6 0 2 25.04 1.83 -4 0 2 1.38 0.88 -2 0 2 18.71 1.87 0 0 2 157.49 12.66 2 0 2 14.83 1.03 4 0 2 1.62 1.09 6 0 2 21.84 2.50 8 0 2 1.66 2.89 10 0 2 24.77 4.20 14 0 2 82.56 8.81 -11 1 2 16.05 3.13 -9 1 2 33.44 4.11 -7 1 2 119.12 2.63 -5 1 2 56.10 1.73 -3 1 2 144.10 3.04 -1 1 2 398.12 2.68 1 1 2 352.15 2.19 3 1 2 123.72 2.04 5 1 2 59.53 3.37 7 1 2 131.39 4.81 9 1 2 50.15 5.69 13 1 2 16.93 4.90 -10 2 2 14.56 2.95 -8 2 2 152.04 3.12 -6 2 2 44.74 1.94 -4 2 2 333.31 4.30 -2 2 2 31.12 2.29 0 2 2 791.22 8.95 2 2 2 15.96 1.41 4 2 2 247.60 4.15 6 2 2 50.65 3.98 8 2 2 171.58 6.01 10 2 2 7.12 3.80 12 2 2 15.27 4.55 14 2 2 6.21 5.52 -11 3 2 37.83 3.70 -9 3 2 252.75 5.98 -7 3 2 36.96 2.15 -5 3 2 9.89 1.97 -3 3 2 88.95 3.07 -1 3 2 93.55 2.30 1 3 2 64.10 1.80 3 3 2 99.87 3.10 5 3 2 8.10 2.12 7 3 2 46.78 4.54 9 3 2 266.60 7.16 11 3 2 57.24 6.45 13 3 2 50.29 6.06 -12 4 2 7.05 3.50 -8 4 2 31.80 3.26 -6 4 2 303.43 5.32 -4 4 2 48.95 3.14 -2 4 2 56.72 2.77 0 4 2 277.20 2.62 2 4 2 55.11 2.48 4 4 2 51.54 3.23 6 4 2 322.31 5.64 8 4 2 32.11 3.62 10 4 2 6.27 3.71 12 4 2 5.47 4.75 -11 5 2 32.88 3.93 -9 5 2 117.18 5.39 -7 5 2 37.93 3.20 -5 5 2 260.82 4.81 -3 5 2 183.36 3.72 -1 5 2 1227.95 5.61 1 5 2 1210.30 5.46 3 5 2 177.72 3.56 5 5 2 239.27 4.97 7 5 2 53.67 4.87 9 5 2 137.89 6.51 11 5 2 40.32 5.05 13 5 2 36.23 5.78 -12 6 2 83.25 6.45 -10 6 2 10.92 3.44 -8 6 2 82.50 5.03 -6 6 2 99.70 4.65 -4 6 2 30.93 2.45 -2 6 2 69.92 3.18 0 6 2 203.31 2.76 2 6 2 90.67 2.94 4 6 2 17.25 2.21 6 6 2 121.54 5.04 8 6 2 102.04 5.81 10 6 2 19.80 4.39 12 6 2 83.79 7.90 -13 7 2 25.53 4.15 -11 7 2 10.19 3.63 -9 7 2 71.46 5.42 -7 7 2 41.66 4.83 -5 7 2 79.25 4.13 -3 7 2 219.05 4.46 -1 7 2 81.49 1.93 1 7 2 87.56 1.75 3 7 2 252.73 4.33 5 7 2 69.12 4.09 7 7 2 63.89 5.19 9 7 2 84.66 6.53 11 7 2 16.85 4.73 13 7 2 26.71 5.83 -12 8 2 9.86 3.89 -10 8 2 59.19 5.78 -8 8 2 -2.24 2.97 -6 8 2 102.03 4.95 -4 8 2 110.85 4.25 -2 8 2 125.78 3.85 0 8 2 6.99 1.09 2 8 2 126.82 3.37 4 8 2 94.29 4.07 6 8 2 118.56 5.24 8 8 2 7.18 3.52 10 8 2 80.83 7.19 12 8 2 6.48 4.98 -13 9 2 7.51 4.17 -9 9 2 32.10 3.90 -7 9 2 216.23 6.24 -5 9 2 32.04 3.14 -3 9 2 692.72 6.95 -1 9 2 146.90 2.44 1 9 2 148.99 2.24 3 9 2 692.88 6.65 5 9 2 25.70 3.24 7 9 2 241.83 6.91 9 9 2 42.69 4.75 11 9 2 34.13 5.41 -12 10 2 13.97 4.25 -10 10 2 24.36 4.17 -8 10 2 72.29 5.79 -6 10 2 -1.46 2.80 -4 10 2 23.35 3.04 -2 10 2 102.25 4.15 0 10 2 436.03 4.41 2 10 2 93.09 3.59 4 10 2 16.07 2.72 6 10 2 2.10 3.28 8 10 2 86.65 6.38 12 10 2 11.49 5.27 -13 11 2 9.81 4.36 -11 11 2 8.93 4.15 -9 11 2 54.74 6.16 -7 11 2 233.87 6.69 -5 11 2 100.82 5.40 -3 11 2 5.06 2.70 -1 11 2 14.33 1.52 1 11 2 24.74 1.67 3 11 2 16.05 2.56 5 11 2 87.74 5.13 7 11 2 264.92 7.77 9 11 2 57.11 6.91 11 11 2 10.66 5.13 -12 12 2 28.17 4.84 -10 12 2 26.20 4.34 -8 12 2 5.39 3.71 -6 12 2 129.01 5.92 -4 12 2 28.82 3.50 -2 12 2 5.72 1.61 0 12 2 18.92 1.65 2 12 2 11.51 2.42 4 12 2 34.71 3.43 6 12 2 142.56 6.27 8 12 2 2.40 4.00 10 12 2 34.02 5.81 12 12 2 41.00 6.59 -11 13 2 35.88 4.92 -9 13 2 27.36 4.39 -7 13 2 33.99 4.14 -5 13 2 186.76 6.59 -3 13 2 55.52 5.13 -1 13 2 38.31 2.34 1 13 2 41.99 2.21 3 13 2 54.24 4.43 5 13 2 209.48 6.73 9 13 2 21.05 5.04 11 13 2 30.08 5.93 -10 14 2 12.04 4.58 -8 14 2 28.54 4.51 -6 14 2 5.35 3.54 -4 14 2 55.87 5.80 -2 14 2 99.95 3.70 0 14 2 7.10 2.03 2 14 2 95.72 4.59 4 14 2 61.11 5.37 6 14 2 5.22 3.82 8 14 2 37.66 5.06 10 14 2 20.88 5.42 -11 15 2 11.75 4.82 -9 15 2 85.05 7.32 -7 15 2 12.63 4.21 -5 15 2 24.34 4.10 -3 15 2 1.20 3.66 -1 15 2 330.07 4.20 1 15 2 348.83 4.17 3 15 2 12.28 3.32 5 15 2 34.26 4.26 7 15 2 15.35 4.72 9 15 2 105.72 8.35 11 15 2 2.55 5.56 -10 16 2 16.78 5.00 -8 16 2 61.56 7.23 -6 16 2 39.94 4.67 -4 16 2 144.47 7.15 -2 16 2 162.21 3.84 0 16 2 0.13 2.02 2 16 2 194.25 5.67 6 16 2 39.01 4.93 8 16 2 47.38 5.84 10 16 2 12.86 5.95 -9 17 2 17.75 5.08 -7 17 2 29.18 4.91 -5 17 2 8.78 4.27 -3 17 2 46.23 4.64 -1 17 2 65.79 3.57 1 17 2 78.57 3.51 3 17 2 52.70 5.79 5 17 2 15.16 4.41 7 17 2 24.96 5.21 9 17 2 24.89 6.00 -10 18 2 25.14 5.58 -8 18 2 35.33 5.70 -6 18 2 9.13 4.58 -4 18 2 8.57 4.43 -2 18 2 82.08 6.33 0 18 2 4.92 2.27 2 18 2 79.03 5.62 4 18 2 13.19 4.22 6 18 2 12.15 4.97 8 18 2 46.01 6.33 10 18 2 26.66 6.57 -9 19 2 16.20 5.44 -7 19 2 44.43 5.91 -5 19 2 34.47 5.14 -3 19 2 6.06 4.45 -1 19 2 306.24 4.88 1 19 2 316.73 6.77 3 19 2 4.83 3.95 5 19 2 53.64 5.65 7 19 2 55.32 6.50 9 19 2 16.91 6.22 -8 20 2 5.19 5.61 -6 20 2 71.30 8.27 -4 20 2 64.08 7.62 -2 20 2 8.36 4.49 0 20 2 17.23 3.79 2 20 2 16.54 4.04 4 20 2 93.51 7.59 6 20 2 63.91 6.52 8 20 2 6.79 6.19 -7 21 2 61.87 6.85 -5 21 2 43.53 5.90 -3 21 2 30.43 5.14 -1 21 2 23.90 2.91 1 21 2 16.92 4.07 3 21 2 37.33 5.06 5 21 2 38.53 5.82 7 21 2 69.83 7.38 9 21 2 7.39 6.56 -8 22 2 44.76 6.92 -6 22 2 9.67 5.77 -4 22 2 12.67 5.32 -2 22 2 47.83 5.48 0 22 2 19.26 4.16 2 22 2 43.62 4.99 4 22 2 8.58 5.03 6 22 2 1.32 5.70 8 22 2 57.14 7.72 -7 23 2 18.64 6.41 -5 23 2 11.04 5.86 -3 23 2 33.76 5.65 1 23 2 15.22 4.55 3 23 2 37.32 5.56 5 23 2 10.42 5.82 7 23 2 11.10 6.39 -6 24 2 20.53 6.62 -4 24 2 84.27 8.97 2 24 2 18.83 5.48 4 24 2 72.95 8.78 6 24 2 9.42 6.48 -5 25 2 50.74 7.42 5 25 2 38.64 7.01 -4 26 2 14.20 6.58 -1 -27 3 1.20 5.94 1 -27 3 -0.53 5.36 3 -27 3 0.10 5.42 -2 -26 3 23.71 6.28 0 -26 3 4.72 5.55 2 -26 3 24.55 5.78 -5 -25 3 18.09 6.19 -3 -25 3 51.26 6.81 -1 -25 3 72.61 8.61 1 -25 3 72.84 8.15 3 -25 3 46.24 5.94 -6 -24 3 1.50 5.92 -4 -24 3 43.37 6.43 -2 -24 3 64.79 6.49 0 -24 3 0.21 5.12 2 -24 3 68.20 7.65 4 -24 3 45.63 5.72 -7 -23 3 5.69 5.86 -5 -23 3 31.97 6.09 -3 -23 3 20.97 5.87 -1 -23 3 15.61 5.21 1 -23 3 9.74 4.78 3 -23 3 19.36 4.78 -6 -22 3 1.63 5.35 -4 -22 3 65.08 7.90 -2 -22 3 13.49 4.93 0 -22 3 2.24 4.55 2 -22 3 15.01 4.52 4 -22 3 61.91 6.64 -7 -21 3 7.30 5.23 -5 -21 3 146.30 8.80 -3 -21 3 95.94 7.38 -1 -21 3 20.97 4.68 1 -21 3 28.69 4.58 3 -21 3 101.63 6.61 5 -21 3 138.21 7.25 -8 -20 3 8.38 5.12 -6 -20 3 1.18 4.74 -4 -20 3 98.36 7.19 -2 -20 3 63.74 6.71 0 -20 3 4.22 4.04 2 -20 3 80.20 6.34 4 -20 3 105.41 6.56 6 -20 3 3.53 4.36 -9 -19 3 55.59 6.07 -7 -19 3 30.05 5.23 -5 -19 3 275.14 8.84 -3 -19 3 253.29 7.90 -1 -19 3 2.92 3.87 1 -19 3 -0.37 3.85 3 -19 3 237.39 6.95 5 -19 3 282.42 7.54 -10 -18 3 11.59 5.06 -8 -18 3 39.44 5.33 -6 -18 3 4.21 4.25 -4 -18 3 36.79 4.60 -2 -18 3 17.97 3.88 0 -18 3 50.89 5.80 2 -18 3 14.11 3.72 4 -18 3 31.33 4.17 6 -18 3 5.20 3.73 -11 -17 3 -2.08 4.81 -9 -17 3 -0.17 4.53 -7 -17 3 5.74 4.14 -5 -17 3 20.16 4.26 -3 -17 3 45.93 5.67 -1 -17 3 77.33 5.62 1 -17 3 78.82 5.45 3 -17 3 51.36 5.10 5 -17 3 15.89 3.79 7 -17 3 2.05 3.82 -10 -16 3 194.73 8.48 -8 -16 3 -1.73 4.05 -6 -16 3 15.15 4.08 -4 -16 3 14.96 3.78 -2 -16 3 212.51 6.33 0 -16 3 15.40 3.46 2 -16 3 229.86 6.27 4 -16 3 12.68 3.45 6 -16 3 12.83 3.53 -11 -15 3 72.90 7.43 -9 -15 3 9.09 4.16 -7 -15 3 8.18 4.00 -5 -15 3 110.94 6.20 -3 -15 3 507.32 8.19 -1 -15 3 260.88 6.13 1 -15 3 271.43 6.28 3 -15 3 463.68 6.97 5 -15 3 122.35 5.52 7 -15 3 11.86 3.54 -10 -14 3 9.48 4.25 -8 -14 3 46.78 4.59 -6 -14 3 149.25 6.54 -4 -14 3 100.20 5.48 -2 -14 3 556.18 7.64 0 -14 3 2.69 2.77 2 -14 3 530.99 7.08 4 -14 3 80.47 4.65 6 -14 3 153.90 5.34 -11 -13 3 44.91 4.98 -9 -13 3 18.32 4.07 -7 -13 3 147.96 6.46 -5 -13 3 18.52 3.51 -3 -13 3 125.16 5.17 -1 -13 3 67.95 4.10 1 -13 3 65.38 4.29 3 -13 3 114.59 2.66 5 -13 3 19.82 3.17 7 -13 3 157.35 5.64 -10 -12 3 9.02 3.76 -8 -12 3 9.46 3.33 -6 -12 3 27.82 3.58 -4 -12 3 11.42 2.88 -2 -12 3 36.56 3.77 0 -12 3 31.79 3.57 2 -12 3 37.08 1.88 4 -12 3 9.07 1.43 6 -12 3 20.07 2.96 8 -12 3 8.79 3.21 -11 -11 3 79.56 6.18 -9 -11 3 17.11 3.63 -5 -11 3 482.30 7.24 -3 -11 3 1034.19 8.71 -1 -11 3 16.19 2.42 1 -11 3 20.28 2.47 3 -11 3 979.55 12.65 5 -11 3 439.34 6.45 7 -11 3 15.35 3.08 -10 -10 3 6.85 3.34 -8 -10 3 66.92 5.18 -6 -10 3 74.55 4.70 -4 -10 3 327.37 5.64 -2 -10 3 118.61 3.90 0 -10 3 5.19 2.03 2 -10 3 125.52 3.63 4 -10 3 325.95 8.70 6 -10 3 50.64 2.69 8 -10 3 50.12 4.67 -11 -9 3 217.83 7.14 -9 -9 3 140.26 5.53 -7 -9 3 26.72 3.07 -5 -9 3 436.10 6.05 -3 -9 3 1004.87 7.70 -1 -9 3 511.01 5.41 1 -9 3 528.58 5.49 3 -9 3 958.87 10.01 5 -9 3 439.89 4.54 7 -9 3 29.40 2.07 9 -9 3 145.72 3.99 -10 -8 3 7.55 3.06 -8 -8 3 10.73 2.80 -6 -8 3 333.31 3.38 -4 -8 3 111.18 2.33 -2 -8 3 67.97 3.15 0 -8 3 43.07 2.82 2 -8 3 55.65 2.79 4 -8 3 100.15 2.03 6 -8 3 323.34 3.60 8 -8 3 8.97 2.01 10 -8 3 6.30 3.75 -9 -7 3 22.04 3.06 -7 -7 3 137.11 2.81 -5 -7 3 23.52 1.62 -3 -7 3 33.53 2.84 -1 -7 3 60.45 2.73 1 -7 3 50.37 2.64 3 -7 3 33.71 1.43 5 -7 3 25.54 1.97 7 -7 3 125.30 3.25 9 -7 3 23.37 2.32 -10 -6 3 36.50 3.36 -8 -6 3 226.61 5.28 -6 -6 3 41.38 2.05 -4 -6 3 844.74 4.34 -2 -6 3 393.10 4.29 0 -6 3 -0.27 1.48 2 -6 3 361.37 4.01 4 -6 3 804.49 5.35 6 -6 3 37.18 2.34 8 -6 3 251.15 4.00 10 -6 3 42.66 3.19 -9 -5 3 328.33 5.89 -7 -5 3 96.09 2.98 -5 -5 3 410.35 3.83 -3 -5 3 1127.71 4.19 -1 -5 3 1434.64 6.47 1 -5 3 1397.17 6.36 3 -5 3 1056.77 8.04 5 -5 3 411.38 3.68 7 -5 3 92.99 2.97 9 -5 3 369.99 4.81 11 -5 3 190.78 7.37 -8 -4 3 0.93 1.44 -6 -4 3 132.06 2.45 -4 -4 3 505.09 3.04 -2 -4 3 716.45 3.67 0 -4 3 9.53 1.40 2 -4 3 661.80 4.49 4 -4 3 552.61 3.27 6 -4 3 144.03 2.78 8 -4 3 -0.20 1.81 10 -4 3 323.78 7.67 12 -4 3 10.08 4.65 -7 -3 3 -0.50 1.29 -5 -3 3 298.91 3.12 -3 -3 3 164.89 1.93 -1 -3 3 145.92 1.69 1 -3 3 116.60 2.25 3 -3 3 156.29 1.89 5 -3 3 322.89 3.10 7 -3 3 1.66 1.64 9 -3 3 14.08 3.40 11 -3 3 7.81 4.09 13 -3 3 25.16 5.15 -8 -2 3 24.44 1.94 -6 -2 3 54.41 2.00 -4 -2 3 96.92 1.79 -2 -2 3 235.15 1.87 0 -2 3 2.13 0.90 2 -2 3 210.14 1.76 4 -2 3 108.83 2.09 6 -2 3 60.81 2.45 8 -2 3 34.42 2.36 10 -2 3 6.74 3.59 12 -2 3 56.98 7.07 14 -2 3 12.05 5.31 -9 -1 3 70.44 4.06 -7 -1 3 20.34 1.53 -5 -1 3 1823.16 16.66 -3 -1 3 2411.93 24.79 -1 -1 3 19.38 0.90 1 -1 3 22.33 0.77 3 -1 3 2297.81 11.40 5 -1 3 1908.56 6.55 7 -1 3 18.83 1.90 9 -1 3 83.79 5.58 11 -1 3 74.05 6.78 13 -1 3 103.73 7.77 -10 0 3 178.21 5.26 -8 0 3 1.64 1.39 -6 0 3 166.10 2.87 -4 0 3 564.56 3.04 -2 0 3 444.56 3.52 0 0 3 7.23 0.40 2 0 3 416.86 2.32 4 0 3 578.28 3.60 6 0 3 179.54 3.07 8 0 3 4.22 3.01 10 0 3 200.16 7.08 12 0 3 20.45 4.56 14 0 3 27.56 5.66 -11 1 3 49.67 4.75 -9 1 3 84.78 4.62 -7 1 3 19.70 1.44 -5 1 3 1742.56 30.29 -3 1 3 2569.54 10.11 -1 1 3 22.37 1.49 1 1 3 19.03 0.77 3 1 3 2329.41 6.65 5 1 3 1897.50 9.74 7 1 3 22.30 2.97 9 1 3 78.68 5.57 11 1 3 65.83 6.62 13 1 3 113.25 8.46 -10 2 3 2.67 2.81 -8 2 3 29.43 3.00 -6 2 3 59.86 3.59 -4 2 3 108.35 3.23 -2 2 3 230.49 3.22 0 2 3 2.53 0.59 2 2 3 212.41 2.11 4 2 3 111.96 3.34 6 2 3 51.50 3.90 8 2 3 26.93 3.52 10 2 3 7.35 3.52 12 2 3 52.23 5.52 -11 3 3 4.19 3.04 -7 3 3 1.99 1.19 -5 3 3 327.01 4.85 -3 3 3 179.10 3.36 -1 3 3 141.33 2.58 1 3 3 127.49 1.23 3 3 3 159.63 3.30 5 3 3 292.15 4.90 7 3 3 -1.78 2.42 9 3 3 21.52 3.56 11 3 3 10.79 4.36 13 3 3 29.45 5.57 -12 4 3 8.46 3.45 -10 4 3 289.42 6.81 -8 4 3 -0.73 2.59 -6 4 3 134.59 4.48 -4 4 3 574.53 5.54 -2 4 3 777.63 5.28 0 4 3 9.08 0.87 2 4 3 717.03 4.86 4 4 3 538.62 5.56 6 4 3 150.64 4.86 8 4 3 2.21 3.03 10 4 3 321.30 8.42 12 4 3 8.44 4.72 -11 5 3 162.21 6.28 -9 5 3 340.90 6.90 -7 5 3 88.27 4.64 -5 5 3 420.30 5.50 -3 5 3 1229.24 7.35 -1 5 3 1579.95 4.58 1 5 3 1434.66 3.62 3 5 3 1142.65 7.01 5 5 3 435.09 5.93 7 5 3 100.51 5.29 9 5 3 390.84 8.29 11 5 3 190.34 8.14 13 5 3 61.90 6.49 -12 6 3 96.31 6.27 -10 6 3 38.02 3.93 -8 6 3 234.56 6.12 -6 6 3 32.45 3.90 -4 6 3 896.29 7.22 -2 6 3 409.91 4.56 0 6 3 0.97 0.93 2 6 3 386.18 4.25 4 6 3 860.61 7.14 6 6 3 45.03 4.43 8 6 3 270.62 6.97 10 6 3 47.63 4.88 12 6 3 121.07 8.51 -13 7 3 38.97 4.54 -11 7 3 21.16 3.91 -9 7 3 24.92 3.59 -7 7 3 120.44 5.10 -5 7 3 25.60 2.63 -3 7 3 33.98 3.15 -1 7 3 59.77 1.89 1 7 3 62.91 1.62 3 7 3 40.49 3.16 5 7 3 25.01 2.72 7 7 3 136.85 5.69 9 7 3 25.97 4.25 11 7 3 23.20 4.93 13 7 3 44.95 6.29 -12 8 3 33.41 4.47 -10 8 3 5.82 3.43 -8 8 3 10.24 3.01 -6 8 3 326.64 6.18 -4 8 3 108.96 4.13 -2 8 3 58.91 3.34 0 8 3 47.60 1.81 2 8 3 76.48 3.21 4 8 3 107.35 4.14 6 8 3 345.64 6.59 8 8 3 9.55 3.56 10 8 3 10.44 4.43 12 8 3 39.99 5.84 -13 9 3 12.16 4.05 -11 9 3 222.08 7.42 -9 9 3 142.55 6.29 -7 9 3 24.05 3.30 -5 9 3 454.25 6.62 -3 9 3 1094.70 8.17 -1 9 3 550.40 3.64 1 9 3 536.48 5.02 3 9 3 1088.88 8.04 5 9 3 489.46 7.15 9 9 3 160.90 7.42 11 9 3 259.63 9.36 -12 10 3 30.51 4.51 -10 10 3 4.42 3.66 -8 10 3 48.91 5.38 -6 10 3 54.24 5.01 -4 10 3 372.54 6.16 -2 10 3 130.12 4.23 0 10 3 4.59 1.25 2 10 3 128.47 3.83 4 10 3 364.85 6.19 6 10 3 60.18 5.31 8 10 3 62.73 6.40 10 10 3 8.30 4.54 12 10 3 48.55 6.40 -11 11 3 84.04 6.90 -9 11 3 10.15 3.61 -7 11 3 8.86 3.16 -5 11 3 484.60 7.49 -3 11 3 1107.81 9.03 -1 11 3 20.53 1.60 1 11 3 16.98 1.40 3 11 3 1133.59 9.08 5 11 3 525.50 7.94 9 11 3 17.00 4.75 11 11 3 103.08 9.09 -12 12 3 7.28 4.23 -10 12 3 15.30 4.15 -8 12 3 5.06 3.54 -6 12 3 22.79 3.45 -4 12 3 13.50 2.99 -2 12 3 52.47 2.80 0 12 3 35.08 2.33 2 12 3 47.92 3.83 4 12 3 13.84 3.03 6 12 3 21.08 3.85 8 12 3 10.41 4.21 10 12 3 21.46 5.07 12 12 3 12.77 5.66 -11 13 3 33.86 5.07 -9 13 3 15.20 4.04 -7 13 3 156.34 6.78 -5 13 3 17.31 3.54 -3 13 3 120.39 5.49 -1 13 3 62.54 2.84 1 13 3 77.64 2.68 3 13 3 134.25 5.13 5 13 3 17.25 3.65 7 13 3 155.62 7.32 9 13 3 35.84 5.16 11 13 3 48.72 6.11 -10 14 3 16.83 4.58 -8 14 3 36.12 4.60 -6 14 3 163.20 6.77 -4 14 3 79.05 5.82 -2 14 3 531.37 4.82 0 14 3 3.78 1.75 2 14 3 566.25 7.13 4 14 3 109.02 5.74 6 14 3 154.80 7.08 8 14 3 48.17 5.48 10 14 3 14.28 5.41 -11 15 3 75.11 7.77 -9 15 3 10.47 4.44 -7 15 3 10.72 4.12 -5 15 3 117.10 6.30 -3 15 3 477.83 7.95 -1 15 3 261.98 4.14 1 15 3 272.74 3.84 3 15 3 530.11 7.75 5 15 3 124.07 6.52 7 15 3 8.99 4.57 9 15 3 15.26 5.37 11 15 3 81.69 9.35 -10 16 3 190.22 8.64 -8 16 3 4.30 4.15 -6 16 3 12.23 4.01 -4 16 3 3.19 3.58 -2 16 3 223.33 4.08 0 16 3 12.62 2.12 2 16 3 245.32 6.13 4 16 3 13.09 3.87 6 16 3 14.11 4.37 8 16 3 3.17 4.95 10 16 3 216.12 10.32 -9 17 3 9.66 4.70 -7 17 3 4.04 4.36 -5 17 3 18.19 4.30 -3 17 3 44.03 4.40 -1 17 3 77.08 3.52 1 17 3 83.08 5.03 3 17 3 52.40 5.69 5 17 3 17.81 4.47 7 17 3 3.49 4.75 9 17 3 5.08 5.49 -10 18 3 15.68 5.35 -8 18 3 35.25 5.36 -6 18 3 6.70 4.40 -4 18 3 24.74 4.41 -2 18 3 15.65 3.84 0 18 3 55.24 3.52 2 18 3 25.46 3.86 4 18 3 43.80 4.93 6 18 3 5.03 4.79 8 18 3 44.15 6.18 10 18 3 9.10 6.13 -9 19 3 53.90 6.10 -7 19 3 31.14 5.43 -5 19 3 282.62 8.89 -3 19 3 251.00 7.78 3 19 3 259.56 7.79 5 19 3 296.84 9.14 7 19 3 26.27 5.79 9 19 3 64.05 7.23 -8 20 3 9.69 5.49 -6 20 3 3.07 5.10 -4 20 3 104.84 7.50 -2 20 3 92.71 6.65 0 20 3 -1.14 3.52 2 20 3 66.74 6.37 4 20 3 111.01 7.52 6 20 3 4.00 5.37 8 20 3 6.36 5.97 -7 21 3 14.36 5.63 -5 21 3 150.16 8.64 -3 21 3 123.09 7.46 -1 21 3 24.35 3.76 1 21 3 20.40 4.36 3 21 3 119.86 7.75 5 21 3 163.71 9.15 7 21 3 8.57 6.19 -6 22 3 7.50 5.63 -4 22 3 67.41 7.77 -2 22 3 18.69 4.63 0 22 3 1.45 4.02 2 22 3 13.19 4.57 4 22 3 74.44 8.22 6 22 3 -3.60 5.80 8 22 3 2.03 6.55 -7 23 3 9.25 5.85 -5 23 3 50.56 6.72 -3 23 3 28.53 5.47 -1 23 3 11.91 4.56 1 23 3 9.49 4.67 3 23 3 23.36 5.43 5 23 3 33.52 6.34 7 23 3 1.40 6.41 -6 24 3 11.60 6.16 -4 24 3 74.23 9.05 2 24 3 54.33 6.14 4 24 3 52.21 6.66 6 24 3 -1.91 6.28 -5 25 3 23.13 6.54 3 25 3 46.41 6.50 5 25 3 24.74 6.83 4 26 3 41.85 7.29 -1 -27 4 29.49 6.47 1 -27 4 37.05 6.19 3 -27 4 1.36 5.47 -2 -26 4 5.43 5.94 0 -26 4 48.09 6.50 2 -26 4 7.02 5.40 4 -26 4 18.18 5.55 -3 -25 4 15.04 5.97 -1 -25 4 27.29 6.09 1 -25 4 28.10 5.73 3 -25 4 5.71 5.27 -4 -24 4 22.22 6.08 -2 -24 4 47.64 6.32 0 -24 4 51.13 6.00 2 -24 4 42.11 5.84 4 -24 4 21.15 5.31 -5 -23 4 1.30 5.22 -3 -23 4 2.86 5.24 -1 -23 4 101.50 8.17 1 -23 4 88.99 7.71 3 -23 4 11.44 5.09 5 -23 4 1.98 4.68 -6 -22 4 16.20 5.54 -4 -22 4 33.01 5.55 -2 -22 4 26.39 5.13 0 -22 4 13.22 4.88 2 -22 4 17.96 4.65 4 -22 4 17.60 4.91 -7 -21 4 3.90 5.15 -5 -21 4 143.21 8.20 -3 -21 4 52.47 5.61 -1 -21 4 2.19 4.37 1 -21 4 3.23 4.15 3 -21 4 65.37 6.48 5 -21 4 128.00 7.25 -8 -20 4 13.31 5.14 -6 -20 4 106.74 8.22 -4 -20 4 20.48 4.68 -2 -20 4 104.54 7.00 0 -20 4 47.67 5.00 2 -20 4 106.98 6.59 4 -20 4 30.22 4.67 6 -20 4 104.05 6.89 -9 -19 4 22.56 5.35 -7 -19 4 16.31 4.85 -5 -19 4 1.62 4.28 -3 -19 4 33.91 4.54 -1 -19 4 266.39 7.84 1 -19 4 253.51 7.38 3 -19 4 32.94 4.23 5 -19 4 7.21 4.03 -10 -18 4 7.72 4.74 -8 -18 4 29.43 5.06 -6 -18 4 52.24 5.16 -4 -18 4 10.26 3.98 -2 -18 4 200.76 6.97 0 -18 4 15.65 3.79 2 -18 4 181.92 6.52 4 -18 4 21.26 4.09 6 -18 4 59.38 5.91 -11 -17 4 14.51 4.95 -9 -17 4 40.59 5.15 -7 -17 4 13.03 4.29 -5 -17 4 15.09 4.06 -3 -17 4 9.62 3.61 -1 -17 4 116.47 5.94 1 -17 4 114.05 5.72 3 -17 4 13.78 3.55 5 -17 4 20.05 3.99 7 -17 4 12.07 3.86 -10 -16 4 7.41 4.42 -8 -16 4 3.58 3.93 -6 -16 4 35.80 4.41 -4 -16 4 39.15 4.15 -2 -16 4 74.01 5.25 0 -16 4 235.05 6.31 2 -16 4 75.16 5.23 4 -16 4 53.42 5.24 6 -16 4 24.78 3.86 -11 -15 4 14.16 4.57 -9 -15 4 142.01 7.40 -7 -15 4 269.74 7.60 -5 -15 4 4.17 3.40 -3 -15 4 32.32 3.70 -1 -15 4 858.97 9.31 1 -15 4 837.58 8.91 3 -15 4 33.18 3.71 5 -15 4 10.31 3.47 7 -15 4 285.80 7.17 -10 -14 4 9.82 4.29 -8 -14 4 65.83 6.19 -6 -14 4 -0.55 3.27 -4 -14 4 116.15 5.81 -2 -14 4 33.34 3.41 0 -14 4 72.86 4.63 2 -14 4 35.10 3.38 4 -14 4 129.06 5.21 6 -14 4 2.47 3.05 8 -14 4 84.41 5.83 -11 -13 4 22.48 4.48 -9 -13 4 24.77 4.05 -7 -13 4 266.67 7.21 -5 -13 4 71.86 5.17 -3 -13 4 16.10 2.97 -1 -13 4 74.42 4.39 1 -13 4 70.66 4.36 3 -13 4 28.03 3.36 5 -13 4 81.35 4.87 7 -13 4 274.11 6.57 -10 -12 4 35.76 4.37 -8 -12 4 34.19 3.92 -6 -12 4 205.69 6.30 -4 -12 4 46.30 4.44 -2 -12 4 273.31 5.46 0 -12 4 9.88 2.49 2 -12 4 304.28 5.45 4 -12 4 54.19 4.27 6 -12 4 208.19 5.49 8 -12 4 33.05 3.73 -9 -11 4 45.35 5.51 -7 -11 4 253.22 6.47 -5 -11 4 319.49 6.26 -3 -11 4 74.20 4.18 -1 -11 4 43.31 3.54 1 -11 4 27.51 3.33 3 -11 4 87.37 4.18 5 -11 4 327.67 5.75 7 -11 4 280.98 6.21 9 -11 4 46.71 5.30 -10 -10 4 34.05 3.84 -8 -10 4 187.45 5.99 -6 -10 4 384.95 6.69 -4 -10 4 125.59 4.40 -2 -10 4 190.24 4.50 0 -10 4 46.04 3.36 2 -10 4 161.61 4.06 4 -10 4 140.46 4.35 6 -10 4 381.49 4.14 8 -10 4 182.49 5.63 -9 -9 4 -0.91 2.72 -7 -9 4 153.48 5.05 -5 -9 4 180.44 3.24 -3 -9 4 587.91 6.27 -1 -9 4 216.27 4.16 1 -9 4 190.24 3.98 3 -9 4 554.06 5.84 5 -9 4 177.74 2.76 7 -9 4 155.76 3.41 9 -9 4 0.40 3.08 -10 -8 4 9.84 3.10 -8 -8 4 28.69 3.09 -6 -8 4 59.63 2.42 -4 -8 4 325.33 3.23 -2 -8 4 548.96 5.53 0 -8 4 24.23 2.73 2 -8 4 517.81 5.39 4 -8 4 264.56 4.42 6 -8 4 60.94 2.61 8 -8 4 41.44 3.15 10 -8 4 16.73 3.56 -9 -7 4 26.10 2.95 -7 -7 4 305.02 3.50 -5 -7 4 30.10 2.03 -3 -7 4 84.18 2.13 -1 -7 4 82.79 2.94 1 -7 4 78.18 2.81 3 -7 4 63.98 3.10 5 -7 4 26.18 2.02 7 -7 4 313.11 3.91 9 -7 4 34.86 2.50 -8 -6 4 87.88 2.80 -6 -6 4 200.43 2.85 -4 -6 4 21.27 1.51 -2 -6 4 160.44 2.31 0 -6 4 690.39 5.27 2 -6 4 146.31 3.27 4 -6 4 22.49 1.48 6 -6 4 202.04 3.09 8 -6 4 91.83 3.36 10 -6 4 5.19 2.38 -9 -5 4 98.92 4.32 -7 -5 4 242.77 3.93 -5 -5 4 3.31 1.09 -3 -5 4 132.63 2.05 -1 -5 4 5758.37 19.64 1 -5 4 5434.69 18.17 3 -5 4 118.24 2.92 5 -5 4 1.57 1.20 7 -5 4 230.36 3.58 9 -5 4 115.09 3.78 11 -5 4 14.82 4.15 -8 -4 4 17.85 2.40 -6 -4 4 19.47 1.40 -4 -4 4 53.51 1.71 -2 -4 4 87.79 1.71 0 -4 4 1554.06 6.39 2 -4 4 115.83 2.74 4 -4 4 53.67 1.82 6 -4 4 28.42 1.99 8 -4 4 15.17 2.07 10 -4 4 31.97 3.99 12 -4 4 8.16 4.33 -9 -3 4 537.70 6.61 -7 -3 4 234.16 5.99 -5 -3 4 131.16 2.14 -3 -3 4 267.39 2.29 -1 -3 4 9.86 0.91 1 -3 4 6.10 1.33 3 -3 4 256.66 2.61 5 -3 4 144.16 2.50 7 -3 4 243.21 3.63 9 -3 4 532.88 5.50 11 -3 4 31.32 4.43 13 -3 4 0.69 4.52 -10 -2 4 31.54 3.06 -8 -2 4 94.41 2.69 -6 -2 4 45.09 1.92 -4 -2 4 69.58 1.66 -2 -2 4 2223.82 33.89 0 -2 4 106.45 1.76 2 -2 4 2067.39 6.48 4 -2 4 76.73 1.99 6 -2 4 46.40 2.36 8 -2 4 85.75 3.38 10 -2 4 30.81 4.05 12 -2 4 13.55 4.32 -9 -1 4 190.27 4.93 -7 -1 4 135.36 2.56 -5 -1 4 439.69 8.41 -3 -1 4 280.53 2.08 -1 -1 4 93.01 1.31 1 -1 4 83.08 1.17 3 -1 4 257.87 2.31 5 -1 4 445.75 3.59 7 -1 4 134.27 3.26 9 -1 4 202.55 6.40 11 -1 4 17.56 4.14 13 -1 4 15.83 5.07 -10 0 4 27.64 3.12 -8 0 4 192.72 4.86 -6 0 4 1295.88 20.18 -4 0 4 54.56 2.71 -2 0 4 5.69 1.28 0 0 4 230.94 1.66 2 0 4 4.65 0.82 4 0 4 57.25 1.95 6 0 4 1395.90 6.39 8 0 4 203.06 5.84 10 0 4 28.64 3.94 12 0 4 36.73 5.04 14 0 4 109.46 8.82 -11 1 4 17.09 3.15 -9 1 4 191.79 5.26 -7 1 4 126.53 2.45 -5 1 4 472.20 5.34 -3 1 4 302.27 3.78 -1 1 4 93.42 2.21 1 1 4 85.86 1.09 3 1 4 252.61 2.47 5 1 4 476.19 4.35 7 1 4 136.40 4.85 9 1 4 197.06 6.18 11 1 4 15.28 4.20 13 1 4 17.26 5.16 -10 2 4 28.42 3.22 -8 2 4 78.13 4.64 -6 2 4 44.15 3.50 -4 2 4 72.72 3.02 -2 2 4 2470.62 8.39 0 2 4 117.02 1.30 2 2 4 2109.33 5.25 4 2 4 72.66 2.21 6 2 4 52.62 3.90 8 2 4 101.27 5.31 10 2 4 40.42 4.50 12 2 4 17.89 4.93 14 2 4 6.17 5.65 -11 3 4 25.76 3.42 -9 3 4 515.81 7.60 -7 3 4 231.34 5.25 -5 3 4 148.63 3.94 -3 3 4 309.32 4.06 -1 3 4 9.83 1.32 1 3 4 6.68 0.70 3 3 4 266.83 3.68 5 3 4 131.62 3.95 7 3 4 240.82 5.79 9 3 4 576.60 8.88 11 3 4 35.04 4.84 13 3 4 1.88 4.84 -12 4 4 1.56 3.19 -10 4 4 25.30 3.52 -8 4 4 23.46 3.07 -6 4 4 29.18 2.71 -4 4 4 52.89 3.14 -2 4 4 131.18 3.06 0 4 4 1536.25 4.09 2 4 4 99.24 2.63 4 4 4 51.75 3.00 6 4 4 18.79 2.69 8 4 4 18.28 3.46 12 4 4 6.25 4.56 -11 5 4 9.47 3.33 -9 5 4 113.36 5.41 -7 5 4 232.26 5.60 -5 5 4 3.15 1.99 -3 5 4 156.84 3.50 -1 5 4 5912.00 14.50 1 5 4 5353.58 19.54 3 5 4 127.26 3.40 5 5 4 4.12 2.11 7 5 4 236.84 6.30 9 5 4 134.94 6.47 11 5 4 13.89 4.54 13 5 4 28.74 5.70 -12 6 4 80.26 6.21 -10 6 4 7.40 3.26 -8 6 4 92.43 5.29 -6 6 4 203.14 5.14 -4 6 4 17.76 2.09 -2 6 4 171.18 3.63 0 6 4 733.13 3.35 2 6 4 149.82 3.29 4 6 4 22.11 2.30 6 6 4 191.51 5.38 8 6 4 105.39 5.85 10 6 4 6.77 4.16 12 6 4 104.29 8.23 -13 7 4 5.63 3.73 -11 7 4 24.78 3.83 -9 7 4 34.39 3.78 -7 7 4 317.95 6.41 -5 7 4 25.89 2.60 -3 7 4 72.67 3.40 -1 7 4 97.55 2.05 1 7 4 83.32 1.66 3 7 4 88.48 3.47 5 7 4 30.10 2.89 7 7 4 344.03 7.23 9 7 4 30.09 4.34 11 7 4 22.32 5.01 13 7 4 9.62 5.30 -12 8 4 2.74 3.58 -10 8 4 15.00 3.67 -8 8 4 37.69 3.66 -6 8 4 60.78 4.47 -4 8 4 316.04 5.30 -2 8 4 570.61 5.72 0 8 4 25.38 1.74 2 8 4 570.14 5.53 4 8 4 331.69 5.53 6 8 4 58.90 4.90 8 8 4 32.86 3.96 10 8 4 11.80 4.39 12 8 4 9.10 5.08 -13 9 4 21.98 4.30 -11 9 4 48.30 6.01 -9 9 4 3.22 3.27 -7 9 4 151.32 5.63 -5 9 4 182.35 5.12 -3 9 4 604.50 6.50 -1 9 4 205.28 2.87 1 9 4 207.89 2.39 3 9 4 606.63 6.38 5 9 4 184.31 5.45 7 9 4 167.96 6.52 9 9 4 4.46 3.89 11 9 4 47.18 5.60 -12 10 4 54.65 6.70 -10 10 4 36.51 4.28 -8 10 4 189.88 6.47 -6 10 4 388.73 7.03 -4 10 4 147.16 5.04 -2 10 4 175.73 4.41 0 10 4 50.80 2.11 2 10 4 186.25 4.19 4 10 4 154.12 5.04 6 10 4 398.10 7.52 8 10 4 204.52 7.51 10 10 4 37.66 5.52 12 10 4 65.59 6.77 -11 11 4 30.17 4.50 -9 11 4 48.97 5.79 -7 11 4 284.75 6.84 -5 11 4 328.61 6.69 -3 11 4 86.09 4.36 -1 11 4 36.04 2.23 1 11 4 44.88 2.11 3 11 4 86.79 4.29 5 11 4 382.17 7.29 7 11 4 278.91 7.65 9 11 4 51.35 5.29 11 11 4 33.36 5.72 -12 12 4 12.06 4.43 -10 12 4 38.45 4.64 -8 12 4 28.47 3.90 -6 12 4 200.79 6.22 -4 12 4 47.70 4.77 -2 12 4 318.90 4.58 0 12 4 8.88 1.51 2 12 4 316.48 5.55 4 12 4 54.93 4.86 6 12 4 229.37 7.16 8 12 4 37.50 4.81 10 12 4 35.64 5.42 12 12 4 8.28 5.53 -11 13 4 26.78 4.83 -9 13 4 26.67 4.22 -7 13 4 266.48 7.49 -5 13 4 77.97 5.54 -3 13 4 23.92 3.18 -1 13 4 85.02 4.26 1 13 4 71.45 2.67 3 13 4 18.06 3.04 5 13 4 75.16 5.63 7 13 4 277.30 8.22 9 13 4 23.20 5.11 11 13 4 25.38 5.84 -10 14 4 9.77 4.40 -8 14 4 71.57 6.24 -6 14 4 2.50 3.30 -4 14 4 117.12 5.81 -2 14 4 31.47 2.51 0 14 4 81.66 2.94 4 14 4 143.25 6.05 6 14 4 4.60 3.85 8 14 4 73.54 7.46 10 14 4 2.56 5.28 -11 15 4 13.27 4.74 -9 15 4 155.57 7.71 -7 15 4 281.47 7.98 -5 15 4 6.10 3.60 -3 15 4 18.60 3.52 -1 15 4 900.87 5.93 1 15 4 875.75 7.98 5 15 4 8.09 3.85 7 15 4 293.48 8.88 9 15 4 154.70 8.98 11 15 4 12.88 5.98 -10 16 4 6.74 4.78 -8 16 4 8.63 4.19 -6 16 4 24.88 4.27 -4 16 4 48.55 5.68 -2 16 4 87.31 3.72 0 16 4 249.66 4.03 2 16 4 94.00 5.42 4 16 4 40.50 4.34 6 16 4 41.71 5.25 8 16 4 6.43 5.00 10 16 4 1.99 5.61 -9 17 4 55.75 5.75 -7 17 4 15.50 4.47 -5 17 4 18.04 4.35 -3 17 4 9.19 3.58 -1 17 4 131.13 3.74 1 17 4 131.76 5.41 3 17 4 12.82 3.74 5 17 4 19.63 4.65 7 17 4 16.73 5.18 9 17 4 45.32 6.39 -10 18 4 8.44 5.21 -8 18 4 40.14 5.42 -6 18 4 57.33 6.79 -4 18 4 15.08 4.12 -2 18 4 181.50 6.27 0 18 4 18.83 2.44 2 18 4 202.74 6.55 4 18 4 21.11 4.62 6 18 4 57.74 5.95 8 18 4 38.36 6.25 10 18 4 1.14 5.99 -9 19 4 27.02 5.50 -7 19 4 30.16 5.40 -5 19 4 13.41 4.68 -3 19 4 41.03 4.60 -1 19 4 256.25 4.67 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6.46 -2 -14 9 66.13 5.31 0 -14 9 12.74 3.35 2 -14 9 52.58 5.33 4 -14 9 185.97 6.58 6 -14 9 49.00 4.73 8 -14 9 4.61 4.06 10 -14 9 3.82 4.62 -7 -13 9 43.06 5.04 -5 -13 9 59.45 5.16 -3 -13 9 158.70 5.66 -1 -13 9 98.35 5.27 1 -13 9 83.26 5.48 3 -13 9 150.63 5.93 5 -13 9 61.96 5.29 7 -13 9 54.96 6.16 9 -13 9 -0.15 4.25 -8 -12 9 2.06 2.95 -6 -12 9 61.50 4.82 -4 -12 9 14.88 2.99 -2 -12 9 123.34 5.21 0 -12 9 0.70 2.84 2 -12 9 139.58 5.44 4 -12 9 18.73 3.39 6 -12 9 50.92 5.61 8 -12 9 3.42 3.99 10 -12 9 29.96 4.81 -7 -11 9 80.62 3.52 -5 -11 9 148.51 5.34 -3 -11 9 188.83 5.41 -1 -11 9 226.21 5.65 1 -11 9 226.24 5.81 3 -11 9 203.93 5.79 5 -11 9 150.25 5.60 7 -11 9 77.70 5.77 9 -11 9 22.29 4.42 11 -11 9 10.31 4.64 -8 -10 9 40.91 4.30 -6 -10 9 56.39 3.12 -4 -10 9 344.51 6.16 -2 -10 9 104.66 4.53 0 -10 9 14.11 2.64 2 -10 9 91.64 4.50 4 -10 9 330.82 6.36 6 -10 9 54.61 5.02 8 -10 9 46.84 4.43 10 -10 9 4.64 4.24 -7 -9 9 92.32 3.30 -5 -9 9 96.76 3.23 -3 -9 9 143.25 4.52 -1 -9 9 512.94 6.45 1 -9 9 464.44 6.38 3 -9 9 138.15 4.63 5 -9 9 106.73 5.33 7 -9 9 96.03 5.71 9 -9 9 185.96 6.87 11 -9 9 35.17 5.04 -8 -8 9 128.09 5.22 -6 -8 9 10.44 1.72 -4 -8 9 26.19 1.85 -2 -8 9 42.24 3.52 0 -8 9 40.38 3.59 2 -8 9 25.05 2.71 4 -8 9 30.33 3.06 6 -8 9 12.08 3.12 8 -8 9 113.86 6.01 10 -8 9 85.01 6.66 12 -8 9 5.90 4.55 -9 -7 9 2.28 3.07 -7 -7 9 59.76 2.86 -5 -7 9 18.51 1.76 -3 -7 9 109.00 2.80 -1 -7 9 19.51 2.29 1 -7 9 24.64 2.45 3 -7 9 102.45 3.95 5 -7 9 11.23 2.81 7 -7 9 50.99 5.08 9 -7 9 3.32 3.75 11 -7 9 38.23 4.87 -8 -6 9 10.95 2.68 -6 -6 9 108.09 2.99 -4 -6 9 377.37 3.74 -2 -6 9 5.69 1.32 0 -6 9 87.90 3.47 2 -6 9 3.44 2.00 4 -6 9 380.26 5.94 6 -6 9 108.98 5.11 8 -6 9 9.07 3.42 10 -6 9 2.08 3.93 -9 -5 9 50.63 4.65 -7 -5 9 53.30 4.26 -5 -5 9 170.33 2.96 -3 -5 9 708.17 4.43 -1 -5 9 106.03 2.42 1 -5 9 97.08 3.33 3 -5 9 665.49 6.67 5 -5 9 154.29 4.73 7 -5 9 56.31 4.88 9 -5 9 57.25 5.64 11 -5 9 230.63 7.82 -10 -4 9 90.82 5.29 -8 -4 9 13.71 2.77 -6 -4 9 88.20 2.57 -4 -4 9 51.15 2.15 -2 -4 9 225.39 2.76 0 -4 9 138.62 3.38 2 -4 9 178.19 3.85 4 -4 9 59.71 3.43 6 -4 9 56.24 2.39 8 -4 9 11.45 3.38 10 -4 9 72.56 6.28 -9 -3 9 104.62 5.04 -7 -3 9 48.90 4.11 -5 -3 9 114.04 2.42 -3 -3 9 308.77 2.99 -1 -3 9 204.50 2.60 1 -3 9 207.48 3.59 3 -3 9 279.17 4.59 5 -3 9 113.36 2.38 7 -3 9 38.86 2.72 9 -3 9 102.44 6.00 -10 -2 9 10.94 3.01 -8 -2 9 140.93 5.06 -6 -2 9 66.17 4.30 -4 -2 9 148.01 2.30 -2 -2 9 10.05 1.11 0 -2 9 16.71 1.22 2 -2 9 8.59 0.95 4 -2 9 131.73 2.22 6 -2 9 49.91 2.48 8 -2 9 143.79 3.67 -11 -1 9 3.07 3.04 -9 -1 9 153.99 5.62 -7 -1 9 32.11 3.03 -5 -1 9 501.26 6.44 -3 -1 9 385.99 2.88 -1 -1 9 36.15 1.64 1 -1 9 31.01 1.31 3 -1 9 353.46 2.83 5 -1 9 429.35 4.19 7 -1 9 24.76 2.02 9 -1 9 158.28 4.29 -10 0 9 93.52 5.50 -8 0 9 82.83 4.91 -6 0 9 454.80 6.59 -4 0 9 42.84 3.22 -2 0 9 391.27 2.72 0 0 9 0.23 0.99 2 0 9 380.49 2.85 4 0 9 45.59 2.03 6 0 9 437.68 4.27 8 0 9 76.32 3.47 10 0 9 91.26 6.06 -11 1 9 4.02 3.12 -9 1 9 162.55 5.75 -7 1 9 25.68 2.95 -5 1 9 469.88 6.31 -3 1 9 370.44 5.02 -1 1 9 37.56 1.58 1 1 9 30.82 1.38 3 1 9 370.24 3.20 5 1 9 459.65 4.04 7 1 9 29.97 2.17 9 1 9 146.60 5.88 11 1 9 2.67 3.83 -12 2 9 31.33 3.99 -10 2 9 12.51 3.16 -8 2 9 146.13 5.45 -6 2 9 52.39 4.10 -4 2 9 147.66 4.11 -2 2 9 8.89 1.73 0 2 9 17.35 0.97 2 2 9 10.29 0.92 4 2 9 142.87 2.66 6 2 9 59.08 2.88 8 2 9 130.98 5.24 10 2 9 10.70 3.79 12 2 9 36.98 5.06 -11 3 9 21.30 3.64 -9 3 9 101.79 5.52 -7 3 9 54.12 4.47 -5 3 9 125.61 4.47 -3 3 9 293.35 4.82 -1 3 9 230.91 2.44 1 3 9 209.25 2.07 3 3 9 286.40 3.16 5 3 9 105.48 2.91 7 3 9 44.44 4.43 9 3 9 101.95 5.79 11 3 9 22.48 4.48 -12 4 9 8.65 3.52 -10 4 9 70.69 5.66 -8 4 9 11.88 2.92 -6 4 9 69.79 4.41 -4 4 9 72.00 3.76 -2 4 9 196.01 4.01 0 4 9 133.39 1.84 2 4 9 204.41 2.31 4 4 9 44.15 3.33 6 4 9 77.87 4.41 8 4 9 11.13 3.25 10 4 9 98.74 6.61 12 4 9 10.58 4.73 -13 5 9 20.01 3.93 -11 5 9 218.06 7.15 -9 5 9 64.80 5.37 -7 5 9 55.14 4.64 -5 5 9 156.05 4.64 -3 5 9 730.69 7.04 -1 5 9 118.98 3.45 1 5 9 88.02 2.08 3 5 9 687.95 6.37 5 5 9 169.01 4.88 7 5 9 54.81 4.83 9 5 9 57.49 5.95 11 5 9 260.80 8.64 13 5 9 30.12 5.62 -12 6 9 79.96 6.31 -10 6 9 1.46 3.15 -8 6 9 12.44 3.08 -6 6 9 108.81 4.71 -4 6 9 390.41 5.93 -2 6 9 2.69 1.87 0 6 9 92.06 2.27 2 6 9 2.17 1.06 4 6 9 366.65 5.69 6 6 9 97.15 4.98 8 6 9 8.16 3.41 10 6 9 5.07 4.01 12 6 9 86.15 7.99 -11 7 9 35.63 4.11 -9 7 9 3.24 3.01 -7 7 9 50.80 4.73 -5 7 9 14.47 2.60 -3 7 9 115.35 4.08 -1 7 9 25.44 2.09 1 7 9 17.80 1.36 3 7 9 115.09 4.04 5 7 9 20.27 2.98 7 7 9 64.88 5.43 9 7 9 2.03 3.79 11 7 9 45.90 5.50 -12 8 9 4.22 3.69 -10 8 9 69.93 5.73 -8 8 9 106.59 5.53 -6 8 9 6.62 2.64 -4 8 9 32.37 2.89 -2 8 9 28.54 3.37 0 8 9 38.07 2.20 2 8 9 28.62 1.87 4 8 9 24.99 2.85 6 8 9 11.65 3.23 8 8 9 128.69 6.59 10 8 9 101.42 7.48 12 8 9 -1.58 4.87 -11 9 9 27.33 4.18 -9 9 9 170.82 6.49 -7 9 9 92.35 5.23 -5 9 9 92.47 4.87 -3 9 9 144.27 4.55 -1 9 9 493.25 4.18 1 9 9 457.31 7.27 3 9 9 143.35 4.72 5 9 9 105.25 5.33 7 9 9 95.74 5.97 9 9 9 186.84 7.78 11 9 9 34.47 5.65 -12 10 9 3.52 3.99 -10 10 9 8.10 3.62 -8 10 9 47.44 5.38 -6 10 9 52.79 4.93 -4 10 9 344.60 6.28 -2 10 9 91.34 4.15 0 10 9 13.05 1.62 2 10 9 92.74 2.42 4 10 9 339.39 6.52 6 10 9 68.75 5.59 8 10 9 43.39 4.72 10 10 9 6.28 4.68 12 10 9 0.22 5.28 -11 11 9 13.80 3.94 -9 11 9 19.62 3.68 -7 11 9 71.83 5.82 -5 11 9 150.42 5.52 -3 11 9 211.05 5.33 -1 11 9 242.19 3.58 1 11 9 213.36 4.41 3 11 9 198.66 5.66 5 11 9 170.17 6.21 7 11 9 86.86 6.55 9 11 9 23.09 4.83 11 11 9 6.40 5.18 -10 12 9 24.08 4.20 -8 12 9 4.69 3.47 -6 12 9 54.63 5.36 -4 12 9 15.35 3.03 -2 12 9 140.10 4.69 0 12 9 2.08 1.66 2 12 9 148.44 5.31 4 12 9 18.60 3.41 6 12 9 69.93 6.26 8 12 9 -0.30 4.28 10 12 9 33.57 5.59 -11 13 9 37.63 4.77 -9 13 9 1.73 3.69 -7 13 9 58.61 5.94 -5 13 9 63.24 5.10 -3 13 9 153.41 5.39 -1 13 9 79.25 3.06 1 13 9 88.45 3.00 3 13 9 150.61 5.96 5 13 9 67.50 5.83 7 13 9 42.14 4.96 9 13 9 3.54 4.96 11 13 9 35.11 6.16 -10 14 9 4.89 3.98 -8 14 9 4.87 3.71 -6 14 9 47.16 5.44 -4 14 9 185.81 6.02 -2 14 9 63.58 4.66 0 14 9 14.94 1.93 2 14 9 65.83 5.22 4 14 9 214.28 6.85 6 14 9 38.40 4.81 8 14 9 7.04 4.84 10 14 9 0.31 5.46 -9 15 9 19.73 4.40 -7 15 9 8.64 3.65 -5 15 9 172.07 6.20 -3 15 9 409.21 7.16 -1 15 9 16.11 2.05 1 15 9 7.32 3.15 3 15 9 398.21 7.97 5 15 9 190.98 7.57 7 15 9 3.45 4.59 9 15 9 23.39 5.85 -8 16 9 5.54 4.03 -6 16 9 6.92 3.62 -4 16 9 3.88 3.26 -2 16 9 103.62 5.49 0 16 9 7.53 3.27 2 16 9 82.40 5.95 4 16 9 4.22 3.93 6 16 9 3.38 4.54 8 16 9 3.28 5.14 -9 17 9 10.08 4.40 -7 17 9 8.90 3.93 -5 17 9 3.97 3.61 -3 17 9 60.29 5.34 -1 17 9 21.93 2.40 1 17 9 27.09 4.09 3 17 9 40.46 4.75 5 17 9 -0.43 4.31 7 17 9 2.56 5.11 9 17 9 10.20 5.92 -8 18 9 25.99 4.75 -6 18 9 37.80 4.59 -4 18 9 5.36 3.52 -2 18 9 16.88 3.58 0 18 9 1.08 3.84 2 18 9 9.91 4.22 4 18 9 9.13 4.58 6 18 9 32.53 5.71 8 18 9 33.81 6.32 -7 19 9 17.30 4.41 -5 19 9 105.06 6.89 -3 19 9 79.82 6.06 -1 19 9 2.20 3.92 1 19 9 3.22 4.21 3 19 9 82.59 7.33 5 19 9 103.98 8.36 7 19 9 14.59 5.97 -6 20 9 21.17 4.47 -4 20 9 8.73 3.93 0 20 9 125.71 7.00 2 20 9 67.87 7.37 4 20 9 5.22 5.04 6 20 9 29.12 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