data_86957
_publ_requested_journal          'Mineralogical Magazine'
_publ_contact_author_name        'Fernando Camara'
_publ_contact_author_address     
;C.N.R. - Istituto di Geoscienze e Georisorse, unit\`a di Pavia
via Ferrata 1, I-27100 Pavia
Italy
;
_publ_contact_author_email       camara@crystal.unipv.it
_publ_contact_author_phone       '+39 0382985867'
_publ_contact_author_fax         +390382985887
loop_
_publ_author_name
_publ_author_address
'Camara, Fernando '
;C.N.R. - Istituto di Geoscienze e Georisorse, unit\`a di Pavia
via Ferrata 1, I-27100 Pavia
Italy
;
'Sokolova, Elena'
;Department of Geological Sciences, University of Manitoba
Winnipeg, Manitoba, R3T 2N2
Canada
;
'Hawthorne, Frank C.'
;Department of Geological Sciences, University of Manitoba
Winnipeg, Manitoba, R3T 2N2
Canada
;
'Abdu, Yassir'
;Department of Geological Sciences, University of Manitoba
Winnipeg, Manitoba, R3T 2N2
Canada
;

_audit_creation_method           SHELXL-97
_chemical_name_systematic        lomonosovite
_chemical_name_common            lomonosovite
_chemical_melting_point          ?
_chemical_formula_moiety         
'Fe0.17 Na1.83 Nb0.77 O26 P2 Si4 Ti3.23, 7.942(Na)'
_chemical_formula_sum            'Fe0.17 Na9.78 Nb0.77 O26 P2 Si4 Ti3.23'
_chemical_formula_weight         1050.89

loop_
_atom_type_symbol
_atom_type_description
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_source
O O-2 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Na NaP1 0.0300 0.0250 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si SiP4 0.0720 0.0710 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
P P 0.1023 0.0942 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Ti TiP4 0.2480 0.4460 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Fe FeP2 0.3010 0.8450 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Nb NbP5 -2.1970 0.6210 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
On O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'
Om O-1 0.0080 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4'

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1'
_symmetry_int_tables_number      2
_symmetry_space_group_name_Hall  '-P 1'

loop_
_symmetry_equiv_pos_as_xyz
'x, y, z'
'-x, -y, -z'

_cell_length_a                   5.4170(7)
_cell_length_b                   7.1190(9)
_cell_length_c                   14.4869(18)
_cell_angle_alpha                99.957(3)
_cell_angle_beta                 96.711(3)
_cell_angle_gamma                90.360(3)
_cell_volume                     546.28(12)
_cell_formula_units_Z            1
_cell_measurement_temperature    298(2)
_cell_measurement_reflns_used    7479
_cell_measurement_theta_min      5.75
_cell_measurement_theta_max      70.21

_exptl_crystal_description       plate
_exptl_crystal_colour            brown
_exptl_crystal_size_max          0.38
_exptl_crystal_size_mid          0.23
_exptl_crystal_size_min          0.10
_exptl_crystal_density_meas      ?
_exptl_crystal_density_diffrn    3.194
_exptl_crystal_density_method    'not measured'
_exptl_crystal_F_000             508.7
_exptl_absorpt_coefficient_mu    2.42
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_correction_T_min  0.519
_exptl_absorpt_correction_T_max  0.786
_exptl_absorpt_process_details   'Bruker SADABS'

_exptl_special_details           
;
SADABS was used to perform the Absorption correction
Parameter refinement on 10041 reflections reduced R(int) from 0.0571 to 0.0224
;

_diffrn_ambient_temperature      298(2)
_diffrn_radiation_probe          x-ray
_diffrn_radiation_type           MoK\a
_diffrn_radiation_wavelength     0.71073
_diffrn_source                   'fine-focus sealed tube'
_diffrn_radiation_monochromator  graphite
_diffrn_measurement_device_type  'SMART APEX CCD'
_diffrn_measurement_method       \\w
_diffrn_detector_area_resol_mean ?
_diffrn_standards_number         ?
_diffrn_standards_interval_count ?
_diffrn_standards_interval_time  ?
_diffrn_standards_decay_%        ?
_diffrn_reflns_number            12104
_diffrn_reflns_av_R_equivalents  0.0224
_diffrn_reflns_av_sigmaI/netI    0.0258
_diffrn_reflns_limit_h_min       -8
_diffrn_reflns_limit_h_max       8
_diffrn_reflns_limit_k_min       -11
_diffrn_reflns_limit_k_max       11
_diffrn_reflns_limit_l_min       -23
_diffrn_reflns_limit_l_max       23
_diffrn_reflns_theta_min         2.88
_diffrn_reflns_theta_max         35.11
_reflns_number_total             4782
_reflns_number_gt                4572
_reflns_threshold_expression     >2sigma(I)

_computing_data_collection       'SMART,version 5.625'
_computing_cell_refinement       'SAINT version 6.28A'
_computing_data_reduction        'SAINT version 6.28A'
_computing_structure_solution    'SHELXS-97 (Sheldrick, 1997)'
_computing_structure_refinement  'SHELXL-97 (Sheldrick, 1997)'
_computing_molecular_graphics    ?
_computing_publication_material  'enCIFer, version 1.2'

_refine_special_details          
;
 Refinement of F^2^ against ALL reflections.  The weighted R-factor wR and
 goodness of fit S are based on F^2^, conventional R-factors R are based
 on F, with F set to zero for negative F^2^. The threshold expression of
 F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is
 not relevant to the choice of reflections for refinement.  R-factors based
 on F^2^ are statistically about twice as large as those based on F, and R-
 factors based on ALL data will be even larger.
;

_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
'calc w=1/[\s^2^(Fo^2^)+(0.0276P)^2^+0.4140P] where P=(Fo^2^+2Fc^2^)/3'
_atom_sites_solution_primary     direct
_atom_sites_solution_secondary   difmap
_atom_sites_solution_hydrogens   .
_refine_ls_hydrogen_treatment    .
_refine_ls_extinction_method     none
_refine_ls_extinction_coef       ?
_refine_ls_number_reflns         4782
_refine_ls_number_parameters     230
_refine_ls_number_restraints     0
_refine_ls_R_factor_all          0.0274
_refine_ls_R_factor_gt           0.0260
_refine_ls_wR_factor_ref         0.0636
_refine_ls_wR_factor_gt          0.0627
_refine_ls_goodness_of_fit_ref   1.064
_refine_ls_restrained_S_all      1.064
_refine_ls_shift/su_max          0.001
_refine_ls_shift/su_mean         0.000

loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_adp_type
_atom_site_occupancy
_atom_site_symmetry_multiplicity
_atom_site_calc_flag
_atom_site_refinement_flags
_atom_site_disorder_assembly
_atom_site_disorder_group
Na1 NaP1 0.17184(12) 0.41851(9) 0.23393(4) 0.01762(18) Uani 0.990(4) 1 d P . .
Na2 NaP1 0.75658(12) 0.88235(9) -0.00370(6) 0.0231(2) Uani 0.991(4) 1 d P . .
Na3A NaP1 0.67740(11) 0.97076(8) 0.36206(4) 0.01884(19) Uani 0.915(3) 1 d P . .
NA3B FeP2 0.67740(11) 0.97076(8) 0.36206(4) 0.01884(19) Uani 0.085(3) 1 d P . .
Na4 NaP1 0.67504(14) 0.45799(9) 0.39770(5) 0.0209(2) Uani 0.990(3) 1 d P . .
Na5 NaP1 0.23788(14) 0.74013(9) 0.41534(5) 0.0218(2) Uani 1.002(4) 1 d P . .
Nb1 NbP5 0.16618(3) 0.92849(2) 0.218105(12) 0.00802(5) Uani 0.210(2) 1 d P . .
Ti1 TiP4 0.16618(3) 0.92849(2) 0.218105(12) 0.00802(5) Uani 0.790(2) 1 d P . .
Nb2 NbP5 0.77151(4) 0.38667(3) -0.007704(14) 0.01301(6) Uani 0.177(2) 1 d P . .
Ti2 TiP4 0.77151(4) 0.38667(3) -0.007704(14) 0.01301(6) Uani 0.823(2) 1 d P . .
Si1A SiP4 0.66653(6) 0.20422(5) 0.17702(2) 0.00737(7) Uani 0.49(4) 1 d P . .
Si1B Si 0.66653(6) 0.20422(5) 0.17702(2) 0.00737(7) Uani 0.51(4) 1 d P . .
Si2A SiP4 0.64976(6) 0.64040(5) 0.19841(2) 0.00704(7) Uani 0.59(4) 1 d P . .
Si2B Si 0.64976(6) 0.64040(5) 0.19841(2) 0.00704(7) Uani 0.41(4) 1 d P . .
P P 0.17814(6) 0.22491(4) 0.43221(2) 0.00914(7) Uani 1 1 d . . .
O1A O-2 0.6733(2) 0.42900(13) 0.23057(7) 0.01306(17) Uani 0.85(5) 1 d P . .
O1B O 0.6733(2) 0.42900(13) 0.23057(7) 0.01306(17) Uani 0.15(5) 1 d P . .
O2A O-2 0.63916(19) 0.19579(14) 0.06524(7) 0.01281(17) Uani 0.78(5) 1 d P . .
O2B O 0.63916(19) 0.19579(14) 0.06524(7) 0.01281(17) Uani 0.22(5) 1 d P . .
O3A O-2 0.9287(2) 0.12229(16) 0.21346(8) 0.0194(2) Uani 0.70(5) 1 d P . .
O3B O 0.9287(2) 0.12229(16) 0.21346(8) 0.0194(2) Uani 0.30(5) 1 d P . .
O4A O-2 0.4366(2) 0.10346(17) 0.21026(9) 0.0219(2) Uani 0.86(5) 1 d P . .
O4B O 0.4366(2) 0.10346(17) 0.21026(9) 0.0219(2) Uani 0.14(5) 1 d P . .
O5A O-2 0.59483(19) 0.60837(14) 0.08374(6) 0.01272(17) Uani 0.87(5) 1 d P . .
O5B O 0.59483(19) 0.60837(14) 0.08374(6) 0.01272(17) Uani 0.13(5) 1 d P . .
O6A O-2 0.90590(19) 0.75276(15) 0.24540(7) 0.01420(17) Uani 0.75(5) 1 d P . .
O6B O 0.90590(19) 0.75276(15) 0.24540(7) 0.01420(17) Uani 0.25(5) 1 d P . .
O7A O-2 0.41669(17) 0.73437(14) 0.24916(7) 0.01174(16) Uani 0.78(7) 1 d P . .
O7B O-1 0.41669(17) 0.73437(14) 0.24916(7) 0.01174(16) Uani 0.22(7) 1 d P . .
O8A O-2 0.12980(19) 0.83454(15) 0.09180(7) 0.01463(18) Uani 0.73(5) 1 d P . .
O8B O 0.12980(19) 0.83454(15) 0.09180(7) 0.01463(18) Uani 0.27(5) 1 d P . .
O9A O-2 0.0880(2) 0.42270(14) 0.07013(7) 0.01374(17) Uani 0.87(5) 1 d P . .
O9B O 0.0880(2) 0.42270(14) 0.07013(7) 0.01374(17) Uani 0.13(5) 1 d P . .
O10A O-2 0.23599(19) 0.03479(13) 0.36655(7) 0.01273(17) Uani 0.61(5) 1 d P . .
O10B O 0.23599(19) 0.03479(13) 0.36655(7) 0.01273(17) Uani 0.39(5) 1 d P . .
O11A O-2 0.9005(2) 0.22363(16) 0.44212(8) 0.0186(2) Uani 0.40(5) 1 d P . .
O11B O 0.9005(2) 0.22363(16) 0.44212(8) 0.0186(2) Uani 0.60(5) 1 d P . .
O12A O-2 0.2497(2) 0.39966(14) 0.39090(8) 0.0180(2) Uani 0.43(5) 1 d P . .
O12B O 0.2497(2) 0.39966(14) 0.39090(8) 0.0180(2) Uani 0.57(5) 1 d P . .
O13A O-2 0.3294(2) 0.23067(16) 0.52885(8) 0.0201(2) Uani 0.68(5) 1 d P . .
O13B O 0.3294(2) 0.23067(16) 0.52885(8) 0.0201(2) Uani 0.32(5) 1 d P . .

loop_
_atom_site_aniso_label
_atom_site_aniso_U_11
_atom_site_aniso_U_22
_atom_site_aniso_U_33
_atom_site_aniso_U_23
_atom_site_aniso_U_13
_atom_site_aniso_U_12
Na1 0.0170(3) 0.0217(3) 0.0139(3) 0.0035(2) 0.0006(2) -0.0037(2)
Na2 0.0126(3) 0.0159(3) 0.0356(4) -0.0045(3) -0.0052(2) 0.0029(2)
Na3A 0.0222(3) 0.0142(3) 0.0181(3) -0.00057(18) -0.00070(19) -0.00027(19)
NA3B 0.0222(3) 0.0142(3) 0.0181(3) -0.00057(18) -0.00070(19) -0.00027(19)
Na4 0.0267(4) 0.0161(3) 0.0186(3) 0.0011(2) 0.0008(2) 0.0033(2)
Na5 0.0312(4) 0.0155(3) 0.0203(3) 0.0058(2) 0.0054(3) 0.0024(2)
Nb1 0.00719(8) 0.00756(8) 0.00951(8) 0.00179(5) 0.00135(5) 0.00042(5)
Ti1 0.00719(8) 0.00756(8) 0.00951(8) 0.00179(5) 0.00135(5) 0.00042(5)
Nb2 0.01770(10) 0.01111(9) 0.00981(9) 0.00161(6) 0.00013(6) 0.00247(6)
Ti2 0.01770(10) 0.01111(9) 0.00981(9) 0.00161(6) 0.00013(6) 0.00247(6)
Si1A 0.00816(14) 0.00654(13) 0.00757(13) 0.00152(10) 0.00123(10) 0.00007(10)
Si1B 0.00816(14) 0.00654(13) 0.00757(13) 0.00152(10) 0.00123(10) 0.00007(10)
Si2A 0.00826(14) 0.00620(13) 0.00650(13) 0.00093(10) 0.00052(10) 0.00012(10)
Si2B 0.00826(14) 0.00620(13) 0.00650(13) 0.00093(10) 0.00052(10) 0.00012(10)
P 0.01025(13) 0.00813(12) 0.00880(13) 0.00058(9) 0.00143(9) 0.00022(9)
O1A 0.0232(5) 0.0063(3) 0.0097(4) 0.0015(3) 0.0019(3) 0.0017(3)
O1B 0.0232(5) 0.0063(3) 0.0097(4) 0.0015(3) 0.0019(3) 0.0017(3)
O2A 0.0156(4) 0.0143(4) 0.0081(4) 0.0013(3) 0.0006(3) 0.0009(3)
O2B 0.0156(4) 0.0143(4) 0.0081(4) 0.0013(3) 0.0006(3) 0.0009(3)
O3A 0.0174(5) 0.0180(5) 0.0214(5) 0.0035(4) -0.0036(4) 0.0091(4)
O3B 0.0174(5) 0.0180(5) 0.0214(5) 0.0035(4) -0.0036(4) 0.0091(4)
O4A 0.0213(5) 0.0208(5) 0.0240(5) 0.0009(4) 0.0098(4) -0.0112(4)
O4B 0.0213(5) 0.0208(5) 0.0240(5) 0.0009(4) 0.0098(4) -0.0112(4)
O5A 0.0183(4) 0.0128(4) 0.0067(3) 0.0015(3) 0.0004(3) -0.0006(3)
O5B 0.0183(4) 0.0128(4) 0.0067(3) 0.0015(3) 0.0004(3) -0.0006(3)
O6A 0.0120(4) 0.0177(4) 0.0126(4) 0.0024(3) 0.0011(3) -0.0065(3)
O6B 0.0120(4) 0.0177(4) 0.0126(4) 0.0024(3) 0.0011(3) -0.0065(3)
O7A 0.0105(4) 0.0133(4) 0.0111(4) 0.0011(3) 0.0010(3) 0.0047(3)
O7B 0.0105(4) 0.0133(4) 0.0111(4) 0.0011(3) 0.0010(3) 0.0047(3)
O8A 0.0144(4) 0.0195(4) 0.0090(4) 0.0001(3) 0.0011(3) -0.0025(3)
O8B 0.0144(4) 0.0195(4) 0.0090(4) 0.0001(3) 0.0011(3) -0.0025(3)
O9A 0.0200(5) 0.0110(4) 0.0105(4) 0.0024(3) 0.0023(3) 0.0004(3)
O9B 0.0200(5) 0.0110(4) 0.0105(4) 0.0024(3) 0.0023(3) 0.0004(3)
O10A 0.0174(4) 0.0091(4) 0.0111(4) -0.0004(3) 0.0024(3) 0.0026(3)
O10B 0.0174(4) 0.0091(4) 0.0111(4) -0.0004(3) 0.0024(3) 0.0026(3)
O11A 0.0117(4) 0.0195(5) 0.0245(5) 0.0011(4) 0.0065(4) 0.0009(3)
O11B 0.0117(4) 0.0195(5) 0.0245(5) 0.0011(4) 0.0065(4) 0.0009(3)
O12A 0.0270(5) 0.0102(4) 0.0175(5) 0.0036(3) 0.0047(4) -0.0026(4)
O12B 0.0270(5) 0.0102(4) 0.0175(5) 0.0036(3) 0.0047(4) -0.0026(4)
O13A 0.0272(6) 0.0172(5) 0.0132(4) 0.0008(4) -0.0059(4) 0.0014(4)
O13B 0.0272(6) 0.0172(5) 0.0132(4) 0.0008(4) -0.0059(4) 0.0014(4)

_geom_special_details            
;
 All esds (except the esd in the dihedral angle between two l.s. planes)
 are estimated using the full covariance matrix.  The cell esds are taken
 into account individually in the estimation of esds in distances, angles
 and torsion angles; correlations between esds in cell parameters are only
 used when they are defined by crystal symmetry.  An approximate (isotropic)
 treatment of cell esds is used for estimating esds involving l.s. planes.
;

loop_
_geom_bond_atom_site_label_1
_geom_bond_atom_site_label_2
_geom_bond_distance
_geom_bond_site_symmetry_2
_geom_bond_publ_flag
Na1 O12A 2.2911(13) . ?
Na1 O9A 2.3687(12) . ?
Na1 O3A 2.4345(14) 1_455 ?
Na1 O7A 2.5665(12) . ?
Na1 O4A 2.6634(15) . ?
Na1 O1A 2.6970(13) 1_455 ?
Na1 O1A 2.7233(13) . ?
Na1 O6A 2.7798(13) 1_455 ?
Na2 O2A 2.2509(12) 2_665 ?
Na2 O8A 2.3738(12) 1_655 ?
Na2 O2A 2.4035(12) 1_565 ?
Na2 O9A 2.4168(12) 2_665 ?
Na2 O8A 2.6697(13) 2_675 ?
Na2 O5A 2.6962(13) . ?
Na2 O4A 3.0714(15) 2_665 ?
Na3A O11A 2.2292(13) 1_565 ?
Na3A O13A 2.3135(13) 2_666 ?
Na3A O10A 2.4432(12) 1_565 ?
Na3A O7A 2.4454(11) . ?
Na3A O6A 2.5304(12) . ?
Na3A O4A 2.7374(14) 1_565 ?
Na3A O3A 3.0201(14) 1_565 ?
Na3A O10A 3.0487(13) 1_665 ?
Na4 O11A 2.2141(13) . ?
Na4 O13A 2.2883(13) 2_666 ?
Na4 O12A 2.3262(14) . ?
Na4 O1A 2.3931(12) . ?
Na4 O12A 3.0335(13) 2_666 ?
Na4 O12A 3.1539(15) 1_655 ?
Na5 O11A 2.2522(14) 2_666 ?
Na5 O10A 2.3262(12) 1_565 ?
Na5 O13A 2.3843(14) 2_666 ?
Na5 O12A 2.3905(12) . ?
Na5 O7A 2.6920(12) . ?
Na5 O6A 2.8891(13) 1_455 ?
Na5 O13A 3.2665(15) 2_566 ?
Nb1 O8A 1.8235(10) . ?
Nb1 O3A 1.8965(10) 1_465 ?
Nb1 O4A 1.9429(11) 1_565 ?
Nb1 O6A 1.9972(10) 1_455 ?
Nb1 O7A 2.0124(9) . ?
Nb1 O10A 2.1410(10) 1_565 ?
Nb2 O9A 1.9284(11) 1_655 ?
Nb2 O8A 1.9363(10) 2_665 ?
Nb2 O9A 1.9523(10) 2_665 ?
Nb2 O2A 2.0343(10) . ?
Nb2 O5A 2.1578(11) 2_665 ?
Nb2 O5A 2.1804(10) . ?
Nb2 Nb2 2.9117(5) 2_765 ?
Si1A O4A 1.5958(11) . ?
Si1A O2A 1.5994(10) . ?
Si1A O3A 1.6056(11) . ?
Si1A O1A 1.6514(10) . ?
Si1A O5A 3.3898(11) . ?
Si2A O6A 1.6141(10) . ?
Si2A O7A 1.6247(10) . ?
Si2A O5A 1.6286(10) . ?
Si2A O1A 1.6521(10) . ?
P O11A 1.5277(11) 1_455 ?
P O13A 1.5312(11) . ?
P O12A 1.5368(11) . ?
P O10A 1.5699(10) . ?
P O3A 3.2538(12) 1_455 ?
O1A O7A 2.5795(13) . ?
O1A O3A 2.5834(14) . ?
O1A O6A 2.5836(14) . ?
O1A O4A 2.5962(15) . ?
O1A O2A 2.6542(14) . ?
O1A O5A 2.6591(13) . ?
O1A O9A 3.4111(14) 1_655 ?
O2A O3A 2.6376(14) . ?
O2A O4A 2.6566(15) . ?
O2A O8A 2.6995(14) 2_665 ?
O2A O9A 2.8976(15) 1_655 ?
O2A O5A 2.9169(14) . ?
O2A O5A 2.9380(14) 2_665 ?
O2A O2A 3.328(2) 2_655 ?
O3A O4A 2.6631(17) . ?
O3A O6A 2.7533(16) 1_545 ?
O3A O4A 2.7605(17) 1_655 ?
O3A O10A 2.7758(15) 1_655 ?
O3A O8A 2.7780(15) 1_645 ?
O4A O10A 2.7381(15) . ?
O4A O8A 2.7439(15) 1_545 ?
O4A O7A 2.7850(16) 1_545 ?
O5A O7A 2.6994(14) . ?
O5A O5A 2.7251(19) 2_665 ?
O5A O6A 2.7575(14) . ?
O5A O9A 2.9496(14) 2_665 ?
O5A O9A 2.9999(15) 1_655 ?
O6A O7A 2.6598(14) . ?
O6A O7A 2.7655(14) 1_655 ?
O6A O8A 2.7985(14) 1_655 ?
O6A O10A 2.8830(14) 1_665 ?
O7A O10A 2.7535(13) 1_565 ?
O7A O8A 2.8051(14) . ?
O8A O9A 2.8441(14) 2_565 ?
O8A O9A 2.8987(15) . ?
O9A O9A 2.566(2) 2_565 ?
O10A O11A 2.5091(14) 1_455 ?
O10A O13A 2.5115(14) . ?
O10A O12A 2.5596(14) . ?
O11A O13A 2.5047(16) 1_655 ?
O11A O12A 2.5140(16) 1_655 ?
O11A O12A 3.4569(16) 2_666 ?
O11A O13A 3.4699(17) . ?
O11A O13A 3.5678(17) 2_656 ?
O12A O13A 2.5028(15) . ?
O12A O13A 3.4238(16) 2_666 ?

loop_
_geom_angle_atom_site_label_1
_geom_angle_atom_site_label_2
_geom_angle_atom_site_label_3
_geom_angle
_geom_angle_site_symmetry_1
_geom_angle_site_symmetry_3
_geom_angle_publ_flag
O12A Na1 O9A 177.38(5) . . ?
O12A Na1 O3A 87.49(4) . 1_455 ?
O9A Na1 O3A 90.11(4) . 1_455 ?
O12A Na1 O7A 94.75(4) . . ?
O9A Na1 O7A 87.66(4) . . ?
O3A Na1 O7A 177.51(4) 1_455 . ?
O12A Na1 O4A 83.95(4) . . ?
O9A Na1 O4A 94.10(4) . . ?
O3A Na1 O4A 65.39(4) 1_455 . ?
O7A Na1 O4A 115.88(4) . . ?
O12A Na1 O1A 95.32(4) . 1_455 ?
O9A Na1 O1A 84.39(4) . 1_455 ?
O3A Na1 O1A 60.20(3) 1_455 1_455 ?
O7A Na1 O1A 118.42(4) . 1_455 ?
O4A Na1 O1A 125.55(4) . 1_455 ?
O12A Na1 O1A 87.45(4) . . ?
O9A Na1 O1A 92.98(4) . . ?
O3A Na1 O1A 123.00(4) 1_455 . ?
O7A Na1 O1A 58.28(3) . . ?
O4A Na1 O1A 57.61(3) . . ?
O1A Na1 O1A 175.95(5) 1_455 . ?
O12A Na1 O6A 100.07(4) . 1_455 ?
O9A Na1 O6A 81.94(4) . 1_455 ?
O3A Na1 O6A 116.42(4) 1_455 1_455 ?
O7A Na1 O6A 62.15(3) . 1_455 ?
O4A Na1 O6A 175.56(4) . 1_455 ?
O1A Na1 O6A 56.27(3) 1_455 1_455 ?
O1A Na1 O6A 120.36(4) . 1_455 ?
O12A Na1 Si1A 102.06(4) . 1_455 ?
O9A Na1 Si1A 76.31(3) . 1_455 ?
O7A Na1 Si1A 146.81(3) . 1_455 ?
O4A Na1 Si1A 94.39(3) . 1_455 ?
O1A Na1 Si1A 149.66(3) . 1_455 ?
O6A Na1 Si1A 86.65(3) 1_455 1_455 ?
O12A Na1 Na5 48.95(3) . . ?
O9A Na1 Na5 133.63(4) . . ?
O3A Na1 Na5 126.41(4) 1_455 . ?
O7A Na1 Na5 54.95(3) . . ?
O4A Na1 Na5 124.89(4) . . ?
O1A Na1 Na5 90.45(3) 1_455 . ?
O1A Na1 Na5 89.14(3) . . ?
O6A Na1 Na5 57.82(3) 1_455 . ?
Si1A Na1 Na5 118.92(3) 1_455 . ?
O12A Na1 Si2A 102.66(4) . . ?
O9A Na1 Si2A 78.94(3) . . ?
O3A Na1 Si2A 149.53(4) 1_455 . ?
O4A Na1 Si2A 86.92(3) . . ?
O1A Na1 Si2A 144.57(3) 1_455 . ?
O6A Na1 Si2A 90.34(3) 1_455 . ?
Si1A Na1 Si2A 155.25(2) 1_455 . ?
Na5 Na1 Si2A 79.25(2) . . ?
O12A Na1 Si1A 94.86(4) . . ?
O9A Na1 Si1A 84.22(3) . . ?
O3A Na1 Si1A 93.35(3) 1_455 . ?
O7A Na1 Si1A 87.54(3) . . ?
O1A Na1 Si1A 151.09(3) 1_455 . ?
O6A Na1 Si1A 147.00(3) 1_455 . ?
Si1A Na1 Si1A 118.82(2) 1_455 . ?
Na5 Na1 Si1A 116.37(2) . . ?
Si2A Na1 Si1A 57.562(16) . . ?
O2A Na2 O8A 152.46(5) 2_665 1_655 ?
O2A Na2 O2A 91.23(4) 2_665 1_565 ?
O8A Na2 O2A 103.19(4) 1_655 1_565 ?
O2A Na2 O9A 93.65(4) 2_665 2_665 ?
O8A Na2 O9A 72.83(4) 1_655 2_665 ?
O2A Na2 O9A 174.98(5) 1_565 2_665 ?
O2A Na2 O8A 102.90(4) 2_665 2_675 ?
O8A Na2 O8A 104.50(4) 1_655 2_675 ?
O2A Na2 O8A 64.05(4) 1_565 2_675 ?
O9A Na2 O8A 113.59(4) 2_665 2_675 ?
O2A Na2 O5A 72.23(4) 2_665 . ?
O8A Na2 O5A 80.54(4) 1_655 . ?
O2A Na2 O5A 112.51(4) 1_565 . ?
O9A Na2 O5A 70.22(4) 2_665 . ?
O8A Na2 O5A 174.29(4) 2_675 . ?
O2A Na2 O4A 57.43(4) 2_665 2_665 ?
O8A Na2 O4A 140.39(4) 1_655 2_665 ?
O2A Na2 O4A 98.14(4) 1_565 2_665 ?
O9A Na2 O4A 83.55(4) 2_665 2_665 ?
O8A Na2 O4A 56.58(3) 2_675 2_665 ?
O5A Na2 O4A 121.01(4) . 2_665 ?
O2A Na2 Na2 150.71(5) 2_665 2_775 ?
O8A Na2 Na2 56.58(3) 1_655 2_775 ?
O2A Na2 Na2 78.32(4) 1_565 2_775 ?
O9A Na2 Na2 96.82(4) 2_665 2_775 ?
O8A Na2 Na2 47.92(3) 2_675 2_775 ?
O5A Na2 Na2 137.05(4) . 2_775 ?
O4A Na2 Na2 96.65(4) 2_665 2_775 ?
O8A Na2 Si1A 157.15(4) 1_655 2_665 ?
O2A Na2 Si1A 99.36(3) 1_565 2_665 ?
O9A Na2 Si1A 84.45(3) 2_665 2_665 ?
O8A Na2 Si1A 82.11(3) 2_675 2_665 ?
O5A Na2 Si1A 94.24(3) . 2_665 ?
Na2 Na2 Si1A 126.03(4) 2_775 2_665 ?
O2A Na2 Nb2 129.04(4) 2_665 2_765 ?
O2A Na2 Nb2 138.72(3) 1_565 2_765 ?
O8A Na2 Nb2 107.90(3) 2_675 2_765 ?
O5A Na2 Nb2 77.73(3) . 2_765 ?
O4A Na2 Nb2 110.53(3) 2_665 2_765 ?
Na2 Na2 Nb2 69.62(2) 2_775 2_765 ?
Si1A Na2 Nb2 120.30(2) 2_665 2_765 ?
O2A Na2 Si1A 100.41(3) 2_665 1_565 ?
O8A Na2 Si1A 83.37(3) 1_655 1_565 ?
O9A Na2 Si1A 150.96(4) 2_665 1_565 ?
O8A Na2 Si1A 87.98(3) 2_675 1_565 ?
O5A Na2 Si1A 89.98(3) . 1_565 ?
O4A Na2 Si1A 125.40(3) 2_665 1_565 ?
Na2 Na2 Si1A 83.17(3) 2_775 1_565 ?
Si1A Na2 Si1A 119.05(2) 2_665 1_565 ?
Nb2 Na2 Si1A 119.98(2) 2_765 1_565 ?
O2A Na2 Na2 47.53(3) 2_665 2_675 ?
O8A Na2 Na2 141.35(5) 1_655 2_675 ?
O9A Na2 Na2 141.17(4) 2_665 2_675 ?
O8A Na2 Na2 80.29(4) 2_675 2_675 ?
O5A Na2 Na2 94.11(4) . 2_675 ?
O4A Na2 Na2 74.49(3) 2_665 2_675 ?
Na2 Na2 Na2 116.96(4) 2_775 2_675 ?
Si1A Na2 Na2 60.80(2) 2_665 2_675 ?
Nb2 Na2 Na2 171.76(4) 2_765 2_675 ?
Si1A Na2 Na2 58.25(2) 1_565 2_675 ?
O11A Na3A O13A 103.50(5) 1_565 2_666 ?
O11A Na3A O10A 108.93(4) 1_565 1_565 ?
O13A Na3A O10A 91.53(4) 2_666 1_565 ?
O11A Na3A O7A 168.17(5) 1_565 . ?
O13A Na3A O7A 88.22(4) 2_666 . ?
O10A Na3A O7A 68.56(4) 1_565 . ?
O11A Na3A O6A 114.65(4) 1_565 . ?
O13A Na3A O6A 96.98(4) 2_666 . ?
O10A Na3A O6A 131.98(4) 1_565 . ?
O7A Na3A O6A 64.60(3) . . ?
O11A Na3A O4A 103.61(4) 1_565 1_565 ?
O13A Na3A O4A 147.92(5) 2_666 1_565 ?
O10A Na3A O4A 63.51(4) 1_565 1_565 ?
O7A Na3A O4A 64.72(4) . 1_565 ?
O6A Na3A O4A 87.01(4) . 1_565 ?
O11A Na3A O3A 75.90(4) 1_565 1_565 ?
O13A Na3A O3A 150.41(4) 2_666 1_565 ?
O10A Na3A O3A 116.96(4) 1_565 1_565 ?
O7A Na3A O3A 94.74(4) . 1_565 ?
O6A Na3A O3A 58.69(3) . 1_565 ?
O4A Na3A O3A 54.84(3) 1_565 1_565 ?
O11A Na3A Si2A 145.81(4) 1_565 . ?
O13A Na3A Si2A 92.44(3) 2_666 . ?
O10A Na3A Si2A 100.53(3) 1_565 . ?
O4A Na3A Si2A 74.16(3) 1_565 . ?
O3A Na3A Si2A 75.49(3) 1_565 . ?
O11A Na3A O10A 54.11(3) 1_565 1_665 ?
O13A Na3A O10A 100.63(4) 2_666 1_665 ?
O10A Na3A O10A 160.94(5) 1_565 1_665 ?
O7A Na3A O10A 125.92(4) . 1_665 ?
O6A Na3A O10A 61.40(3) . 1_665 ?
O4A Na3A O10A 109.05(4) 1_565 1_665 ?
O3A Na3A O10A 54.44(3) 1_565 1_665 ?
Si2A Na3A O10A 93.61(2) . 1_665 ?
O11A Na3A Na5 131.24(4) 1_565 . ?
O13A Na3A Na5 49.24(4) 2_666 . ?
O10A Na3A Na5 47.43(3) 1_565 . ?
O7A Na3A Na5 56.18(3) . . ?
O6A Na3A Na5 108.94(3) . . ?
O4A Na3A Na5 99.32(3) 1_565 . ?
O3A Na3A Na5 149.30(3) 1_565 . ?
Si2A Na3A Na5 81.82(2) . . ?
O10A Na3A Na5 148.88(3) 1_665 . ?
O13A Na3A P 104.03(4) 2_666 1_665 ?
O10A Na3A P 133.60(3) 1_565 1_665 ?
O7A Na3A P 152.99(3) . 1_665 ?
O6A Na3A P 89.76(3) . 1_665 ?
O4A Na3A P 107.82(3) 1_565 1_665 ?
O3A Na3A P 62.85(3) 1_565 1_665 ?
Si2A Na3A P 121.67(2) . 1_665 ?
Na5 Na3A P 147.83(2) . 1_665 ?
O11A Na3A Nb1 132.57(4) 1_565 . ?
O13A Na3A Nb1 111.24(4) 2_666 . ?
O6A Na3A Nb1 92.47(3) . . ?
O3A Na3A Nb1 88.08(3) 1_565 . ?
Si2A Na3A Nb1 64.357(14) . . ?
O10A Na3A Nb1 141.22(3) 1_665 . ?
Na5 Na3A Nb1 63.284(19) . . ?
P Na3A Nb1 144.08(2) 1_665 . ?
O11A Na4 O13A 128.43(5) . 2_666 ?
O11A Na4 O12A 112.85(5) . . ?
O13A Na4 O12A 95.80(5) 2_666 . ?
O11A Na4 O1A 107.04(5) . . ?
O13A Na4 O1A 112.25(5) 2_666 . ?
O12A Na4 O1A 95.01(5) . . ?
O11A Na4 O12A 80.77(4) . 2_666 ?
O13A Na4 O12A 53.93(4) 2_666 2_666 ?
O12A Na4 O12A 94.71(4) . 2_666 ?
O1A Na4 O12A 163.92(4) . 2_666 ?
O11A Na4 P 99.93(4) . 2_666 ?
O12A Na4 P 107.04(4) . 2_666 ?
O1A Na4 P 134.90(4) . 2_666 ?
O11A Na4 Na5 152.51(4) . . ?
O13A Na4 Na5 49.44(4) 2_666 . ?
O12A Na4 Na5 49.49(3) . . ?
O1A Na4 Na5 96.41(3) . . ?
O12A Na4 Na5 80.33(3) 2_666 . ?
P Na4 Na5 71.67(2) 2_666 . ?
O11A Na4 O12A 52.36(4) . 1_655 ?
O13A Na4 O12A 101.32(4) 2_666 1_655 ?
O12A Na4 O12A 162.40(5) . 1_655 ?
O1A Na4 O12A 82.37(4) . 1_655 ?
O12A Na4 O12A 92.07(3) 2_666 1_655 ?
P Na4 O12A 86.55(3) 2_666 1_655 ?
Na5 Na4 O12A 148.01(3) . 1_655 ?
O13A Na4 P 117.99(4) 2_666 1_655 ?
O12A Na4 P 136.80(4) . 1_655 ?
O1A Na4 P 95.90(3) . 1_655 ?
O12A Na4 P 85.68(3) 2_666 1_655 ?
P Na4 P 94.03(2) 2_666 1_655 ?
Na5 Na4 P 165.40(3) . 1_655 ?
O13A Na4 Na5 98.43(4) 2_666 2_666 ?
O12A Na4 Na5 89.11(4) . 2_666 ?
O1A Na4 Na5 148.38(4) . 2_666 ?
P Na4 Na5 72.36(2) 2_666 2_666 ?
Na5 Na4 Na5 109.75(3) . 2_666 ?
O12A Na4 Na5 84.37(3) 1_655 2_666 ?
P Na4 Na5 61.503(19) 1_655 2_666 ?
O11A Na4 P 88.05(4) . . ?
O13A Na4 P 110.19(4) 2_666 . ?
O1A Na4 P 106.89(3) . . ?
O12A Na4 P 87.10(3) 2_666 . ?
P Na4 P 109.54(2) 2_666 . ?
Na5 Na4 P 71.23(2) . . ?
O12A Na4 P 139.85(3) 1_655 . ?
P Na4 P 112.40(2) 1_655 . ?
Na5 Na4 P 67.27(2) 2_666 . ?
O11A Na4 Si2A 129.85(4) . . ?
O13A Na4 Si2A 84.86(4) 2_666 . ?
O12A Na4 Si2A 96.51(3) . . ?
O12A Na4 Si2A 138.16(3) 2_666 . ?
P Na4 Si2A 109.40(2) 2_666 . ?
Na5 Na4 Si2A 76.93(2) . . ?
O12A Na4 Si2A 89.15(3) 1_655 . ?
P Na4 Si2A 111.69(2) 1_655 . ?
Na5 Na4 Si2A 173.19(3) 2_666 . ?
P Na4 Si2A 117.28(2) . . ?
O11A Na5 O10A 108.68(5) 2_666 1_565 ?
O11A Na5 O13A 96.86(5) 2_666 2_666 ?
O10A Na5 O13A 92.72(5) 1_565 2_666 ?
O11A Na5 O12A 96.20(5) 2_666 . ?
O10A Na5 O12A 154.01(5) 1_565 . ?
O13A Na5 O12A 91.62(5) 2_666 . ?
O11A Na5 O7A 174.22(5) 2_666 . ?
O10A Na5 O7A 66.09(4) 1_565 . ?
O13A Na5 O7A 81.26(4) 2_666 . ?
O12A Na5 O7A 89.33(4) . . ?
O11A Na5 O6A 121.64(5) 2_666 1_455 ?
O10A Na5 O6A 66.10(4) 1_565 1_455 ?
O13A Na5 O6A 139.86(4) 2_666 1_455 ?
O12A Na5 O6A 94.74(4) . 1_455 ?
O7A Na5 O6A 59.28(3) . 1_455 ?
O11A Na5 Na4 112.59(4) 2_666 . ?
O10A Na5 Na4 123.88(4) 1_565 . ?
O13A Na5 Na4 46.82(3) 2_666 . ?
O12A Na5 Na4 47.71(3) . . ?
O7A Na5 Na4 70.08(3) . . ?
O6A Na5 Na4 116.76(3) 1_455 . ?
O11A Na5 Na3A 126.05(4) 2_666 . ?
O10A Na5 Na3A 50.67(3) 1_565 . ?
O13A Na5 Na3A 47.31(3) 2_666 . ?
O12A Na5 Na3A 119.11(4) . . ?
O7A Na5 Na3A 49.00(3) . . ?
O6A Na5 Na3A 96.25(3) 1_455 . ?
Na4 Na5 Na3A 74.34(3) . . ?
O11A Na5 Na1 134.34(4) 2_666 . ?
O10A Na5 Na1 108.22(4) 1_565 . ?
O13A Na5 Na1 107.29(4) 2_666 . ?
O12A Na5 Na1 46.28(3) . . ?
O7A Na5 Na1 51.30(3) . . ?
O6A Na5 Na1 54.53(3) 1_455 . ?
Na4 Na5 Na1 65.04(2) . . ?
Na3A Na5 Na1 98.18(3) . . ?
O10A Na5 Na4 142.43(4) 1_565 2_666 ?
O13A Na5 Na4 72.47(4) 2_666 2_666 ?
O12A Na5 Na4 62.87(3) . 2_666 ?
O7A Na5 Na4 140.32(3) . 2_666 ?
O6A Na5 Na4 143.95(4) 1_455 2_666 ?
Na4 Na5 Na4 70.25(3) . 2_666 ?
Na3A Na5 Na4 119.03(3) . 2_666 ?
Na1 Na5 Na4 109.13(3) . 2_666 ?
O11A Na5 O13A 49.94(4) 2_666 2_566 ?
O10A Na5 O13A 94.41(4) 1_565 2_566 ?
O13A Na5 O13A 146.50(5) 2_666 2_566 ?
O12A Na5 O13A 96.00(4) . 2_566 ?
O7A Na5 O13A 131.25(4) . 2_566 ?
O6A Na5 O13A 71.98(3) 1_455 2_566 ?
Na4 Na5 O13A 141.44(3) . 2_566 ?
Na3A Na5 O13A 144.10(3) . 2_566 ?
Na1 Na5 O13A 101.41(3) . 2_566 ?
Na4 Na5 O13A 82.17(3) 2_666 2_566 ?
O10A Na5 P 104.57(3) 1_565 2_566 ?
O13A Na5 P 119.99(4) 2_666 2_566 ?
O12A Na5 P 95.31(3) . 2_566 ?
O7A Na5 P 157.99(3) . 2_566 ?
O6A Na5 P 98.83(3) 1_455 2_566 ?
Na4 Na5 P 127.75(3) . 2_566 ?
Na3A Na5 P 140.95(3) . 2_566 ?
Na1 Na5 P 119.86(3) . 2_566 ?
Na4 Na5 P 58.968(19) 2_666 2_566 ?
O8A Nb1 O3A 96.61(5) . 1_465 ?
O8A Nb1 O4A 93.47(5) . 1_565 ?
O3A Nb1 O4A 91.94(5) 1_465 1_565 ?
O8A Nb1 O6A 94.08(4) . 1_455 ?
O3A Nb1 O6A 89.96(5) 1_465 1_455 ?
O4A Nb1 O6A 171.95(5) 1_565 1_455 ?
O8A Nb1 O7A 93.86(4) . . ?
O3A Nb1 O7A 169.33(5) 1_465 . ?
O4A Nb1 O7A 89.50(5) 1_565 . ?
O6A Nb1 O7A 87.22(4) 1_455 . ?
O8A Nb1 O10A 176.00(4) . 1_565 ?
O3A Nb1 O10A 86.64(4) 1_465 1_565 ?
O4A Nb1 O10A 84.06(5) 1_565 1_565 ?
O6A Nb1 O10A 88.25(4) 1_455 1_565 ?
O7A Nb1 O10A 82.99(4) . 1_565 ?
O8A Nb1 Na3A 127.16(4) . . ?
O3A Nb1 Na3A 124.29(4) 1_465 . ?
O4A Nb1 Na3A 57.30(4) 1_565 . ?
O6A Nb1 Na3A 115.46(3) 1_455 . ?
O7A Nb1 Na3A 48.81(3) . . ?
O10A Nb1 Na3A 48.84(3) 1_565 . ?
O8A Nb1 Na5 135.54(4) . . ?
O3A Nb1 Na5 116.40(4) 1_465 . ?
O4A Nb1 Na5 113.03(4) 1_565 . ?
O6A Nb1 Na5 59.26(3) 1_455 . ?
O7A Nb1 Na5 53.60(3) . . ?
Na3A Nb1 Na5 56.636(18) . . ?
O8A Nb1 Na1 104.82(4) . 1_565 ?
O4A Nb1 Na1 50.04(4) 1_565 1_565 ?
O6A Nb1 Na1 130.02(3) 1_455 1_565 ?
O7A Nb1 Na1 135.50(3) . 1_565 ?
O10A Nb1 Na1 75.99(3) 1_565 1_565 ?
Na3A Nb1 Na1 88.977(15) . 1_565 ?
Na5 Nb1 Na1 119.607(17) . 1_565 ?
O8A Nb1 Na3A 124.84(3) . 1_455 ?
O3A Nb1 Na3A 58.53(4) 1_465 1_455 ?
O4A Nb1 Na3A 131.50(4) 1_565 1_455 ?
O7A Nb1 Na3A 113.25(3) . 1_455 ?
O10A Nb1 Na3A 58.93(3) 1_565 1_455 ?
Na3A Nb1 Na3A 105.859(19) . 1_455 ?
Na5 Nb1 Na3A 61.618(17) . 1_455 ?
Na1 Nb1 Na3A 88.604(15) 1_565 1_455 ?
O3A Nb1 Na2 65.26(4) 1_465 1_455 ?
O4A Nb1 Na2 106.95(4) 1_565 1_455 ?
O6A Nb1 Na2 80.93(3) 1_455 1_455 ?
O7A Nb1 Na2 124.27(3) . 1_455 ?
O10A Nb1 Na2 149.68(3) 1_565 1_455 ?
Na3A Nb1 Na2 159.175(17) . 1_455 ?
Na5 Nb1 Na2 139.764(19) . 1_455 ?
Na1 Nb1 Na2 89.453(16) 1_565 1_455 ?
Na3A Nb1 Na2 94.859(18) 1_455 1_455 ?
O3A Nb1 Na2 74.71(4) 1_465 2_675 ?
O4A Nb1 Na2 57.10(4) 1_565 2_675 ?
O6A Nb1 Na2 130.90(3) 1_455 2_675 ?
O7A Nb1 Na2 114.69(3) . 2_675 ?
O10A Nb1 Na2 135.33(3) 1_565 2_675 ?
Na3A Nb1 Na2 111.543(17) . 2_675 ?
Na5 Nb1 Na2 166.642(17) . 2_675 ?
Na1 Nb1 Na2 62.642(16) 1_565 2_675 ?
Na3A Nb1 Na2 131.293(15) 1_455 2_675 ?
Na2 Nb1 Na2 50.15(2) 1_455 2_675 ?
O9A Nb2 O8A 94.77(4) 1_655 2_665 ?
O9A Nb2 O9A 82.77(4) 1_655 2_665 ?
O8A Nb2 O9A 96.39(4) 2_665 2_665 ?
O9A Nb2 O2A 93.94(4) 1_655 . ?
O8A Nb2 O2A 85.63(4) 2_665 . ?
O9A Nb2 O2A 176.26(4) 2_665 . ?
O9A Nb2 O5A 170.84(4) 1_655 2_665 ?
O8A Nb2 O5A 94.12(4) 2_665 2_665 ?
O9A Nb2 O5A 94.05(4) 2_665 2_665 ?
O2A Nb2 O5A 88.94(4) . 2_665 ?
O9A Nb2 O5A 93.59(4) 1_655 . ?
O8A Nb2 O5A 169.53(4) 2_665 . ?
O9A Nb2 O5A 90.90(4) 2_665 . ?
O2A Nb2 O5A 87.51(4) . . ?
O5A Nb2 O5A 77.83(4) 2_665 . ?
O8A Nb2 Nb2 97.45(3) 2_665 2_765 ?
O2A Nb2 Nb2 135.61(3) . 2_765 ?
O5A Nb2 Nb2 134.52(3) 2_665 2_765 ?
O5A Nb2 Nb2 92.98(3) . 2_765 ?
O9A Nb2 Na2 48.64(3) 1_655 2_765 ?
O8A Nb2 Na2 47.38(3) 2_665 2_765 ?
O9A Nb2 Na2 98.24(4) 2_665 2_765 ?
O2A Nb2 Na2 80.80(3) . 2_765 ?
O5A Nb2 Na2 140.52(3) 2_665 2_765 ?
O5A Nb2 Na2 138.86(3) . 2_765 ?
Nb2 Nb2 Na2 70.029(18) 2_765 2_765 ?
O9A Nb2 Na2 131.98(3) 1_655 2_665 ?
O8A Nb2 Na2 85.84(3) 2_665 2_665 ?
O9A Nb2 Na2 145.02(3) 2_665 2_665 ?
O5A Nb2 Na2 51.02(3) 2_665 2_665 ?
O5A Nb2 Na2 83.88(3) . 2_665 ?
Nb2 Nb2 Na2 172.914(17) 2_765 2_665 ?
Na2 Nb2 Na2 108.36(2) 2_765 2_665 ?
O9A Nb2 Na2 89.13(3) 1_655 . ?
O8A Nb2 Na2 136.43(3) 2_665 . ?
O2A Nb2 Na2 137.46(3) . . ?
O5A Nb2 Na2 82.89(3) 2_665 . ?
O5A Nb2 Na2 49.94(3) . . ?
Nb2 Nb2 Na2 58.961(14) 2_765 . ?
Na2 Nb2 Na2 128.990(13) 2_765 . ?
Na2 Nb2 Na2 122.246(14) 2_665 . ?
O9A Nb2 Na2 92.14(3) 1_655 1_545 ?
O8A Nb2 Na2 46.55(3) 2_665 1_545 ?
O9A Nb2 Na2 142.22(3) 2_665 1_545 ?
O5A Nb2 Na2 95.58(3) 2_665 1_545 ?
O5A Nb2 Na2 126.83(3) . 1_545 ?
Nb2 Nb2 Na2 123.688(15) 2_765 1_545 ?
Na2 Nb2 Na2 53.71(2) 2_765 1_545 ?
Na2 Nb2 Na2 54.834(19) 2_665 1_545 ?
Na2 Nb2 Na2 176.64(3) . 1_545 ?
O9A Nb2 Na1 108.53(3) 1_655 2_665 ?
O8A Nb2 Na1 77.34(3) 2_665 2_665 ?
O2A Nb2 Na1 152.65(3) . 2_665 ?
O5A Nb2 Na1 71.36(3) 2_665 2_665 ?
O5A Nb2 Na1 105.89(3) . 2_665 ?
Nb2 Nb2 Na1 68.663(13) 2_765 2_665 ?
Na2 Nb2 Na1 102.18(2) 2_765 2_665 ?
Na2 Nb2 Na1 118.296(17) 2_665 2_665 ?
Na2 Nb2 Na1 60.449(17) . 2_665 ?
Na2 Nb2 Na1 121.932(17) 1_545 2_665 ?
O4A Si1A O2A 112.50(6) . . ?
O4A Si1A O3A 112.58(7) . . ?
O2A Si1A O3A 110.77(6) . . ?
O4A Si1A O1A 106.16(6) . . ?
O2A Si1A O1A 109.46(5) . . ?
O3A Si1A O1A 104.96(6) . . ?
O4A Si1A Na1 147.42(5) . 1_655 ?
O2A Si1A Na1 100.08(4) . 1_655 ?
O3A Si1A Na1 51.65(5) . 1_655 ?
O1A Si1A Na1 60.96(4) . 1_655 ?
O4A Si1A Na2 71.84(5) . 2_665 ?
O3A Si1A Na2 139.41(5) . 2_665 ?
O1A Si1A Na2 112.46(4) . 2_665 ?
Na1 Si1A Na2 140.02(2) 1_655 2_665 ?
O4A Si1A Na1 55.73(5) . . ?
O2A Si1A Na1 102.20(4) . . ?
O3A Si1A Na1 146.71(5) . . ?
O1A Si1A Na1 57.95(4) . . ?
Na1 Si1A Na1 118.82(2) 1_655 . ?
Na2 Si1A Na1 70.92(2) 2_665 . ?
O4A Si1A Na2 98.68(5) . 1_545 ?
O3A Si1A Na2 78.75(4) . 1_545 ?
O1A Si1A Na2 150.72(4) . 1_545 ?
Na1 Si1A Na2 104.31(2) 1_655 1_545 ?
Na2 Si1A Na2 60.95(2) 2_665 1_545 ?
Na1 Si1A Na2 130.989(19) . 1_545 ?
O4A Si1A Na4 80.30(5) . . ?
O2A Si1A Na4 150.00(4) . . ?
O3A Si1A Na4 86.75(4) . . ?
Na1 Si1A Na4 71.203(19) 1_655 . ?
Na2 Si1A Na4 132.36(2) 2_665 . ?
Na1 Si1A Na4 61.463(18) . . ?
Na2 Si1A Na4 163.88(2) 1_545 . ?
O4A Si1A Na3A 52.94(5) . 1_545 ?
O2A Si1A Na3A 148.82(4) . 1_545 ?
O3A Si1A Na3A 63.12(5) . 1_545 ?
O1A Si1A Na3A 101.49(4) . 1_545 ?
Na1 Si1A Na3A 98.104(19) 1_655 1_545 ?
Na2 Si1A Na3A 121.26(2) 2_665 1_545 ?
Na1 Si1A Na3A 90.781(18) . 1_545 ?
Na2 Si1A Na3A 105.81(2) 1_545 1_545 ?
Na4 Si1A Na3A 60.648(18) . 1_545 ?
O4A Si1A O5A 121.07(5) . . ?
O2A Si1A O5A 59.27(4) . . ?
O3A Si1A O5A 124.99(5) . . ?
O1A Si1A O5A 50.33(4) . . ?
Na1 Si1A O5A 75.68(2) 1_655 . ?
Na2 Si1A O5A 72.78(2) 2_665 . ?
Na1 Si1A O5A 68.85(2) . . ?
Na2 Si1A O5A 103.28(2) 1_545 . ?
Na4 Si1A O5A 90.76(2) . . ?
Na3A Si1A O5A 150.88(2) 1_545 . ?
O4A Si1A O9A 169.74(5) . 1_655 ?
O2A Si1A O9A 57.87(4) . 1_655 ?
O3A Si1A O9A 75.95(5) . 1_655 ?
O1A Si1A O9A 75.95(4) . 1_655 ?
Na2 Si1A O9A 98.01(3) 2_665 1_655 ?
Na1 Si1A O9A 120.33(2) . 1_655 ?
Na2 Si1A O9A 76.93(2) 1_545 1_655 ?
Na4 Si1A O9A 106.51(2) . 1_655 ?
Na3A Si1A O9A 137.01(2) 1_545 1_655 ?
O5A Si1A O9A 52.34(3) . 1_655 ?
O6A Si2A O7A 110.41(5) . . ?
O6A Si2A O5A 116.50(5) . . ?
O7A Si2A O5A 112.14(5) . . ?
O6A Si2A O1A 104.55(6) . . ?
O7A Si2A O1A 103.85(5) . . ?
O5A Si2A O1A 108.29(5) . . ?
O6A Si2A Na3A 56.72(4) . . ?
O7A Si2A Na3A 53.72(4) . . ?
O5A Si2A Na3A 137.50(4) . . ?
O1A Si2A Na3A 113.98(4) . . ?
O6A Si2A Na1 146.18(4) . . ?
O7A Si2A Na1 53.89(4) . . ?
O5A Si2A Na1 97.24(4) . . ?
O1A Si2A Na1 59.42(4) . . ?
Na3A Si2A Na1 100.21(2) . . ?
O6A Si2A Na1 57.85(4) . 1_655 ?
O7A Si2A Na1 143.79(4) . 1_655 ?
O5A Si2A Na1 103.00(4) . 1_655 ?
O1A Si2A Na1 55.03(4) . 1_655 ?
Na3A Si2A Na1 104.387(19) . 1_655 ?
Na1 Si2A Na1 114.45(2) . 1_655 ?
O6A Si2A Na4 85.74(4) . . ?
O7A Si2A Na4 76.03(4) . . ?
O5A Si2A Na4 148.86(4) . . ?
Na3A Si2A Na4 72.332(19) . . ?
Na1 Si2A Na4 62.292(18) . . ?
Na1 Si2A Na4 69.285(18) 1_655 . ?
O6A Si2A O9A 75.85(4) . 1_655 ?
O7A Si2A O9A 173.27(4) . 1_655 ?
O5A Si2A O9A 61.87(4) . 1_655 ?
O1A Si2A O9A 76.28(4) . 1_655 ?
Na3A Si2A O9A 132.56(2) . 1_655 ?
Na1 Si2A O9A 122.18(2) . 1_655 ?
Na4 Si2A O9A 107.45(2) . 1_655 ?
O6A Si2A O2A 122.33(4) . . ?
O7A Si2A O2A 124.60(4) . . ?
O5A Si2A O2A 58.80(4) . . ?
O1A Si2A O2A 49.64(4) . . ?
Na3A Si2A O2A 163.63(2) . . ?
Na1 Si2A O2A 72.29(2) . . ?
Na1 Si2A O2A 67.38(2) 1_655 . ?
Na4 Si2A O2A 91.34(2) . . ?
O9A Si2A O2A 50.38(2) 1_655 . ?
O6A Si2A Na2 82.39(4) . . ?
O7A Si2A Na2 110.03(4) . . ?
O1A Si2A Na2 140.46(4) . . ?
Na3A Si2A Na2 102.44(2) . . ?
Na1 Si2A Na2 129.735(18) . . ?
Na1 Si2A Na2 102.403(18) 1_655 . ?
Na4 Si2A Na2 167.964(19) . . ?
O9A Si2A Na2 67.69(2) 1_655 . ?
O2A Si2A Na2 93.33(2) . . ?
O11A P O13A 109.94(7) 1_455 . ?
O11A P O12A 110.24(7) 1_455 . ?
O13A P O12A 109.32(7) . . ?
O11A P O10A 108.19(6) 1_455 . ?
O13A P O10A 108.16(6) . . ?
O12A P O10A 110.95(6) . . ?
O11A P Na4 95.81(5) 1_455 2_666 ?
O13A P Na4 46.14(4) . 2_666 ?
O12A P Na4 74.26(5) . 2_666 ?
O10A P Na4 150.82(4) . 2_666 ?
O13A P Na3A 123.61(5) . 1_445 ?
O12A P Na3A 124.28(5) . 1_445 ?
O10A P Na3A 69.75(4) . 1_445 ?
Na4 P Na3A 132.51(2) 2_666 1_445 ?
O13A P Na4 124.11(5) . 1_455 ?
O12A P Na4 73.21(5) . 1_455 ?
O10A P Na4 123.20(4) . 1_455 ?
Na4 P Na4 85.97(2) 2_666 1_455 ?
Na3A P Na4 64.034(19) 1_445 1_455 ?
O11A P O3A 77.74(5) 1_455 1_455 ?
O13A P O3A 166.54(5) . 1_455 ?
O12A P O3A 76.92(5) . 1_455 ?
O10A P O3A 58.44(4) . 1_455 ?
Na4 P O3A 146.09(3) 2_666 1_455 ?
Na3A P O3A 55.68(2) 1_445 1_455 ?
Na4 P O3A 68.75(2) 1_455 1_455 ?
O11A P Na4 148.84(5) 1_455 . ?
O13A P Na4 81.15(5) . . ?
O10A P Na4 94.82(4) . . ?
Na4 P Na4 70.46(2) 2_666 . ?
Na3A P Na4 153.43(2) 1_445 . ?
Na4 P Na4 112.40(2) 1_455 . ?
O3A P Na4 97.93(3) 1_455 . ?
O13A P Na5 74.74(5) . 2_566 ?
O12A P Na5 120.36(5) . 2_566 ?
O10A P Na5 124.34(4) . 2_566 ?
Na4 P Na5 68.55(2) 2_666 2_566 ?
Na3A P Na5 64.639(19) 1_445 2_566 ?
Na4 P Na5 59.529(19) 1_455 2_566 ?
O3A P Na5 112.99(3) 1_455 2_566 ?
Na4 P Na5 138.63(2) . 2_566 ?
O11A P Na1 100.05(5) 1_455 . ?
O13A P Na1 140.96(5) . . ?
O10A P Na1 84.51(4) . . ?
Na4 P Na1 107.87(2) 2_666 . ?
Na3A P Na1 95.425(18) 1_445 . ?
Na4 P Na1 69.354(19) 1_455 . ?
Na4 P Na1 60.695(17) . . ?
Na5 P Na1 128.85(2) 2_566 . ?
O11A P Na3A 147.30(5) 1_455 1_545 ?
O13A P Na3A 80.91(5) . 1_545 ?
O12A P Na3A 93.76(5) . 1_545 ?
Na4 P Na3A 112.34(2) 2_666 1_545 ?
Na3A P Na3A 109.50(2) 1_445 1_545 ?
Na4 P Na3A 154.217(19) 1_455 1_545 ?
O3A P Na3A 86.87(2) 1_455 1_545 ?
Na4 P Na3A 61.260(18) . 1_545 ?
Na5 P Na3A 142.959(19) 2_566 1_545 ?
Na1 P Na3A 87.248(18) . 1_545 ?
Si1A O1A Si2A 136.64(6) . . ?
Si1A O1A Na4 112.31(5) . . ?
Si2A O1A Na4 110.67(5) . . ?
Si1A O1A O7A 143.15(6) . . ?
Na4 O1A O7A 84.77(4) . . ?
Si2A O1A O3A 142.84(6) . . ?
Na4 O1A O3A 94.71(4) . . ?
O7A O1A O3A 179.42(6) . . ?
Si1A O1A O6A 142.93(6) . . ?
Na4 O1A O6A 93.00(4) . . ?
O7A O1A O6A 62.02(4) . . ?
O3A O1A O6A 118.29(5) . . ?
Si2A O1A O4A 141.59(6) . . ?
Na4 O1A O4A 88.68(4) . . ?
O7A O1A O4A 117.83(5) . . ?
O3A O1A O4A 61.88(4) . . ?
O6A O1A O4A 178.28(5) . . ?
Si2A O1A O2A 102.04(5) . . ?
Na4 O1A O2A 146.68(5) . . ?
O7A O1A O2A 119.92(5) . . ?
O3A O1A O2A 60.46(4) . . ?
O6A O1A O2A 117.67(5) . . ?
O4A O1A O2A 60.78(4) . . ?
Si1A O1A O5A 101.11(5) . . ?
Na4 O1A O5A 145.22(5) . . ?
O7A O1A O5A 62.01(4) . . ?
O3A O1A O5A 118.55(5) . . ?
O6A O1A O5A 63.45(4) . . ?
O4A O1A O5A 114.88(5) . . ?
O2A O1A O5A 66.59(4) . . ?
Si1A O1A Na1 86.68(4) . 1_655 ?
Si2A O1A Na1 94.84(5) . 1_655 ?
Na4 O1A Na1 95.43(4) . 1_655 ?
O7A O1A Na1 125.43(5) . 1_655 ?
O3A O1A Na1 54.86(4) . 1_655 ?
O6A O1A Na1 63.48(4) . 1_655 ?
O4A O1A Na1 116.73(5) . 1_655 ?
O2A O1A Na1 87.79(4) . 1_655 ?
O5A O1A Na1 95.87(4) . 1_655 ?
Si1A O1A Na1 91.13(5) . . ?
Si2A O1A Na1 89.09(4) . . ?
Na4 O1A Na1 82.25(4) . . ?
O7A O1A Na1 57.81(3) . . ?
O3A O1A Na1 121.88(5) . . ?
O6A O1A Na1 119.83(4) . . ?
O4A O1A Na1 60.03(4) . . ?
O2A O1A Na1 92.34(4) . . ?
O5A O1A Na1 87.89(4) . . ?
Na1 O1A Na1 175.95(5) 1_655 . ?
Si1A O1A O9A 76.03(4) . 1_655 ?
Si2A O1A O9A 75.65(4) . 1_655 ?
Na4 O1A O9A 138.89(5) . 1_655 ?
O7A O1A O9A 113.08(4) . 1_655 ?
O3A O1A O9A 67.48(4) . 1_655 ?
O6A O1A O9A 67.24(4) . 1_655 ?
O4A O1A O9A 111.64(4) . 1_655 ?
O2A O1A O9A 55.39(3) . 1_655 ?
O5A O1A O9A 57.65(3) . 1_655 ?
Na1 O1A O9A 138.82(4) . 1_655 ?
Si1A O2A Nb2 128.19(6) . . ?
Si1A O2A Na2 109.60(6) . 2_665 ?
Nb2 O2A Na2 107.96(5) . 2_665 ?
Si1A O2A Na2 106.99(5) . 1_545 ?
Nb2 O2A Na2 108.20(5) . 1_545 ?
Na2 O2A Na2 88.77(4) 2_665 1_545 ?
Nb2 O2A O3A 117.20(5) . . ?
Na2 O2A O3A 134.49(5) 2_665 . ?
Na2 O2A O3A 82.69(4) 1_545 . ?
Nb2 O2A O1A 96.26(4) . . ?
Na2 O2A O1A 112.92(5) 2_665 . ?
Na2 O2A O1A 140.59(5) 1_545 . ?
O3A O2A O1A 58.44(4) . . ?
Nb2 O2A O4A 152.94(5) . . ?
Na2 O2A O4A 77.00(5) 2_665 . ?
Na2 O2A O4A 98.37(5) 1_545 . ?
O3A O2A O4A 60.40(4) . . ?
O1A O2A O4A 58.53(4) . . ?
Si1A O2A O8A 147.10(6) . 2_665 ?
Nb2 O2A O8A 45.66(3) . 2_665 ?
Na2 O2A O8A 101.63(5) 2_665 2_665 ?
Na2 O2A O8A 62.77(4) 1_545 2_665 ?
O3A O2A O8A 113.38(5) . 2_665 ?
O1A O2A O8A 135.92(5) . 2_665 ?
O4A O2A O8A 161.14(5) . 2_665 ?
Si1A O2A O9A 94.26(5) . 1_655 ?
Na2 O2A O9A 149.44(5) 2_665 1_655 ?
Na2 O2A O9A 102.58(4) 1_545 1_655 ?
O3A O2A O9A 75.63(4) . 1_655 ?
O1A O2A O9A 75.68(4) . 1_655 ?
O4A O2A O9A 127.88(5) . 1_655 ?
O8A O2A O9A 60.96(4) 2_665 1_655 ?
Si1A O2A O5A 92.61(5) . . ?
Nb2 O2A O5A 48.32(3) . . ?
Na2 O2A O5A 96.99(4) 2_665 . ?
Na2 O2A O5A 156.45(5) 1_545 . ?
O3A O2A O5A 108.35(4) . . ?
O1A O2A O5A 56.78(3) . . ?
O4A O2A O5A 105.17(4) . . ?
O8A O2A O5A 93.68(4) 2_665 . ?
O9A O2A O5A 62.12(4) 1_655 . ?
Si1A O2A O5A 141.76(6) . 2_665 ?
Nb2 O2A O5A 47.25(3) . 2_665 ?
Na2 O2A O5A 60.92(4) 2_665 2_665 ?
Na2 O2A O5A 109.56(4) 1_545 2_665 ?
O3A O2A O5A 161.98(5) . 2_665 ?
O1A O2A O5A 109.74(4) . 2_665 ?
O4A O2A O5A 127.70(5) . 2_665 ?
O8A O2A O5A 64.16(4) 2_665 2_665 ?
O9A O2A O5A 88.53(4) 1_655 2_665 ?
O5A O2A O5A 55.48(4) . 2_665 ?
Si1A O2A O2A 115.96(6) . 2_655 ?
Nb2 O2A O2A 115.73(5) . 2_655 ?
Na2 O2A O2A 46.22(3) 2_665 2_655 ?
O3A O2A O2A 112.46(5) . 2_655 ?
O1A O2A O2A 145.22(6) . 2_655 ?
O4A O2A O2A 87.31(5) . 2_655 ?
O8A O2A O2A 78.81(4) 2_665 2_655 ?
O9A O2A O2A 137.71(5) 1_655 2_655 ?
O5A O2A O2A 138.10(5) . 2_655 ?
O5A O2A O2A 85.01(4) 2_665 2_655 ?
Si1A O3A Nb1 153.55(8) . 1_645 ?
Si1A O3A Na1 97.20(5) . 1_655 ?
Nb1 O3A Na1 105.19(5) 1_645 1_655 ?
Nb1 O3A O1A 168.30(6) 1_645 . ?
Na1 O3A O1A 64.95(4) 1_655 . ?
Nb1 O3A O2A 128.08(6) 1_645 . ?
Na1 O3A O2A 93.94(5) 1_655 . ?
O1A O3A O2A 61.10(4) . . ?
Nb1 O3A O4A 130.07(6) 1_645 . ?
Na1 O3A O4A 124.24(5) 1_655 . ?
O1A O3A O4A 59.30(4) . . ?
O2A O3A O4A 60.15(4) . . ?
Si1A O3A O6A 114.65(6) . 1_545 ?
Nb1 O3A O6A 46.50(3) 1_645 1_545 ?
Na1 O3A O6A 147.46(5) 1_655 1_545 ?
O1A O3A O6A 140.18(6) . 1_545 ?
O2A O3A O6A 115.85(5) . 1_545 ?
O4A O3A O6A 84.13(5) . 1_545 ?
Si1A O3A O4A 149.47(7) . 1_655 ?
Na1 O3A O4A 61.31(4) 1_655 1_655 ?
O1A O3A O4A 126.21(6) . 1_655 ?
O2A O3A O4A 120.18(6) . 1_655 ?
O4A O3A O4A 174.34(7) . 1_655 ?
O6A O3A O4A 90.93(4) 1_545 1_655 ?
Si1A O3A O10A 146.58(7) . 1_655 ?
Nb1 O3A O10A 50.35(3) 1_645 1_655 ?
Na1 O3A O10A 87.09(4) 1_655 1_655 ?
O1A O3A O10A 120.52(5) . 1_655 ?
O2A O3A O10A 178.36(5) . 1_655 ?
O4A O3A O10A 120.21(6) . 1_655 ?
O6A O3A O10A 62.85(4) 1_545 1_655 ?
O4A O3A O10A 59.28(4) 1_655 1_655 ?
Si1A O3A O8A 117.62(6) . 1_645 ?
Na1 O3A O8A 111.01(5) 1_655 1_645 ?
O1A O3A O8A 146.91(5) . 1_645 ?
O2A O3A O8A 87.42(5) . 1_645 ?
O4A O3A O8A 115.47(5) . 1_645 ?
O6A O3A O8A 60.79(4) 1_545 1_645 ?
O4A O3A O8A 59.39(4) 1_655 1_645 ?
O10A O3A O8A 91.02(4) 1_655 1_645 ?
Si1A O3A Na3A 88.57(5) . 1_545 ?
Nb1 O3A Na3A 89.08(4) 1_645 1_545 ?
Na1 O3A Na3A 126.92(5) 1_655 1_545 ?
O1A O3A Na3A 92.26(4) . 1_545 ?
O2A O3A Na3A 116.87(5) . 1_545 ?
O4A O3A Na3A 57.18(4) . 1_545 ?
O6A O3A Na3A 51.74(3) 1_545 1_545 ?
O4A O3A Na3A 121.38(5) 1_655 1_545 ?
O10A O3A Na3A 63.31(3) 1_655 1_545 ?
O8A O3A Na3A 112.41(4) 1_645 1_545 ?
Si1A O3A P 122.51(6) . 1_655 ?
Nb1 O3A P 78.70(4) 1_645 1_655 ?
Na1 O3A P 71.54(3) 1_655 1_655 ?
O1A O3A P 91.74(4) . 1_655 ?
O2A O3A P 152.82(5) . 1_655 ?
O4A O3A P 108.57(5) . 1_655 ?
O6A O3A P 85.16(4) 1_545 1_655 ?
O4A O3A P 73.65(4) 1_655 1_655 ?
O8A O3A P 118.97(4) 1_645 1_655 ?
Na3A O3A P 61.47(3) 1_545 1_655 ?
Si1A O4A Nb1 163.53(8) . 1_545 ?
Nb1 O4A O1A 157.17(7) 1_545 . ?
Nb1 O4A O2A 132.54(6) 1_545 . ?
O1A O4A O2A 60.69(4) . . ?
Nb1 O4A O3A 141.77(7) 1_545 . ?
O1A O4A O3A 58.82(4) . . ?
O2A O4A O3A 59.45(4) . . ?
Si1A O4A Na1 94.59(5) . . ?
Nb1 O4A Na1 95.96(5) 1_545 . ?
O1A O4A Na1 62.35(4) . . ?
O2A O4A Na1 93.64(5) . . ?
O3A O4A Na1 121.14(5) . . ?
Si1A O4A Na3A 99.33(6) . 1_545 ?
Nb1 O4A Na3A 86.03(4) 1_545 1_545 ?
O1A O4A Na3A 98.81(5) . 1_545 ?
O2A O4A Na3A 126.87(5) . 1_545 ?
O3A O4A Na3A 67.99(4) . 1_545 ?
Na1 O4A Na3A 120.89(5) . 1_545 ?
Si1A O4A O10A 143.19(7) . . ?
Nb1 O4A O10A 51.05(3) 1_545 . ?
O1A O4A O10A 115.18(5) . . ?
O2A O4A O10A 175.83(6) . . ?
O3A O4A O10A 119.55(6) . . ?
Na1 O4A O10A 83.52(4) . . ?
Na3A O4A O10A 53.00(3) 1_545 . ?
Si1A O4A O8A 122.99(6) . 1_545 ?
O1A O4A O8A 146.40(6) . 1_545 ?
O2A O4A O8A 91.14(5) . 1_545 ?
O3A O4A O8A 124.46(5) . 1_545 ?
Na1 O4A O8A 105.35(5) . 1_545 ?
Na3A O4A O8A 113.47(5) 1_545 1_545 ?
O10A O4A O8A 92.56(4) . 1_545 ?
Si1A O4A O3A 142.56(7) . 1_455 ?
O1A O4A O3A 115.65(6) . 1_455 ?
O2A O4A O3A 119.90(6) . 1_455 ?
O3A O4A O3A 174.34(7) . 1_455 ?
Na1 O4A O3A 53.30(4) . 1_455 ?
Na3A O4A O3A 113.18(5) 1_545 1_455 ?
O10A O4A O3A 60.64(4) . 1_455 ?
O8A O4A O3A 60.62(4) 1_545 1_455 ?
Si1A O4A O7A 126.54(7) . 1_545 ?
Nb1 O4A O7A 46.27(3) 1_545 1_545 ?
O1A O4A O7A 149.22(6) . 1_545 ?
O2A O4A O7A 123.91(5) . 1_545 ?
O3A O4A O7A 95.70(5) . 1_545 ?
Na1 O4A O7A 138.22(5) . 1_545 ?
Na3A O4A O7A 52.56(3) 1_545 1_545 ?
O10A O4A O7A 59.80(4) . 1_545 ?
O8A O4A O7A 60.97(4) 1_545 1_545 ?
O3A O4A O7A 89.15(4) 1_455 1_545 ?
Si1A O4A Na2 78.58(5) . 2_665 ?
Nb1 O4A Na2 90.82(5) 1_545 2_665 ?
O1A O4A Na2 92.12(4) . 2_665 ?
O2A O4A Na2 45.57(3) . 2_665 ?
O3A O4A Na2 103.50(5) . 2_665 ?
Na1 O4A Na2 80.06(4) . 2_665 ?
Na3A O4A Na2 159.01(5) 1_545 2_665 ?
O10A O4A Na2 136.36(5) . 2_665 ?
O8A O4A Na2 54.30(3) 1_545 2_665 ?
O3A O4A Na2 77.27(4) 1_455 2_665 ?
O7A O4A Na2 111.93(4) 1_545 2_665 ?
Si2A O5A Nb2 123.75(6) . 2_665 ?
Si2A O5A Nb2 122.50(5) . . ?
Nb2 O5A Nb2 102.17(4) 2_665 . ?
Nb2 O5A O1A 121.01(5) 2_665 . ?
Nb2 O5A O1A 92.65(4) . . ?
Si2A O5A Na2 117.68(5) . . ?
Nb2 O5A Na2 90.51(4) 2_665 . ?
Nb2 O5A Na2 91.82(4) . . ?
O1A O5A Na2 146.28(5) . . ?
Nb2 O5A O7A 90.93(4) 2_665 . ?
Nb2 O5A O7A 149.80(5) . . ?
O1A O5A O7A 57.55(4) . . ?
Na2 O5A O7A 115.43(4) . . ?
Si2A O5A O5A 150.45(7) . 2_665 ?
Nb2 O5A O5A 51.46(3) 2_665 2_665 ?
Nb2 O5A O5A 50.72(3) . 2_665 ?
O1A O5A O5A 116.42(6) . 2_665 ?
Na2 O5A O5A 91.86(5) . 2_665 ?
O7A O5A O5A 134.77(6) . 2_665 ?
Nb2 O5A O6A 146.01(5) 2_665 . ?
Nb2 O5A O6A 111.75(5) . . ?
O1A O5A O6A 56.94(4) . . ?
Na2 O5A O6A 90.51(4) . . ?
O7A O5A O6A 58.33(4) . . ?
O5A O5A O6A 162.37(7) 2_665 . ?
Si2A O5A O2A 92.67(4) . . ?
Nb2 O5A O2A 98.32(4) 2_665 . ?
O1A O5A O2A 56.62(3) . . ?
Na2 O5A O2A 135.98(4) . . ?
O7A O5A O2A 107.49(4) . . ?
O5A O5A O2A 62.65(4) 2_665 . ?
O6A O5A O2A 104.31(4) . . ?
Si2A O5A O2A 139.52(6) . 2_665 ?
Nb2 O5A O2A 97.17(4) . 2_665 ?
O1A O5A O2A 163.51(5) . 2_665 ?
Na2 O5A O2A 46.85(3) . 2_665 ?
O7A O5A O2A 110.78(4) . 2_665 ?
O5A O5A O2A 61.87(4) 2_665 2_665 ?
O6A O5A O2A 129.68(5) . 2_665 ?
O2A O5A O2A 124.52(4) . 2_665 ?
Si2A O5A O9A 134.19(6) . 2_665 ?
Nb2 O5A O9A 101.69(4) 2_665 2_665 ?
O1A O5A O9A 124.49(5) . 2_665 ?
Na2 O5A O9A 50.45(3) . 2_665 ?
O7A O5A O9A 160.49(5) . 2_665 ?
O5A O5A O9A 63.93(4) 2_665 2_665 ?
O6A O5A O9A 105.01(5) . 2_665 ?
O2A O5A O9A 85.56(4) . 2_665 ?
O2A O5A O9A 70.69(4) 2_665 2_665 ?
Si2A O5A O9A 89.53(5) . 1_655 ?
Nb2 O5A O9A 141.99(4) 2_665 1_655 ?
O1A O5A O9A 73.86(4) . 1_655 ?
Na2 O5A O9A 88.73(4) . 1_655 ?
O7A O5A O9A 123.34(4) . 1_655 ?
O5A O5A O9A 90.58(5) 2_665 1_655 ?
O6A O5A O9A 72.00(4) . 1_655 ?
O2A O5A O9A 58.62(3) . 1_655 ?
O2A O5A O9A 121.75(4) 2_665 1_655 ?
O9A O5A O9A 51.08(4) 2_665 1_655 ?
Si2A O6A Nb1 141.68(6) . 1_655 ?
Si2A O6A Na3A 91.06(5) . . ?
Nb1 O6A Na3A 102.24(4) 1_655 . ?
Nb1 O6A O1A 155.06(6) 1_655 . ?
Na3A O6A O1A 102.70(4) . . ?
Nb1 O6A O7A 139.71(6) 1_655 . ?
Na3A O6A O7A 56.15(3) . . ?
O1A O6A O7A 58.92(4) . . ?
Si2A O6A O3A 113.28(6) . 1_565 ?
Na3A O6A O3A 69.58(4) . 1_565 ?
O1A O6A O3A 151.46(5) . 1_565 ?
O7A O6A O3A 96.53(5) . 1_565 ?
Nb1 O6A O5A 110.95(5) 1_655 . ?
Na3A O6A O5A 111.31(5) . . ?
O1A O6A O5A 59.61(4) . . ?
O7A O6A O5A 59.74(4) . . ?
O3A O6A O5A 96.61(4) 1_565 . ?
Si2A O6A O7A 142.42(6) . 1_655 ?
Nb1 O6A O7A 46.62(3) 1_655 1_655 ?
Na3A O6A O7A 125.65(4) . 1_655 ?
O1A O6A O7A 115.38(5) . 1_655 ?
O7A O6A O7A 173.65(6) . 1_655 ?
O3A O6A O7A 89.69(4) 1_565 1_655 ?
O5A O6A O7A 120.88(5) . 1_655 ?
Si2A O6A Na1 92.70(5) . 1_655 ?
Nb1 O6A Na1 99.36(4) 1_655 1_655 ?
Na3A O6A Na1 139.62(4) . 1_655 ?
O1A O6A Na1 60.25(4) . 1_655 ?
O7A O6A Na1 119.10(4) . 1_655 ?
O3A O6A Na1 142.37(5) 1_565 1_655 ?
O5A O6A Na1 91.79(4) . 1_655 ?
O7A O6A Na1 55.14(3) 1_655 1_655 ?
Si2A O6A O8A 104.43(5) . 1_655 ?
Na3A O6A O8A 129.46(5) . 1_655 ?
O1A O6A O8A 119.24(5) . 1_655 ?
O7A O6A O8A 123.92(5) . 1_655 ?
O3A O6A O8A 60.04(4) 1_565 1_655 ?
O5A O6A O8A 72.53(4) . 1_655 ?
O7A O6A O8A 60.55(4) 1_655 1_655 ?
Na1 O6A O8A 88.20(4) 1_655 1_655 ?
Si2A O6A O10A 159.17(6) . 1_665 ?
Nb1 O6A O10A 47.93(3) 1_655 1_665 ?
Na3A O6A O10A 68.19(3) . 1_665 ?
O1A O6A O10A 145.50(5) . 1_665 ?
O7A O6A O10A 124.27(5) . 1_665 ?
O3A O6A O10A 58.96(4) 1_565 1_665 ?
O5A O6A O10A 154.82(5) . 1_665 ?
O7A O6A O10A 58.30(3) 1_655 1_665 ?
Na1 O6A O10A 104.20(4) 1_655 1_665 ?
O8A O6A O10A 88.42(4) 1_655 1_665 ?
Si2A O6A Na5 133.65(5) . 1_655 ?
Nb1 O6A Na5 84.28(4) 1_655 1_655 ?
Na3A O6A Na5 81.00(3) . 1_655 ?
O1A O6A Na5 99.07(4) . 1_655 ?
O7A O6A Na5 119.74(4) . 1_655 ?
O3A O6A Na5 106.42(4) 1_565 1_655 ?
O5A O6A Na5 156.66(5) . 1_655 ?
O7A O6A Na5 56.81(3) 1_655 1_655 ?
Na1 O6A Na5 67.65(3) 1_655 1_655 ?
O8A O6A Na5 115.80(4) 1_655 1_655 ?
O10A O6A Na5 47.53(3) 1_665 1_655 ?
Si2A O7A Nb1 133.49(6) . . ?
Si2A O7A Na3A 93.89(5) . . ?
Nb1 O7A Na3A 92.92(4) . . ?
Si2A O7A Na1 95.35(5) . . ?
Nb1 O7A Na1 106.22(4) . . ?
Na3A O7A Na1 142.73(5) . . ?
Nb1 O7A O1A 159.89(5) . . ?
Na3A O7A O1A 105.25(4) . . ?
Na1 O7A O1A 63.90(4) . . ?
Nb1 O7A O6A 127.50(5) . . ?
Na3A O7A O6A 59.25(3) . . ?
Na1 O7A O6A 122.97(4) . . ?
O1A O7A O6A 59.07(4) . . ?
Si2A O7A Na5 136.64(5) . . ?
Nb1 O7A Na5 89.41(4) . . ?
Na3A O7A Na5 74.82(3) . . ?
Na1 O7A Na5 73.75(3) . . ?
O1A O7A Na5 103.43(4) . . ?
O6A O7A Na5 119.25(4) . . ?
Nb1 O7A O5A 103.99(4) . . ?
Na3A O7A O5A 116.12(5) . . ?
Na1 O7A O5A 90.33(4) . . ?
O1A O7A O5A 60.44(4) . . ?
O6A O7A O5A 61.93(4) . . ?
Na5 O7A O5A 161.69(5) . . ?
Si2A O7A O10A 148.26(6) . 1_565 ?
Nb1 O7A O10A 50.51(3) . 1_565 ?
Na3A O7A O10A 55.68(3) . 1_565 ?
Na1 O7A O10A 114.24(4) . 1_565 ?
O1A O7A O10A 148.69(5) . 1_565 ?
O6A O7A O10A 114.12(5) . 1_565 ?
Na5 O7A O10A 50.56(3) . 1_565 ?
O5A O7A O10A 147.56(5) . 1_565 ?
Si2A O7A O6A 147.11(6) . 1_455 ?
Nb1 O7A O6A 46.16(3) . 1_455 ?
Na3A O7A O6A 118.55(4) . 1_455 ?
Na1 O7A O6A 62.71(3) . 1_455 ?
O1A O7A O6A 126.54(5) . 1_455 ?
O6A O7A O6A 173.65(6) . 1_455 ?
Na5 O7A O6A 63.91(3) . 1_455 ?
O5A O7A O6A 117.06(4) . 1_455 ?
O10A O7A O6A 62.98(4) 1_565 1_455 ?
Si2A O7A O4A 101.04(5) . 1_565 ?
Na3A O7A O4A 62.72(4) . 1_565 ?
Na1 O7A O4A 148.69(5) . 1_565 ?
O1A O7A O4A 139.06(5) . 1_565 ?
O6A O7A O4A 83.57(4) . 1_565 ?
Na5 O7A O4A 109.65(4) . 1_565 ?
O5A O7A O4A 88.65(4) . 1_565 ?
O10A O7A O4A 59.25(4) 1_565 1_565 ?
O6A O7A O4A 90.16(4) 1_455 1_565 ?
Si2A O7A O8A 99.41(5) . . ?
Na3A O7A O8A 121.44(4) . . ?
Na1 O7A O8A 92.45(4) . . ?
O1A O7A O8A 120.08(5) . . ?
O6A O7A O8A 115.03(5) . . ?
Na5 O7A O8A 122.44(4) . . ?
O5A O7A O8A 66.04(4) . . ?
O10A O7A O8A 90.92(4) 1_565 . ?
O6A O7A O8A 60.31(4) 1_455 . ?
O4A O7A O8A 58.79(4) 1_565 . ?
Nb1 O8A Nb2 138.02(6) . 2_665 ?
Nb1 O8A Na2 120.20(5) . 1_455 ?
Nb2 O8A Na2 95.73(4) 2_665 1_455 ?
Nb1 O8A Na2 107.49(5) . 2_675 ?
Nb2 O8A Na2 101.68(4) 2_665 2_675 ?
Na2 O8A Na2 75.50(4) 1_455 2_675 ?
Nb1 O8A O2A 143.35(6) . 2_665 ?
Nb2 O8A O2A 48.71(3) 2_665 2_665 ?
Na2 O8A O2A 87.45(4) 1_455 2_665 ?
Na2 O8A O2A 53.18(3) 2_675 2_665 ?
Nb2 O8A O4A 127.13(5) 2_665 1_565 ?
Na2 O8A O4A 128.23(5) 1_455 1_565 ?
Na2 O8A O4A 69.12(4) 2_675 1_565 ?
O2A O8A O4A 99.66(5) 2_665 1_565 ?
Nb2 O8A O3A 172.01(6) 2_665 1_465 ?
Na2 O8A O3A 80.26(4) 1_455 1_465 ?
Na2 O8A O3A 84.09(4) 2_675 1_465 ?
O2A O8A O3A 137.27(5) 2_665 1_465 ?
O4A O8A O3A 59.99(4) 1_565 1_465 ?
Nb1 O8A O6A 45.39(3) . 1_455 ?
Nb2 O8A O6A 114.89(5) 2_665 1_455 ?
Na2 O8A O6A 96.66(5) 1_455 1_455 ?
Na2 O8A O6A 143.26(5) 2_675 1_455 ?
O2A O8A O6A 163.55(5) 2_665 1_455 ?
O4A O8A O6A 90.32(4) 1_565 1_455 ?
O3A O8A O6A 59.17(4) 1_465 1_455 ?
Nb1 O8A O7A 45.71(3) . . ?
Nb2 O8A O7A 92.71(4) 2_665 . ?
Na2 O8A O7A 155.64(5) 1_455 . ?
Na2 O8A O7A 124.96(5) 2_675 . ?
O2A O8A O7A 114.96(5) 2_665 . ?
O4A O8A O7A 60.24(4) 1_565 . ?
O3A O8A O7A 88.39(4) 1_465 . ?
O6A O8A O7A 59.14(4) 1_455 . ?
Nb1 O8A O9A 152.15(6) . 2_565 ?
Na2 O8A O9A 54.28(3) 1_455 2_565 ?
Na2 O8A O9A 97.53(4) 2_675 2_565 ?
O2A O8A O9A 62.96(4) 2_665 2_565 ?
O4A O8A O9A 162.60(5) 1_565 2_565 ?
O3A O8A O9A 131.79(5) 1_465 2_565 ?
O6A O8A O9A 106.79(4) 1_455 2_565 ?
O7A O8A O9A 126.00(5) . 2_565 ?
Nb1 O8A O9A 107.12(5) . . ?
Na2 O8A O9A 97.82(4) 1_455 . ?
Na2 O8A O9A 143.03(4) 2_675 . ?
O2A O8A O9A 90.68(4) 2_665 . ?
O4A O8A O9A 132.90(5) 1_565 . ?
O3A O8A O9A 131.33(5) 1_465 . ?
O6A O8A O9A 73.01(4) 1_455 . ?
O7A O8A O9A 73.68(4) . . ?
O9A O8A O9A 53.06(4) 2_565 . ?
Nb1 O8A O5A 98.57(4) . . ?
Nb2 O8A O5A 45.82(3) 2_665 . ?
Na2 O8A O5A 140.59(5) 1_455 . ?
Na2 O8A O5A 100.81(4) 2_675 . ?
O2A O8A O5A 61.78(4) 2_665 . ?
O4A O8A O5A 83.56(4) 1_565 . ?
O3A O8A O5A 139.01(5) 1_465 . ?
O6A O8A O5A 106.92(4) 1_455 . ?
O7A O8A O5A 55.28(3) . . ?
O9A O8A O5A 88.31(4) 2_565 . ?
O9A O8A O5A 61.33(4) . . ?
Nb2 O9A Nb2 97.23(4) 1_455 2_665 ?
Nb2 O9A Na1 127.99(5) 1_455 . ?
Nb2 O9A Na1 123.75(5) 2_665 . ?
Nb2 O9A Na2 94.57(4) 1_455 2_665 ?
Nb2 O9A Na2 106.90(5) 2_665 2_665 ?
Na1 O9A Na2 101.35(4) . 2_665 ?
Nb2 O9A O9A 49.02(4) 1_455 2_565 ?
Nb2 O9A O9A 48.22(3) 2_665 2_565 ?
Na1 O9A O9A 152.30(7) . 2_565 ?
Na2 O9A O9A 106.33(6) 2_665 2_565 ?
Nb2 O9A O8A 99.27(4) 2_665 2_565 ?
Na1 O9A O8A 136.07(5) . 2_565 ?
Na2 O9A O8A 52.89(3) 2_665 2_565 ?
O9A O9A O8A 64.56(5) 2_565 2_565 ?
Nb2 O9A O2A 141.66(5) 2_665 1_455 ?
Na1 O9A O2A 89.00(4) . 1_455 ?
Na2 O9A O2A 82.26(4) 2_665 1_455 ?
O9A O9A O2A 93.46(6) 2_565 1_455 ?
O8A O9A O2A 56.08(3) 2_565 1_455 ?
Nb2 O9A O8A 98.07(4) 1_455 . ?
Na1 O9A O8A 94.42(4) . . ?
Na2 O9A O8A 147.23(5) 2_665 . ?
O9A O9A O8A 62.38(4) 2_565 . ?
O8A O9A O8A 126.94(4) 2_565 . ?
O2A O9A O8A 126.94(5) 1_455 . ?
Nb2 O9A O5A 97.45(4) 1_455 2_665 ?
Nb2 O9A O5A 47.66(3) 2_665 2_665 ?
Na1 O9A O5A 133.17(5) . 2_665 ?
Na2 O9A O5A 59.33(3) 2_665 2_665 ?
O9A O9A O5A 65.47(5) 2_565 2_665 ?
O8A O9A O5A 69.09(4) 2_565 2_665 ?
O2A O9A O5A 124.92(4) 1_455 2_665 ?
O8A O9A O5A 89.01(4) . 2_665 ?
Nb2 O9A O5A 46.50(3) 1_455 1_455 ?
Nb2 O9A O5A 95.30(4) 2_665 1_455 ?
Na1 O9A O5A 94.85(4) . 1_455 ?
Na2 O9A O5A 137.89(5) 2_665 1_455 ?
O9A O9A O5A 63.44(5) 2_565 1_455 ?
O8A O9A O5A 89.06(4) 2_565 1_455 ?
O2A O9A O5A 59.26(3) 1_455 1_455 ?
O8A O9A O5A 67.70(4) . 1_455 ?
O5A O9A O5A 128.92(4) 2_665 1_455 ?
Nb2 O9A O5A 142.12(5) 1_455 . ?
Nb2 O9A O5A 45.64(3) 2_665 . ?
Na1 O9A O5A 87.11(4) . . ?
Na2 O9A O5A 91.06(4) 2_665 . ?
O9A O9A O5A 93.51(5) 2_565 . ?
O8A O9A O5A 123.31(4) 2_565 . ?
O2A O9A O5A 171.47(5) 1_455 . ?
O8A O9A O5A 61.01(3) . . ?
O5A O9A O5A 54.41(4) 2_665 . ?
O5A O9A O5A 128.66(5) 1_455 . ?
Nb2 O9A O6A 97.05(4) 1_455 1_455 ?
Nb2 O9A O6A 93.64(4) 2_665 1_455 ?
Na1 O9A O6A 54.28(3) . 1_455 ?
Na2 O9A O6A 154.89(5) 2_665 1_455 ?
O9A O9A O6A 98.07(5) 2_565 1_455 ?
O8A O9A O6A 138.79(5) 2_565 1_455 ?
O2A O9A O6A 90.59(4) 1_455 1_455 ?
O8A O9A O6A 52.14(3) . 1_455 ?
O5A O9A O6A 140.05(4) 2_665 1_455 ?
O5A O9A O6A 50.68(3) 1_455 1_455 ?
O5A O9A O6A 93.29(4) . 1_455 ?
P O10A Nb1 134.56(6) . 1_545 ?
P O10A Na5 122.64(6) . 1_545 ?
Nb1 O10A Na5 96.86(4) 1_545 1_545 ?
P O10A Na3A 115.11(5) . 1_545 ?
Nb1 O10A Na3A 89.88(4) 1_545 1_545 ?
Na5 O10A Na3A 81.90(4) 1_545 1_545 ?
Nb1 O10A O11A 117.19(5) 1_545 1_455 ?
Na5 O10A O11A 107.01(5) 1_545 1_455 ?
Na3A O10A O11A 149.34(5) 1_545 1_455 ?
Nb1 O10A O13A 167.02(5) 1_545 . ?
Na5 O10A O13A 96.03(5) 1_545 . ?
Na3A O10A O13A 90.47(5) 1_545 . ?
O11A O10A O13A 59.85(4) 1_455 . ?
Nb1 O10A O12A 108.06(5) 1_545 . ?
Na5 O10A O12A 154.95(5) 1_545 . ?
Na3A O10A O12A 100.21(5) 1_545 . ?
O11A O10A O12A 59.46(4) 1_455 . ?
O13A O10A O12A 59.14(4) . . ?
P O10A O4A 111.78(6) . . ?
Na5 O10A O4A 124.07(5) 1_545 . ?
Na3A O10A O4A 63.49(4) 1_545 . ?
O11A O10A O4A 125.46(5) 1_455 . ?
O13A O10A O4A 124.76(6) . . ?
O12A O10A O4A 77.67(4) . . ?
P O10A O7A 169.68(6) . 1_545 ?
Nb1 O10A O7A 46.50(3) 1_545 1_545 ?
Na5 O10A O7A 63.35(4) 1_545 1_545 ?
Na3A O10A O7A 55.76(3) 1_545 1_545 ?
O11A O10A O7A 154.48(5) 1_455 1_545 ?
O13A O10A O7A 141.02(5) . 1_545 ?
O12A O10A O7A 137.89(5) . 1_545 ?
O4A O10A O7A 60.95(4) . 1_545 ?
P O10A O3A 92.75(5) . 1_455 ?
Na5 O10A O3A 124.46(5) 1_545 1_455 ?
Na3A O10A O3A 123.01(5) 1_545 1_455 ?
O11A O10A O3A 76.76(5) 1_455 1_455 ?
O13A O10A O3A 128.14(5) . 1_455 ?
O12A O10A O3A 75.45(4) . 1_455 ?
O4A O10A O3A 60.08(4) . 1_455 ?
O7A O10A O3A 89.48(4) 1_545 1_455 ?
P O10A O6A 130.51(6) . 1_445 ?
Na5 O10A O6A 66.37(4) 1_545 1_445 ?
Na3A O10A O6A 114.36(4) 1_545 1_445 ?
O11A O10A O6A 95.83(5) 1_455 1_445 ?
O13A O10A O6A 145.60(5) . 1_445 ?
O12A O10A O6A 132.00(5) . 1_445 ?
O4A O10A O6A 88.69(4) . 1_445 ?
O7A O10A O6A 58.71(4) 1_545 1_445 ?
O3A O10A O6A 58.19(4) 1_455 1_445 ?
P O10A Na3A 81.37(4) . 1_445 ?
Nb1 O10A Na3A 84.09(3) 1_545 1_445 ?
Na5 O10A Na3A 80.90(4) 1_545 1_445 ?
Na3A O10A Na3A 160.94(5) 1_545 1_445 ?
O11A O10A Na3A 46.03(3) 1_455 1_445 ?
O13A O10A Na3A 99.44(4) . 1_445 ?
O12A O10A Na3A 98.85(4) . 1_445 ?
O4A O10A Na3A 121.14(4) . 1_445 ?
O7A O10A Na3A 108.52(4) 1_545 1_445 ?
O3A O10A Na3A 62.26(4) 1_455 1_445 ?
O6A O10A Na3A 50.41(3) 1_445 1_445 ?
P O11A Na4 118.42(7) 1_655 . ?
P O11A Na3A 116.31(6) 1_655 1_545 ?
Na4 O11A Na3A 100.56(5) . 1_545 ?
P O11A Na5 121.47(7) 1_655 2_666 ?
Na4 O11A Na5 93.47(5) . 2_666 ?
Na3A O11A Na5 102.37(5) 1_545 2_666 ?
Na4 O11A O13A 130.33(6) . 1_655 ?
Na3A O11A O13A 127.97(6) 1_545 1_655 ?
Na5 O11A O13A 86.56(5) 2_666 1_655 ?
Na4 O11A O10A 130.95(6) . 1_655 ?
Na3A O11A O10A 79.85(4) 1_545 1_655 ?
Na5 O11A O10A 134.84(6) 2_666 1_655 ?
O13A O11A O10A 60.12(4) 1_655 1_655 ?
Na4 O11A O12A 83.42(5) . 1_655 ?
Na3A O11A O12A 128.37(6) 1_545 1_655 ?
Na5 O11A O12A 128.96(6) 2_666 1_655 ?
O13A O11A O12A 59.83(5) 1_655 1_655 ?
O10A O11A O12A 61.27(4) 1_655 1_655 ?
P O11A O3A 75.26(5) 1_655 . ?
Na4 O11A O3A 80.93(4) . . ?
Na3A O11A O3A 62.98(4) 1_545 . ?
Na5 O11A O3A 162.61(5) 2_666 . ?
O13A O11A O3A 109.65(5) 1_655 . ?
O10A O11A O3A 55.27(4) 1_655 . ?
O12A O11A O3A 67.06(4) 1_655 . ?
P O11A O12A 111.65(6) 1_655 2_666 ?
Na4 O11A O12A 60.02(4) . 2_666 ?
Na3A O11A O12A 131.61(5) 1_545 2_666 ?
O13A O11A O12A 89.31(5) 1_655 2_666 ?
O10A O11A O12A 147.53(5) 1_655 2_666 ?
O12A O11A O12A 95.18(5) 1_655 2_666 ?
O3A O11A O12A 139.16(5) . 2_666 ?
P O11A O13A 164.45(7) 1_655 . ?
Na4 O11A O13A 69.62(4) . . ?
Na3A O11A O13A 72.58(4) 1_545 . ?
O13A O11A O13A 129.39(6) 1_655 . ?
O10A O11A O13A 148.88(5) 1_655 . ?
O12A O11A O13A 149.42(5) 1_655 . ?
O3A O11A O13A 120.09(4) . . ?
O12A O11A O13A 59.25(3) 2_666 . ?
P O11A Na4 58.92(4) 1_655 2_766 ?
Na4 O11A Na4 93.20(4) . 2_766 ?
Na3A O11A Na4 165.69(5) 1_545 2_766 ?
Na5 O11A Na4 72.62(4) 2_666 2_766 ?
O10A O11A Na4 94.14(4) 1_655 2_766 ?
O12A O11A Na4 56.83(4) 1_655 2_766 ?
O3A O11A Na4 123.88(4) . 2_766 ?
O12A O11A Na4 53.39(3) 2_666 2_766 ?
O13A O11A Na4 109.15(4) . 2_766 ?
P O11A O13A 112.75(6) 1_655 2_656 ?
Na4 O11A O13A 126.26(5) . 2_656 ?
Na5 O11A O13A 72.42(4) 2_666 2_656 ?
O13A O11A O13A 101.04(5) 1_655 2_656 ?
O10A O11A O13A 84.31(4) 1_655 2_656 ?
O12A O11A O13A 145.36(5) 1_655 2_656 ?
O3A O11A O13A 97.56(4) . 2_656 ?
O12A O11A O13A 114.37(4) 2_666 2_656 ?
O13A O11A O13A 65.22(4) . 2_656 ?
Na4 O11A O13A 127.85(4) 2_766 2_656 ?
P O12A Na1 123.51(6) . . ?
P O12A Na4 114.99(6) . . ?
Na1 O12A Na4 93.91(5) . . ?
P O12A Na5 142.82(7) . . ?
Na1 O12A Na5 84.78(4) . . ?
Na4 O12A Na5 82.80(4) . . ?
Na1 O12A O13A 155.02(6) . . ?
Na4 O12A O13A 89.59(5) . . ?
Na5 O12A O13A 120.20(5) . . ?
Na1 O12A O11A 110.69(6) . 1_455 ?
Na4 O12A O11A 148.62(6) . 1_455 ?
Na5 O12A O11A 117.50(6) . 1_455 ?
O13A O12A O11A 59.90(5) . 1_455 ?
Na1 O12A O10A 95.60(5) . . ?
Na4 O12A O10A 100.46(5) . . ?
Na5 O12A O10A 176.67(6) . . ?
O13A O12A O10A 59.47(4) . . ?
O11A O12A O10A 59.27(4) 1_455 . ?
P O12A Na4 76.56(5) . 2_666 ?
Na1 O12A Na4 157.29(5) . 2_666 ?
Na4 O12A Na4 85.29(4) . 2_666 ?
Na5 O12A Na4 72.59(3) . 2_666 ?
O13A O12A Na4 47.65(3) . 2_666 ?
O11A O12A Na4 79.25(4) 1_455 2_666 ?
O10A O12A Na4 106.88(4) . 2_666 ?
P O12A Na4 78.98(5) . 1_455 ?
Na1 O12A Na4 86.14(4) . 1_455 ?
Na4 O12A Na4 162.40(5) . 1_455 ?
Na5 O12A Na4 79.67(4) . 1_455 ?
O13A O12A Na4 97.80(5) . 1_455 ?
O10A O12A Na4 97.05(4) . 1_455 ?
Na4 O12A Na4 87.93(3) 2_666 1_455 ?
P O12A O3A 75.82(5) . 1_455 ?
Na1 O12A O3A 48.07(3) . 1_455 ?
Na4 O12A O3A 122.77(5) . 1_455 ?
Na5 O12A O3A 123.46(5) . 1_455 ?
O13A O12A O3A 110.28(5) . 1_455 ?
O11A O12A O3A 67.85(4) 1_455 1_455 ?
O10A O12A O3A 55.27(4) . 1_455 ?
Na4 O12A O3A 147.09(5) 2_666 1_455 ?
Na4 O12A O3A 69.51(3) 1_455 1_455 ?
P O12A O4A 88.50(5) . . ?
Na1 O12A O4A 52.80(4) . . ?
Na4 O12A O4A 73.91(4) . . ?
Na5 O12A O4A 128.56(5) . . ?
O13A O12A O4A 105.06(5) . . ?
O11A O12A O4A 105.22(5) 1_455 . ?
O10A O12A O4A 53.56(4) . . ?
Na4 O12A O4A 146.40(5) 2_666 . ?
Na4 O12A O4A 118.90(4) 1_455 . ?
O3A O12A O4A 49.49(3) 1_455 . ?
P O12A O13A 132.68(6) . 2_666 ?
Na1 O12A O13A 101.60(4) . 2_666 ?
O13A O12A O13A 97.42(5) . 2_666 ?
O11A O12A O13A 141.39(5) 1_455 2_666 ?
O10A O12A O13A 138.76(5) . 2_666 ?
Na4 O12A O13A 63.30(3) 2_666 2_666 ?
Na4 O12A O13A 121.09(4) 1_455 2_666 ?
O3A O12A O13A 149.11(5) 1_455 2_666 ?
O4A O12A O13A 111.09(4) . 2_666 ?
P O13A Na4 105.01(6) . 2_666 ?
P O13A Na3A 130.95(7) . 2_666 ?
Na4 O13A Na3A 110.20(5) 2_666 2_666 ?
P O13A Na5 134.14(7) . 2_666 ?
Na4 O13A Na5 83.74(4) 2_666 2_666 ?
Na3A O13A Na5 83.45(4) 2_666 2_666 ?
Na4 O13A O12A 78.43(5) 2_666 . ?
Na3A O13A O12A 166.27(6) 2_666 . ?
Na5 O13A O12A 108.59(6) 2_666 . ?
Na4 O13A O11A 95.85(5) 2_666 1_455 ?
Na3A O13A O11A 107.30(6) 2_666 1_455 ?
Na5 O13A O11A 168.54(6) 2_666 1_455 ?
O12A O13A O11A 60.27(5) . 1_455 ?
Na4 O13A O10A 139.34(6) 2_666 . ?
Na3A O13A O10A 108.27(5) 2_666 . ?
Na5 O13A O10A 113.46(6) 2_666 . ?
O12A O13A O10A 61.39(4) . . ?
O11A O13A O10A 60.03(4) 1_455 . ?
P O13A Na5 78.37(5) . 2_566 ?
Na4 O13A Na5 78.63(4) 2_666 2_566 ?
Na3A O13A Na5 76.38(4) 2_666 2_566 ?
Na5 O13A Na5 146.50(5) 2_666 2_566 ?
O12A O13A Na5 95.54(5) . 2_566 ?
O10A O13A Na5 98.27(5) . 2_566 ?
P O13A O7A 171.77(7) . 2_666 ?
Na4 O13A O7A 70.90(4) 2_666 2_666 ?
Na3A O13A O7A 47.53(3) 2_666 2_666 ?
Na5 O13A O7A 53.41(3) 2_666 2_666 ?
O12A O13A O7A 145.44(5) . 2_666 ?
O11A O13A O7A 137.18(6) 1_455 2_666 ?
O10A O13A O7A 149.17(5) . 2_666 ?
Na5 O13A O7A 93.69(4) 2_566 2_666 ?
P O13A Na4 72.46(5) . . ?
Na4 O13A Na4 77.50(4) 2_666 . ?
Na3A O13A Na4 147.49(5) 2_666 . ?
Na5 O13A Na4 65.64(4) 2_666 . ?
O11A O13A Na4 103.05(5) 1_455 . ?
O10A O13A Na4 77.25(4) . . ?
Na5 O13A Na4 135.57(4) 2_566 . ?
O7A O13A Na4 112.76(4) 2_666 . ?
P O13A O10A 138.31(6) . 2_656 ?
Na4 O13A O10A 114.11(4) 2_666 2_656 ?
Na3A O13A O10A 45.76(3) 2_666 2_656 ?
O12A O13A O10A 141.56(6) . 2_656 ?
O11A O13A O10A 144.43(5) 1_455 2_656 ?
O10A O13A O10A 101.93(4) . 2_656 ?
Na5 O13A O10A 122.05(4) 2_566 2_656 ?
O7A O13A O10A 48.33(3) 2_666 2_656 ?
Na4 O13A O10A 101.85(4) . 2_656 ?
P O13A O12A 117.98(6) . 2_666 ?
Na3A O13A O12A 111.06(4) 2_666 2_666 ?
O12A O13A O12A 82.58(5) . 2_666 ?
O11A O13A O12A 130.93(5) 1_455 2_666 ?
O10A O13A O12A 129.62(5) . 2_666 ?
Na5 O13A O12A 120.52(4) 2_566 2_666 ?
O7A O13A O12A 64.15(3) 2_666 2_666 ?
Na4 O13A O12A 52.75(3) . 2_666 ?
O10A O13A O12A 84.54(4) 2_656 2_666 ?

_diffrn_measured_fraction_theta_max 0.985
_diffrn_reflns_theta_full        35.11
_diffrn_measured_fraction_theta_full 0.985
_refine_diff_density_max         1.416
_refine_diff_density_min         -1.252
_refine_diff_density_rms         0.127
_chemical_compound_source        'Fersman Museum #86957'