#======================================================================= data_global #======================================================================= _audit_creation_method 'Jana2000 Version : 22/12/2005' # 1. PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full 'Acta Crystallographica Section C' _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #======================================================================= # 2. SUBMISSION DETAILS _publ_contact_author_name ? _publ_contact_author_address ; ? ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal 'Acta Crystallographica Section C' _publ_requested_category ? _publ_contact_letter ; ? ; #======================================================================= # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; _publ_section_title_footnote ; ? ; loop_ _publ_author_name _publ_author_footnote _publ_author_address ? # name ; ? # footnote ; ; ? # address ; #======================================================================= # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_introduction ; ? ; _publ_section_experimental ; ? ; _publ_section_exptl_prep ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_exptl_solution ; ? ; _publ_section_discussion ; ? ; _publ_section_acknowledgements ; ? ; _publ_section_references ; Petricek, V., Dusek, M. & Palatinus L. (2000). Jana2000. Structure Determination Software Programs. Institute of Physics, Praha, Czech Republic. # use this reference if Diamond ver. 2 was used for visualization Brandenburg, K. (1999). DIAMOND. Version. 2.1c. Crystal Impact GbR, Bonn, Germany. # use this reference if Diamond ver. 3 was used for visualization in preparation # use this reference if SIR97 was used for solving of the structure Altomare, A., Burla, M. C., Camalli, M., Cascarano, G., Giacovazzo, C., Guagliardi, A., Moliterni, A. G. G., Polidori, G., Spagna, R. (1997). SIR97. A Package for Crystal Structure Solution by Direct Methods and Refinement, Bari, Rome, Italy. # use this reference if bond valences were calculated Brown, I. D. (1996). J. Appl. Cryst. 29, 479-480. # use this reference if Xshape wase used for crystal shape refinement Stoe & Cie (1998). X-SHAPE. Stoe & Cie, Darmstadt, Germany. ; _publ_section_figure_captions ; ? ; _publ_section_table_legends ; ? ; #======================================================================= data_(I) #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Al2 O5 Si1' _chemical_formula_weight 162 _chemical_melting_point ? _chemical_compound_source ? #======================================================================= # 6. CRYSTAL DATA _symmetry_cell_setting triclinic _symmetry_space_group_name_H-M 'P -1' _symmetry_space_group_name_Hall '-P 1' loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,-y,-z _cell_length_a 7.1280(11) _cell_length_b 7.8550(11) _cell_length_c 5.5770(8) _cell_angle_alpha 90.050(10) _cell_angle_beta 101.120(13) _cell_angle_gamma 105.980(13) _cell_volume 294.07(8) _cell_formula_units_Z 1 _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _cell_measurement_temperature ? _cell_special_details ; ? ; _exptl_crystal_density_diffrn 0.9147 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 320 _exptl_absorpt_coefficient_mu 0.316 _exptl_crystal_description ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_absorpt_correction_type None _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min 1.000 _exptl_absorpt_correction_T_max 1.000 #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source ? _diffrn_radiation_monochromator ? _diffrn_measurement_device_type ? _diffrn_detector_area_resol_mean ? _diffrn_measurement_method ? _diffrn_reflns_number 6290 _diffrn_reflns_theta_min 2.70 _diffrn_reflns_theta_max 34.70 _diffrn_reflns_theta_full 23.00 _diffrn_measured_fraction_theta_max ? _diffrn_measured_fraction_theta_full 0.95 _diffrn_reflns_av_R_equivalents 0.0707 _diffrn_reflns_av_sigmaI/netI 0.0169 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_k_min -11 _diffrn_reflns_limit_k_max 11 _diffrn_reflns_limit_l_min -8 _diffrn_reflns_limit_l_max 8 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? #======================================================================= # 8. REFINEMENT DATA _refine_special_details ; ? ; _reflns_number_total 1372 _reflns_number_gt 1068 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0493 _refine_ls_wR_factor_gt 0.0504 _refine_ls_R_factor_all 0.0608 _refine_ls_wR_factor_ref 0.0525 _refine_ls_goodness_of_fit_ref 2.88 _refine_ls_goodness_of_fit_gt 3.19 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 1372 _refine_ls_number_parameters 145 _refine_ls_number_restraints ? _refine_ls_number_constraints ? _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(F)+0.0001F^2^)' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0468 _refine_ls_shift/su_mean 0.0088 _refine_diff_density_max 0.73 _refine_diff_density_min -0.62 _refine_ls_extinction_method 'none' _refine_ls_extinction_coef ? loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c Al 0.064 0.051 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 6.4202 3.0387 1.9002 0.7426 1.5936 31.547199 1.9646 85.0886 1.1151 Si 0.082 0.070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 6.2915 2.4386 3.0353 32.333698 1.9891 0.6785 1.541 81.693703 1.1407 O 0.011 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.867 32.908901 0.2508 _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement '(Jana2000; Petricek and Dusek, 2000)' _computing_molecular_graphics ? _computing_publication_material '(Jana2000; Petricek and Dusek, 2000)' #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Al1 Al 0.32492(20) 0.70403(13) 0.4580(2) Uani 0.0113(4) 2 1 d . . . Al2 Al 0.29797(10) 0.69881(12) 0.9507(2) Uani 0.0091(4) 2 1 d . . . Al3 Al 0.10044(10) 0.38633(13) 0.6409(2) Uani 0.0106(2) 2 1 d . . . Al4 Al 0.11249(20) 0.91761(13) 0.1649(2) Uani 0.0108(4) 2 1 d . . . Si1 Si 0.29610(10) 0.06473(11) 0.7057(2) Uani 0.0107(4) 2 1 d . . . Si2 Si 0.29142(10) 0.33187(12) 0.1900(2) Uani 0.0110(4) 2 1 d . . . O1 O 0.1090(4) 0.1469(3) 0.1286(5) Uani 0.0115(9) 2 1 d . . . O2 O 0.1227(4) 0.6854(3) 0.1800(5) Uani 0.0099(8) 2 1 d . . . O3 O 0.2749(4) 0.4538(3) 0.9542(5) Uani 0.0111(9) 2 1 d . . . O4 O 0.2852(4) 0.9365(3) 0.9369(5) Uani 0.0120(9) 2 1 d . . . O5 O 0.1091(3) 0.1527(3) 0.6686(5) Uani 0.0100(9) 2 1 d . . . O6 O 0.1222(3) 0.6307(3) 0.6398(5) Uani 0.0098(8) 2 1 d . . . O7 O 0.2818(4) 0.4444(3) 0.4288(5) Uani 0.0098(9) 2 1 d . . . O8 O 0.2902(3) 0.9473(3) 0.4653(5) Uani 0.0088(8) 2 1 d . . . O9 O 0.5006(3) 0.2749(3) 0.2433(5) Uani 0.0115(9) 2 1 d . . . O10 O 0.5014(3) 0.2302(3) 0.7556(5) Uani 0.0125(9) 2 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 Al1 Al 0.0163(5) 0.0048(5) 0.0143(7) 0.0045(4) 0.0043(5) 0.0017(4) Al2 Al 0.0141(5) 0.0024(4) 0.0124(7) 0.0038(4) 0.0039(5) 0.0005(4) Al3 Al 0.0140(5) 0.0026(5) 0.0162(7) 0.0035(5) 0.0039(4) 0.0006(4) Al4 Al 0.0155(5) 0.0036(5) 0.0155(7) 0.0047(4) 0.0050(4) 0.0011(4) Si1 Si 0.0147(5) 0.0034(4) 0.0153(7) 0.0043(4) 0.0038(4) 0.0011(4) Si2 Si 0.0144(5) 0.0038(4) 0.0164(7) 0.0044(4) 0.0044(4) 0.0021(4) O1 O 0.0163(12) 0.0051(11) 0.0151(17) 0.0054(10) 0.0046(11) 0.0002(9) O2 O 0.0153(12) 0.0051(11) 0.0100(16) 0.0038(9) 0.0028(11) 0.0001(9) O3 O 0.0168(13) 0.0042(11) 0.0129(17) 0.0041(9) 0.0029(11) 0.0010(10) O4 O 0.0197(13) 0.0058(11) 0.0139(17) 0.0071(10) 0.0066(11) 0.0025(10) O5 O 0.0161(12) 0.0040(11) 0.0113(16) 0.0040(9) 0.0043(11) -0.0021(10) O6 O 0.0116(12) 0.0035(11) 0.0157(17) 0.0038(9) 0.0035(11) -0.0013(10) O7 O 0.0160(12) 0.0019(11) 0.0141(17) 0.0031(9) 0.0080(11) -0.0008(9) O8 O 0.0120(12) 0.0042(11) 0.0107(17) 0.0027(9) 0.0028(11) -0.0022(10) O9 O 0.0144(12) 0.0053(11) 0.0155(17) 0.0036(9) 0.0035(11) 0.0008(10) O10 O 0.0130(13) 0.0053(11) 0.0207(18) 0.0041(9) 0.0051(11) 0.0013(11) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag Al1 O2 . . 1.877(3) yes Al1 O6 . . 1.885(3) yes Al1 O7 . . 1.978(2) yes Al1 O8 . . 1.994(3) yes Al1 O9 . 2_666 1.854(3) yes Al1 O10 . 2_666 1.854(3) yes Al2 O2 . 1_556 1.937(3) yes Al2 O3 . . 1.886(3) yes Al2 O4 . . 1.895(3) yes Al2 O6 . . 1.911(3) yes Al2 O9 . 2_666 1.926(3) yes Al2 O10 . 2_667 1.922(3) yes Al3 O2 . 2_566 1.991(3) yes Al3 O3 . . 1.918(3) yes Al3 O5 . . 1.859(3) yes Al3 O6 . . 1.883(3) yes Al3 O6 . 2_566 1.978(3) yes Al3 O7 . . 1.883(3) yes Al4 O1 . 1_565 1.819(3) yes Al4 O1 . 2_565 1.997(3) yes Al4 O2 . . 1.847(3) yes Al4 O4 . 1_554 1.913(3) yes Al4 O5 . 2_566 1.936(3) yes Al4 O8 . . 1.866(3) yes Si1 O4 . 1_545 1.637(3) yes Si1 O5 . . 1.642(3) yes Si1 O8 . 1_545 1.614(3) yes Si1 O10 . . 1.644(2) yes Si2 O1 . . 1.645(2) yes Si2 O3 . 1_554 1.633(3) yes Si2 O7 . . 1.621(3) yes Si2 O9 . . 1.646(3) yes loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_2 _geom_angle_site_symmetry_3 _geom_angle _geom_angle_publ_flag O2 Al1 O6 . . . 87.45(12) yes O2 Al1 O7 . . . 89.50(11) yes O2 Al1 O8 . . . 79.19(11) yes O2 Al1 O9 . . 2_666 172.27(15) yes O2 Al1 O10 . . 2_666 85.37(12) yes O6 Al1 O7 . . . 80.58(11) yes O6 Al1 O8 . . . 88.83(12) yes O6 Al1 O9 . . 2_666 85.37(12) yes O6 Al1 O10 . . 2_666 172.76(12) yes O7 Al1 O8 . . . 164.87(11) yes O7 Al1 O9 . . 2_666 92.14(11) yes O7 Al1 O10 . . 2_666 98.39(12) yes O8 Al1 O9 . . 2_666 97.78(11) yes O8 Al1 O10 . . 2_666 90.76(12) yes O9 Al1 O10 2_666 . 2_666 101.85(12) yes O2 Al2 O3 1_556 . . 92.93(12) yes O2 Al2 O4 1_556 . . 82.81(12) yes O2 Al2 O6 1_556 . . 104.47(12) yes O2 Al2 O9 1_556 . 2_666 172.79(11) yes O2 Al2 O10 1_556 . 2_667 81.90(12) yes O3 Al2 O4 . . . 172.71(12) yes O3 Al2 O6 . . . 82.65(11) yes O3 Al2 O9 . . 2_666 88.82(12) yes O3 Al2 O10 . . 2_667 97.03(11) yes O4 Al2 O6 . . . 92.65(11) yes O4 Al2 O9 . . 2_666 96.14(12) yes O4 Al2 O10 . . 2_667 88.25(11) yes O6 Al2 O9 . . 2_666 82.69(12) yes O6 Al2 O10 . . 2_667 173.63(14) yes O9 Al2 O10 2_666 . 2_667 90.94(12) yes O2 Al3 O3 2_566 . . 87.15(12) yes O2 Al3 O5 2_566 . . 84.84(12) yes O2 Al3 O6 2_566 . . 97.72(12) yes O2 Al3 O6 2_566 . 2_566 81.88(11) yes O2 Al3 O7 2_566 . . 171.44(11) yes O3 Al3 O5 . . . 90.99(11) yes O3 Al3 O6 . . . 82.58(11) yes O3 Al3 O6 . . 2_566 161.23(14) yes O3 Al3 O7 . . . 101.40(12) yes O5 Al3 O6 . . . 172.93(11) yes O5 Al3 O6 . . 2_566 103.06(10) yes O5 Al3 O7 . . . 95.27(13) yes O6 Al3 O6 . . 2_566 83.85(11) yes O6 Al3 O7 . . . 83.18(12) yes O6 Al3 O6 2_566 . . 83.85(11) yes O6 Al3 O7 2_566 . . 89.78(12) yes O1 Al4 O1 1_565 . 2_565 87.31(11) yes O1 Al4 O2 1_565 . . 175.71(15) yes O1 Al4 O4 1_565 . 1_554 91.18(13) yes O1 Al4 O5 1_565 . 2_566 96.89(13) yes O1 Al4 O8 1_565 . . 98.86(11) yes O1 Al4 O1 2_565 . 1_565 87.31(11) yes O1 Al4 O2 2_565 . . 91.01(11) yes O1 Al4 O4 2_565 . 1_554 85.51(12) yes O1 Al4 O5 2_565 . 2_566 81.41(11) yes O1 Al4 O8 2_565 . . 169.95(12) yes O2 Al4 O4 . . 1_554 84.75(12) yes O2 Al4 O5 . . 2_566 86.75(12) yes O2 Al4 O8 . . . 83.36(11) yes O4 Al4 O5 1_554 . 2_566 164.26(11) yes O4 Al4 O8 1_554 . . 102.19(12) yes O5 Al4 O8 2_566 . . 89.93(12) yes O4 Si1 O5 1_545 . . 109.27(15) yes O4 Si1 O8 1_545 . 1_545 108.47(13) yes O4 Si1 O10 1_545 . . 111.60(13) yes O5 Si1 O8 . . 1_545 111.69(13) yes O5 Si1 O10 . . . 106.82(12) yes O8 Si1 O10 1_545 . . 109.01(14) yes O1 Si2 O3 . . 1_554 108.03(13) yes O1 Si2 O7 . . . 112.76(14) yes O1 Si2 O9 . . . 106.77(13) yes O3 Si2 O7 1_554 . . 108.45(14) yes O3 Si2 O9 1_554 . . 112.27(15) yes O7 Si2 O9 . . . 108.63(14) yes #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_intensity_meas _refln_intensity_calc _refln_intensity_sigma _refln_observed_status 2 0 0 97028.7 127189.2 1970.7 o 3 0 0 9731.1 12556.6 209.0 o 4 0 0 417.3 604.0 42.6 o 5 0 0 347360.0 363847.5 7005.2 o 6 0 0 61.7 39.4 25.3 < 7 0 0 28284.3 27260.2 657.9 o 8 0 0 53.6 126.1 70.5 < -9 1 0 97.9 150.2 231.7 < -8 1 0 133.5 158.3 52.5 < -7 1 0 1647.4 1854.1 90.9 o -6 1 0 88.5 137.3 28.5 o -5 1 0 4612.0 5658.2 140.4 o -4 1 0 1064.5 1288.6 49.3 o -3 1 0 55.2 6.6 16.3 o -2 1 0 9345.5 9110.7 207.9 o -1 1 0 1800.2 1650.9 51.7 o 0 1 0 17.2 0.2 18.4 < 1 1 0 6453.4 5735.5 139.5 o 2 1 0 3418.9 3669.3 81.8 o 3 1 0 335.5 319.4 28.4 o 4 1 0 55.3 40.2 22.4 < 5 1 0 7848.9 8683.4 199.6 o 6 1 0 41.4 6.7 30.1 < 7 1 0 4360.6 4542.3 155.8 o 8 1 0 159.9 175.2 75.1 < -9 2 0 159.4 17.2 75.8 < -8 2 0 104.0 36.2 46.8 < -7 2 0 18259.9 16704.6 418.6 o -6 2 0 8639.3 10807.8 229.5 o -5 2 0 1939.1 1942.5 76.5 o -4 2 0 223.4 284.9 38.6 o -3 2 0 40147.8 29543.5 823.3 o -2 2 0 23938.1 23655.1 499.5 o -1 2 0 11007.1 10415.0 235.4 o 0 2 0 11022.2 9809.5 231.5 o 1 2 0 23205.4 21038.6 478.1 o 2 2 0 37389.3 26737.0 757.6 o 3 2 0 111.8 126.1 19.5 o 4 2 0 572.4 548.8 50.2 o 5 2 0 14798.2 14172.0 351.9 o 6 2 0 12150.7 12956.8 297.7 o 7 2 0 76.2 26.1 44.8 < 8 2 0 91.0 89.7 123.0 < -9 3 0 4266.7 4428.4 177.6 o -8 3 0 2931.1 3015.4 126.0 o -7 3 0 22804.4 22452.3 523.0 o -6 3 0 125.0 130.9 37.5 o -5 3 0 33144.1 33998.2 688.1 o -4 3 0 27881.1 28089.6 585.3 o -3 3 0 8533.0 8325.0 189.1 o -2 3 0 94959.0 95166.3 1909.4 o -1 3 0 14116.4 13613.8 293.0 o 0 3 0 102790.5 98535.6 2064.8 o 1 3 0 59151.6 53635.5 1192.1 o 2 3 0 4964.8 4780.7 110.9 o 3 3 0 48862.9 44352.4 1009.7 o 4 3 0 13689.4 13933.4 314.4 o 5 3 0 32042.3 29333.1 681.8 o 6 3 0 10418.9 9885.3 259.0 o 7 3 0 602.8 1191.7 90.1 o 8 3 0 1825.1 2925.7 266.5 o -9 4 0 6802.1 6431.5 228.7 o -8 4 0 162.9 28.7 56.5 < -7 4 0 318.8 540.7 70.1 o -6 4 0 81374.0 69725.0 1681.3 o -5 4 0 19868.1 21466.8 425.1 o -4 4 0 7586.5 7439.7 185.4 o -3 4 0 56.0 30.9 20.6 < -2 4 0 12806.3 12096.6 268.5 o -1 4 0 372771.3 351665.7 7463.5 o 0 4 0 15213.7 13941.0 312.6 o 1 4 0 55.2 31.8 15.7 o 2 4 0 6867.1 6813.8 165.4 o 3 4 0 16560.0 14722.7 378.8 o 4 4 0 72572.6 64628.9 1506.8 o 5 4 0 210.5 400.8 45.1 o 6 4 0 115.3 8.2 52.3 < 7 4 0 3589.6 5077.9 241.8 o -9 5 0 786.3 1072.5 117.3 o -8 5 0 13384.5 11190.8 422.1 o -7 5 0 2377.5 3623.6 119.9 o -6 5 0 849.5 1105.6 81.8 o -5 5 0 32959.0 36232.2 694.4 o -4 5 0 7579.8 7806.5 179.6 o -3 5 0 73958.8 72372.1 1504.9 o -2 5 0 12001.3 11723.5 262.7 o -1 5 0 673.8 746.6 32.7 o 0 5 0 70788.0 64669.1 1433.8 o 1 5 0 18510.0 16818.6 394.7 o 2 5 0 62822.4 55309.7 1287.5 o 3 5 0 3565.2 3495.4 135.1 o 4 5 0 88.9 73.1 40.0 < 5 5 0 11254.4 11020.9 283.6 o 6 5 0 5859.4 6299.4 196.0 o -9 6 0 1865.5 2152.4 200.3 o -8 6 0 5946.8 5391.9 323.9 o -7 6 0 10843.8 9146.3 278.4 o -6 6 0 434.3 462.3 56.5 o -5 6 0 58.4 45.9 28.2 < -4 6 0 5101.7 5136.2 133.5 o -3 6 0 4937.6 4841.9 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