data_R110042 _audit_creation_method JANA2006 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Ag16 As4 Cu0 Hg S15' _chemical_formula_weight 2707.09 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Ag' 'Ag' -0.8971 1.1015 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Hg' 'Hg' -2.3894 9.2266 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Cu' 'Cu' 0.3201 1.2651 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' _cell_length_a 26.030(2) _cell_length_b 15.0590(10) _cell_length_c 15.5240(10) _cell_angle_alpha 90.00 _cell_angle_beta 90.450(10) _cell_angle_gamma 90.00 _cell_volume 6085.0(7) _cell_formula_units_Z 8 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 5.910 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 9632 _exptl_absorpt_coefficient_mu 20.407 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71069 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 17368 _diffrn_reflns_av_R_equivalents 0.0000 _diffrn_reflns_av_sigmaI/netI 0.2111 _diffrn_reflns_limit_h_min -40 _diffrn_reflns_limit_h_max 41 _diffrn_reflns_limit_k_min -23 _diffrn_reflns_limit_k_max 23 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 24 _diffrn_reflns_theta_min 3.77 _diffrn_reflns_theta_max 34.79 _reflns_number_total 17368 _reflns_number_gt 7445 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0224P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.0(4) _refine_ls_number_reflns 17368 _refine_ls_number_parameters 659 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0489 _refine_ls_R_factor_gt 0.0430 _refine_ls_wR_factor_ref 0.0854 _refine_ls_wR_factor_gt 0.0846 _refine_ls_goodness_of_fit_ref 0.566 _refine_ls_restrained_S_all 0.566 _refine_ls_shift/su_max 0.031 _refine_ls_shift/su_mean 0.002 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Hg1 Hg 0.12317(5) 0.10741(6) 0.50142(7) 0.0259(3) Uani 0.811(4) 1 d P . . Cu1 Cu 0.12317(5) 0.10741(6) 0.50142(7) 0.0259(3) Uani 0.189(4) 1 d P . . Hg2 Hg 0.13044(4) 0.61371(6) 0.50032(7) 0.0245(3) Uani 0.762(4) 1 d P . . Cu2 Cu 0.13044(4) 0.61371(6) 0.50032(7) 0.0245(3) Uani 0.238(4) 1 d P . . Ag1 Ag 0.27942(7) 0.83547(9) 0.91487(11) 0.0303(4) Uani 1 1 d . . . Ag2 Ag 0.07787(7) 0.46518(8) 0.08665(10) 0.0231(4) Uani 1 1 d . . . Ag3 Ag 0.04799(6) 0.61918(9) -0.09576(9) 0.0207(3) Uani 1 1 d . . . Ag4 Ag -0.02886(7) 0.38295(9) 0.08959(11) 0.0276(4) Uani 1 1 d . . . Ag5 Ag -0.03282(7) -0.11871(9) 0.09015(10) 0.0269(4) Uani 1 1 d . . . Ag6 Ag 0.07739(7) -0.02527(8) 0.08672(11) 0.0240(4) Uani 1 1 d . . . Ag7 Ag 0.04706(7) 0.11772(10) 0.90500(11) 0.0304(4) Uani 1 1 d . . . Ag8 Ag 0.16718(7) 0.24399(8) 0.91076(10) 0.0240(4) Uani 1 1 d . . . Ag9 Ag 0.20512(7) 0.09588(9) 0.09778(11) 0.0301(4) Uani 1 1 d . . . Ag10 Ag 0.28159(6) 0.32376(8) 0.91149(10) 0.0234(4) Uani 1 1 d . . . Ag11 Ag 0.17838(7) 0.74481(9) 0.91217(11) 0.0287(4) Uani 1 1 d . . . Ag12 Ag 0.20066(7) 0.60997(10) 0.09356(11) 0.0330(4) Uani 1 1 d . . . Ag13 Ag 0.12931(6) -0.12908(8) 0.71132(10) 0.0227(3) Uani 1 1 d . . . Ag14 Ag 0.11725(6) 0.62574(9) 0.30257(10) 0.0288(4) Uani 1 1 d . . . Ag15 Ag 0.01748(7) 0.72701(9) 0.30817(10) 0.0262(4) Uani 1 1 d . . . Ag16 Ag 0.01481(7) 0.22641(10) 0.29645(10) 0.0304(4) Uani 1 1 d . . . Ag17 Ag 0.13132(6) 0.37339(8) 0.70689(9) 0.0196(3) Uani 1 1 d . . . Ag18 Ag 0.23574(7) 0.48206(8) 0.69797(11) 0.0248(4) Uani 1 1 d . . . Ag19 Ag 0.12004(6) 0.12922(9) 0.30833(10) 0.0264(4) Uani 1 1 d . . . Ag20 Ag 0.0000 0.73161(13) 0.5000 0.0302(5) Uani 1 2 d S . . Ag21 Ag 0.13640(6) 0.07349(9) 0.68981(10) 0.0239(3) Uani 1 1 d . . . Ag22 Ag 0.18294(6) 0.29352(9) 0.50066(10) 0.0268(4) Uani 1 1 d . . . Ag23 Ag 0.13781(7) 0.57552(9) 0.69449(11) 0.0282(4) Uani 1 1 d . . . Ag24 Ag 0.11447(6) 0.32572(8) 0.29886(9) 0.0221(3) Uani 1 1 d . . . Ag25 Ag 0.17866(6) 0.80057(9) 0.49758(10) 0.0258(4) Uani 1 1 d . . . Ag26 Ag 0.23458(7) -0.01717(8) 0.69532(11) 0.0269(4) Uani 1 1 d . . . Ag27 Ag 0.06951(6) -0.08579(8) 0.50236(9) 0.0211(3) Uani 1 1 d . . . Ag28 Ag 0.11660(7) 0.83255(9) 0.29365(11) 0.0283(4) Uani 1 1 d . . . Ag29 Ag 0.24810(6) 0.13996(7) 0.50085(9) 0.0220(3) Uani 1 1 d . . . Ag30 Ag 0.0000 0.28735(13) 0.5000 0.0230(5) Uani 1 2 d S . . Ag31 Ag 0.24918(7) 0.44863(8) 0.50166(11) 0.0234(3) Uani 1 1 d . . . Ag32 Ag 0.0000 0.09451(11) 0.5000 0.0262(5) Uani 1 2 d S . . Ag33 Ag 0.07276(6) 0.41872(9) 0.50135(9) 0.0222(4) Uani 1 1 d . . . Ag34 Ag 0.0000 0.57624(12) 0.5000 0.0217(5) Uani 1 2 d S . . As1 As 0.08490(9) 0.22497(12) 0.07298(13) 0.0233(5) Uani 1 1 d . . . As2 As 0.08056(10) 0.72482(12) 0.07406(14) 0.0257(6) Uani 1 1 d . . . As3 As 0.16697(9) 0.48559(10) 0.92885(14) 0.0211(6) Uani 1 1 d . . . As4 As 0.16915(9) -0.01251(10) 0.92661(14) 0.0194(5) Uani 1 1 d . . . As5 As 0.24888(9) 0.73253(11) 0.28503(13) 0.0207(5) Uani 1 1 d . . . As6 As 0.00058(9) 0.47155(11) 0.28595(14) 0.0208(5) Uani 1 1 d . . . As7 As 0.00114(9) -0.02443(11) 0.71493(14) 0.0209(5) Uani 1 1 d . . . As8 As 0.25080(9) 0.23280(11) 0.28486(13) 0.0200(5) Uani 1 1 d . . . S1 S 0.0061(2) 0.7417(3) 0.1519(4) 0.0329(14) Uani 1 1 d . . . S2 S 0.1173(3) 0.1103(3) 0.1532(4) 0.0393(16) Uani 1 1 d . . . S3 S 0.2440(3) 0.4662(3) 0.8581(4) 0.0391(17) Uani 1 1 d . . . S4 S 0.1353(2) 0.6030(3) 0.8549(4) 0.0297(13) Uani 1 1 d . . . S5 S 0.0105(3) 0.2421(4) 0.1396(4) 0.0418(17) Uani 1 1 d . . . S6 S 0.1261(2) -0.1170(3) 0.8736(3) 0.0306(14) Uani 1 1 d . . . S7 S 0.1212(2) 0.3769(3) 0.8620(4) 0.0294(13) Uani 1 1 d . . . S8 S 0.1228(2) 0.8401(3) 0.1300(4) 0.0351(15) Uani 1 1 d . . . S9 S 0.1128(2) 0.6095(3) 0.1467(4) 0.0341(14) Uani 1 1 d . . . S10 S 0.1258(3) 0.3348(3) 0.1339(4) 0.0365(15) Uani 1 1 d . . . S11 S 0.2417(3) -0.0276(3) 0.8567(4) 0.0416(18) Uani 1 1 d . . . S12 S 0.2542(2) 0.7008(3) -0.0032(3) 0.0339(13) Uani 1 1 d . . . S13 S 0.1325(3) 0.0953(3) 0.8512(4) 0.0373(15) Uani 1 1 d . . . S14 S 0.0000 0.5141(5) 0.0000 0.040(2) Uani 1 2 d S . . S15 S 0.0000 0.0140(4) 0.0000 0.0320(18) Uani 1 2 d S . . S16 S 0.2133(3) 0.8494(3) 0.3597(4) 0.0384(16) Uani 1 1 d . . . S17 S 0.0755(3) -0.0261(3) 0.3536(4) 0.0369(16) Uani 1 1 d . . . S18 S 0.0857(2) 0.7403(3) 0.4531(4) 0.0316(14) Uani 1 1 d . . . S19 S 0.0828(3) 0.2305(3) 0.4414(4) 0.0376(15) Uani 1 1 d . . . S20 S 0.1668(3) -0.0242(3) 0.5465(4) 0.0335(16) Uani 1 1 d . . . S21 S 0.2126(2) 0.6145(3) 0.3510(4) 0.0355(14) Uani 1 1 d . . . S22 S 0.0742(3) 0.4732(3) 0.3511(4) 0.0372(16) Uani 1 1 d . . . S23 S 0.0431(3) -0.1346(3) 0.6504(4) 0.0340(14) Uani 1 1 d . . . S24 S -0.0376(3) 0.3610(3) 0.3509(4) 0.0337(15) Uani 1 1 d . . . S25 S -0.0358(2) 0.5870(3) 0.3551(4) 0.0305(13) Uani 1 1 d . . . S26 S 0.1733(2) 0.2390(3) 0.6447(4) 0.0329(15) Uani 1 1 d . . . S27 S 0.2113(3) 0.3491(3) 0.3564(4) 0.0331(15) Uani 1 1 d . . . S28 S 0.2857(2) 0.6165(4) 0.6493(4) 0.0364(14) Uani 1 1 d . . . S29 S -0.0336(2) 0.0893(3) 0.3612(4) 0.0331(13) Uani 1 1 d . . . S30 S 0.1692(3) 0.7296(3) 0.6442(4) 0.0376(15) Uani 1 1 d . . . S31 S 0.1605(3) 0.4818(3) 0.5593(4) 0.0326(15) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Hg1 0.0255(5) 0.0257(4) 0.0264(4) 0.0003(3) -0.0002(4) -0.0002(3) Cu1 0.0255(5) 0.0257(4) 0.0264(4) 0.0003(3) -0.0002(4) -0.0002(3) Hg2 0.0246(6) 0.0243(4) 0.0247(5) 0.0003(3) 0.0012(4) -0.0005(4) Cu2 0.0246(6) 0.0243(4) 0.0247(5) 0.0003(3) 0.0012(4) -0.0005(4) Ag1 0.0296(11) 0.0316(8) 0.0297(9) -0.0004(6) 0.0004(8) 0.0003(7) Ag2 0.0238(10) 0.0217(6) 0.0240(9) -0.0008(5) 0.0006(7) -0.0020(6) Ag3 0.0204(9) 0.0208(6) 0.0209(7) -0.0003(5) -0.0003(6) -0.0005(6) Ag4 0.0268(11) 0.0281(7) 0.0278(9) 0.0004(5) -0.0004(8) -0.0001(7) Ag5 0.0296(11) 0.0259(7) 0.0252(8) 0.0004(5) 0.0028(8) 0.0006(6) Ag6 0.0260(11) 0.0221(6) 0.0239(9) -0.0012(5) 0.0014(8) -0.0012(6) Ag7 0.0304(10) 0.0293(7) 0.0316(9) 0.0013(6) 0.0004(8) 0.0010(7) Ag8 0.0236(11) 0.0249(7) 0.0235(8) 0.0008(5) -0.0013(7) 0.0022(6) Ag9 0.0308(11) 0.0302(8) 0.0295(9) 0.0002(5) 0.0028(8) -0.0011(7) Ag10 0.0239(10) 0.0225(7) 0.0237(8) -0.0008(5) 0.0011(7) -0.0010(6) Ag11 0.0300(11) 0.0262(7) 0.0298(9) -0.0005(5) -0.0012(8) -0.0026(6) Ag12 0.0306(10) 0.0355(7) 0.0328(8) 0.0007(6) -0.0004(8) -0.0006(7) Ag13 0.0241(9) 0.0220(6) 0.0220(7) 0.0000(5) 0.0013(6) 0.0000(6) Ag14 0.0295(10) 0.0279(7) 0.0289(8) 0.0000(5) -0.0009(7) -0.0008(6) Ag15 0.0249(10) 0.0271(6) 0.0267(8) 0.0002(5) -0.0025(8) 0.0000(6) Ag16 0.0287(11) 0.0324(7) 0.0301(9) -0.0007(6) -0.0004(8) -0.0013(7) Ag17 0.0184(9) 0.0200(6) 0.0204(7) 0.0006(4) -0.0014(6) 0.0004(5) Ag18 0.0236(11) 0.0252(7) 0.0257(9) -0.0002(5) 0.0013(8) -0.0006(6) Ag19 0.0286(9) 0.0252(7) 0.0253(8) 0.0000(5) 0.0012(7) 0.0000(6) Ag20 0.0323(14) 0.0286(10) 0.0296(10) 0.000 0.0041(10) 0.000 Ag21 0.0224(9) 0.0259(6) 0.0234(8) 0.0007(5) -0.0029(7) 0.0011(6) Ag22 0.0284(10) 0.0267(6) 0.0253(7) -0.0004(5) -0.0011(7) -0.0004(6) Ag23 0.0271(10) 0.0296(7) 0.0277(8) 0.0013(5) -0.0018(7) 0.0001(6) Ag24 0.0230(9) 0.0211(6) 0.0222(7) 0.0010(4) -0.0002(6) 0.0010(5) Ag25 0.0259(10) 0.0257(7) 0.0258(8) -0.0009(5) 0.0005(7) -0.0004(6) Ag26 0.0270(12) 0.0263(7) 0.0274(10) -0.0005(5) 0.0007(9) -0.0013(6) Ag27 0.0232(10) 0.0193(6) 0.0206(7) -0.0006(4) 0.0022(7) -0.0003(6) Ag28 0.0286(11) 0.0283(7) 0.0281(9) 0.0001(5) -0.0005(8) 0.0015(7) Ag29 0.0214(9) 0.0210(6) 0.0235(7) -0.0005(5) 0.0014(6) -0.0006(6) Ag30 0.0242(12) 0.0207(8) 0.0242(9) 0.000 0.0036(8) 0.000 Ag31 0.0204(7) 0.0252(6) 0.0246(6) -0.0006(5) -0.0023(5) -0.0012(6) Ag32 0.0255(13) 0.0275(10) 0.0257(10) 0.000 -0.0003(10) 0.000 Ag33 0.0218(9) 0.0227(6) 0.0221(7) 0.0004(5) 0.0017(7) -0.0005(6) Ag34 0.0233(14) 0.0200(9) 0.0219(11) 0.000 0.0011(10) 0.000 As1 0.0220(15) 0.0255(9) 0.0222(10) -0.0004(7) -0.0016(10) 0.0007(9) As2 0.0254(16) 0.0255(9) 0.0261(11) -0.0010(7) -0.0013(11) -0.0007(9) As3 0.0219(15) 0.0206(9) 0.0210(12) -0.0004(6) -0.0002(11) -0.0003(8) As4 0.0198(14) 0.0195(9) 0.0191(11) -0.0007(6) 0.0016(10) -0.0007(7) As5 0.0209(13) 0.0209(8) 0.0201(10) -0.0016(7) -0.0012(9) -0.0001(8) As6 0.0193(13) 0.0208(8) 0.0223(12) -0.0002(6) -0.0001(10) -0.0025(8) As7 0.0203(14) 0.0215(8) 0.0209(12) -0.0014(6) -0.0005(10) 0.0012(8) As8 0.0188(13) 0.0208(8) 0.0203(10) 0.0000(7) -0.0020(9) -0.0003(8) S1 0.031(4) 0.035(3) 0.033(3) 0.0012(18) -0.002(3) 0.006(2) S2 0.037(4) 0.037(3) 0.044(4) 0.001(2) 0.003(3) 0.004(3) S3 0.040(4) 0.031(3) 0.047(4) -0.003(2) 0.004(3) 0.002(2) S4 0.028(3) 0.033(2) 0.028(3) -0.0019(17) -0.001(3) -0.004(2) S5 0.039(5) 0.048(3) 0.039(4) -0.001(2) 0.001(3) 0.005(3) S6 0.042(4) 0.026(2) 0.024(3) 0.0024(16) 0.001(3) 0.000(2) S7 0.029(4) 0.027(2) 0.032(3) 0.0018(18) -0.002(3) -0.002(2) S8 0.035(4) 0.030(2) 0.040(3) -0.0007(19) -0.002(3) 0.003(2) S9 0.036(4) 0.030(2) 0.037(3) 0.0012(19) 0.001(3) 0.002(2) S10 0.037(4) 0.036(3) 0.036(3) 0.000(2) -0.003(3) -0.001(2) S11 0.042(5) 0.042(3) 0.041(4) -0.004(2) 0.000(4) -0.003(3) S12 0.029(4) 0.037(2) 0.036(3) 0.001(2) -0.010(3) 0.002(2) S13 0.041(4) 0.035(3) 0.036(3) -0.0004(19) -0.002(3) -0.003(2) S14 0.034(5) 0.029(3) 0.057(6) 0.000 -0.001(4) 0.000 S15 0.024(5) 0.027(3) 0.045(5) 0.000 0.002(4) 0.000 S16 0.049(5) 0.032(2) 0.034(3) 0.0034(19) 0.007(3) 0.004(2) S17 0.028(4) 0.041(3) 0.042(4) 0.003(2) -0.001(3) 0.004(2) S18 0.029(4) 0.032(2) 0.033(3) -0.0021(18) 0.005(3) 0.002(2) S19 0.034(4) 0.046(3) 0.033(3) -0.003(2) 0.003(3) -0.004(2) S20 0.037(4) 0.034(2) 0.030(3) 0.0056(18) 0.006(3) -0.002(2) S21 0.047(4) 0.025(2) 0.034(3) -0.0003(19) 0.002(3) 0.002(2) S22 0.027(4) 0.046(3) 0.039(4) 0.007(2) -0.003(3) 0.007(2) S23 0.039(4) 0.029(2) 0.034(3) 0.0011(18) 0.001(3) 0.004(2) S24 0.041(4) 0.035(2) 0.026(3) -0.0015(18) 0.002(3) 0.001(2) S25 0.030(3) 0.024(2) 0.038(3) 0.0023(18) 0.001(3) 0.004(2) S26 0.034(4) 0.030(2) 0.035(3) -0.0001(18) 0.004(3) -0.003(2) S27 0.038(4) 0.026(2) 0.035(3) 0.0002(18) 0.004(3) -0.001(2) S28 0.039(4) 0.038(2) 0.032(3) -0.003(2) -0.003(3) -0.006(3) S29 0.023(3) 0.035(2) 0.041(3) 0.0031(19) -0.004(3) 0.005(2) S30 0.042(4) 0.036(2) 0.034(3) 0.002(2) 0.001(3) -0.004(2) S31 0.037(4) 0.031(2) 0.031(3) -0.0014(17) 0.008(3) -0.004(2) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Hg1 S19 2.323(6) . ? Hg1 S20 2.386(6) . ? Hg1 Ag21 2.986(2) . ? Hg1 Ag19 3.016(2) . ? Hg1 Ag22 3.2056(19) . ? Hg1 Ag32 3.2118(13) . ? Hg1 Ag27 3.2274(17) . ? Hg1 Ag29 3.289(2) . ? Hg2 S31 2.321(5) . ? Hg2 S18 2.348(6) . ? Hg2 S30 3.002(6) . ? Hg2 Ag23 3.073(2) . ? Hg2 Ag25 3.0816(17) . ? Hg2 Ag14 3.092(2) . ? Hg2 Ag29 3.1864(19) 4_556 ? Hg2 Ag33 3.2981(17) . ? Ag1 S11 2.453(7) 1_565 ? Ag1 S12 2.485(5) 1_556 ? Ag1 S10 2.586(6) 4_556 ? Ag1 Ag11 2.963(2) . ? Ag1 Ag10 3.1443(19) 4_557 ? Ag1 Ag8 3.331(3) 4_557 ? Ag2 S10 2.436(6) . ? Ag2 S14 2.533(3) . ? Ag2 S9 2.531(6) . ? Ag2 Ag4 3.042(2) . ? Ag2 Ag4 3.254(3) 2 ? Ag3 S4 2.417(5) 1_554 ? Ag3 S1 2.475(6) 2 ? Ag3 S14 2.511(5) . ? Ag4 S5 2.477(6) . ? Ag4 S7 2.525(6) 2_556 ? Ag4 S14 2.533(6) . ? Ag4 Ag4 3.172(3) 2 ? Ag4 Ag2 3.254(3) 2 ? Ag5 S6 2.498(6) 2_556 ? Ag5 S1 2.520(5) 1_545 ? Ag5 S15 2.589(5) . ? Ag5 Ag6 3.196(2) . ? Ag5 Ag6 3.289(3) 2 ? Ag5 Ag5 3.291(3) 2 ? Ag6 S8 2.439(6) 1_545 ? Ag6 S15 2.486(3) . ? Ag6 S2 2.508(6) . ? Ag6 Ag5 3.289(3) 2 ? Ag7 S13 2.407(6) . ? Ag7 S15 2.478(5) 1_556 ? Ag7 S5 2.493(7) 2_556 ? Ag8 S7 2.449(5) . ? Ag8 S12 2.574(6) 4_546 ? Ag8 S13 2.583(6) . ? Ag8 Ag10 3.211(2) . ? Ag8 Ag1 3.331(3) 4_547 ? Ag9 S12 2.407(5) 4_545 ? Ag9 S2 2.459(6) . ? Ag9 S3 2.453(6) 4_546 ? Ag10 S3 2.497(6) . ? Ag10 S12 2.520(5) 4_546 ? Ag10 S8 2.586(6) 4_546 ? Ag10 Ag1 3.144(2) 4_547 ? Ag10 Ag11 3.154(2) 4_547 ? Ag10 Ag12 3.2535(19) 4_546 ? Ag11 S12 2.453(6) 1_556 ? Ag11 S6 2.555(5) 1_565 ? Ag11 S4 2.567(6) . ? Ag11 Ag10 3.154(2) 4_557 ? Ag12 S9 2.438(6) . ? Ag12 S12 2.471(5) . ? Ag12 S11 2.669(7) 4_556 ? Ag12 Ag10 3.2535(19) 4_556 ? Ag13 S23 2.429(7) . ? Ag13 S6 2.528(5) . ? Ag13 S30 2.591(5) 1_545 ? Ag13 Ag21 3.0744(19) . ? Ag13 Ag26 3.228(2) . ? Ag14 S9 2.434(6) . ? Ag14 S21 2.593(7) . ? Ag14 S22 2.667(5) . ? Ag14 Ag15 3.014(2) . ? Ag14 Ag28 3.117(2) . ? Ag15 S1 2.452(6) . ? Ag15 S25 2.630(5) . ? Ag15 S23 2.694(5) 2_566 ? Ag15 S18 2.862(7) . ? Ag15 Ag20 3.0169(15) . ? Ag15 Ag28 3.040(2) . ? Ag16 S5 2.448(7) . ? Ag16 S24 2.588(5) . ? Ag16 S29 2.622(5) . ? Ag16 S19 2.852(7) . ? Ag16 Ag24 2.994(2) . ? Ag16 Ag19 3.110(2) . ? Ag16 Ag30 3.3159(17) . ? Ag17 S7 2.425(6) . ? Ag17 S26 2.498(5) . ? Ag17 S24 2.600(7) 2_556 ? Ag17 S31 2.919(5) . ? Ag17 Ag23 3.0546(19) . ? Ag17 Ag18 3.177(2) . ? Ag18 S3 2.505(7) . ? Ag18 S28 2.525(5) . ? Ag18 S16 2.563(5) 4_546 ? Ag18 S31 2.899(8) . ? Ag18 Ag23 2.912(2) . ? Ag18 Ag31 3.111(2) . ? Ag19 S2 2.426(6) . ? Ag19 S28 2.543(7) 4_546 ? Ag19 S17 2.706(5) . ? Ag19 S19 2.750(5) . ? Ag19 Ag24 2.9662(18) . ? Ag20 Ag34 2.340(2) . ? Ag20 S18 2.355(6) 2_556 ? Ag20 S18 2.355(6) . ? Ag20 Ag15 3.0169(15) 2_556 ? Ag20 Ag27 3.292(2) 2_566 ? Ag20 Ag27 3.292(2) 1_565 ? Ag21 S13 2.529(6) . ? Ag21 S26 2.763(5) . ? Ag21 S29 2.795(7) 2_556 ? Ag21 S20 2.787(5) . ? Ag21 Ag26 2.898(2) . ? Ag22 S26 2.397(6) . ? Ag22 S27 2.508(5) . ? Ag22 Ag29 2.8677(19) . ? Ag22 Ag31 2.903(2) . ? Ag22 S19 2.916(7) . ? Ag23 S4 2.526(6) . ? Ag23 S30 2.582(5) . ? Ag23 S31 2.601(5) . ? Ag23 S25 2.764(7) 2_556 ? Ag24 S22 2.589(5) . ? Ag24 S10 2.584(6) . ? Ag24 S27 2.692(7) . ? Ag24 S19 2.767(5) . ? Ag25 S16 2.442(5) . ? Ag25 S30 2.528(6) . ? Ag25 S18 2.671(7) . ? Ag25 S20 2.764(5) 1_565 ? Ag25 Ag31 2.915(2) 4_556 ? Ag25 Ag29 3.0796(19) 4_556 ? Ag25 Ag27 3.3181(17) 1_565 ? Ag26 S21 2.521(5) 4_546 ? Ag26 S11 2.516(7) . ? Ag26 S27 2.588(5) 4_546 ? Ag26 S20 2.898(8) . ? Ag26 Ag31 3.133(2) 4_546 ? Ag27 S17 2.484(6) . ? Ag27 S23 2.514(5) . ? Ag27 S18 2.762(5) 1_545 ? Ag27 S20 2.778(7) . ? Ag27 Ag32 3.2629(19) . ? Ag27 Ag20 3.292(2) 1_545 ? Ag27 Ag25 3.3181(17) 1_545 ? Ag28 S8 2.550(6) . ? Ag28 S17 2.561(5) 1_565 ? Ag28 S16 2.723(8) . ? Ag28 S18 2.956(5) . ? Ag29 S28 2.510(6) 4_546 ? Ag29 S21 2.539(6) 4_546 ? Ag29 Ag31 2.8824(16) 4_546 ? Ag29 Ag25 3.0796(19) 4_546 ? Ag29 Hg2 3.1864(19) 4_546 ? Ag29 Cu2 3.1864(19) 4_546 ? Ag30 S19 2.497(6) 2_556 ? Ag30 S19 2.497(6) . ? Ag30 Ag33 2.739(2) 2_556 ? Ag30 Ag33 2.739(2) . ? Ag30 S24 2.740(6) 2_556 ? Ag30 S24 2.740(6) . ? Ag30 Ag32 2.904(3) . ? Ag30 Ag16 3.3159(17) 2_556 ? Ag31 S20 2.353(6) 4_556 ? Ag31 S31 2.532(6) . ? Ag31 S16 2.790(7) 4_546 ? Ag31 S27 2.875(6) . ? Ag31 Ag29 2.8824(16) 4_556 ? Ag31 Ag25 2.915(2) 4_546 ? Ag31 Ag26 3.133(2) 4_556 ? Ag32 S29 2.321(7) 2_556 ? Ag32 S29 2.321(7) . ? Ag32 Cu1 3.2118(13) 2_556 ? Ag32 Hg1 3.2118(13) 2_556 ? Ag32 Ag27 3.2629(19) 2_556 ? Ag33 S22 2.473(6) . ? Ag33 S24 2.625(5) 2_556 ? Ag33 S31 2.626(7) . ? Ag33 Ag34 3.0354(19) . ? Ag34 S25 2.433(6) 2_556 ? Ag34 S25 2.433(6) . ? Ag34 Ag33 3.035(2) 2_556 ? As1 S10 2.179(6) . ? As1 S5 2.218(6) . ? As1 S2 2.286(6) . ? As2 S8 2.228(6) . ? As2 S9 2.231(6) . ? As2 S1 2.305(6) . ? As3 S4 2.260(6) . ? As3 S7 2.271(6) . ? As3 S3 2.312(6) . ? As4 S6 2.095(6) . ? As4 S11 2.196(6) . ? As4 S13 2.213(6) . ? As5 S21 2.261(5) . ? As5 S26 2.295(7) 4_556 ? As5 S16 2.306(5) . ? As6 S22 2.159(8) . ? As6 S24 2.188(5) . ? As6 S25 2.256(5) . ? As7 S23 2.229(5) . ? As7 S29 2.249(5) 2_556 ? As7 S17 2.253(8) 2_556 ? As8 S28 2.242(6) 4_546 ? As8 S27 2.319(5) . ? As8 S30 2.348(8) 4_546 ? S1 Ag3 2.475(6) 2 ? S1 Ag5 2.520(5) 1_565 ? S3 Ag9 2.453(6) 4_556 ? S4 Ag3 2.417(5) 1_556 ? S5 Ag7 2.493(7) 2_556 ? S6 Ag5 2.498(6) 2_556 ? S6 Ag11 2.555(5) 1_545 ? S7 Ag4 2.525(6) 2_556 ? S8 Ag6 2.439(6) 1_565 ? S8 Ag10 2.586(6) 4_556 ? S10 Ag1 2.586(6) 4_546 ? S11 Ag1 2.453(7) 1_545 ? S11 Ag12 2.669(7) 4_546 ? S12 Ag9 2.407(5) 4 ? S12 Ag11 2.453(6) 1_554 ? S12 Ag1 2.485(5) 1_554 ? S12 Ag10 2.520(5) 4_556 ? S12 Ag8 2.574(6) 4_556 ? S14 Ag3 2.511(5) 2 ? S14 Ag2 2.533(3) 2 ? S14 Ag4 2.533(6) 2 ? S15 Ag7 2.478(4) 2_556 ? S15 Ag7 2.478(4) 1_554 ? S15 Ag6 2.486(3) 2 ? S15 Ag5 2.589(5) 2 ? S16 Ag18 2.563(5) 4_556 ? S16 Ag31 2.790(7) 4_556 ? S17 As7 2.253(8) 2_556 ? S17 Ag28 2.561(5) 1_545 ? S18 Ag27 2.762(5) 1_565 ? S20 Ag31 2.353(6) 4_546 ? S20 Ag25 2.764(5) 1_545 ? S21 Ag26 2.521(5) 4_556 ? S21 Ag29 2.539(6) 4_556 ? S23 Ag15 2.694(5) 2_546 ? S24 Ag17 2.600(7) 2_556 ? S24 Ag33 2.625(5) 2_556 ? S25 Ag23 2.764(7) 2_556 ? S26 As5 2.295(7) 4_546 ? S27 Ag26 2.588(5) 4_556 ? S28 As8 2.242(6) 4_556 ? S28 Ag29 2.510(6) 4_556 ? S28 Ag19 2.543(7) 4_556 ? S29 As7 2.249(5) 2_556 ? S29 Ag21 2.795(7) 2_556 ? S30 As8 2.348(8) 4_556 ? S30 Ag13 2.591(5) 1_565 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S19 Hg1 S20 173.4(2) . . ? S19 Hg1 Ag21 125.31(14) . . ? S20 Hg1 Ag21 61.29(14) . . ? S19 Hg1 Ag19 60.36(13) . . ? S20 Hg1 Ag19 113.03(14) . . ? Ag21 Hg1 Ag19 173.75(6) . . ? S19 Hg1 Ag22 61.23(16) . . ? S20 Hg1 Ag22 119.82(17) . . ? Ag21 Hg1 Ag22 95.79(5) . . ? Ag19 Hg1 Ag22 84.86(5) . . ? S19 Hg1 Ag32 66.25(16) . . ? S20 Hg1 Ag32 115.12(15) . . ? Ag21 Hg1 Ag32 95.96(4) . . ? Ag19 Hg1 Ag32 88.89(5) . . ? Ag22 Hg1 Ag32 122.50(5) . . ? S19 Hg1 Ag27 121.81(17) . . ? S20 Hg1 Ag27 56.98(16) . . ? Ag21 Hg1 Ag27 83.57(5) . . ? Ag19 Hg1 Ag27 95.42(5) . . ? Ag22 Hg1 Ag27 176.60(6) . . ? Ag32 Hg1 Ag27 60.89(5) . . ? S19 Hg1 Ag29 108.91(15) . . ? S20 Hg1 Ag29 69.89(15) . . ? Ag21 Hg1 Ag29 85.51(5) . . ? Ag19 Hg1 Ag29 90.01(5) . . ? Ag22 Hg1 Ag29 52.39(4) . . ? Ag32 Hg1 Ag29 174.87(5) . . ? Ag27 Hg1 Ag29 124.22(5) . . ? S31 Hg2 S18 169.4(2) . . ? S31 Hg2 S30 95.4(2) . . ? S18 Hg2 S30 85.63(19) . . ? S31 Hg2 Ag23 55.57(13) . . ? S18 Hg2 Ag23 119.02(13) . . ? S30 Hg2 Ag23 50.29(10) . . ? S31 Hg2 Ag25 130.61(18) . . ? S18 Hg2 Ag25 57.04(15) . . ? S30 Hg2 Ag25 49.09(10) . . ? Ag23 Hg2 Ag25 99.33(5) . . ? S31 Hg2 Ag14 118.45(14) . . ? S18 Hg2 Ag14 65.89(13) . . ? S30 Hg2 Ag14 137.61(10) . . ? Ag23 Hg2 Ag14 172.09(6) . . ? Ag25 Hg2 Ag14 88.56(5) . . ? S31 Hg2 Ag29 77.11(15) . 4_556 ? S18 Hg2 Ag29 112.81(14) . 4_556 ? S30 Hg2 Ag29 66.70(12) . 4_556 ? Ag23 Hg2 Ag29 88.54(5) . 4_556 ? Ag25 Hg2 Ag29 58.83(4) . 4_556 ? Ag14 Hg2 Ag29 95.13(5) . 4_556 ? S31 Hg2 Ag33 52.27(17) . . ? S18 Hg2 Ag33 119.94(16) . . ? S30 Hg2 Ag33 131.61(10) . . ? Ag23 Hg2 Ag33 81.58(5) . . ? Ag25 Hg2 Ag33 176.92(7) . . ? Ag14 Hg2 Ag33 90.57(5) . . ? Ag29 Hg2 Ag33 124.21(5) 4_556 . ? S11 Ag1 S12 140.1(2) 1_565 1_556 ? S11 Ag1 S10 106.0(2) 1_565 4_556 ? S12 Ag1 S10 113.76(18) 1_556 4_556 ? S11 Ag1 Ag11 91.67(18) 1_565 . ? S12 Ag1 Ag11 52.64(14) 1_556 . ? S10 Ag1 Ag11 147.42(14) 4_556 . ? S11 Ag1 Ag10 99.14(15) 1_565 4_557 ? S12 Ag1 Ag10 51.57(12) 1_556 4_557 ? S10 Ag1 Ag10 137.73(16) 4_556 4_557 ? Ag11 Ag1 Ag10 62.10(5) . 4_557 ? S11 Ag1 Ag8 144.08(18) 1_565 4_557 ? S12 Ag1 Ag8 49.98(14) 1_556 4_557 ? S10 Ag1 Ag8 80.98(15) 4_556 4_557 ? Ag11 Ag1 Ag8 100.70(6) . 4_557 ? Ag10 Ag1 Ag8 59.37(5) 4_557 4_557 ? S10 Ag2 S14 143.1(2) . . ? S10 Ag2 S9 113.6(2) . . ? S14 Ag2 S9 103.3(2) . . ? S10 Ag2 Ag4 97.65(16) . . ? S14 Ag2 Ag4 53.08(13) . . ? S9 Ag2 Ag4 132.00(14) . . ? S10 Ag2 Ag4 98.21(16) . 2 ? S14 Ag2 Ag4 50.02(13) . 2 ? S9 Ag2 Ag4 140.68(15) . 2 ? Ag4 Ag2 Ag4 60.38(6) . 2 ? S4 Ag3 S1 119.84(18) 1_554 2 ? S4 Ag3 S14 126.71(17) 1_554 . ? S1 Ag3 S14 113.18(16) 2 . ? S5 Ag4 S7 105.56(19) . 2_556 ? S5 Ag4 S14 135.70(17) . . ? S7 Ag4 S14 118.60(14) 2_556 . ? S5 Ag4 Ag2 88.71(17) . . ? S7 Ag4 Ag2 152.93(13) 2_556 . ? S14 Ag4 Ag2 53.10(5) . . ? S5 Ag4 Ag4 94.42(14) . 2 ? S7 Ag4 Ag4 136.02(17) 2_556 2 ? S14 Ag4 Ag4 51.23(11) . 2 ? Ag2 Ag4 Ag4 63.12(6) . 2 ? S5 Ag4 Ag2 138.37(17) . 2 ? S7 Ag4 Ag2 84.04(15) 2_556 2 ? S14 Ag4 Ag2 50.04(5) . 2 ? Ag2 Ag4 Ag2 100.64(7) . 2 ? Ag4 Ag4 Ag2 56.50(6) 2 2 ? S6 Ag5 S1 108.19(18) 2_556 1_545 ? S6 Ag5 S15 116.06(14) 2_556 . ? S1 Ag5 S15 135.74(16) 1_545 . ? S6 Ag5 Ag6 150.89(12) 2_556 . ? S1 Ag5 Ag6 90.87(15) 1_545 . ? S15 Ag5 Ag6 49.54(4) . . ? S6 Ag5 Ag6 81.16(14) 2_556 2 ? S1 Ag5 Ag6 144.36(14) 1_545 2 ? S15 Ag5 Ag6 48.25(4) . 2 ? Ag6 Ag5 Ag6 96.23(6) . 2 ? S6 Ag5 Ag5 134.75(16) 2_556 2 ? S1 Ag5 Ag5 96.51(12) 1_545 2 ? S15 Ag5 Ag5 50.54(10) . 2 ? Ag6 Ag5 Ag5 60.90(6) . 2 ? Ag6 Ag5 Ag5 58.13(6) 2 2 ? S8 Ag6 S15 137.4(2) 1_545 . ? S8 Ag6 S2 111.4(2) 1_545 . ? S15 Ag6 S2 111.1(2) . . ? S8 Ag6 Ag5 93.61(16) 1_545 . ? S15 Ag6 Ag5 52.42(12) . . ? S2 Ag6 Ag5 136.06(14) . . ? S8 Ag6 Ag5 92.38(16) 1_545 2 ? S15 Ag6 Ag5 50.99(12) . 2 ? S2 Ag6 Ag5 146.49(15) . 2 ? Ag5 Ag6 Ag5 60.97(5) . 2 ? S13 Ag7 S15 125.51(17) . 1_556 ? S13 Ag7 S5 124.36(19) . 2_556 ? S15 Ag7 S5 109.86(17) 1_556 2_556 ? S7 Ag8 S12 139.78(19) . 4_546 ? S7 Ag8 S13 115.4(2) . . ? S12 Ag8 S13 104.7(2) 4_546 . ? S7 Ag8 Ag10 98.43(14) . . ? S12 Ag8 Ag10 50.17(12) 4_546 . ? S13 Ag8 Ag10 130.30(15) . . ? S7 Ag8 Ag1 96.49(15) . 4_547 ? S12 Ag8 Ag1 47.66(12) 4_546 4_547 ? S13 Ag8 Ag1 142.35(15) . 4_547 ? Ag10 Ag8 Ag1 57.41(5) . 4_547 ? S12 Ag9 S2 124.75(19) 4_545 . ? S12 Ag9 S3 117.0(2) 4_545 4_546 ? S2 Ag9 S3 118.29(19) . 4_546 ? S3 Ag10 S12 132.35(19) . 4_546 ? S3 Ag10 S8 102.16(19) . 4_546 ? S12 Ag10 S8 124.85(18) 4_546 4_546 ? S3 Ag10 Ag1 92.12(14) . 4_547 ? S12 Ag10 Ag1 50.58(12) 4_546 4_547 ? S8 Ag10 Ag1 134.54(16) 4_546 4_547 ? S3 Ag10 Ag11 137.54(16) . 4_547 ? S12 Ag10 Ag11 49.71(14) 4_546 4_547 ? S8 Ag10 Ag11 86.57(15) 4_546 4_547 ? Ag1 Ag10 Ag11 56.13(5) 4_547 4_547 ? S3 Ag10 Ag8 87.68(16) . . ? S12 Ag10 Ag8 51.68(14) 4_546 . ? S8 Ag10 Ag8 158.22(13) 4_546 . ? Ag1 Ag10 Ag8 63.22(5) 4_547 . ? Ag11 Ag10 Ag8 99.33(6) 4_547 . ? S3 Ag10 Ag12 153.86(19) . 4_546 ? S12 Ag10 Ag12 48.66(12) 4_546 4_546 ? S8 Ag10 Ag12 87.20(12) 4_546 4_546 ? Ag1 Ag10 Ag12 98.56(5) 4_547 4_546 ? Ag11 Ag10 Ag12 66.54(5) 4_547 4_546 ? Ag8 Ag10 Ag12 76.21(5) . 4_546 ? S12 Ag11 S6 140.36(19) 1_556 1_565 ? S12 Ag11 S4 107.9(2) 1_556 . ? S6 Ag11 S4 111.5(2) 1_565 . ? S12 Ag11 Ag1 53.61(13) 1_556 . ? S6 Ag11 Ag1 95.66(14) 1_565 . ? S4 Ag11 Ag1 140.63(13) . . ? S12 Ag11 Ag10 51.57(13) 1_556 4_557 ? S6 Ag11 Ag10 93.90(14) 1_565 4_557 ? S4 Ag11 Ag10 138.98(14) . 4_557 ? Ag1 Ag11 Ag10 61.76(5) . 4_557 ? S9 Ag12 S12 137.97(19) . . ? S9 Ag12 S11 115.29(19) . 4_556 ? S12 Ag12 S11 106.66(19) . 4_556 ? S9 Ag12 Ag10 98.33(12) . 4_556 ? S12 Ag12 Ag10 49.96(12) . 4_556 ? S11 Ag12 Ag10 134.06(18) 4_556 4_556 ? S23 Ag13 S6 110.7(2) . . ? S23 Ag13 S30 100.8(2) . 1_545 ? S6 Ag13 S30 118.46(18) . 1_545 ? S23 Ag13 Ag21 92.76(13) . . ? S6 Ag13 Ag21 92.24(11) . . ? S30 Ag13 Ag21 138.32(12) 1_545 . ? S23 Ag13 Ag26 140.35(13) . . ? S6 Ag13 Ag26 94.21(14) . . ? S30 Ag13 Ag26 93.14(14) 1_545 . ? Ag21 Ag13 Ag26 54.69(5) . . ? S9 Ag14 S21 108.65(19) . . ? S9 Ag14 S22 100.2(2) . . ? S21 Ag14 S22 105.39(19) . . ? S9 Ag14 Ag15 92.57(15) . . ? S21 Ag14 Ag15 147.98(13) . . ? S22 Ag14 Ag15 93.64(14) . . ? S9 Ag14 Hg2 170.18(13) . . ? S21 Ag14 Hg2 67.04(12) . . ? S22 Ag14 Hg2 73.31(16) . . ? Ag15 Ag14 Hg2 95.17(5) . . ? S9 Ag14 Ag28 93.21(12) . . ? S21 Ag14 Ag28 94.76(12) . . ? S22 Ag14 Ag28 150.56(13) . . ? Ag15 Ag14 Ag28 59.43(5) . . ? Hg2 Ag14 Ag28 95.92(6) . . ? S1 Ag15 S25 106.66(19) . . ? S1 Ag15 S23 95.76(18) . 2_566 ? S25 Ag15 S23 104.04(15) . 2_566 ? S1 Ag15 S18 147.23(18) . . ? S25 Ag15 S18 99.40(17) . . ? S23 Ag15 S18 96.84(18) 2_566 . ? S1 Ag15 Ag14 96.56(14) . . ? S25 Ag15 Ag14 93.39(13) . . ? S23 Ag15 Ag14 154.76(16) 2_566 . ? S18 Ag15 Ag14 61.88(10) . . ? S1 Ag15 Ag20 163.10(15) . . ? S25 Ag15 Ag20 70.17(13) . . ? S23 Ag15 Ag20 69.72(13) 2_566 . ? S18 Ag15 Ag20 47.14(10) . . ? Ag14 Ag15 Ag20 100.18(6) . . ? S1 Ag15 Ag28 88.58(15) . . ? S25 Ag15 Ag28 152.81(15) . . ? S23 Ag15 Ag28 96.44(13) 2_566 . ? S18 Ag15 Ag28 60.02(11) . . ? Ag14 Ag15 Ag28 61.99(5) . . ? Ag20 Ag15 Ag28 101.29(6) . . ? S5 Ag16 S24 103.23(19) . . ? S5 Ag16 S29 116.0(2) . . ? S24 Ag16 S29 103.63(16) . . ? S5 Ag16 S19 143.7(2) . . ? S24 Ag16 S19 92.90(19) . . ? S29 Ag16 S19 90.69(18) . . ? S5 Ag16 Ag24 89.83(17) . . ? S24 Ag16 Ag24 93.62(15) . . ? S29 Ag16 Ag24 143.81(16) . . ? S19 Ag16 Ag24 56.43(11) . . ? S5 Ag16 Ag19 97.93(16) . . ? S24 Ag16 Ag19 144.60(17) . . ? S29 Ag16 Ag19 91.86(13) . . ? S19 Ag16 Ag19 54.73(11) . . ? Ag24 Ag16 Ag19 58.11(5) . . ? S5 Ag16 Ag30 156.39(15) . . ? S24 Ag16 Ag30 53.61(14) . . ? S29 Ag16 Ag30 78.06(13) . . ? S19 Ag16 Ag30 47.03(11) . . ? Ag24 Ag16 Ag30 87.54(6) . . ? Ag19 Ag16 Ag30 100.52(6) . . ? S7 Ag17 S26 116.93(18) . . ? S7 Ag17 S24 103.58(19) . 2_556 ? S26 Ag17 S24 102.8(2) . 2_556 ? S7 Ag17 S31 142.97(16) . . ? S26 Ag17 S31 91.86(15) . . ? S24 Ag17 S31 91.07(18) 2_556 . ? S7 Ag17 Ag23 92.71(11) . . ? S26 Ag17 Ag23 139.33(12) . . ? S24 Ag17 Ag23 95.85(12) 2_556 . ? S31 Ag17 Ag23 51.56(9) . . ? S7 Ag17 Ag18 97.59(14) . . ? S26 Ag17 Ag18 91.35(14) . . ? S24 Ag17 Ag18 145.39(12) 2_556 . ? S31 Ag17 Ag18 56.60(15) . . ? Ag23 Ag17 Ag18 55.68(5) . . ? S3 Ag18 S28 109.4(2) . . ? S3 Ag18 S16 103.42(19) . 4_546 ? S28 Ag18 S16 104.57(18) . 4_546 ? S3 Ag18 S31 142.10(19) . . ? S28 Ag18 S31 97.20(18) . . ? S16 Ag18 S31 95.04(19) 4_546 . ? S3 Ag18 Ag23 97.63(15) . . ? S28 Ag18 Ag23 93.40(15) . . ? S16 Ag18 Ag23 145.63(18) 4_546 . ? S31 Ag18 Ag23 53.18(10) . . ? S3 Ag18 Ag31 161.31(14) . . ? S28 Ag18 Ag31 76.98(13) . . ? S16 Ag18 Ag31 57.94(15) 4_546 . ? S31 Ag18 Ag31 49.68(10) . . ? Ag23 Ag18 Ag31 99.51(7) . . ? S3 Ag18 Ag17 88.55(15) . . ? S28 Ag18 Ag17 150.32(17) . . ? S16 Ag18 Ag17 93.39(15) 4_546 . ? S31 Ag18 Ag17 57.20(10) . . ? Ag23 Ag18 Ag17 60.04(5) . . ? Ag31 Ag18 Ag17 93.56(6) . . ? S2 Ag19 S28 105.6(2) . 4_546 ? S2 Ag19 S17 98.4(2) . . ? S28 Ag19 S17 106.4(2) 4_546 . ? S2 Ag19 S19 143.4(2) . . ? S28 Ag19 S19 101.1(2) 4_546 . ? S17 Ag19 S19 97.48(17) . . ? S2 Ag19 Ag24 93.84(13) . . ? S28 Ag19 Ag24 97.73(13) 4_546 . ? S17 Ag19 Ag24 148.67(13) . . ? S19 Ag19 Ag24 57.75(11) . . ? S2 Ag19 Hg1 166.99(14) . . ? S28 Ag19 Hg1 73.53(13) 4_546 . ? S17 Ag19 Hg1 69.88(15) . . ? S19 Ag19 Hg1 47.24(13) . . ? Ag24 Ag19 Hg1 99.14(5) . . ? S2 Ag19 Ag16 88.69(16) . . ? S28 Ag19 Ag16 153.97(14) 4_546 . ? S17 Ag19 Ag16 92.47(15) . . ? S19 Ag19 Ag16 57.86(15) . . ? Ag24 Ag19 Ag16 59.00(5) . . ? Hg1 Ag19 Ag16 97.30(5) . . ? Ag34 Ag20 S18 93.17(11) . 2_556 ? Ag34 Ag20 S18 93.17(11) . . ? S18 Ag20 S18 173.7(2) 2_556 . ? Ag34 Ag20 Ag15 88.68(4) . 2_556 ? S18 Ag20 Ag15 62.97(16) 2_556 2_556 ? S18 Ag20 Ag15 117.20(16) . 2_556 ? Ag34 Ag20 Ag15 88.68(4) . . ? S18 Ag20 Ag15 117.20(16) 2_556 . ? S18 Ag20 Ag15 62.97(16) . . ? Ag15 Ag20 Ag15 177.37(9) 2_556 . ? Ag34 Ag20 Ag27 146.65(3) . 2_566 ? S18 Ag20 Ag27 55.63(11) 2_556 2_566 ? S18 Ag20 Ag27 118.17(13) . 2_566 ? Ag15 Ag20 Ag27 86.73(5) 2_556 2_566 ? Ag15 Ag20 Ag27 95.47(5) . 2_566 ? Ag34 Ag20 Ag27 146.65(3) . 1_565 ? S18 Ag20 Ag27 118.17(13) 2_556 1_565 ? S18 Ag20 Ag27 55.63(11) . 1_565 ? Ag15 Ag20 Ag27 95.47(5) 2_556 1_565 ? Ag15 Ag20 Ag27 86.73(5) . 1_565 ? Ag27 Ag20 Ag27 66.69(6) 2_566 1_565 ? S13 Ag21 S26 98.67(17) . . ? S13 Ag21 S29 102.9(2) . 2_556 ? S26 Ag21 S29 100.67(18) . 2_556 ? S13 Ag21 S20 150.79(19) . . ? S26 Ag21 S20 99.92(14) . . ? S29 Ag21 S20 95.5(2) 2_556 . ? S13 Ag21 Ag26 94.23(16) . . ? S26 Ag21 Ag26 97.13(14) . . ? S29 Ag21 Ag26 152.97(12) 2_556 . ? S20 Ag21 Ag26 61.26(16) . . ? S13 Ag21 Hg1 160.51(14) . . ? S26 Ag21 Hg1 68.60(13) . . ? S29 Ag21 Hg1 66.75(12) 2_556 . ? S20 Ag21 Hg1 48.68(13) . . ? Ag26 Ag21 Hg1 101.79(6) . . ? S13 Ag21 Ag13 91.04(12) . . ? S26 Ag21 Ag13 160.69(12) . . ? S29 Ag21 Ag13 93.28(11) 2_556 . ? S20 Ag21 Ag13 65.21(10) . . ? Ag26 Ag21 Ag13 65.36(5) . . ? Hg1 Ag21 Ag13 105.63(6) . . ? S26 Ag22 S27 168.9(2) . . ? S26 Ag22 Ag29 77.82(13) . . ? S27 Ag22 Ag29 95.27(13) . . ? S26 Ag22 Ag31 109.70(16) . . ? S27 Ag22 Ag31 63.69(14) . . ? Ag29 Ag22 Ag31 107.31(7) . . ? S26 Ag22 S19 94.8(2) . . ? S27 Ag22 S19 95.5(2) . . ? Ag29 Ag22 S19 105.38(12) . . ? Ag31 Ag22 S19 142.43(13) . . ? S26 Ag22 Hg1 69.07(14) . . ? S27 Ag22 Hg1 116.22(14) . . ? Ag29 Ag22 Hg1 65.30(4) . . ? Ag31 Ag22 Hg1 172.59(7) . . ? S19 Ag22 Hg1 44.29(11) . . ? S4 Ag23 S30 99.29(18) . . ? S4 Ag23 S31 153.16(19) . . ? S30 Ag23 S31 99.72(16) . . ? S4 Ag23 S25 103.46(18) . 2_556 ? S30 Ag23 S25 99.49(19) . 2_556 ? S31 Ag23 S25 91.9(2) . 2_556 ? S4 Ag23 Ag18 95.16(15) . . ? S30 Ag23 Ag18 99.24(15) . . ? S31 Ag23 Ag18 63.15(16) . . ? S25 Ag23 Ag18 150.96(11) 2_556 . ? S4 Ag23 Ag17 95.71(11) . . ? S30 Ag23 Ag17 158.73(13) . . ? S31 Ag23 Ag17 61.52(11) . . ? S25 Ag23 Ag17 91.53(10) 2_556 . ? Ag18 Ag23 Ag17 64.28(5) . . ? S4 Ag23 Hg2 159.15(13) . . ? S30 Ag23 Hg2 63.43(14) . . ? S31 Ag23 Hg2 47.38(13) . . ? S25 Ag23 Hg2 70.28(11) 2_556 . ? Ag18 Ag23 Hg2 99.00(6) . . ? Ag17 Ag23 Hg2 104.19(6) . . ? S22 Ag24 S10 108.34(19) . . ? S22 Ag24 S27 99.46(19) . . ? S10 Ag24 S27 102.01(19) . . ? S22 Ag24 S19 94.02(17) . . ? S10 Ag24 S19 148.97(18) . . ? S27 Ag24 S19 94.98(19) . . ? S22 Ag24 Ag19 149.33(13) . . ? S10 Ag24 Ag19 95.51(12) . . ? S27 Ag24 Ag19 93.95(11) . . ? S19 Ag24 Ag19 57.20(11) . . ? S22 Ag24 Ag16 94.56(15) . . ? S10 Ag24 Ag16 96.87(15) . . ? S27 Ag24 Ag16 151.50(12) . . ? S19 Ag24 Ag16 59.19(15) . . ? Ag19 Ag24 Ag16 62.90(5) . . ? S16 Ag25 S30 162.8(2) . . ? S16 Ag25 S18 102.5(2) . . ? S30 Ag25 S18 89.7(2) . . ? S16 Ag25 S20 89.77(16) . 1_565 ? S30 Ag25 S20 98.31(17) . 1_565 ? S18 Ag25 S20 107.0(2) . 1_565 ? S16 Ag25 Ag31 62.02(16) . 4_556 ? S30 Ag25 Ag31 112.77(16) . 4_556 ? S18 Ag25 Ag31 147.52(13) . 4_556 ? S20 Ag25 Ag31 48.86(13) 1_565 4_556 ? S16 Ag25 Ag29 90.61(14) . 4_556 ? S30 Ag25 Ag29 74.06(14) . 4_556 ? S18 Ag25 Ag29 107.14(11) . 4_556 ? S20 Ag25 Ag29 144.90(17) 1_565 4_556 ? Ag31 Ag25 Ag29 101.65(6) 4_556 4_556 ? S16 Ag25 Hg2 116.13(15) . . ? S30 Ag25 Hg2 63.82(14) . . ? S18 Ag25 Hg2 47.53(11) . . ? S20 Ag25 Hg2 145.24(12) 1_565 . ? Ag31 Ag25 Hg2 163.90(7) 4_556 . ? Ag29 Ag25 Hg2 62.28(4) 4_556 . ? S16 Ag25 Ag27 100.74(16) . 1_565 ? S30 Ag25 Ag27 96.23(15) . 1_565 ? S18 Ag25 Ag27 53.61(10) . 1_565 ? S20 Ag25 Ag27 53.41(15) 1_565 1_565 ? Ag31 Ag25 Ag27 99.05(5) 4_556 1_565 ? Ag29 Ag25 Ag27 159.23(5) 4_556 1_565 ? Hg2 Ag25 Ag27 96.99(5) . 1_565 ? S21 Ag26 S11 107.3(2) 4_546 . ? S21 Ag26 S27 102.96(18) 4_546 4_546 ? S11 Ag26 S27 103.0(2) . 4_546 ? S21 Ag26 Ag21 95.96(14) 4_546 . ? S11 Ag26 Ag21 96.68(17) . . ? S27 Ag26 Ag21 147.03(17) 4_546 . ? S21 Ag26 S20 97.55(18) 4_546 . ? S11 Ag26 S20 146.20(19) . . ? S27 Ag26 S20 93.07(19) 4_546 . ? Ag21 Ag26 S20 57.47(11) . . ? S21 Ag26 Ag31 76.88(13) 4_546 4_546 ? S11 Ag26 Ag31 162.26(16) . 4_546 ? S27 Ag26 Ag31 59.43(14) 4_546 4_546 ? Ag21 Ag26 Ag31 100.04(7) . 4_546 ? S20 Ag26 Ag31 45.73(11) . 4_546 ? S21 Ag26 Ag13 153.87(16) 4_546 . ? S11 Ag26 Ag13 86.92(16) . . ? S27 Ag26 Ag13 94.70(14) 4_546 . ? Ag21 Ag26 Ag13 59.95(5) . . ? S20 Ag26 Ag13 61.99(11) . . ? Ag31 Ag26 Ag13 96.34(6) 4_546 . ? S17 Ag27 S23 167.2(2) . . ? S17 Ag27 S18 94.31(17) . 1_545 ? S23 Ag27 S18 91.08(16) . 1_545 ? S17 Ag27 S20 92.6(2) . . ? S23 Ag27 S20 97.3(2) . . ? S18 Ag27 S20 104.17(19) 1_545 . ? S17 Ag27 Hg1 68.85(15) . . ? S23 Ag27 Hg1 112.91(14) . . ? S18 Ag27 Hg1 141.90(12) 1_545 . ? S20 Ag27 Hg1 46.07(11) . . ? S17 Ag27 Ag32 74.16(13) . . ? S23 Ag27 Ag32 95.64(13) . . ? S18 Ag27 Ag32 150.66(16) 1_545 . ? S20 Ag27 Ag32 103.24(11) . . ? Hg1 Ag27 Ag32 59.32(3) . . ? S17 Ag27 Ag20 109.30(16) . 1_545 ? S23 Ag27 Ag20 67.14(14) . 1_545 ? S18 Ag27 Ag20 44.73(12) 1_545 1_545 ? S20 Ag27 Ag20 141.42(12) . 1_545 ? Hg1 Ag27 Ag20 172.25(6) . 1_545 ? Ag32 Ag27 Ag20 112.97(5) . 1_545 ? S17 Ag27 Ag25 96.09(14) . 1_545 ? S23 Ag27 Ag25 96.30(15) . 1_545 ? S18 Ag27 Ag25 51.13(14) 1_545 1_545 ? S20 Ag27 Ag25 53.04(10) . 1_545 ? Hg1 Ag27 Ag25 95.40(5) . 1_545 ? Ag32 Ag27 Ag25 154.66(5) . 1_545 ? Ag20 Ag27 Ag25 92.27(4) 1_545 1_545 ? S8 Ag28 S17 110.80(19) . 1_565 ? S8 Ag28 S16 107.78(19) . . ? S17 Ag28 S16 100.0(2) 1_565 . ? S8 Ag28 S18 151.09(17) . . ? S17 Ag28 S18 88.23(16) 1_565 . ? S16 Ag28 S18 89.17(18) . . ? S8 Ag28 Ag15 99.10(15) . . ? S17 Ag28 Ag15 92.89(15) 1_565 . ? S16 Ag28 Ag15 143.47(12) . . ? S18 Ag28 Ag15 56.99(14) . . ? S8 Ag28 Ag14 95.08(12) . . ? S17 Ag28 Ag14 144.73(13) 1_565 . ? S16 Ag28 Ag14 94.12(12) . . ? S18 Ag28 Ag14 59.64(9) . . ? Ag15 Ag28 Ag14 58.59(5) . . ? S28 Ag29 S21 162.91(18) 4_546 4_546 ? S28 Ag29 Ag22 84.81(14) 4_546 . ? S21 Ag29 Ag22 110.90(13) 4_546 . ? S28 Ag29 Ag31 81.69(13) 4_546 4_546 ? S21 Ag29 Ag31 81.46(12) 4_546 4_546 ? Ag22 Ag29 Ag31 145.15(7) . 4_546 ? S28 Ag29 Ag25 109.27(14) 4_546 4_546 ? S21 Ag29 Ag25 82.33(13) 4_546 4_546 ? Ag22 Ag29 Ag25 74.50(5) . 4_546 ? Ag31 Ag29 Ag25 140.34(7) 4_546 4_546 ? S28 Ag29 Hg2 108.51(14) 4_546 4_546 ? S21 Ag29 Hg2 66.03(13) 4_546 4_546 ? Ag22 Ag29 Hg2 133.38(6) . 4_546 ? Ag31 Ag29 Hg2 81.45(5) 4_546 4_546 ? Ag25 Ag29 Hg2 58.89(4) 4_546 4_546 ? S28 Ag29 Cu2 108.51(14) 4_546 4_546 ? S21 Ag29 Cu2 66.03(13) 4_546 4_546 ? Ag22 Ag29 Cu2 133.38(6) . 4_546 ? Ag31 Ag29 Cu2 81.45(5) 4_546 4_546 ? Ag25 Ag29 Cu2 58.89(4) 4_546 4_546 ? Hg2 Ag29 Cu2 0.00(5) 4_546 4_546 ? S28 Ag29 Hg1 69.05(14) 4_546 . ? S21 Ag29 Hg1 111.49(13) 4_546 . ? Ag22 Ag29 Hg1 62.31(5) . . ? Ag31 Ag29 Hg1 82.85(5) 4_546 . ? Ag25 Ag29 Hg1 136.81(5) 4_546 . ? Hg2 Ag29 Hg1 164.30(5) 4_546 . ? Cu2 Ag29 Hg1 164.30(5) 4_546 . ? S19 Ag30 S19 139.9(3) 2_556 . ? S19 Ag30 Ag33 69.60(13) 2_556 2_556 ? S19 Ag30 Ag33 147.50(14) . 2_556 ? S19 Ag30 Ag33 147.50(14) 2_556 . ? S19 Ag30 Ag33 69.60(13) . . ? Ag33 Ag30 Ag33 87.50(8) 2_556 . ? S19 Ag30 S24 97.70(19) 2_556 2_556 ? S19 Ag30 S24 98.2(2) . 2_556 ? Ag33 Ag30 S24 87.49(14) 2_556 2_556 ? Ag33 Ag30 S24 57.25(11) . 2_556 ? S19 Ag30 S24 98.2(2) 2_556 . ? S19 Ag30 S24 97.70(19) . . ? Ag33 Ag30 S24 57.25(11) 2_556 . ? Ag33 Ag30 S24 87.49(14) . . ? S24 Ag30 S24 132.2(2) 2_556 . ? S19 Ag30 Ag32 69.97(13) 2_556 . ? S19 Ag30 Ag32 69.97(13) . . ? Ag33 Ag30 Ag32 136.25(4) 2_556 . ? Ag33 Ag30 Ag32 136.25(4) . . ? S24 Ag30 Ag32 113.88(12) 2_556 . ? S24 Ag30 Ag32 113.88(12) . . ? S19 Ag30 Ag16 56.68(15) 2_556 2_556 ? S19 Ag30 Ag16 111.08(15) . 2_556 ? Ag33 Ag30 Ag16 96.99(4) 2_556 2_556 ? Ag33 Ag30 Ag16 106.15(5) . 2_556 ? S24 Ag30 Ag16 49.49(11) 2_556 2_556 ? S24 Ag30 Ag16 150.89(12) . 2_556 ? Ag32 Ag30 Ag16 73.93(4) . 2_556 ? S19 Ag30 Ag16 111.08(15) 2_556 . ? S19 Ag30 Ag16 56.68(15) . . ? Ag33 Ag30 Ag16 106.15(5) 2_556 . ? Ag33 Ag30 Ag16 96.99(4) . . ? S24 Ag30 Ag16 150.89(12) 2_556 . ? S24 Ag30 Ag16 49.49(11) . . ? Ag32 Ag30 Ag16 73.93(4) . . ? Ag16 Ag30 Ag16 147.86(8) 2_556 . ? S20 Ag31 S31 158.47(16) 4_556 . ? S20 Ag31 S16 91.0(2) 4_556 4_546 ? S31 Ag31 S16 98.49(19) . 4_546 ? S20 Ag31 S27 98.92(19) 4_556 . ? S31 Ag31 S27 94.15(19) . . ? S16 Ag31 S27 116.20(16) 4_546 . ? S20 Ag31 Ag29 78.39(12) 4_556 4_556 ? S31 Ag31 Ag29 80.22(11) . 4_556 ? S16 Ag31 Ag29 122.50(13) 4_546 4_556 ? S27 Ag31 Ag29 121.24(12) . 4_556 ? S20 Ag31 Ag22 133.77(12) 4_556 . ? S31 Ag31 Ag22 67.52(11) . . ? S16 Ag31 Ag22 77.14(14) 4_546 . ? S27 Ag31 Ag22 51.44(11) . . ? Ag29 Ag31 Ag22 144.97(8) 4_556 . ? S20 Ag31 Ag25 62.22(13) 4_556 4_546 ? S31 Ag31 Ag25 137.61(12) . 4_546 ? S16 Ag31 Ag25 50.63(11) 4_546 4_546 ? S27 Ag31 Ag25 79.71(13) . 4_546 ? Ag29 Ag31 Ag25 138.47(8) 4_556 4_546 ? Ag22 Ag31 Ag25 76.54(6) . 4_546 ? S20 Ag31 Ag18 113.27(18) 4_556 . ? S31 Ag31 Ag18 60.80(16) . . ? S16 Ag31 Ag18 51.13(11) 4_546 . ? S27 Ag31 Ag18 144.31(12) . . ? Ag29 Ag31 Ag18 81.63(5) 4_556 . ? Ag22 Ag31 Ag18 93.67(5) . . ? Ag25 Ag31 Ag18 101.37(7) 4_546 . ? S20 Ag31 Ag26 61.86(18) 4_556 4_556 ? S31 Ag31 Ag26 116.29(17) . 4_556 ? S16 Ag31 Ag26 142.36(12) 4_546 4_556 ? S27 Ag31 Ag26 50.81(10) . 4_556 ? Ag29 Ag31 Ag26 79.57(5) 4_556 4_556 ? Ag22 Ag31 Ag26 102.22(7) . 4_556 ? Ag25 Ag31 Ag26 92.17(5) 4_546 4_556 ? Ag18 Ag31 Ag26 161.18(6) . 4_556 ? S29 Ag32 S29 176.2(2) 2_556 . ? S29 Ag32 Ag30 91.92(12) 2_556 . ? S29 Ag32 Ag30 91.92(12) . . ? S29 Ag32 Cu1 112.15(13) 2_556 2_556 ? S29 Ag32 Cu1 68.10(13) . 2_556 ? Ag30 Ag32 Cu1 86.53(4) . 2_556 ? S29 Ag32 Hg1 112.15(13) 2_556 2_556 ? S29 Ag32 Hg1 68.10(13) . 2_556 ? Ag30 Ag32 Hg1 86.53(4) . 2_556 ? Cu1 Ag32 Hg1 0.000(3) 2_556 2_556 ? S29 Ag32 Hg1 68.10(13) 2_556 . ? S29 Ag32 Hg1 112.15(13) . . ? Ag30 Ag32 Hg1 86.53(4) . . ? Cu1 Ag32 Hg1 173.07(7) 2_556 . ? Hg1 Ag32 Hg1 173.07(7) 2_556 . ? S29 Ag32 Ag27 100.80(13) 2_556 2_556 ? S29 Ag32 Ag27 75.93(13) . 2_556 ? Ag30 Ag32 Ag27 146.32(3) . 2_556 ? Cu1 Ag32 Ag27 59.79(4) 2_556 2_556 ? Hg1 Ag32 Ag27 59.79(4) 2_556 2_556 ? Hg1 Ag32 Ag27 127.14(6) . 2_556 ? S29 Ag32 Ag27 75.93(13) 2_556 . ? S29 Ag32 Ag27 100.80(13) . . ? Ag30 Ag32 Ag27 146.32(3) . . ? Cu1 Ag32 Ag27 127.14(6) 2_556 . ? Hg1 Ag32 Ag27 127.14(6) 2_556 . ? Hg1 Ag32 Ag27 59.79(4) . . ? Ag27 Ag32 Ag27 67.36(6) 2_556 . ? S22 Ag33 S24 160.4(2) . 2_556 ? S22 Ag33 S31 100.6(2) . . ? S24 Ag33 S31 97.4(2) 2_556 . ? S22 Ag33 Ag30 104.36(17) . . ? S24 Ag33 Ag30 61.41(14) 2_556 . ? S31 Ag33 Ag30 149.71(13) . . ? S22 Ag33 Ag34 75.42(13) . . ? S24 Ag33 Ag34 92.44(13) 2_556 . ? S31 Ag33 Ag34 105.11(11) . . ? Ag30 Ag33 Ag34 97.64(6) . . ? S22 Ag33 Hg2 71.93(15) . . ? S24 Ag33 Hg2 117.45(13) 2_556 . ? S31 Ag33 Hg2 44.34(11) . . ? Ag30 Ag33 Hg2 163.32(7) . . ? Ag34 Ag33 Hg2 65.69(4) . . ? Ag20 Ag34 S25 86.17(11) . 2_556 ? Ag20 Ag34 S25 86.17(11) . . ? S25 Ag34 S25 172.3(2) 2_556 . ? Ag20 Ag34 Ag33 141.40(3) . 2_556 ? S25 Ag34 Ag33 107.05(12) 2_556 2_556 ? S25 Ag34 Ag33 79.12(12) . 2_556 ? Ag20 Ag34 Ag33 141.40(3) . . ? S25 Ag34 Ag33 79.12(12) 2_556 . ? S25 Ag34 Ag33 107.05(12) . . ? Ag33 Ag34 Ag33 77.21(7) 2_556 . ? S10 As1 S5 97.8(2) . . ? S10 As1 S2 99.2(2) . . ? S5 As1 S2 98.8(2) . . ? S8 As2 S9 103.1(2) . . ? S8 As2 S1 97.2(2) . . ? S9 As2 S1 97.7(2) . . ? S4 As3 S7 98.3(2) . . ? S4 As3 S3 99.9(2) . . ? S7 As3 S3 98.4(2) . . ? S6 As4 S11 100.8(2) . . ? S6 As4 S13 96.7(3) . . ? S11 As4 S13 100.5(2) . . ? S21 As5 S26 100.9(2) . 4_556 ? S21 As5 S16 101.63(18) . . ? S26 As5 S16 94.9(2) 4_556 . ? S22 As6 S24 101.4(3) . . ? S22 As6 S25 98.2(2) . . ? S24 As6 S25 99.98(19) . . ? S23 As7 S29 98.3(2) . 2_556 ? S23 As7 S17 102.4(2) . 2_556 ? S29 As7 S17 95.4(2) 2_556 2_556 ? S28 As8 S27 100.44(18) 4_546 . ? S28 As8 S30 98.5(2) 4_546 4_546 ? S27 As8 S30 100.7(2) . 4_546 ? As2 S1 Ag15 114.4(3) . . ? As2 S1 Ag3 102.2(2) . 2 ? Ag15 S1 Ag3 110.18(19) . 2 ? As2 S1 Ag5 103.3(2) . 1_565 ? Ag15 S1 Ag5 119.8(2) . 1_565 ? Ag3 S1 Ag5 105.2(3) 2 1_565 ? As1 S2 Ag19 117.4(2) . . ? As1 S2 Ag9 102.5(2) . . ? Ag19 S2 Ag9 109.7(3) . . ? As1 S2 Ag6 104.0(3) . . ? Ag19 S2 Ag6 120.9(2) . . ? Ag9 S2 Ag6 99.64(19) . . ? As3 S3 Ag9 103.6(2) . 4_556 ? As3 S3 Ag10 106.8(2) . . ? Ag9 S3 Ag10 112.5(3) 4_556 . ? As3 S3 Ag18 113.0(3) . . ? Ag9 S3 Ag18 104.1(2) 4_556 . ? Ag10 S3 Ag18 116.2(2) . . ? As3 S4 Ag3 104.92(19) . 1_556 ? As3 S4 Ag23 111.13(19) . . ? Ag3 S4 Ag23 111.1(3) 1_556 . ? As3 S4 Ag11 108.6(3) . . ? Ag3 S4 Ag11 102.45(17) 1_556 . ? Ag23 S4 Ag11 117.62(18) . . ? As1 S5 Ag16 114.8(3) . . ? As1 S5 Ag4 108.3(2) . . ? Ag16 S5 Ag4 114.2(2) . . ? As1 S5 Ag7 107.9(2) . 2_556 ? Ag16 S5 Ag7 103.1(2) . 2_556 ? Ag4 S5 Ag7 108.1(3) . 2_556 ? As4 S6 Ag5 115.9(2) . 2_556 ? As4 S6 Ag13 115.1(2) . . ? Ag5 S6 Ag13 105.3(2) 2_556 . ? As4 S6 Ag11 103.7(3) . 1_545 ? Ag5 S6 Ag11 117.09(18) 2_556 1_545 ? Ag13 S6 Ag11 98.82(17) . 1_545 ? As3 S7 Ag17 114.1(2) . . ? As3 S7 Ag8 101.2(3) . . ? Ag17 S7 Ag8 103.42(18) . . ? As3 S7 Ag4 109.6(2) . 2_556 ? Ag17 S7 Ag4 114.1(3) . 2_556 ? Ag8 S7 Ag4 113.69(18) . 2_556 ? As2 S8 Ag6 107.7(3) . 1_565 ? As2 S8 Ag28 108.6(2) . . ? Ag6 S8 Ag28 106.08(19) 1_565 . ? As2 S8 Ag10 107.6(2) . 4_556 ? Ag6 S8 Ag10 118.4(2) 1_565 4_556 ? Ag28 S8 Ag10 108.2(3) . 4_556 ? As2 S9 Ag12 100.17(19) . . ? As2 S9 Ag14 116.1(2) . . ? Ag12 S9 Ag14 107.4(3) . . ? As2 S9 Ag2 110.5(3) . . ? Ag12 S9 Ag2 102.29(18) . . ? Ag14 S9 Ag2 117.8(2) . . ? As1 S10 Ag2 103.5(3) . . ? As1 S10 Ag1 109.9(2) . 4_546 ? Ag2 S10 Ag1 113.3(2) . 4_546 ? As1 S10 Ag24 109.3(2) . . ? Ag2 S10 Ag24 106.18(19) . . ? Ag1 S10 Ag24 114.0(3) 4_546 . ? As4 S11 Ag1 104.4(2) . 1_545 ? As4 S11 Ag26 115.4(4) . . ? Ag1 S11 Ag26 116.4(2) 1_545 . ? As4 S11 Ag12 105.1(2) . 4_546 ? Ag1 S11 Ag12 108.9(3) 1_545 4_546 ? Ag26 S11 Ag12 106.0(2) . 4_546 ? Ag9 S12 Ag11 101.9(2) 4 1_554 ? Ag9 S12 Ag12 105.1(2) 4 . ? Ag11 S12 Ag12 91.13(19) 1_554 . ? Ag9 S12 Ag1 96.00(17) 4 1_554 ? Ag11 S12 Ag1 73.75(16) 1_554 1_554 ? Ag12 S12 Ag1 156.3(2) . 1_554 ? Ag9 S12 Ag10 173.4(2) 4 4_556 ? Ag11 S12 Ag10 78.72(16) 1_554 4_556 ? Ag12 S12 Ag10 81.38(15) . 4_556 ? Ag1 S12 Ag10 77.85(15) 1_554 4_556 ? Ag9 S12 Ag8 98.9(2) 4 4_556 ? Ag11 S12 Ag8 149.6(2) 1_554 4_556 ? Ag12 S12 Ag8 104.5(2) . 4_556 ? Ag1 S12 Ag8 82.35(17) 1_554 4_556 ? Ag10 S12 Ag8 78.15(16) 4_556 4_556 ? As4 S13 Ag7 108.3(2) . . ? As4 S13 Ag21 114.1(2) . . ? Ag7 S13 Ag21 114.0(3) . . ? As4 S13 Ag8 107.4(3) . . ? Ag7 S13 Ag8 94.30(18) . . ? Ag21 S13 Ag8 116.79(19) . . ? Ag3 S14 Ag3 101.8(3) 2 . ? Ag3 S14 Ag2 95.62(8) 2 2 ? Ag3 S14 Ag2 105.58(9) . 2 ? Ag3 S14 Ag2 105.58(9) 2 . ? Ag3 S14 Ag2 95.62(8) . . ? Ag2 S14 Ag2 146.2(3) 2 . ? Ag3 S14 Ag4 90.87(5) 2 . ? Ag3 S14 Ag4 165.4(2) . . ? Ag2 S14 Ag4 79.94(16) 2 . ? Ag2 S14 Ag4 73.82(14) . . ? Ag3 S14 Ag4 165.4(2) 2 2 ? Ag3 S14 Ag4 90.87(5) . 2 ? Ag2 S14 Ag4 73.82(14) 2 2 ? Ag2 S14 Ag4 79.94(16) . 2 ? Ag4 S14 Ag4 77.5(2) . 2 ? Ag7 S15 Ag7 101.9(3) 2_556 1_554 ? Ag7 S15 Ag6 94.02(9) 2_556 2 ? Ag7 S15 Ag6 103.30(9) 1_554 2 ? Ag7 S15 Ag6 103.30(9) 2_556 . ? Ag7 S15 Ag6 94.02(9) 1_554 . ? Ag6 S15 Ag6 152.4(3) 2 . ? Ag7 S15 Ag5 89.89(5) 2_556 . ? Ag7 S15 Ag5 167.1(2) 1_554 . ? Ag6 S15 Ag5 80.76(14) 2 . ? Ag6 S15 Ag5 78.04(14) . . ? Ag7 S15 Ag5 167.1(2) 2_556 2 ? Ag7 S15 Ag5 89.89(5) 1_554 2 ? Ag6 S15 Ag5 78.04(14) 2 2 ? Ag6 S15 Ag5 80.76(14) . 2 ? Ag5 S15 Ag5 78.9(2) . 2 ? As5 S16 Ag25 111.3(2) . . ? As5 S16 Ag18 102.0(2) . 4_556 ? Ag25 S16 Ag18 137.4(3) . 4_556 ? As5 S16 Ag28 96.5(2) . . ? Ag25 S16 Ag28 87.4(2) . . ? Ag18 S16 Ag28 114.9(2) 4_556 . ? As5 S16 Ag31 131.1(3) . 4_556 ? Ag25 S16 Ag31 67.35(16) . 4_556 ? Ag18 S16 Ag31 70.93(16) 4_556 4_556 ? Ag28 S16 Ag31 131.1(2) . 4_556 ? As7 S17 Ag27 112.4(2) 2_556 . ? As7 S17 Ag28 102.0(2) 2_556 1_545 ? Ag27 S17 Ag28 93.80(19) . 1_545 ? As7 S17 Ag19 104.3(2) 2_556 . ? Ag27 S17 Ag19 125.8(3) . . ? Ag28 S17 Ag19 116.3(2) 1_545 . ? Hg2 S18 Ag20 109.11(19) . . ? Hg2 S18 Ag25 75.4(2) . . ? Ag20 S18 Ag25 142.9(2) . . ? Hg2 S18 Ag27 139.4(3) . 1_565 ? Ag20 S18 Ag27 79.65(15) . 1_565 ? Ag25 S18 Ag27 75.26(14) . 1_565 ? Hg2 S18 Ag15 119.48(19) . . ? Ag20 S18 Ag15 69.90(18) . . ? Ag25 S18 Ag15 141.46(19) . . ? Ag27 S18 Ag15 100.90(19) 1_565 . ? Hg2 S18 Ag28 120.34(19) . . ? Ag20 S18 Ag28 123.4(3) . . ? Ag25 S18 Ag28 78.72(14) . . ? Ag27 S18 Ag28 80.16(13) 1_565 . ? Ag15 S18 Ag28 62.99(13) . . ? Hg1 S19 Ag30 121.1(2) . . ? Hg1 S19 Ag19 72.40(15) . . ? Ag30 S19 Ag19 140.7(3) . . ? Hg1 S19 Ag24 126.7(2) . . ? Ag30 S19 Ag24 112.2(2) . . ? Ag19 S19 Ag24 65.05(12) . . ? Hg1 S19 Ag16 125.1(2) . . ? Ag30 S19 Ag16 76.29(19) . . ? Ag19 S19 Ag16 67.41(14) . . ? Ag24 S19 Ag16 64.39(14) . . ? Hg1 S19 Ag22 74.5(2) . . ? Ag30 S19 Ag22 123.1(2) . . ? Ag19 S19 Ag22 95.63(19) . . ? Ag24 S19 Ag22 79.21(15) . . ? Ag16 S19 Ag22 143.49(19) . . ? Ag31 S20 Hg1 119.5(2) 4_546 . ? Ag31 S20 Ag25 68.92(13) 4_546 1_545 ? Hg1 S20 Ag25 140.0(3) . 1_545 ? Ag31 S20 Ag27 135.3(2) 4_546 . ? Hg1 S20 Ag27 77.0(2) . . ? Ag25 S20 Ag27 73.55(15) 1_545 . ? Ag31 S20 Ag21 128.0(3) 4_546 . ? Hg1 S20 Ag21 70.03(13) . . ? Ag25 S20 Ag21 139.14(19) 1_545 . ? Ag27 S20 Ag21 96.28(18) . . ? Ag31 S20 Ag26 72.4(2) 4_546 . ? Hg1 S20 Ag26 119.3(2) . . ? Ag25 S20 Ag26 100.7(2) 1_545 . ? Ag27 S20 Ag26 139.21(19) . . ? Ag21 S20 Ag26 61.27(15) . . ? As5 S21 Ag26 105.0(2) . 4_556 ? As5 S21 Ag29 97.2(2) . 4_556 ? Ag26 S21 Ag29 99.2(2) 4_556 4_556 ? As5 S21 Ag14 102.7(2) . . ? Ag26 S21 Ag14 119.5(2) 4_556 . ? Ag29 S21 Ag14 129.1(2) 4_556 . ? As6 S22 Ag33 114.7(2) . . ? As6 S22 Ag24 101.7(3) . . ? Ag33 S22 Ag24 91.14(18) . . ? As6 S22 Ag14 104.5(2) . . ? Ag33 S22 Ag14 124.2(3) . . ? Ag24 S22 Ag14 118.6(2) . . ? As7 S23 Ag13 104.7(2) . . ? As7 S23 Ag27 109.4(2) . . ? Ag13 S23 Ag27 95.0(2) . . ? As7 S23 Ag15 100.3(2) . 2_546 ? Ag13 S23 Ag15 118.3(2) . 2_546 ? Ag27 S23 Ag15 127.5(2) . 2_546 ? As6 S24 Ag16 101.7(2) . . ? As6 S24 Ag17 102.4(2) . 2_556 ? Ag16 S24 Ag17 116.0(2) . 2_556 ? As6 S24 Ag33 108.3(2) . 2_556 ? Ag16 S24 Ag33 137.1(2) . 2_556 ? Ag17 S24 Ag33 86.83(18) 2_556 2_556 ? As6 S24 Ag30 122.5(3) . . ? Ag16 S24 Ag30 76.90(17) . . ? Ag17 S24 Ag30 130.4(2) 2_556 . ? Ag33 S24 Ag30 61.34(13) 2_556 . ? As6 S25 Ag34 103.2(2) . . ? As6 S25 Ag15 105.15(19) . . ? Ag34 S25 Ag15 96.3(2) . . ? As6 S25 Ag23 103.0(2) . 2_556 ? Ag34 S25 Ag23 127.85(19) . 2_556 ? Ag15 S25 Ag23 118.7(2) . 2_556 ? As5 S26 Ag22 111.1(2) 4_546 . ? As5 S26 Ag17 103.8(2) 4_546 . ? Ag22 S26 Ag17 97.60(19) . . ? As5 S26 Ag21 98.5(2) 4_546 . ? Ag22 S26 Ag21 125.8(2) . . ? Ag17 S26 Ag21 118.61(19) . . ? As8 S27 Ag22 108.1(2) . . ? As8 S27 Ag26 101.26(19) . 4_556 ? Ag22 S27 Ag26 134.6(3) . 4_556 ? As8 S27 Ag24 99.2(2) . . ? Ag22 S27 Ag24 88.31(18) . . ? Ag26 S27 Ag24 120.6(2) 4_556 . ? As8 S27 Ag31 128.3(3) . . ? Ag22 S27 Ag31 64.87(14) . . ? Ag26 S27 Ag31 69.77(15) 4_556 . ? Ag24 S27 Ag31 130.0(2) . . ? As8 S28 Ag29 99.6(2) 4_556 4_556 ? As8 S28 Ag18 105.6(2) 4_556 . ? Ag29 S28 Ag18 102.3(2) 4_556 . ? As8 S28 Ag19 103.6(2) 4_556 4_556 ? Ag29 S28 Ag19 124.0(2) 4_556 4_556 ? Ag18 S28 Ag19 118.7(2) . 4_556 ? As7 S29 Ag32 111.9(2) 2_556 . ? As7 S29 Ag16 102.41(19) 2_556 . ? Ag32 S29 Ag16 98.7(2) . . ? As7 S29 Ag21 98.6(2) 2_556 2_556 ? Ag32 S29 Ag21 128.2(2) . 2_556 ? Ag16 S29 Ag21 114.9(2) . 2_556 ? As8 S30 Ag25 108.7(2) 4_556 . ? As8 S30 Ag23 99.1(2) 4_556 . ? Ag25 S30 Ag23 133.3(3) . . ? As8 S30 Ag13 98.7(2) 4_556 1_565 ? Ag25 S30 Ag13 93.25(18) . 1_565 ? Ag23 S30 Ag13 119.2(2) . 1_565 ? As8 S30 Hg2 130.7(2) 4_556 . ? Ag25 S30 Hg2 67.09(15) . . ? Ag23 S30 Hg2 66.28(14) . . ? Ag13 S30 Hg2 130.0(3) 1_565 . ? Hg2 S31 Ag31 109.57(18) . . ? Hg2 S31 Ag23 77.05(13) . . ? Ag31 S31 Ag23 127.3(3) . . ? Hg2 S31 Ag33 83.4(2) . . ? Ag31 S31 Ag33 126.9(2) . . ? Ag23 S31 Ag33 105.7(2) . . ? Hg2 S31 Ag18 121.0(2) . . ? Ag31 S31 Ag18 69.53(18) . . ? Ag23 S31 Ag18 63.67(15) . . ? Ag33 S31 Ag18 146.68(19) . . ? Hg2 S31 Ag17 134.4(2) . . ? Ag31 S31 Ag17 114.2(2) . . ? Ag23 S31 Ag17 66.92(12) . . ? Ag33 S31 Ag17 80.53(14) . . ? Ag18 S31 Ag17 66.19(15) . . ? _diffrn_measured_fraction_theta_max 0.652 _diffrn_reflns_theta_full 34.79 _diffrn_measured_fraction_theta_full 0.652 _refine_diff_density_max 3.958 _refine_diff_density_min -1.227 _refine_diff_density_rms 0.341