data_shelxl _audit_creation_method SHELXL-2012 _chemical_name_systematic ; ? ; _chemical_name_mineral chabazite _chemical_compound_source 'Monte Somma, Vesuvius, Italy' _chemical_formula_sum 'Al0 K3 O24 Si12' _chemical_formula_weight 838.38 _publ_section_title 'Structural intergrowth of merlinoite/phillipsite and its temperature dehydration behavior' loop_ _publ_author_name 'Danisi, R.M.' 'Armbruster, T.' 'Nagashima, M.' _publ_contact_author_name 'Danisi, R.M.' _publ_contact_author_address 'University of Bern, Freiestr. 3, CH-3012 Bern' _publ_contact_author_email 'rosa.danisi@krist.unibe.ch' _publ_requested_journal 'Mineralogical Magazine' loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Al' 'Al' 0.0645 0.0514 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K' 'K' 0.2009 0.2494 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system trigonal _space_group_IT_number 166 _space_group_name_H-M_alt 'R -3 m :H' _space_group_name_Hall '-R 3 2"' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-y, x-y, z' '-x+y, -x, z' 'y, x, -z' 'x-y, -y, -z' '-x, -x+y, -z' 'x+2/3, y+1/3, z+1/3' '-y+2/3, x-y+1/3, z+1/3' '-x+y+2/3, -x+1/3, z+1/3' 'y+2/3, x+1/3, -z+1/3' 'x-y+2/3, -y+1/3, -z+1/3' '-x+2/3, -x+y+1/3, -z+1/3' 'x+1/3, y+2/3, z+2/3' '-y+1/3, x-y+2/3, z+2/3' '-x+y+1/3, -x+2/3, z+2/3' 'y+1/3, x+2/3, -z+2/3' 'x-y+1/3, -y+2/3, -z+2/3' '-x+1/3, -x+y+2/3, -z+2/3' '-x, -y, -z' 'y, -x+y, -z' 'x-y, x, -z' '-y, -x, z' '-x+y, y, z' 'x, x-y, z' '-x+2/3, -y+1/3, -z+1/3' 'y+2/3, -x+y+1/3, -z+1/3' 'x-y+2/3, x+1/3, -z+1/3' '-y+2/3, -x+1/3, z+1/3' '-x+y+2/3, y+1/3, z+1/3' 'x+2/3, x-y+1/3, z+1/3' '-x+1/3, -y+2/3, -z+2/3' 'y+1/3, -x+y+2/3, -z+2/3' 'x-y+1/3, x+2/3, -z+2/3' '-y+1/3, -x+2/3, z+2/3' '-x+y+1/3, y+2/3, z+2/3' 'x+1/3, x-y+2/3, z+2/3' _cell_length_a 13.6950(19) _cell_length_b 13.6950(19) _cell_length_c 14.993(3) _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 120 _cell_volume 2435.3(8) _cell_formula_units_Z 2 _cell_measurement_temperature 398(2) _exptl_crystal_density_method 'not measured' _exptl_crystal_density_diffrn 1.715 _exptl_crystal_F_000 1251 _exptl_absorpt_coefficient_mu 0.942 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details sadabs _exptl_special_details ; ? ; _diffrn_ambient_temperature 398(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device 'two circle diffractometer' _diffrn_measurement_device_type 'Apex II SMART' _diffrn_reflns_number 34669 _diffrn_reflns_av_unetI/netI 0.0779 _diffrn_reflns_av_R_equivalents 0.3655 _diffrn_reflns_limit_h_min -19 _diffrn_reflns_limit_h_max 19 _diffrn_reflns_limit_k_min -19 _diffrn_reflns_limit_k_max 19 _diffrn_reflns_limit_l_min -20 _diffrn_reflns_limit_l_max 20 _diffrn_reflns_theta_min 2.189 _diffrn_reflns_theta_max 29.708 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.999 _diffrn_measured_fraction_theta_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.999 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.999 _diffrn_reflns_point_group_measured_fraction_full 0.998 _reflns_number_total 861 _reflns_number_gt 486 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. Chabazite represents a very minor inclusion within a merlinoite-phillipsite intergrowth. The chemical composition of this chabazite is unknown. Some of the chabazite reflections were overlapping with those of merlinoite/phillipsite explaining the very poor internal R values. The poor data only allowed to resolve the framework sites and major channel occupants. ; _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-2012 (Sheldrick, 2012)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details ; w=1/[\s^2^(Fo^2^)+(0.1000P)^2^] where P=(Fo^2^+2Fc^2^)/3 ; _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 861 _refine_ls_number_parameters 36 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.2453 _refine_ls_R_factor_gt 0.1716 _refine_ls_wR_factor_ref 0.3931 _refine_ls_wR_factor_gt 0.3646 _refine_ls_goodness_of_fit_ref 2.240 _refine_ls_restrained_S_all 2.240 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group K1 K 0.6667 0.3333 1.0220(16) 0.124(8) Uiso 0.55(2) 6 d S U . . . K3 K 0.6667 -0.1667 0.8333 0.124(8) Uiso 0.38(2) 4 d S U . . . Si1 Si 0.6666(2) 0.1050(2) 0.93725(17) 0.0246(8) Uani 1 1 d . . . . . O1 O 0.6493(9) 0.0000 1.0000 0.047(3) Uani 1 2 d S T P . . O2 O 0.5685(6) 0.1370(13) 0.9581(8) 0.062(4) Uani 1 2 d S T P . . O3 O 0.7851(6) 0.2149(6) 0.9643(8) 0.056(3) Uani 1 2 d S T P . . O4 O 0.6667 0.0645(9) 0.8333 0.053(3) Uani 1 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0200(13) 0.0222(15) 0.0281(13) 0.0051(11) -0.0005(10) 0.0079(12) O1 0.058(6) 0.027(6) 0.045(6) 0.021(5) 0.010(2) 0.014(3) O2 0.045(5) 0.092(11) 0.064(8) -0.004(8) -0.002(4) 0.046(6) O3 0.038(4) 0.038(4) 0.063(8) 0.002(4) -0.002(4) -0.001(6) O4 0.075(9) 0.057(5) 0.033(6) 0.000(3) 0.000(6) 0.037(5) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag K1 O2 2.518(17) . ? K1 O2 2.518(17) 2_655 ? K1 O2 2.518(17) 3_665 ? K1 O3 2.940(16) . ? K1 O3 2.940(16) 3_665 ? K1 O3 2.940(16) 2_655 ? K1 Si1 3.375(9) . ? K1 Si1 3.375(9) 22_665 ? K1 Si1 3.375(9) 23_655 ? K1 Si1 3.375(9) 2_655 ? K1 Si1 3.375(9) 3_665 ? K1 Si1 3.375(9) 24 ? K3 O4 3.166(13) . ? K3 O4 3.167(13) 31_646 ? K3 O3 3.242(12) 21_547 ? K3 O3 3.242(12) 15_654 ? K3 K1 4.509(12) 19_657 ? K3 K1 4.509(12) 13_544 ? Si1 O3 1.619(4) . ? Si1 O1 1.634(4) . ? Si1 O2 1.639(5) . ? Si1 O4 1.654(5) . ? O1 Si1 1.634(4) 5_557 ? O2 Si1 1.639(5) 23_655 ? O3 Si1 1.619(4) 22_665 ? O3 K3 3.242(12) 8_545 ? O4 Si1 1.654(5) 18_656 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O2 K1 O2 106.4(6) . 2_655 ? O2 K1 O2 106.4(6) . 3_665 ? O2 K1 O2 106.4(6) 2_655 3_665 ? O2 K1 O3 56.4(2) . . ? O2 K1 O3 56.4(2) 2_655 . ? O2 K1 O3 140.5(11) 3_665 . ? O2 K1 O3 56.4(2) . 3_665 ? O2 K1 O3 140.5(11) 2_655 3_665 ? O2 K1 O3 56.4(2) 3_665 3_665 ? O3 K1 O3 111.7(5) . 3_665 ? O2 K1 O3 140.5(11) . 2_655 ? O2 K1 O3 56.4(2) 2_655 2_655 ? O2 K1 O3 56.4(2) 3_665 2_655 ? O3 K1 O3 111.7(5) . 2_655 ? O3 K1 O3 111.7(5) 3_665 2_655 ? O2 K1 Si1 27.71(10) . . ? O2 K1 Si1 81.8(3) 2_655 . ? O2 K1 Si1 126.8(8) 3_665 . ? O3 K1 Si1 28.66(12) . . ? O3 K1 Si1 83.6(3) 3_665 . ? O3 K1 Si1 131.0(7) 2_655 . ? O2 K1 Si1 81.8(3) . 22_665 ? O2 K1 Si1 27.71(10) 2_655 22_665 ? O2 K1 Si1 126.8(8) 3_665 22_665 ? O3 K1 Si1 28.66(12) . 22_665 ? O3 K1 Si1 131.0(7) 3_665 22_665 ? O3 K1 Si1 83.6(3) 2_655 22_665 ? Si1 K1 Si1 55.20(19) . 22_665 ? O2 K1 Si1 27.71(10) . 23_655 ? O2 K1 Si1 126.8(8) 2_655 23_655 ? O2 K1 Si1 81.8(3) 3_665 23_655 ? O3 K1 Si1 83.6(3) . 23_655 ? O3 K1 Si1 28.66(12) 3_665 23_655 ? O3 K1 Si1 131.0(7) 2_655 23_655 ? Si1 K1 Si1 55.17(18) . 23_655 ? Si1 K1 Si1 106.7(4) 22_665 23_655 ? O2 K1 Si1 126.8(8) . 2_655 ? O2 K1 Si1 27.71(10) 2_655 2_655 ? O2 K1 Si1 81.8(3) 3_665 2_655 ? O3 K1 Si1 83.6(3) . 2_655 ? O3 K1 Si1 131.0(7) 3_665 2_655 ? O3 K1 Si1 28.66(12) 2_655 2_655 ? Si1 K1 Si1 106.7(4) . 2_655 ? Si1 K1 Si1 55.17(18) 22_665 2_655 ? Si1 K1 Si1 135.8(8) 23_655 2_655 ? O2 K1 Si1 81.8(3) . 3_665 ? O2 K1 Si1 126.8(8) 2_655 3_665 ? O2 K1 Si1 27.71(10) 3_665 3_665 ? O3 K1 Si1 131.0(7) . 3_665 ? O3 K1 Si1 28.66(12) 3_665 3_665 ? O3 K1 Si1 83.6(3) 2_655 3_665 ? Si1 K1 Si1 106.7(4) . 3_665 ? Si1 K1 Si1 135.8(8) 22_665 3_665 ? Si1 K1 Si1 55.20(19) 23_655 3_665 ? Si1 K1 Si1 106.7(4) 2_655 3_665 ? O2 K1 Si1 126.8(8) . 24 ? O2 K1 Si1 81.8(3) 2_655 24 ? O2 K1 Si1 27.71(10) 3_665 24 ? O3 K1 Si1 131.0(7) . 24 ? O3 K1 Si1 83.6(3) 3_665 24 ? O3 K1 Si1 28.66(12) 2_655 24 ? Si1 K1 Si1 135.8(8) . 24 ? Si1 K1 Si1 106.7(4) 22_665 24 ? Si1 K1 Si1 106.7(4) 23_655 24 ? Si1 K1 Si1 55.20(19) 2_655 24 ? Si1 K1 Si1 55.17(18) 3_665 24 ? O4 K3 O4 180.0 . 31_646 ? O4 K3 O3 90.000(1) . 21_547 ? O4 K3 O3 90.002(1) 31_646 21_547 ? O4 K3 O3 90.001(1) . 15_654 ? O4 K3 O3 90.0 31_646 15_654 ? O3 K3 O3 180.0 21_547 15_654 ? O4 K3 K1 90.001(1) . 19_657 ? O4 K3 K1 90.001(3) 31_646 19_657 ? O3 K3 K1 40.6(4) 21_547 19_657 ? O3 K3 K1 139.4(4) 15_654 19_657 ? O4 K3 K1 90.000(3) . 13_544 ? O4 K3 K1 89.998(1) 31_646 13_544 ? O3 K3 K1 139.4(4) 21_547 13_544 ? O3 K3 K1 40.6(4) 15_654 13_544 ? K1 K3 K1 180.0 19_657 13_544 ? O3 Si1 O1 108.1(5) . . ? O3 Si1 O2 106.2(7) . . ? O1 Si1 O2 110.4(7) . . ? O3 Si1 O4 112.3(5) . . ? O1 Si1 O4 105.8(5) . . ? O2 Si1 O4 114.0(5) . . ? O3 Si1 K1 60.6(5) . . ? O1 Si1 K1 122.1(4) . . ? O2 Si1 K1 45.6(5) . . ? O4 Si1 K1 131.7(6) . . ? Si1 O1 Si1 145.7(8) 5_557 . ? Si1 O2 Si1 145.0(9) . 23_655 ? Si1 O2 K1 106.7(5) . . ? Si1 O2 K1 106.7(5) 23_655 . ? Si1 O3 Si1 150.0(9) . 22_665 ? Si1 O3 K1 90.8(5) . . ? Si1 O3 K1 90.8(5) 22_665 . ? Si1 O3 K3 104.9(4) . 8_545 ? Si1 O3 K3 104.9(4) 22_665 8_545 ? K1 O3 K3 93.5(6) . 8_545 ? Si1 O4 Si1 140.8(9) . 18_656 ? Si1 O4 K3 109.6(4) . . ? Si1 O4 K3 109.6(4) 18_656 . ? _refine_diff_density_max 3.358 _refine_diff_density_min -1.330 _refine_diff_density_rms 0.320 _shelxl_version_number 2012-9 _shelx_res_file ; TITL Chaba125 in R-3m CELL 0.71073 13.6950 13.6950 14.9934 90.000 90.000 120.000 ZERR 3.00 0.0019 0.0019 0.0030 0.000 0.000 0.000 LATT 3 SYMM -Y, X-Y, Z SYMM -X+Y, -X, Z SYMM Y, X, -Z SYMM X-Y, -Y, -Z SYMM -X, -X+Y, -Z SFAC O AL SI K UNIT 72 0 36 9 TEMP 23.000 L.S. 10 BOND FMAP 2 ACTA PLAN 20 WGHT 0.100000 FVAR 0.16409 0.12416 K1 4 0.666667 0.333333 1.022023 0.09202 21.00000 K3 4 0.666667 -0.166667 0.833333 0.09399 21.00000 SI1 3 0.666626 0.105013 0.937253 11.00000 0.02000 0.02221 = 0.02813 0.00514 -0.00050 0.00786 O1 1 0.649310 0.000000 1.000000 10.50000 0.05756 0.02744 = 0.04455 0.02059 0.01029 0.01372 O2 1 0.568521 0.137041 0.958118 10.50000 0.04549 0.09194 = 0.06361 -0.00441 -0.00221 0.04597 O3 1 0.785134 0.214866 0.964319 10.50000 0.03833 0.03833 = 0.06342 0.00159 -0.00159 -0.00111 O4 1 0.666667 0.064543 0.833333 10.50000 0.07477 0.05669 = 0.03286 -0.00002 -0.00004 0.03739 HKLF 4 REM Chaba125 in R-3m REM R1 = 0.1716 for 486 Fo > 4sig(Fo) and 0.2453 for all 861 data REM 36 parameters refined using 0 restraints END WGHT 0.2000 0.0000 REM Highest difference peak 3.358, deepest hole -1.330, 1-sigma level 0.320 Q1 1 0.5619 -0.1042 0.9391 11.00000 0.05 3.36 Q2 1 0.7723 -0.0018 1.0629 11.00000 0.05 2.77 Q3 1 0.6667 0.3333 0.8333 10.08333 0.05 2.14 Q4 1 0.5310 -0.2345 0.7132 10.50000 0.05 1.42 Q5 1 0.6667 0.3333 0.9807 10.16667 0.05 1.15 Q6 1 0.7188 0.4375 1.1650 10.50000 0.05 1.04 Q7 1 0.6667 0.3333 1.1437 10.16667 0.05 1.04 Q8 1 0.6038 -0.0633 0.8367 11.00000 0.05 0.93 Q9 1 0.6667 0.3333 0.8977 10.16667 0.05 0.92 Q10 1 0.6020 0.2040 1.1527 10.50000 0.05 0.92 Q11 1 0.7819 0.2181 1.0376 10.50000 0.05 0.92 Q12 1 0.6667 0.3333 1.3333 10.08333 0.05 0.91 Q13 1 0.5725 0.1450 1.0044 10.50000 0.05 0.88 Q14 1 0.7743 0.2257 0.9946 10.50000 0.05 0.87 Q15 1 0.9173 0.0827 0.8906 10.50000 0.05 0.74 Q16 1 0.8791 0.1209 0.9626 10.50000 0.05 0.73 Q17 1 0.8166 0.0000 1.0000 10.50000 0.05 0.66 Q18 1 0.7575 0.2425 0.9413 10.50000 0.05 0.63 Q19 1 0.5584 -0.2208 0.8112 10.50000 0.05 0.63 Q20 1 0.6249 -0.0034 0.9621 11.00000 0.05 0.62 ; _shelx_res_checksum 17233 _shelx_hkl_file ; 0 0 -3 3170.00 48.00 0 0 -3 2540.90 42.70 0 0 -3 2586.70 48.40 0 0 -3 2240.60 46.00 0 0 -3 2381.40 47.30 0 0 3 2757.90 46.30 0 0 3 2868.70 45.30 0 0 3 2540.00 48.60 0 0 3 2476.00 42.60 0 0 3 2319.10 47.00 0 0 3 2474.60 48.60 0 0 -6 81.40 16.65 0 0 -6 45.36 15.96 0 0 -6 14.87 14.20 0 0 -6 46.03 14.57 0 0 -6 6.74 12.42 0 0 -6 17.76 14.46 0 0 6 51.57 16.21 0 0 6 54.18 15.40 0 0 6 37.71 16.37 0 0 6 37.75 16.99 0 0 6 22.90 14.05 0 0 6 15.89 13.89 0 0 6 29.82 14.71 0 0 -9 3044.70 99.10 0 0 -9 4359.50 95.80 0 0 -9 3736.80 101.90 0 0 -9 3560.20 100.90 0 0 -9 4487.60 92.60 0 0 -9 3458.60 100.30 0 0 -9 3630.20 102.60 0 0 9 3418.00 104.60 0 0 9 4539.00 100.60 0 0 9 4015.50 86.40 0 0 9 3332.20 100.00 0 0 9 3747.90 96.00 0 0 9 3524.10 103.10 0 0 9 3856.60 108.30 0 0 -12 -0.83 30.96 0 0 -12 34.28 32.76 0 0 -12 4.33 27.20 0 0 12 36.79 40.80 0 0 12 -31.85 28.61 0 0 12 -10.27 28.28 0 0 12 14.16 27.43 0 0 12 54.86 34.04 0 0 -15 296.22 51.68 0 0 -15 321.54 52.18 0 0 -15 398.57 55.66 0 0 -15 304.74 51.75 0 0 -15 323.73 49.88 0 0 15 263.89 56.63 0 0 15 336.28 45.88 0 0 15 354.46 51.10 0 0 15 352.05 58.22 0 0 -18 140.21 48.23 0 0 -18 220.96 54.71 0 0 -18 269.11 59.32 0 0 -18 208.46 54.59 0 0 -18 259.50 52.91 0 0 18 125.92 56.19 0 0 18 305.64 60.55 0 0 18 231.87 44.56 0 0 18 190.79 47.35 -1 0 20 -29.60 51.38 -1 0 20 10.03 54.50 -1 0 20 41.06 41.66 -1 1 -20 -6.84 40.12 -1 1 -20 11.54 41.02 0 -1 -20 7.73 42.91 0 -1 -20 26.61 50.33 0 -1 -20 53.48 55.09 0 -1 -20 -23.58 51.63 0 -1 -20 57.51 42.20 0 1 20 35.44 56.75 0 1 20 79.29 53.74 0 1 20 3.95 40.44 0 1 20 25.10 42.50 1 -1 20 42.76 57.90 1 -1 20 29.11 42.02 1 0 -20 38.27 42.36 1 0 -20 -9.18 52.58 1 0 -20 -24.57 45.48 1 0 -20 -8.58 38.00 -1 0 17 -48.73 45.46 -1 0 17 1.45 46.17 -1 0 17 7.74 32.56 -1 0 17 32.70 34.68 -1 1 -17 35.44 39.32 -1 1 -17 169.79 51.42 -1 1 -17 169.67 48.05 -1 1 -17 1.79 35.48 0 -1 -17 -2.80 33.92 0 -1 -17 -2.60 37.18 0 -1 -17 -69.58 40.52 0 -1 -17 3.04 36.72 0 -1 -17 -14.59 30.27 0 1 17 22.75 44.27 0 1 17 16.26 33.33 0 1 17 5.67 34.07 1 -1 17 20.91 47.34 1 -1 17 110.23 45.52 1 -1 17 47.21 35.77 1 -1 17 5.48 34.91 1 0 -17 -8.27 33.06 1 0 -17 31.75 38.89 1 0 -17 -64.32 43.78 1 0 -17 -32.77 37.28 1 0 -17 -26.65 29.17 -1 0 14 152.95 47.25 -1 0 14 109.94 35.21 -1 0 14 107.16 33.82 -1 0 14 71.03 31.54 -1 0 14 70.81 36.74 -1 1 -14 63.00 33.40 -1 1 -14 97.31 36.93 -1 1 -14 62.70 33.27 0 -1 -14 71.29 34.53 0 -1 -14 93.75 35.05 0 -1 -14 45.20 39.52 0 -1 -14 9.02 33.51 0 -1 -14 56.50 30.23 0 1 14 107.81 41.78 0 1 14 70.11 31.82 0 1 14 51.31 29.46 0 1 14 90.84 36.27 1 -1 14 58.31 41.46 1 -1 14 64.36 28.91 1 -1 14 41.86 30.68 1 -1 14 40.78 31.13 1 -1 14 102.59 40.52 1 0 -14 114.10 38.55 1 0 -14 60.66 36.15 1 0 -14 172.51 44.97 1 0 -14 102.55 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