data_new2 _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'Cl6 Mg4 O2 Pb13' _chemical_formula_weight 3035.41 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'Cl' 'Cl' 0.1484 0.1585 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mg' 'Mg' 0.0486 0.0363 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, z' '-x, y, z' 'x, -y, z' _cell_length_a 5.8034(5) _cell_length_b 11.3574(9) _cell_length_c 12.9393(16) _cell_angle_alpha 90.00 _cell_angle_beta 90.00 _cell_angle_gamma 90.00 _cell_volume 852.85(15) _cell_formula_units_Z 4 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 5.910 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 1232 _exptl_absorpt_coefficient_mu 64.430 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 6061 _diffrn_reflns_av_R_equivalents 0.0773 _diffrn_reflns_av_sigmaI/netI 0.0614 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_k_min -14 _diffrn_reflns_limit_k_max 12 _diffrn_reflns_limit_l_min -16 _diffrn_reflns_limit_l_max 16 _diffrn_reflns_theta_min 6.91 _diffrn_reflns_theta_max 26.93 _reflns_number_total 2058 _reflns_number_gt 1318 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0488P)^2^+93.6534P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.48(6) _refine_ls_number_reflns 2058 _refine_ls_number_parameters 109 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.1034 _refine_ls_R_factor_gt 0.0627 _refine_ls_wR_factor_ref 0.1517 _refine_ls_wR_factor_gt 0.1320 _refine_ls_goodness_of_fit_ref 1.028 _refine_ls_restrained_S_all 1.028 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.5000 0.7746(2) 0.60117(18) 0.0168(5) Uani 1 2 d S . . Pb2 Pb 1.0000 0.7669(3) 0.1011(2) 0.0317(7) Uani 1 2 d S . . Pb3 Pb 1.0000 0.7762(2) 0.8001(2) 0.0246(7) Uani 1 2 d S . . Pb4 Pb 1.0000 1.0000 0.6033(3) 0.0191(8) Uani 1 4 d S . . Pb5 Pb 0.5000 1.0000 0.8000(3) 0.0175(8) Uani 1 4 d S . . Pb6 Pb 0.5000 0.7673(4) 0.2988(3) 0.0468(10) Uani 1 2 d S . . Pb7 Pb 0.5000 1.0000 0.1031(3) 0.0265(9) Uani 1 4 d S . . Pb8 Pb 1.0000 1.0000 0.2991(3) 0.0355(11) Uani 1 4 d S . . Pb9 Pb 0.5000 0.5000 1.0015(6) 0.0387(14) Uani 0.80 4 d SP . . Pb10 Pb 0.5000 0.5000 1.072(3) 0.022(6) Uiso 0.10 4 d SP . . Pb11 Pb 1.0000 0.5000 0.4064(6) 0.0288(12) Uani 0.777(7) 4 d SP . . Pb12 Pb 1.0000 0.5000 0.4913(11) 0.020 Uiso 0.223(7) 4 d SP . . Pb13 Pb 1.0000 0.5000 1.007(2) 0.020 Uiso 0.10 4 d SP . . Cl1 Cl 1.0000 0.750(2) 0.4604(15) 0.049(6) Uani 1 2 d S . . Cl2 Cl 0.5000 0.7498(14) 0.9618(12) 0.016(3) Uani 1 2 d S . . Cl3 Cl 1.0000 1.0000 0.9692(13) 0.012(4) Uani 1 4 d S . . Cl4 Cl 0.5000 1.0000 0.4624(16) 0.036(6) Uani 1 4 d S . . Mg Mg 0.752(5) 0.5000 0.700(3) 0.024(3) Uani 1 2 d S . . O1 O 0.743(7) 0.8756(14) 0.706(3) 0.018(4) Uiso 1 1 d . . . O2 O 0.754(9) 0.8687(17) 0.201(4) 0.035(5) Uiso 1 1 d . . . OH1 O 1.0000 0.371(4) 0.670(4) 0.034(5) Uiso 1 2 d S . . OH2 O 0.5000 0.387(4) 0.718(4) 0.034(5) Uiso 1 2 d S . . OH3 O 0.802(8) 0.5000 0.848(3) 0.034(5) Uiso 1 2 d S . . OH4 O 0.311(8) 0.5000 0.528(3) 0.034(5) Uiso 1 2 d S . . OH5 O 0.5000 0.626(5) 0.179(4) 0.010 Uiso 0.51(6) 2 d SP . . OH6 O 0.782(14) 0.577(6) 0.210(8) 0.010 Uiso 0.25(3) 1 d P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.0161(11) 0.0145(12) 0.0199(12) -0.0028(9) 0.000 0.000 Pb2 0.0305(14) 0.0447(17) 0.0200(13) 0.0097(13) 0.000 0.000 Pb3 0.0194(12) 0.0200(14) 0.0343(17) 0.0012(11) 0.000 0.000 Pb4 0.0232(18) 0.0189(18) 0.0150(15) 0.000 0.000 0.000 Pb5 0.0062(13) 0.0109(16) 0.035(2) 0.000 0.000 0.000 Pb6 0.0408(18) 0.059(2) 0.040(2) 0.0213(17) 0.000 0.000 Pb7 0.030(2) 0.038(2) 0.0116(15) 0.000 0.000 0.000 Pb8 0.0146(17) 0.061(3) 0.031(2) 0.000 0.000 0.000 Pb9 0.043(3) 0.018(3) 0.055(4) 0.000 0.000 0.000 Pb11 0.018(2) 0.032(3) 0.036(3) 0.000 0.000 0.000 Cl1 0.089(17) 0.043(11) 0.014(10) -0.001(7) 0.000 0.000 Cl2 0.005(5) 0.022(7) 0.021(9) 0.000(6) 0.000 0.000 Cl3 0.011(8) 0.017(8) 0.009(9) 0.000 0.000 0.000 Cl4 0.044(15) 0.055(16) 0.010(11) 0.000 0.000 0.000 Mg 0.022(6) 0.020(6) 0.031(7) 0.000 0.004(6) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 O1 2.27(4) . ? Pb1 O1 2.27(4) 3_655 ? Pb1 OH2 2.38(5) 2_665 ? Pb1 Cl4 3.127(12) . ? Pb1 Cl1 3.438(10) 1_455 ? Pb1 Cl1 3.438(10) . ? Pb1 Pb5 3.629(4) . ? Pb1 Mg 3.674(18) . ? Pb1 Mg 3.674(19) 2_665 ? Pb1 Pb4 3.8695(16) . ? Pb1 Pb4 3.8695(16) 1_455 ? Pb1 Pb3 3.8790(16) . ? Pb1 Pb3 3.8790(16) 1_455 ? Pb1 Pb6 3.914(4) . ? Pb1 Pb12 4.491(5) 1_455 ? Pb1 Pb12 4.491(5) . ? Pb2 O2 2.24(5) 3_755 ? Pb2 O2 2.24(5) . ? Pb2 OH6 2.87(8) . ? Pb2 OH6 2.87(8) 3_755 ? Pb2 Cl3 3.150(10) 1_554 ? Pb2 Pb13 3.266(11) 1_554 ? Pb2 Cl2 3.422(8) 1_554 ? Pb2 Cl2 3.422(8) 1_654 ? Pb2 Pb8 3.684(5) . ? Pb2 Pb6 3.868(2) 1_655 ? Pb2 Pb6 3.868(2) . ? Pb2 Pb3 3.896(4) 1_554 ? Pb2 Pb7 3.928(2) 1_655 ? Pb2 Pb7 3.928(2) . ? Pb2 Pb10 4.213(4) 1_554 ? Pb2 Pb10 4.213(4) 1_654 ? Pb2 Pb9 4.390(4) 1_554 ? Pb2 Pb9 4.390(4) 1_654 ? Pb3 O1 2.23(4) 3_755 ? Pb3 O1 2.23(4) . ? Pb3 OH1 2.38(5) 2_765 ? Pb3 Cl3 3.354(12) . ? Pb3 Pb4 3.598(4) . ? Pb3 Mg 3.687(19) . ? Pb3 Mg 3.687(18) 2_765 ? Pb3 Pb5 3.8575(18) 1_655 ? Pb3 Pb5 3.8575(18) . ? Pb3 Pb1 3.8790(16) 1_655 ? Pb3 Pb2 3.896(4) 1_556 ? Pb3 Pb13 4.126(19) . ? Pb4 O1 2.44(3) 2_775 ? Pb4 O1 2.44(3) 4_575 ? Pb4 O1 2.44(3) . ? Pb4 O1 2.44(3) 3_755 ? Pb4 Cl1 3.39(2) . ? Pb4 Cl1 3.39(2) 2_775 ? Pb4 Cl4 3.427(11) . ? Pb4 Cl4 3.427(11) 1_655 ? Pb4 Pb3 3.598(4) 2_775 ? Pb4 Pb5 3.860(2) 1_655 ? Pb4 Pb5 3.860(2) . ? Pb4 Pb1 3.8695(17) 2_775 ? Pb4 Pb1 3.8695(16) 1_655 ? Pb4 Pb1 3.8695(16) 2_675 ? Pb4 Pb8 3.936(5) . ? Pb5 O1 2.34(3) 4_575 ? Pb5 O1 2.34(3) 3_655 ? Pb5 O1 2.34(3) 2_675 ? Pb5 O1 2.34(3) . ? Pb5 Pb1 3.629(4) 2_675 ? Pb5 Pb3 3.8575(18) 2_775 ? Pb5 Pb3 3.8575(18) 1_455 ? Pb5 Pb3 3.8575(18) 2_675 ? Pb5 Pb4 3.860(2) 1_455 ? Pb5 Pb7 3.922(5) 1_556 ? Pb6 OH5 2.23(5) . ? Pb6 O2 2.26(5) 3_655 ? Pb6 O2 2.26(5) . ? Pb6 OH6 2.95(8) 3_655 ? Pb6 OH6 2.95(8) . ? Pb6 Cl4 3.386(14) . ? Pb6 Pb7 3.660(5) . ? Pb6 Pb2 3.868(2) 1_455 ? Pb6 Pb8 3.925(3) . ? Pb6 Pb8 3.925(3) 1_455 ? Pb6 Pb10 4.22(2) 1_554 ? Pb6 Pb11 4.424(4) 1_455 ? Pb6 Pb11 4.424(4) . ? Pb7 O2 2.45(5) 4_575 ? Pb7 O2 2.45(4) 2_675 ? Pb7 O2 2.45(4) . ? Pb7 O2 2.45(4) 3_655 ? Pb7 Cl2 3.379(16) 1_554 ? Pb7 Cl2 3.379(16) 2_674 ? Pb7 Cl3 3.380(9) 1_454 ? Pb7 Cl3 3.380(9) 1_554 ? Pb7 Pb6 3.660(5) 2_675 ? Pb7 Pb8 3.854(2) . ? Pb7 Pb8 3.854(2) 1_455 ? Pb7 Pb5 3.922(5) 1_554 ? Pb7 Pb2 3.928(2) 2_775 ? Pb7 Pb2 3.928(2) 1_455 ? Pb7 Pb2 3.928(2) 2_675 ? Pb8 O2 2.42(5) . ? Pb8 O2 2.42(5) 2_775 ? Pb8 O2 2.42(5) 4_575 ? Pb8 O2 2.42(5) 3_755 ? Pb8 Pb2 3.684(5) 2_775 ? Pb8 Pb7 3.854(2) 1_655 ? Pb8 Pb6 3.925(3) 2_775 ? Pb8 Pb6 3.925(3) 2_675 ? Pb8 Pb6 3.925(3) 1_655 ? Pb9 Pb10 0.91(3) . ? Pb9 OH3 2.65(5) 2_665 ? Pb9 OH3 2.65(5) . ? Pb9 OH5 2.71(5) 1_556 ? Pb9 OH5 2.71(5) 2_666 ? Pb9 Cl2 2.883(16) 2_665 ? Pb9 Cl2 2.883(16) . ? Pb9 Pb13 2.9027(10) . ? Pb9 Pb13 2.9027(9) 1_455 ? Pb9 Pb2 4.390(4) 1_556 ? Pb9 Pb2 4.390(4) 1_456 ? Pb9 Pb2 4.390(4) 2_666 ? Pb9 Pb2 4.390(4) 2_766 ? Pb10 OH5 1.99(6) 1_556 ? Pb10 OH5 1.99(6) 2_666 ? Pb10 OH6 2.57(9) 1_556 ? Pb10 OH6 2.57(9) 4_566 ? Pb10 OH6 2.57(9) 3_656 ? Pb10 OH6 2.57(9) 2_666 ? Pb10 Pb13 3.020(12) 1_455 ? Pb10 Pb13 3.020(12) . ? Pb10 Cl2 3.17(2) 2_665 ? Pb10 Cl2 3.17(2) . ? Pb10 Pb2 4.213(4) 1_556 ? Pb10 Pb2 4.213(4) 2_666 ? Pb10 Pb2 4.213(4) 1_456 ? Pb10 Pb2 4.213(4) 2_766 ? Pb10 Pb6 4.22(2) 1_556 ? Pb10 Pb6 4.22(2) 2_666 ? Pb11 Pb12 1.099(14) . ? Pb11 OH4 2.39(5) 1_655 ? Pb11 OH4 2.39(5) 2_665 ? Pb11 Cl1 2.93(2) . ? Pb11 Cl1 2.93(2) 2_765 ? Pb11 OH6 2.97(9) 4_565 ? Pb11 OH6 2.97(9) 3_755 ? Pb11 OH6 2.97(9) . ? Pb11 OH6 2.97(9) 2_765 ? Pb11 Mg 4.06(4) 2_765 ? Pb11 Mg 4.06(4) . ? Pb11 Pb6 4.424(4) 2_665 ? Pb11 Pb6 4.424(4) 1_655 ? Pb11 Pb6 4.424(4) 2_765 ? Pb12 OH4 1.87(5) 1_655 ? Pb12 OH4 1.87(5) 2_665 ? Pb12 OH1 2.73(5) 2_765 ? Pb12 OH1 2.73(5) . ? Pb12 Cl1 2.87(2) . ? Pb12 Cl1 2.87(2) 2_765 ? Pb12 Mg 3.06(4) 2_765 ? Pb12 Mg 3.06(4) . ? Pb12 Pb1 4.491(5) 1_655 ? Pb12 Pb1 4.491(5) 2_665 ? Pb12 Pb1 4.491(5) 2_765 ? Pb13 OH3 2.36(5) . ? Pb13 OH3 2.36(5) 2_765 ? Pb13 Pb9 2.9027(8) 1_655 ? Pb13 Pb10 3.020(12) 1_655 ? Pb13 OH6 3.04(10) 3_756 ? Pb13 OH6 3.04(10) 2_766 ? Pb13 OH6 3.04(10) 1_556 ? Pb13 OH6 3.04(10) 4_566 ? Pb13 Pb2 3.266(12) 1_556 ? Pb13 Pb2 3.266(12) 2_766 ? Pb13 Pb3 4.126(19) 2_765 ? Cl1 Pb1 3.438(10) 1_655 ? Cl2 Pb7 3.379(16) 1_556 ? Cl2 Pb2 3.422(8) 1_556 ? Cl2 Pb2 3.422(8) 1_456 ? Cl3 Pb2 3.150(10) 2_776 ? Cl3 Pb2 3.150(10) 1_556 ? Cl3 Pb3 3.354(12) 2_775 ? Cl3 Pb7 3.380(9) 1_656 ? Cl3 Pb7 3.380(9) 1_556 ? Cl4 Pb1 3.127(12) 2_675 ? Cl4 Pb6 3.386(14) 2_675 ? Cl4 Pb4 3.427(11) 1_455 ? Mg OH3 1.94(5) . ? Mg OH2 1.96(4) . ? Mg OH2 1.96(4) 2_665 ? Mg OH1 2.09(4) 2_765 ? Mg OH1 2.09(4) . ? Mg OH4 2.26(6) 2_665 ? Mg Mg 2.88(6) 2_765 ? Mg Mg 2.93(6) 2_665 ? Mg Pb1 3.674(18) 2_665 ? OH1 Mg 2.09(4) 2_765 ? OH1 Pb3 2.38(5) 2_765 ? OH2 Mg 1.96(4) 2_665 ? OH2 Pb1 2.38(5) 2_665 ? OH4 Pb12 1.87(5) 1_455 ? OH4 Mg 2.26(6) 2_665 ? OH4 Pb11 2.39(5) 1_455 ? OH5 OH6 1.78(8) . ? OH5 OH6 1.78(8) 3_655 ? OH5 Pb10 1.99(6) 1_554 ? OH5 Pb9 2.71(5) 1_554 ? OH6 OH6 1.74(13) 4_565 ? OH6 Pb10 2.57(9) 1_554 ? OH6 Pb13 3.04(10) 1_554 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1 Pb1 O1 77.0(19) . 3_655 ? O1 Pb1 OH2 90.6(11) . 2_665 ? O1 Pb1 OH2 90.6(11) 3_655 2_665 ? O1 Pb1 Cl4 85.9(7) . . ? O1 Pb1 Cl4 85.9(7) 3_655 . ? OH2 Pb1 Cl4 175.6(11) 2_665 . ? O1 Pb1 Cl1 152.0(8) . 1_455 ? O1 Pb1 Cl1 80.3(10) 3_655 1_455 ? OH2 Pb1 Cl1 105.9(6) 2_665 1_455 ? Cl4 Pb1 Cl1 76.2(4) . 1_455 ? O1 Pb1 Cl1 80.3(10) . . ? O1 Pb1 Cl1 152.0(8) 3_655 . ? OH2 Pb1 Cl1 105.9(6) 2_665 . ? Cl4 Pb1 Cl1 76.2(4) . . ? Cl1 Pb1 Cl1 115.2(5) 1_455 . ? O1 Pb1 Pb5 38.8(9) . . ? O1 Pb1 Pb5 38.8(9) 3_655 . ? OH2 Pb1 Pb5 95.4(11) 2_665 . ? Cl4 Pb1 Pb5 80.2(3) . . ? Cl1 Pb1 Pb5 115.6(3) 1_455 . ? Cl1 Pb1 Pb5 115.6(4) . . ? O1 Pb1 Mg 88.5(8) . . ? O1 Pb1 Mg 118.0(9) 3_655 . ? OH2 Pb1 Mg 28.8(8) 2_665 . ? Cl4 Pb1 Mg 153.4(5) . . ? Cl1 Pb1 Mg 116.8(6) 1_455 . ? Cl1 Pb1 Mg 77.2(6) . . ? Pb5 Pb1 Mg 110.6(5) . . ? O1 Pb1 Mg 118.0(9) . 2_665 ? O1 Pb1 Mg 88.5(8) 3_655 2_665 ? OH2 Pb1 Mg 28.8(8) 2_665 2_665 ? Cl4 Pb1 Mg 153.4(5) . 2_665 ? Cl1 Pb1 Mg 77.2(6) 1_455 2_665 ? Cl1 Pb1 Mg 116.8(6) . 2_665 ? Pb5 Pb1 Mg 110.6(5) . 2_665 ? Mg Pb1 Mg 46.9(9) . 2_665 ? O1 Pb1 Pb4 36.3(9) . . ? O1 Pb1 Pb4 97.4(8) 3_655 . ? OH2 Pb1 Pb4 120.4(5) 2_665 . ? Cl4 Pb1 Pb4 57.48(15) . . ? Cl1 Pb1 Pb4 133.7(4) 1_455 . ? Cl1 Pb1 Pb4 54.9(4) . . ? Pb5 Pb1 Pb4 61.87(5) . . ? Mg Pb1 Pb4 105.1(4) . . ? Mg Pb1 Pb4 149.1(5) 2_665 . ? O1 Pb1 Pb4 97.4(8) . 1_455 ? O1 Pb1 Pb4 36.3(9) 3_655 1_455 ? OH2 Pb1 Pb4 120.4(5) 2_665 1_455 ? Cl4 Pb1 Pb4 57.48(15) . 1_455 ? Cl1 Pb1 Pb4 54.9(4) 1_455 1_455 ? Cl1 Pb1 Pb4 133.7(4) . 1_455 ? Pb5 Pb1 Pb4 61.87(5) . 1_455 ? Mg Pb1 Pb4 149.1(5) . 1_455 ? Mg Pb1 Pb4 105.1(4) 2_665 1_455 ? Pb4 Pb1 Pb4 97.16(6) . 1_455 ? O1 Pb1 Pb3 30.2(6) . . ? O1 Pb1 Pb3 93.9(10) 3_655 . ? OH2 Pb1 Pb3 65.3(6) 2_665 . ? Cl4 Pb1 Pb3 112.2(2) . . ? Cl1 Pb1 Pb3 169.6(3) 1_455 . ? Cl1 Pb1 Pb3 73.8(3) . . ? Pb5 Pb1 Pb3 61.73(6) . . ? Mg Pb1 Pb3 58.4(5) . . ? Mg Pb1 Pb3 94.1(5) 2_665 . ? Pb4 Pb1 Pb3 55.34(7) . . ? Pb4 Pb1 Pb3 123.59(9) 1_455 . ? O1 Pb1 Pb3 93.9(10) . 1_455 ? O1 Pb1 Pb3 30.2(6) 3_655 1_455 ? OH2 Pb1 Pb3 65.3(6) 2_665 1_455 ? Cl4 Pb1 Pb3 112.2(2) . 1_455 ? Cl1 Pb1 Pb3 73.8(3) 1_455 1_455 ? Cl1 Pb1 Pb3 169.6(3) . 1_455 ? Pb5 Pb1 Pb3 61.73(6) . 1_455 ? Mg Pb1 Pb3 94.1(5) . 1_455 ? Mg Pb1 Pb3 58.4(5) 2_665 1_455 ? Pb4 Pb1 Pb3 123.59(9) . 1_455 ? Pb4 Pb1 Pb3 55.34(7) 1_455 1_455 ? Pb3 Pb1 Pb3 96.85(5) . 1_455 ? O1 Pb1 Pb6 127.4(10) . . ? O1 Pb1 Pb6 127.4(9) 3_655 . ? OH2 Pb1 Pb6 128.2(11) 2_665 . ? Cl4 Pb1 Pb6 56.2(3) . . ? Cl1 Pb1 Pb6 57.9(3) 1_455 . ? Cl1 Pb1 Pb6 57.9(3) . . ? Pb5 Pb1 Pb6 136.36(11) . . ? Mg Pb1 Pb6 109.2(6) . . ? Mg Pb1 Pb6 109.2(6) 2_665 . ? Pb4 Pb1 Pb6 91.21(9) . . ? Pb4 Pb1 Pb6 91.21(9) 1_455 . ? Pb3 Pb1 Pb6 131.57(3) . . ? Pb3 Pb1 Pb6 131.57(3) 1_455 . ? O1 Pb1 Pb12 160.5(8) . 1_455 ? O1 Pb1 Pb12 97.9(8) 3_655 1_455 ? OH2 Pb1 Pb12 70.4(8) 2_665 1_455 ? Cl4 Pb1 Pb12 112.8(3) . 1_455 ? Cl1 Pb1 Pb12 39.7(4) 1_455 1_455 ? Cl1 Pb1 Pb12 108.8(4) . 1_455 ? Pb5 Pb1 Pb12 135.58(12) . 1_455 ? Mg Pb1 Pb12 77.2(5) . 1_455 ? Mg Pb1 Pb12 42.5(6) 2_665 1_455 ? Pb4 Pb1 Pb12 161.12(17) . 1_455 ? Pb4 Pb1 Pb12 88.69(2) 1_455 1_455 ? Pb3 Pb1 Pb12 134.15(14) . 1_455 ? Pb3 Pb1 Pb12 74.33(15) 1_455 1_455 ? Pb6 Pb1 Pb12 70.66(17) . 1_455 ? O1 Pb1 Pb12 97.9(8) . . ? O1 Pb1 Pb12 160.5(8) 3_655 . ? OH2 Pb1 Pb12 70.4(8) 2_665 . ? Cl4 Pb1 Pb12 112.8(3) . . ? Cl1 Pb1 Pb12 108.8(4) 1_455 . ? Cl1 Pb1 Pb12 39.7(4) . . ? Pb5 Pb1 Pb12 135.58(12) . . ? Mg Pb1 Pb12 42.5(6) . . ? Mg Pb1 Pb12 77.2(5) 2_665 . ? Pb4 Pb1 Pb12 88.69(2) . . ? Pb4 Pb1 Pb12 161.12(17) 1_455 . ? Pb3 Pb1 Pb12 74.33(14) . . ? Pb3 Pb1 Pb12 134.15(14) 1_455 . ? Pb6 Pb1 Pb12 70.66(17) . . ? Pb12 Pb1 Pb12 80.50(10) 1_455 . ? O2 Pb2 O2 79(3) 3_755 . ? O2 Pb2 OH6 113(2) 3_755 . ? O2 Pb2 OH6 80.0(18) . . ? O2 Pb2 OH6 80.0(18) 3_755 3_755 ? O2 Pb2 OH6 113(2) . 3_755 ? OH6 Pb2 OH6 52(3) . 3_755 ? O2 Pb2 Cl3 83.0(10) 3_755 1_554 ? O2 Pb2 Cl3 83.0(10) . 1_554 ? OH6 Pb2 Cl3 153.9(15) . 1_554 ? OH6 Pb2 Cl3 153.9(15) 3_755 1_554 ? O2 Pb2 Pb13 133.8(10) 3_755 1_554 ? O2 Pb2 Pb13 133.8(10) . 1_554 ? OH6 Pb2 Pb13 58.9(18) . 1_554 ? OH6 Pb2 Pb13 58.9(18) 3_755 1_554 ? Cl3 Pb2 Pb13 125.4(6) 1_554 1_554 ? O2 Pb2 Cl2 150.6(10) 3_755 1_554 ? O2 Pb2 Cl2 78.1(14) . 1_554 ? OH6 Pb2 Cl2 80.9(17) . 1_554 ? OH6 Pb2 Cl2 126.0(16) 3_755 1_554 ? Cl3 Pb2 Cl2 76.2(3) 1_554 1_554 ? Pb13 Pb2 Cl2 75.6(3) 1_554 1_554 ? O2 Pb2 Cl2 78.1(14) 3_755 1_654 ? O2 Pb2 Cl2 150.6(10) . 1_654 ? OH6 Pb2 Cl2 126.0(16) . 1_654 ? OH6 Pb2 Cl2 80.9(17) 3_755 1_654 ? Cl3 Pb2 Cl2 76.2(3) 1_554 1_654 ? Pb13 Pb2 Cl2 75.6(3) 1_554 1_654 ? Cl2 Pb2 Cl2 116.0(4) 1_554 1_654 ? O2 Pb2 Pb8 39.6(12) 3_755 . ? O2 Pb2 Pb8 39.6(12) . . ? OH6 Pb2 Pb8 101.6(18) . . ? OH6 Pb2 Pb8 101.6(18) 3_755 . ? Cl3 Pb2 Pb8 76.9(3) 1_554 . ? Pb13 Pb2 Pb8 157.8(5) 1_554 . ? Cl2 Pb2 Pb8 114.0(3) 1_554 . ? Cl2 Pb2 Pb8 114.0(3) 1_654 . ? O2 Pb2 Pb6 31.0(8) 3_755 1_655 ? O2 Pb2 Pb6 95.5(14) . 1_655 ? OH6 Pb2 Pb6 90.4(17) . 1_655 ? OH6 Pb2 Pb6 49.2(17) 3_755 1_655 ? Cl3 Pb2 Pb6 110.9(2) 1_554 1_655 ? Pb13 Pb2 Pb6 104.3(3) 1_554 1_655 ? Cl2 Pb2 Pb6 169.9(2) 1_554 1_655 ? Cl2 Pb2 Pb6 73.3(2) 1_654 1_655 ? Pb8 Pb2 Pb6 62.57(9) . 1_655 ? O2 Pb2 Pb6 95.5(14) 3_755 . ? O2 Pb2 Pb6 31.0(8) . . ? OH6 Pb2 Pb6 49.2(16) . . ? OH6 Pb2 Pb6 90.4(17) 3_755 . ? Cl3 Pb2 Pb6 110.9(2) 1_554 . ? Pb13 Pb2 Pb6 104.3(3) 1_554 . ? Cl2 Pb2 Pb6 73.3(2) 1_554 . ? Cl2 Pb2 Pb6 169.9(2) 1_654 . ? Pb8 Pb2 Pb6 62.57(9) . . ? Pb6 Pb2 Pb6 97.21(7) 1_655 . ? O2 Pb2 Pb3 124.1(13) 3_755 1_554 ? O2 Pb2 Pb3 124.1(13) . 1_554 ? OH6 Pb2 Pb3 120.7(18) . 1_554 ? OH6 Pb2 Pb3 120.7(18) 3_755 1_554 ? Cl3 Pb2 Pb3 55.6(3) 1_554 1_554 ? Pb13 Pb2 Pb3 69.7(5) 1_554 1_554 ? Cl2 Pb2 Pb3 58.3(2) 1_554 1_554 ? Cl2 Pb2 Pb3 58.3(2) 1_654 1_554 ? Pb8 Pb2 Pb3 132.51(12) . 1_554 ? Pb6 Pb2 Pb3 131.38(3) 1_655 1_554 ? Pb6 Pb2 Pb3 131.38(3) . 1_554 ? O2 Pb2 Pb7 34.9(13) 3_755 1_655 ? O2 Pb2 Pb7 96.8(10) . 1_655 ? OH6 Pb2 Pb7 146.0(17) . 1_655 ? OH6 Pb2 Pb7 100.3(15) 3_755 1_655 ? Cl3 Pb2 Pb7 55.75(13) 1_554 1_655 ? Pb13 Pb2 Pb7 128.90(16) 1_554 1_655 ? Cl2 Pb2 Pb7 131.9(3) 1_554 1_655 ? Cl2 Pb2 Pb7 54.2(3) 1_654 1_655 ? Pb8 Pb2 Pb7 60.74(6) . 1_655 ? Pb6 Pb2 Pb7 56.00(9) 1_655 1_655 ? Pb6 Pb2 Pb7 123.31(13) . 1_655 ? Pb3 Pb2 Pb7 89.33(9) 1_554 1_655 ? O2 Pb2 Pb7 96.8(10) 3_755 . ? O2 Pb2 Pb7 34.9(13) . . ? OH6 Pb2 Pb7 100.3(15) . . ? OH6 Pb2 Pb7 146.0(17) 3_755 . ? Cl3 Pb2 Pb7 55.75(13) 1_554 . ? Pb13 Pb2 Pb7 128.90(16) 1_554 . ? Cl2 Pb2 Pb7 54.2(3) 1_554 . ? Cl2 Pb2 Pb7 131.9(3) 1_654 . ? Pb8 Pb2 Pb7 60.74(6) . . ? Pb6 Pb2 Pb7 123.31(13) 1_655 . ? Pb6 Pb2 Pb7 56.00(9) . . ? Pb3 Pb2 Pb7 89.33(9) 1_554 . ? Pb7 Pb2 Pb7 95.25(8) 1_655 . ? O2 Pb2 Pb10 149.3(13) 3_755 1_554 ? O2 Pb2 Pb10 89.1(11) . 1_554 ? OH6 Pb2 Pb10 36.8(18) . 1_554 ? OH6 Pb2 Pb10 78.8(16) 3_755 1_554 ? Cl3 Pb2 Pb10 123.8(4) 1_554 1_554 ? Pb13 Pb2 Pb10 45.5(2) 1_554 1_554 ? Cl2 Pb2 Pb10 47.8(4) 1_554 1_554 ? Cl2 Pb2 Pb10 119.7(4) 1_654 1_554 ? Pb8 Pb2 Pb10 125.4(4) . 1_554 ? Pb6 Pb2 Pb10 125.2(4) 1_655 1_554 ? Pb6 Pb2 Pb10 62.8(4) . 1_554 ? Pb3 Pb2 Pb10 86.0(4) 1_554 1_554 ? Pb7 Pb2 Pb10 173.8(4) 1_655 1_554 ? Pb7 Pb2 Pb10 88.666(12) . 1_554 ? O2 Pb2 Pb10 89.1(11) 3_755 1_654 ? O2 Pb2 Pb10 149.3(13) . 1_654 ? OH6 Pb2 Pb10 78.8(16) . 1_654 ? OH6 Pb2 Pb10 36.8(18) 3_755 1_654 ? Cl3 Pb2 Pb10 123.8(4) 1_554 1_654 ? Pb13 Pb2 Pb10 45.5(2) 1_554 1_654 ? Cl2 Pb2 Pb10 119.7(4) 1_554 1_654 ? Cl2 Pb2 Pb10 47.8(4) 1_654 1_654 ? Pb8 Pb2 Pb10 125.4(4) . 1_654 ? Pb6 Pb2 Pb10 62.8(4) 1_655 1_654 ? Pb6 Pb2 Pb10 125.2(4) . 1_654 ? Pb3 Pb2 Pb10 86.0(4) 1_554 1_654 ? Pb7 Pb2 Pb10 88.666(12) 1_655 1_654 ? Pb7 Pb2 Pb10 173.8(4) . 1_654 ? Pb10 Pb2 Pb10 87.05(10) 1_554 1_654 ? O2 Pb2 Pb9 160.9(11) 3_755 1_554 ? O2 Pb2 Pb9 96.0(11) . 1_554 ? OH6 Pb2 Pb9 48.2(18) . 1_554 ? OH6 Pb2 Pb9 85.1(16) 3_755 1_554 ? Cl3 Pb2 Pb9 114.9(2) 1_554 1_554 ? Pb13 Pb2 Pb9 41.39(4) 1_554 1_554 ? Cl2 Pb2 Pb9 41.0(3) 1_554 1_554 ? Cl2 Pb2 Pb9 111.5(3) 1_654 1_554 ? Pb8 Pb2 Pb9 134.47(8) . 1_554 ? Pb6 Pb2 Pb9 133.69(14) 1_655 1_554 ? Pb6 Pb2 Pb9 72.49(11) . 1_554 ? Pb3 Pb2 Pb9 74.04(12) 1_554 1_554 ? Pb7 Pb2 Pb9 162.86(14) 1_655 1_554 ? Pb7 Pb2 Pb9 88.80(2) . 1_554 ? Pb10 Pb2 Pb9 11.9(4) 1_554 1_554 ? Pb10 Pb2 Pb9 86.10(15) 1_654 1_554 ? O2 Pb2 Pb9 96.0(11) 3_755 1_654 ? O2 Pb2 Pb9 160.9(11) . 1_654 ? OH6 Pb2 Pb9 85.1(16) . 1_654 ? OH6 Pb2 Pb9 48.2(18) 3_755 1_654 ? Cl3 Pb2 Pb9 114.9(2) 1_554 1_654 ? Pb13 Pb2 Pb9 41.39(4) 1_554 1_654 ? Cl2 Pb2 Pb9 111.5(3) 1_554 1_654 ? Cl2 Pb2 Pb9 41.0(3) 1_654 1_654 ? Pb8 Pb2 Pb9 134.47(8) . 1_654 ? Pb6 Pb2 Pb9 72.49(11) 1_655 1_654 ? Pb6 Pb2 Pb9 133.69(14) . 1_654 ? Pb3 Pb2 Pb9 74.04(12) 1_554 1_654 ? Pb7 Pb2 Pb9 88.80(2) 1_655 1_654 ? Pb7 Pb2 Pb9 162.86(14) . 1_654 ? Pb10 Pb2 Pb9 86.10(14) 1_554 1_654 ? Pb10 Pb2 Pb9 11.9(4) 1_654 1_654 ? Pb9 Pb2 Pb9 82.75(9) 1_554 1_654 ? O1 Pb3 O1 83.7(19) 3_755 . ? O1 Pb3 OH1 88.2(11) 3_755 2_765 ? O1 Pb3 OH1 88.2(11) . 2_765 ? O1 Pb3 Cl3 88.5(8) 3_755 . ? O1 Pb3 Cl3 88.5(8) . . ? OH1 Pb3 Cl3 175.5(12) 2_765 . ? O1 Pb3 Pb4 41.9(9) 3_755 . ? O1 Pb3 Pb4 41.9(9) . . ? OH1 Pb3 Pb4 89.7(11) 2_765 . ? Cl3 Pb3 Pb4 85.8(2) . . ? O1 Pb3 Mg 119.9(10) 3_755 . ? O1 Pb3 Mg 88.7(8) . . ? OH1 Pb3 Mg 31.9(9) 2_765 . ? Cl3 Pb3 Mg 151.0(6) . . ? Pb4 Pb3 Mg 110.6(5) . . ? O1 Pb3 Mg 88.7(8) 3_755 2_765 ? O1 Pb3 Mg 119.9(10) . 2_765 ? OH1 Pb3 Mg 31.9(9) 2_765 2_765 ? Cl3 Pb3 Mg 151.0(6) . 2_765 ? Pb4 Pb3 Mg 110.6(5) . 2_765 ? Mg Pb3 Mg 45.9(9) . 2_765 ? O1 Pb3 Pb5 33.3(9) 3_755 1_655 ? O1 Pb3 Pb5 99.7(8) . 1_655 ? OH1 Pb3 Pb5 117.6(6) 2_765 1_655 ? Cl3 Pb3 Pb5 60.06(13) . 1_655 ? Pb4 Pb3 Pb5 62.24(5) . 1_655 ? Mg Pb3 Pb5 148.6(5) . 1_655 ? Mg Pb3 Pb5 105.5(4) 2_765 1_655 ? O1 Pb3 Pb5 99.7(7) 3_755 . ? O1 Pb3 Pb5 33.3(9) . . ? OH1 Pb3 Pb5 117.6(6) 2_765 . ? Cl3 Pb3 Pb5 60.06(13) . . ? Pb4 Pb3 Pb5 62.24(5) . . ? Mg Pb3 Pb5 105.5(4) . . ? Mg Pb3 Pb5 148.6(5) 2_765 . ? Pb5 Pb3 Pb5 97.57(6) 1_655 . ? O1 Pb3 Pb1 98.0(10) 3_755 . ? O1 Pb3 Pb1 30.7(7) . . ? OH1 Pb3 Pb1 61.7(6) 2_765 . ? Cl3 Pb3 Pb1 115.88(14) . . ? Pb4 Pb3 Pb1 62.20(6) . . ? Mg Pb3 Pb1 58.0(5) . . ? Mg Pb3 Pb1 93.1(5) 2_765 . ? Pb5 Pb3 Pb1 124.44(10) 1_655 . ? Pb5 Pb3 Pb1 55.95(7) . . ? O1 Pb3 Pb1 30.7(6) 3_755 1_655 ? O1 Pb3 Pb1 98.0(10) . 1_655 ? OH1 Pb3 Pb1 61.7(6) 2_765 1_655 ? Cl3 Pb3 Pb1 115.88(14) . 1_655 ? Pb4 Pb3 Pb1 62.20(6) . 1_655 ? Mg Pb3 Pb1 93.1(5) . 1_655 ? Mg Pb3 Pb1 58.0(5) 2_765 1_655 ? Pb5 Pb3 Pb1 55.95(7) 1_655 1_655 ? Pb5 Pb3 Pb1 124.44(10) . 1_655 ? Pb1 Pb3 Pb1 96.85(5) . 1_655 ? O1 Pb3 Pb2 124.1(10) 3_755 1_556 ? O1 Pb3 Pb2 124.1(10) . 1_556 ? OH1 Pb3 Pb2 133.7(11) 2_765 1_556 ? Cl3 Pb3 Pb2 50.8(2) . 1_556 ? Pb4 Pb3 Pb2 136.61(11) . 1_556 ? Mg Pb3 Pb2 109.2(6) . 1_556 ? Mg Pb3 Pb2 109.2(6) 2_765 1_556 ? Pb5 Pb3 Pb2 91.04(9) 1_655 1_556 ? Pb5 Pb3 Pb2 91.04(9) . 1_556 ? Pb1 Pb3 Pb2 131.55(3) . 1_556 ? Pb1 Pb3 Pb2 131.55(3) 1_655 1_556 ? O1 Pb3 Pb13 137.7(9) 3_755 . ? O1 Pb3 Pb13 137.7(9) . . ? OH1 Pb3 Pb13 85.7(12) 2_765 . ? Cl3 Pb3 Pb13 98.8(4) . . ? Pb4 Pb3 Pb13 175.4(3) . . ? Mg Pb3 Pb13 65.3(6) . . ? Mg Pb3 Pb13 65.3(6) 2_765 . ? Pb5 Pb3 Pb13 120.08(16) 1_655 . ? Pb5 Pb3 Pb13 120.08(16) . . ? Pb1 Pb3 Pb13 115.31(19) . . ? Pb1 Pb3 Pb13 115.31(19) 1_655 . ? Pb2 Pb3 Pb13 47.9(3) 1_556 . ? O1 Pb4 O1 75.0(17) 2_775 4_575 ? O1 Pb4 O1 114.2(18) 2_775 . ? O1 Pb4 O1 70.6(13) 4_575 . ? O1 Pb4 O1 70.6(13) 2_775 3_755 ? O1 Pb4 O1 114.2(18) 4_575 3_755 ? O1 Pb4 O1 75.0(17) . 3_755 ? O1 Pb4 Cl1 141.3(8) 2_775 . ? O1 Pb4 Cl1 141.3(8) 4_575 . ? O1 Pb4 Cl1 79.2(7) . . ? O1 Pb4 Cl1 79.2(7) 3_755 . ? O1 Pb4 Cl1 79.2(7) 2_775 2_775 ? O1 Pb4 Cl1 79.2(7) 4_575 2_775 ? O1 Pb4 Cl1 141.3(8) . 2_775 ? O1 Pb4 Cl1 141.3(8) 3_755 2_775 ? Cl1 Pb4 Cl1 113.8(7) . 2_775 ? O1 Pb4 Cl4 143.6(7) 2_775 . ? O1 Pb4 Cl4 76.9(10) 4_575 . ? O1 Pb4 Cl4 76.9(10) . . ? O1 Pb4 Cl4 143.6(7) 3_755 . ? Cl1 Pb4 Cl4 73.1(2) . . ? Cl1 Pb4 Cl4 73.1(2) 2_775 . ? O1 Pb4 Cl4 76.9(10) 2_775 1_655 ? O1 Pb4 Cl4 143.6(7) 4_575 1_655 ? O1 Pb4 Cl4 143.6(7) . 1_655 ? O1 Pb4 Cl4 76.9(10) 3_755 1_655 ? Cl1 Pb4 Cl4 73.1(2) . 1_655 ? Cl1 Pb4 Cl4 73.1(2) 2_775 1_655 ? Cl4 Pb4 Cl4 115.7(6) . 1_655 ? O1 Pb4 Pb3 37.6(9) 2_775 2_775 ? O1 Pb4 Pb3 37.6(9) 4_575 2_775 ? O1 Pb4 Pb3 91.4(7) . 2_775 ? O1 Pb4 Pb3 91.4(7) 3_755 2_775 ? Cl1 Pb4 Pb3 168.0(4) . 2_775 ? Cl1 Pb4 Pb3 78.1(4) 2_775 2_775 ? Cl4 Pb4 Pb3 112.12(19) . 2_775 ? Cl4 Pb4 Pb3 112.12(19) 1_655 2_775 ? O1 Pb4 Pb3 91.4(7) 2_775 . ? O1 Pb4 Pb3 91.4(7) 4_575 . ? O1 Pb4 Pb3 37.6(9) . . ? O1 Pb4 Pb3 37.6(9) 3_755 . ? Cl1 Pb4 Pb3 78.1(4) . . ? Cl1 Pb4 Pb3 168.0(4) 2_775 . ? Cl4 Pb4 Pb3 112.12(19) . . ? Cl4 Pb4 Pb3 112.12(19) 1_655 . ? Pb3 Pb4 Pb3 89.88(13) 2_775 . ? O1 Pb4 Pb5 35.3(6) 2_775 1_655 ? O1 Pb4 Pb5 95.7(10) 4_575 1_655 ? O1 Pb4 Pb5 95.7(10) . 1_655 ? O1 Pb4 Pb5 35.3(6) 3_755 1_655 ? Cl1 Pb4 Pb5 111.1(2) . 1_655 ? Cl1 Pb4 Pb5 111.1(2) 2_775 1_655 ? Cl4 Pb4 Pb5 170.9(3) . 1_655 ? Cl4 Pb4 Pb5 73.4(3) 1_655 1_655 ? Pb3 Pb4 Pb5 62.17(5) 2_775 1_655 ? Pb3 Pb4 Pb5 62.17(5) . 1_655 ? O1 Pb4 Pb5 95.7(10) 2_775 . ? O1 Pb4 Pb5 35.3(6) 4_575 . ? O1 Pb4 Pb5 35.3(6) . . ? O1 Pb4 Pb5 95.7(10) 3_755 . ? Cl1 Pb4 Pb5 111.1(2) . . ? Cl1 Pb4 Pb5 111.1(2) 2_775 . ? Cl4 Pb4 Pb5 73.4(3) . . ? Cl4 Pb4 Pb5 170.9(3) 1_655 . ? Pb3 Pb4 Pb5 62.17(5) 2_775 . ? Pb3 Pb4 Pb5 62.17(5) . . ? Pb5 Pb4 Pb5 97.48(7) 1_655 . ? O1 Pb4 Pb1 33.4(9) 2_775 2_775 ? O1 Pb4 Pb1 94.5(7) 4_575 2_775 ? O1 Pb4 Pb1 147.4(9) . 2_775 ? O1 Pb4 Pb1 86.0(7) 3_755 2_775 ? Cl1 Pb4 Pb1 123.40(18) . 2_775 ? Cl1 Pb4 Pb1 56.08(15) 2_775 2_775 ? Cl4 Pb4 Pb1 129.14(17) . 2_775 ? Cl4 Pb4 Pb1 50.30(16) 1_655 2_775 ? Pb3 Pb4 Pb1 62.46(4) 2_775 2_775 ? Pb3 Pb4 Pb1 118.18(9) . 2_775 ? Pb5 Pb4 Pb1 56.01(6) 1_655 2_775 ? Pb5 Pb4 Pb1 124.63(7) . 2_775 ? O1 Pb4 Pb1 147.4(9) 2_775 . ? O1 Pb4 Pb1 86.0(7) 4_575 . ? O1 Pb4 Pb1 33.4(9) . . ? O1 Pb4 Pb1 94.5(7) 3_755 . ? Cl1 Pb4 Pb1 56.08(15) . . ? Cl1 Pb4 Pb1 123.40(18) 2_775 . ? Cl4 Pb4 Pb1 50.30(16) . . ? Cl4 Pb4 Pb1 129.14(17) 1_655 . ? Pb3 Pb4 Pb1 118.18(9) 2_775 . ? Pb3 Pb4 Pb1 62.46(4) . . ? Pb5 Pb4 Pb1 124.63(7) 1_655 . ? Pb5 Pb4 Pb1 56.01(6) . . ? Pb1 Pb4 Pb1 179.20(15) 2_775 . ? O1 Pb4 Pb1 86.0(7) 2_775 1_655 ? O1 Pb4 Pb1 147.4(9) 4_575 1_655 ? O1 Pb4 Pb1 94.5(7) . 1_655 ? O1 Pb4 Pb1 33.4(9) 3_755 1_655 ? Cl1 Pb4 Pb1 56.08(15) . 1_655 ? Cl1 Pb4 Pb1 123.40(18) 2_775 1_655 ? Cl4 Pb4 Pb1 129.14(17) . 1_655 ? Cl4 Pb4 Pb1 50.30(16) 1_655 1_655 ? Pb3 Pb4 Pb1 118.18(9) 2_775 1_655 ? Pb3 Pb4 Pb1 62.46(4) . 1_655 ? Pb5 Pb4 Pb1 56.01(6) 1_655 1_655 ? Pb5 Pb4 Pb1 124.63(7) . 1_655 ? Pb1 Pb4 Pb1 82.83(6) 2_775 1_655 ? Pb1 Pb4 Pb1 97.16(6) . 1_655 ? O1 Pb4 Pb1 94.5(7) 2_775 2_675 ? O1 Pb4 Pb1 33.4(9) 4_575 2_675 ? O1 Pb4 Pb1 86.0(7) . 2_675 ? O1 Pb4 Pb1 147.4(9) 3_755 2_675 ? Cl1 Pb4 Pb1 123.40(18) . 2_675 ? Cl1 Pb4 Pb1 56.08(15) 2_775 2_675 ? Cl4 Pb4 Pb1 50.30(16) . 2_675 ? Cl4 Pb4 Pb1 129.14(17) 1_655 2_675 ? Pb3 Pb4 Pb1 62.46(4) 2_775 2_675 ? Pb3 Pb4 Pb1 118.18(9) . 2_675 ? Pb5 Pb4 Pb1 124.63(7) 1_655 2_675 ? Pb5 Pb4 Pb1 56.01(6) . 2_675 ? Pb1 Pb4 Pb1 97.16(6) 2_775 2_675 ? Pb1 Pb4 Pb1 82.83(6) . 2_675 ? Pb1 Pb4 Pb1 179.20(15) 1_655 2_675 ? O1 Pb4 Pb8 122.9(9) 2_775 . ? O1 Pb4 Pb8 122.9(9) 4_575 . ? O1 Pb4 Pb8 122.9(9) . . ? O1 Pb4 Pb8 122.9(9) 3_755 . ? Cl1 Pb4 Pb8 56.9(4) . . ? Cl1 Pb4 Pb8 56.9(4) 2_775 . ? Cl4 Pb4 Pb8 57.9(3) . . ? Cl4 Pb4 Pb8 57.9(3) 1_655 . ? Pb3 Pb4 Pb8 135.06(7) 2_775 . ? Pb3 Pb4 Pb8 135.06(7) . . ? Pb5 Pb4 Pb8 131.26(4) 1_655 . ? Pb5 Pb4 Pb8 131.26(4) . . ? Pb1 Pb4 Pb8 89.60(7) 2_775 . ? Pb1 Pb4 Pb8 89.60(7) . . ? Pb1 Pb4 Pb8 89.60(7) 1_655 . ? Pb1 Pb4 Pb8 89.60(7) 2_675 . ? O1 Pb5 O1 117.3(18) 4_575 3_655 ? O1 Pb5 O1 74.3(18) 4_575 2_675 ? O1 Pb5 O1 74.3(13) 3_655 2_675 ? O1 Pb5 O1 74.3(13) 4_575 . ? O1 Pb5 O1 74.3(18) 3_655 . ? O1 Pb5 O1 117.3(18) 2_675 . ? O1 Pb5 Pb1 93.3(8) 4_575 . ? O1 Pb5 Pb1 37.4(9) 3_655 . ? O1 Pb5 Pb1 93.3(8) 2_675 . ? O1 Pb5 Pb1 37.4(9) . . ? O1 Pb5 Pb1 37.4(9) 4_575 2_675 ? O1 Pb5 Pb1 93.3(8) 3_655 2_675 ? O1 Pb5 Pb1 37.4(9) 2_675 2_675 ? O1 Pb5 Pb1 93.3(8) . 2_675 ? Pb1 Pb5 Pb1 89.71(13) . 2_675 ? O1 Pb5 Pb3 31.6(10) 4_575 2_775 ? O1 Pb5 Pb3 148.5(10) 3_655 2_775 ? O1 Pb5 Pb3 93.2(8) 2_675 2_775 ? O1 Pb5 Pb3 86.8(8) . 2_775 ? Pb1 Pb5 Pb3 117.71(9) . 2_775 ? Pb1 Pb5 Pb3 62.32(4) 2_675 2_775 ? O1 Pb5 Pb3 148.5(10) 4_575 1_455 ? O1 Pb5 Pb3 31.6(10) 3_655 1_455 ? O1 Pb5 Pb3 86.8(8) 2_675 1_455 ? O1 Pb5 Pb3 93.2(8) . 1_455 ? Pb1 Pb5 Pb3 62.32(4) . 1_455 ? Pb1 Pb5 Pb3 117.71(9) 2_675 1_455 ? Pb3 Pb5 Pb3 179.95(15) 2_775 1_455 ? O1 Pb5 Pb3 93.2(8) 4_575 2_675 ? O1 Pb5 Pb3 86.8(8) 3_655 2_675 ? O1 Pb5 Pb3 31.6(9) 2_675 2_675 ? O1 Pb5 Pb3 148.5(10) . 2_675 ? Pb1 Pb5 Pb3 117.71(9) . 2_675 ? Pb1 Pb5 Pb3 62.32(4) 2_675 2_675 ? Pb3 Pb5 Pb3 97.57(6) 2_775 2_675 ? Pb3 Pb5 Pb3 82.43(6) 1_455 2_675 ? O1 Pb5 Pb3 86.8(8) 4_575 . ? O1 Pb5 Pb3 93.2(8) 3_655 . ? O1 Pb5 Pb3 148.5(10) 2_675 . ? O1 Pb5 Pb3 31.6(9) . . ? Pb1 Pb5 Pb3 62.32(4) . . ? Pb1 Pb5 Pb3 117.71(9) 2_675 . ? Pb3 Pb5 Pb3 82.43(6) 2_775 . ? Pb3 Pb5 Pb3 97.57(6) 1_455 . ? Pb3 Pb5 Pb3 179.95(15) 2_675 . ? O1 Pb5 Pb4 96.4(10) 4_575 1_455 ? O1 Pb5 Pb4 37.2(7) 3_655 1_455 ? O1 Pb5 Pb4 37.2(7) 2_675 1_455 ? O1 Pb5 Pb4 96.4(10) . 1_455 ? Pb1 Pb5 Pb4 62.13(4) . 1_455 ? Pb1 Pb5 Pb4 62.13(4) 2_675 1_455 ? Pb3 Pb5 Pb4 124.45(7) 2_775 1_455 ? Pb3 Pb5 Pb4 55.58(6) 1_455 1_455 ? Pb3 Pb5 Pb4 55.58(6) 2_675 1_455 ? Pb3 Pb5 Pb4 124.45(7) . 1_455 ? O1 Pb5 Pb4 37.2(7) 4_575 . ? O1 Pb5 Pb4 96.4(10) 3_655 . ? O1 Pb5 Pb4 96.4(10) 2_675 . ? O1 Pb5 Pb4 37.2(7) . . ? Pb1 Pb5 Pb4 62.13(4) . . ? Pb1 Pb5 Pb4 62.13(4) 2_675 . ? Pb3 Pb5 Pb4 55.58(6) 2_775 . ? Pb3 Pb5 Pb4 124.45(7) 1_455 . ? Pb3 Pb5 Pb4 124.45(7) 2_675 . ? Pb3 Pb5 Pb4 55.58(6) . . ? Pb4 Pb5 Pb4 97.48(7) 1_455 . ? O1 Pb5 Pb7 121.4(9) 4_575 1_556 ? O1 Pb5 Pb7 121.4(9) 3_655 1_556 ? O1 Pb5 Pb7 121.4(9) 2_675 1_556 ? O1 Pb5 Pb7 121.4(9) . 1_556 ? Pb1 Pb5 Pb7 135.14(6) . 1_556 ? Pb1 Pb5 Pb7 135.14(6) 2_675 1_556 ? Pb3 Pb5 Pb7 89.98(8) 2_775 1_556 ? Pb3 Pb5 Pb7 89.98(8) 1_455 1_556 ? Pb3 Pb5 Pb7 89.98(8) 2_675 1_556 ? Pb3 Pb5 Pb7 89.98(8) . 1_556 ? Pb4 Pb5 Pb7 131.26(4) 1_455 1_556 ? Pb4 Pb5 Pb7 131.26(4) . 1_556 ? OH5 Pb6 O2 88.5(15) . 3_655 ? OH5 Pb6 O2 88.5(15) . . ? O2 Pb6 O2 82(3) 3_655 . ? OH5 Pb6 OH6 37.0(17) . 3_655 ? O2 Pb6 OH6 78.0(18) 3_655 3_655 ? O2 Pb6 OH6 121(2) . 3_655 ? OH5 Pb6 OH6 37.0(17) . . ? O2 Pb6 OH6 121(2) 3_655 . ? O2 Pb6 OH6 78.0(18) . . ? OH6 Pb6 OH6 67(3) 3_655 . ? OH5 Pb6 Cl4 174.5(14) . . ? O2 Pb6 Cl4 87.3(10) 3_655 . ? O2 Pb6 Cl4 87.3(10) . . ? OH6 Pb6 Cl4 144.8(15) 3_655 . ? OH6 Pb6 Cl4 144.8(16) . . ? OH5 Pb6 Pb7 92.1(14) . . ? O2 Pb6 Pb7 40.9(12) 3_655 . ? O2 Pb6 Pb7 40.9(12) . . ? OH6 Pb6 Pb7 105.1(18) 3_655 . ? OH6 Pb6 Pb7 105.1(18) . . ? Cl4 Pb6 Pb7 82.5(3) . . ? OH5 Pb6 Pb2 62.5(8) . 1_455 ? O2 Pb6 Pb2 30.7(8) 3_655 1_455 ? O2 Pb6 Pb2 96.9(14) . 1_455 ? OH6 Pb6 Pb2 47.5(16) 3_655 1_455 ? OH6 Pb6 Pb2 99.1(17) . 1_455 ? Cl4 Pb6 Pb2 114.47(19) . 1_455 ? Pb7 Pb6 Pb2 62.82(7) . 1_455 ? OH5 Pb6 Pb2 62.5(8) . . ? O2 Pb6 Pb2 96.9(14) 3_655 . ? O2 Pb6 Pb2 30.7(8) . . ? OH6 Pb6 Pb2 99.1(17) 3_655 . ? OH6 Pb6 Pb2 47.5(16) . . ? Cl4 Pb6 Pb2 114.47(19) . . ? Pb7 Pb6 Pb2 62.82(7) . . ? Pb2 Pb6 Pb2 97.21(7) 1_455 . ? OH5 Pb6 Pb1 135.4(14) . . ? O2 Pb6 Pb1 123.4(13) 3_655 . ? O2 Pb6 Pb1 123.4(13) . . ? OH6 Pb6 Pb1 114.0(18) 3_655 . ? OH6 Pb6 Pb1 114.0(18) . . ? Cl4 Pb6 Pb1 50.1(3) . . ? Pb7 Pb6 Pb1 132.56(14) . . ? Pb2 Pb6 Pb1 131.39(4) 1_455 . ? Pb2 Pb6 Pb1 131.39(4) . . ? OH5 Pb6 Pb8 118.9(8) . . ? O2 Pb6 Pb8 98.1(10) 3_655 . ? O2 Pb6 Pb8 34.4(13) . . ? OH6 Pb6 Pb8 154.9(17) 3_655 . ? OH6 Pb6 Pb8 94.8(15) . . ? Cl4 Pb6 Pb8 58.25(15) . . ? Pb7 Pb6 Pb8 60.95(7) . . ? Pb2 Pb6 Pb8 123.77(13) 1_455 . ? Pb2 Pb6 Pb8 56.41(9) . . ? Pb1 Pb6 Pb8 89.13(10) . . ? OH5 Pb6 Pb8 118.9(8) . 1_455 ? O2 Pb6 Pb8 34.4(13) 3_655 1_455 ? O2 Pb6 Pb8 98.1(10) . 1_455 ? OH6 Pb6 Pb8 94.8(15) 3_655 1_455 ? OH6 Pb6 Pb8 154.9(17) . 1_455 ? Cl4 Pb6 Pb8 58.25(15) . 1_455 ? Pb7 Pb6 Pb8 60.95(7) . 1_455 ? Pb2 Pb6 Pb8 56.41(9) 1_455 1_455 ? Pb2 Pb6 Pb8 123.77(13) . 1_455 ? Pb1 Pb6 Pb8 89.13(10) . 1_455 ? Pb8 Pb6 Pb8 95.34(9) . 1_455 ? OH5 Pb6 Pb10 0.1(14) . 1_554 ? O2 Pb6 Pb10 88.6(11) 3_655 1_554 ? O2 Pb6 Pb10 88.6(11) . 1_554 ? OH6 Pb6 Pb10 36.9(16) 3_655 1_554 ? OH6 Pb6 Pb10 36.9(16) . 1_554 ? Cl4 Pb6 Pb10 174.6(4) . 1_554 ? Pb7 Pb6 Pb10 92.2(3) . 1_554 ? Pb2 Pb6 Pb10 62.58(19) 1_455 1_554 ? Pb2 Pb6 Pb10 62.58(19) . 1_554 ? Pb1 Pb6 Pb10 135.3(3) . 1_554 ? Pb8 Pb6 Pb10 119.0(2) . 1_554 ? Pb8 Pb6 Pb10 119.0(2) 1_455 1_554 ? OH5 Pb6 Pb11 74.1(10) . 1_455 ? O2 Pb6 Pb11 95.6(11) 3_655 1_455 ? O2 Pb6 Pb11 162.6(11) . 1_455 ? OH6 Pb6 Pb11 41.8(18) 3_655 1_455 ? OH6 Pb6 Pb11 89.0(15) . 1_455 ? Cl4 Pb6 Pb11 109.8(2) . 1_455 ? Pb7 Pb6 Pb11 135.49(8) . 1_455 ? Pb2 Pb6 Pb11 73.46(11) 1_455 1_455 ? Pb2 Pb6 Pb11 134.37(16) . 1_455 ? Pb1 Pb6 Pb11 72.54(11) . 1_455 ? Pb8 Pb6 Pb11 161.20(15) . 1_455 ? Pb8 Pb6 Pb11 88.67(3) 1_455 1_455 ? Pb10 Pb6 Pb11 74.1(3) 1_554 1_455 ? OH5 Pb6 Pb11 74.1(10) . . ? O2 Pb6 Pb11 162.6(11) 3_655 . ? O2 Pb6 Pb11 95.6(11) . . ? OH6 Pb6 Pb11 89.0(15) 3_655 . ? OH6 Pb6 Pb11 41.8(18) . . ? Cl4 Pb6 Pb11 109.8(2) . . ? Pb7 Pb6 Pb11 135.49(8) . . ? Pb2 Pb6 Pb11 134.37(16) 1_455 . ? Pb2 Pb6 Pb11 73.46(11) . . ? Pb1 Pb6 Pb11 72.54(11) . . ? Pb8 Pb6 Pb11 88.67(3) . . ? Pb8 Pb6 Pb11 161.20(15) 1_455 . ? Pb10 Pb6 Pb11 74.1(3) 1_554 . ? Pb11 Pb6 Pb11 81.97(9) 1_455 . ? O2 Pb7 O2 74(2) 4_575 2_675 ? O2 Pb7 O2 75.0(18) 4_575 . ? O2 Pb7 O2 118(2) 2_675 . ? O2 Pb7 O2 118(2) 4_575 3_655 ? O2 Pb7 O2 75.0(18) 2_675 3_655 ? O2 Pb7 O2 74(2) . 3_655 ? O2 Pb7 Cl2 142.3(11) 4_575 1_554 ? O2 Pb7 Cl2 142.3(11) 2_675 1_554 ? O2 Pb7 Cl2 76.5(10) . 1_554 ? O2 Pb7 Cl2 76.5(10) 3_655 1_554 ? O2 Pb7 Cl2 76.5(10) 4_575 2_674 ? O2 Pb7 Cl2 76.5(10) 2_675 2_674 ? O2 Pb7 Cl2 142.3(11) . 2_674 ? O2 Pb7 Cl2 142.3(11) 3_655 2_674 ? Cl2 Pb7 Cl2 114.5(6) 1_554 2_674 ? O2 Pb7 Cl3 141.4(9) 4_575 1_454 ? O2 Pb7 Cl3 75.4(13) 2_675 1_454 ? O2 Pb7 Cl3 141.4(9) . 1_454 ? O2 Pb7 Cl3 75.4(13) 3_655 1_454 ? Cl2 Pb7 Cl3 73.90(19) 1_554 1_454 ? Cl2 Pb7 Cl3 73.90(19) 2_674 1_454 ? O2 Pb7 Cl3 75.4(13) 4_575 1_554 ? O2 Pb7 Cl3 141.4(9) 2_675 1_554 ? O2 Pb7 Cl3 75.4(13) . 1_554 ? O2 Pb7 Cl3 141.4(9) 3_655 1_554 ? Cl2 Pb7 Cl3 73.90(19) 1_554 1_554 ? Cl2 Pb7 Cl3 73.90(19) 2_674 1_554 ? Cl3 Pb7 Cl3 118.3(5) 1_454 1_554 ? O2 Pb7 Pb6 37.2(12) 4_575 2_675 ? O2 Pb7 Pb6 37.2(12) 2_675 2_675 ? O2 Pb7 Pb6 94.7(10) . 2_675 ? O2 Pb7 Pb6 94.7(10) 3_655 2_675 ? Cl2 Pb7 Pb6 169.0(3) 1_554 2_675 ? Cl2 Pb7 Pb6 76.5(3) 2_674 2_675 ? Cl3 Pb7 Pb6 110.77(17) 1_454 2_675 ? Cl3 Pb7 Pb6 110.77(17) 1_554 2_675 ? O2 Pb7 Pb6 94.7(10) 4_575 . ? O2 Pb7 Pb6 94.7(10) 2_675 . ? O2 Pb7 Pb6 37.2(12) . . ? O2 Pb7 Pb6 37.2(12) 3_655 . ? Cl2 Pb7 Pb6 76.5(3) 1_554 . ? Cl2 Pb7 Pb6 169.0(3) 2_674 . ? Cl3 Pb7 Pb6 110.77(17) 1_454 . ? Cl3 Pb7 Pb6 110.77(17) 1_554 . ? Pb6 Pb7 Pb6 92.45(16) 2_675 . ? O2 Pb7 Pb8 37.5(9) 4_575 . ? O2 Pb7 Pb8 96.6(13) 2_675 . ? O2 Pb7 Pb8 37.5(9) . . ? O2 Pb7 Pb8 96.6(13) 3_655 . ? Cl2 Pb7 Pb8 110.86(17) 1_554 . ? Cl2 Pb7 Pb8 110.86(17) 2_674 . ? Cl3 Pb7 Pb8 169.7(3) 1_454 . ? Cl3 Pb7 Pb8 72.0(3) 1_554 . ? Pb6 Pb7 Pb8 62.92(5) 2_675 . ? Pb6 Pb7 Pb8 62.92(5) . . ? O2 Pb7 Pb8 96.6(13) 4_575 1_455 ? O2 Pb7 Pb8 37.5(9) 2_675 1_455 ? O2 Pb7 Pb8 96.6(13) . 1_455 ? O2 Pb7 Pb8 37.5(9) 3_655 1_455 ? Cl2 Pb7 Pb8 110.86(17) 1_554 1_455 ? Cl2 Pb7 Pb8 110.86(17) 2_674 1_455 ? Cl3 Pb7 Pb8 72.0(3) 1_454 1_455 ? Cl3 Pb7 Pb8 169.7(3) 1_554 1_455 ? Pb6 Pb7 Pb8 62.92(5) 2_675 1_455 ? Pb6 Pb7 Pb8 62.92(5) . 1_455 ? Pb8 Pb7 Pb8 97.70(8) . 1_455 ? O2 Pb7 Pb5 121.1(12) 4_575 1_554 ? O2 Pb7 Pb5 121.1(12) 2_675 1_554 ? O2 Pb7 Pb5 121.1(12) . 1_554 ? O2 Pb7 Pb5 121.1(12) 3_655 1_554 ? Cl2 Pb7 Pb5 57.2(3) 1_554 1_554 ? Cl2 Pb7 Pb5 57.2(3) 2_674 1_554 ? Cl3 Pb7 Pb5 59.2(3) 1_454 1_554 ? Cl3 Pb7 Pb5 59.2(3) 1_554 1_554 ? Pb6 Pb7 Pb5 133.77(8) 2_675 1_554 ? Pb6 Pb7 Pb5 133.77(8) . 1_554 ? Pb8 Pb7 Pb5 131.15(4) . 1_554 ? Pb8 Pb7 Pb5 131.15(4) 1_455 1_554 ? O2 Pb7 Pb2 31.6(12) 4_575 2_775 ? O2 Pb7 Pb2 92.2(10) 2_675 2_775 ? O2 Pb7 Pb2 88.2(10) . 2_775 ? O2 Pb7 Pb2 149.2(12) 3_655 2_775 ? Cl2 Pb7 Pb2 124.28(15) 1_554 2_775 ? Cl2 Pb7 Pb2 55.23(12) 2_674 2_775 ? Cl3 Pb7 Pb2 129.12(15) 1_454 2_775 ? Cl3 Pb7 Pb2 50.38(13) 1_554 2_775 ? Pb6 Pb7 Pb2 61.18(4) 2_675 2_775 ? Pb6 Pb7 Pb2 119.42(9) . 2_775 ? Pb8 Pb7 Pb2 56.50(7) . 2_775 ? Pb8 Pb7 Pb2 124.09(7) 1_455 2_775 ? Pb5 Pb7 Pb2 89.63(8) 1_554 2_775 ? O2 Pb7 Pb2 149.2(12) 4_575 1_455 ? O2 Pb7 Pb2 88.2(10) 2_675 1_455 ? O2 Pb7 Pb2 92.2(10) . 1_455 ? O2 Pb7 Pb2 31.6(12) 3_655 1_455 ? Cl2 Pb7 Pb2 55.23(12) 1_554 1_455 ? Cl2 Pb7 Pb2 124.28(15) 2_674 1_455 ? Cl3 Pb7 Pb2 50.38(13) 1_454 1_455 ? Cl3 Pb7 Pb2 129.12(15) 1_554 1_455 ? Pb6 Pb7 Pb2 119.42(9) 2_675 1_455 ? Pb6 Pb7 Pb2 61.18(4) . 1_455 ? Pb8 Pb7 Pb2 124.09(7) . 1_455 ? Pb8 Pb7 Pb2 56.50(7) 1_455 1_455 ? Pb5 Pb7 Pb2 89.63(8) 1_554 1_455 ? Pb2 Pb7 Pb2 179.25(15) 2_775 1_455 ? O2 Pb7 Pb2 92.2(10) 4_575 2_675 ? O2 Pb7 Pb2 31.6(12) 2_675 2_675 ? O2 Pb7 Pb2 149.2(12) . 2_675 ? O2 Pb7 Pb2 88.2(10) 3_655 2_675 ? Cl2 Pb7 Pb2 124.28(15) 1_554 2_675 ? Cl2 Pb7 Pb2 55.23(12) 2_674 2_675 ? Cl3 Pb7 Pb2 50.38(13) 1_454 2_675 ? Cl3 Pb7 Pb2 129.12(15) 1_554 2_675 ? Pb6 Pb7 Pb2 61.18(4) 2_675 2_675 ? Pb6 Pb7 Pb2 119.42(9) . 2_675 ? Pb8 Pb7 Pb2 124.09(7) . 2_675 ? Pb8 Pb7 Pb2 56.50(7) 1_455 2_675 ? Pb5 Pb7 Pb2 89.63(8) 1_554 2_675 ? Pb2 Pb7 Pb2 95.25(8) 2_775 2_675 ? Pb2 Pb7 Pb2 84.74(8) 1_455 2_675 ? O2 Pb7 Pb2 88.2(10) 4_575 . ? O2 Pb7 Pb2 149.2(12) 2_675 . ? O2 Pb7 Pb2 31.6(12) . . ? O2 Pb7 Pb2 92.2(10) 3_655 . ? Cl2 Pb7 Pb2 55.23(12) 1_554 . ? Cl2 Pb7 Pb2 124.28(15) 2_674 . ? Cl3 Pb7 Pb2 129.12(15) 1_454 . ? Cl3 Pb7 Pb2 50.38(13) 1_554 . ? Pb6 Pb7 Pb2 119.42(9) 2_675 . ? Pb6 Pb7 Pb2 61.18(4) . . ? Pb8 Pb7 Pb2 56.50(7) . . ? Pb8 Pb7 Pb2 124.09(7) 1_455 . ? Pb5 Pb7 Pb2 89.63(8) 1_554 . ? Pb2 Pb7 Pb2 84.74(8) 2_775 . ? Pb2 Pb7 Pb2 95.25(8) 1_455 . ? Pb2 Pb7 Pb2 179.25(15) 2_675 . ? O2 Pb8 O2 117(2) . 2_775 ? O2 Pb8 O2 76.0(17) . 4_575 ? O2 Pb8 O2 72(2) 2_775 4_575 ? O2 Pb8 O2 72(2) . 3_755 ? O2 Pb8 O2 76.0(17) 2_775 3_755 ? O2 Pb8 O2 117(2) 4_575 3_755 ? O2 Pb8 Pb2 36.2(12) . . ? O2 Pb8 Pb2 94.4(10) 2_775 . ? O2 Pb8 Pb2 94.4(10) 4_575 . ? O2 Pb8 Pb2 36.2(12) 3_755 . ? O2 Pb8 Pb2 94.4(10) . 2_775 ? O2 Pb8 Pb2 36.2(12) 2_775 2_775 ? O2 Pb8 Pb2 36.2(12) 4_575 2_775 ? O2 Pb8 Pb2 94.4(10) 3_755 2_775 ? Pb2 Pb8 Pb2 91.88(14) . 2_775 ? O2 Pb8 Pb7 38.0(9) . . ? O2 Pb8 Pb7 95.6(13) 2_775 . ? O2 Pb8 Pb7 38.0(9) 4_575 . ? O2 Pb8 Pb7 95.6(13) 3_755 . ? Pb2 Pb8 Pb7 62.77(5) . . ? Pb2 Pb8 Pb7 62.77(5) 2_775 . ? O2 Pb8 Pb7 95.6(13) . 1_655 ? O2 Pb8 Pb7 38.0(9) 2_775 1_655 ? O2 Pb8 Pb7 95.6(13) 4_575 1_655 ? O2 Pb8 Pb7 38.0(9) 3_755 1_655 ? Pb2 Pb8 Pb7 62.77(5) . 1_655 ? Pb2 Pb8 Pb7 62.77(5) 2_775 1_655 ? Pb7 Pb8 Pb7 97.70(8) . 1_655 ? O2 Pb8 Pb6 148.1(13) . 2_775 ? O2 Pb8 Pb6 31.8(12) 2_775 2_775 ? O2 Pb8 Pb6 91.1(10) 4_575 2_775 ? O2 Pb8 Pb6 88.8(10) 3_755 2_775 ? Pb2 Pb8 Pb6 118.90(10) . 2_775 ? Pb2 Pb8 Pb6 61.02(5) 2_775 2_775 ? Pb7 Pb8 Pb6 123.78(9) . 2_775 ? Pb7 Pb8 Pb6 56.13(7) 1_655 2_775 ? O2 Pb8 Pb6 31.8(12) . . ? O2 Pb8 Pb6 148.1(13) 2_775 . ? O2 Pb8 Pb6 88.8(10) 4_575 . ? O2 Pb8 Pb6 91.1(10) 3_755 . ? Pb2 Pb8 Pb6 61.02(5) . . ? Pb2 Pb8 Pb6 118.90(10) 2_775 . ? Pb7 Pb8 Pb6 56.13(7) . . ? Pb7 Pb8 Pb6 123.78(9) 1_655 . ? Pb6 Pb8 Pb6 179.89(17) 2_775 . ? O2 Pb8 Pb6 88.8(10) . 2_675 ? O2 Pb8 Pb6 91.1(10) 2_775 2_675 ? O2 Pb8 Pb6 31.8(12) 4_575 2_675 ? O2 Pb8 Pb6 148.1(13) 3_755 2_675 ? Pb2 Pb8 Pb6 118.90(10) . 2_675 ? Pb2 Pb8 Pb6 61.02(5) 2_775 2_675 ? Pb7 Pb8 Pb6 56.13(7) . 2_675 ? Pb7 Pb8 Pb6 123.78(9) 1_655 2_675 ? Pb6 Pb8 Pb6 95.34(9) 2_775 2_675 ? Pb6 Pb8 Pb6 84.66(9) . 2_675 ? O2 Pb8 Pb6 91.1(10) . 1_655 ? O2 Pb8 Pb6 88.8(10) 2_775 1_655 ? O2 Pb8 Pb6 148.1(13) 4_575 1_655 ? O2 Pb8 Pb6 31.8(12) 3_755 1_655 ? Pb2 Pb8 Pb6 61.02(5) . 1_655 ? Pb2 Pb8 Pb6 118.90(10) 2_775 1_655 ? Pb7 Pb8 Pb6 123.78(9) . 1_655 ? Pb7 Pb8 Pb6 56.13(7) 1_655 1_655 ? Pb6 Pb8 Pb6 84.66(9) 2_775 1_655 ? Pb6 Pb8 Pb6 95.34(9) . 1_655 ? Pb6 Pb8 Pb6 179.89(17) 2_675 1_655 ? O2 Pb8 Pb4 121.7(12) . . ? O2 Pb8 Pb4 121.7(12) 2_775 . ? O2 Pb8 Pb4 121.7(12) 4_575 . ? O2 Pb8 Pb4 121.7(12) 3_755 . ? Pb2 Pb8 Pb4 134.06(7) . . ? Pb2 Pb8 Pb4 134.06(7) 2_775 . ? Pb7 Pb8 Pb4 131.15(4) . . ? Pb7 Pb8 Pb4 131.15(4) 1_655 . ? Pb6 Pb8 Pb4 90.05(9) 2_775 . ? Pb6 Pb8 Pb4 90.05(9) . . ? Pb6 Pb8 Pb4 90.05(9) 2_675 . ? Pb6 Pb8 Pb4 90.05(9) 1_655 . ? Pb10 Pb9 OH3 138.6(10) . 2_665 ? Pb10 Pb9 OH3 138.6(10) . . ? OH3 Pb9 OH3 82.9(19) 2_665 . ? Pb10 Pb9 OH5 32.0(12) . 1_556 ? OH3 Pb9 OH5 129.5(9) 2_665 1_556 ? OH3 Pb9 OH5 129.5(9) . 1_556 ? Pb10 Pb9 OH5 32.0(12) . 2_666 ? OH3 Pb9 OH5 129.5(9) 2_665 2_666 ? OH3 Pb9 OH5 129.5(9) . 2_666 ? OH5 Pb9 OH5 64(2) 1_556 2_666 ? Pb10 Pb9 Cl2 100.3(3) . 2_665 ? OH3 Pb9 Cl2 82.3(3) 2_665 2_665 ? OH3 Pb9 Cl2 82.3(3) . 2_665 ? OH5 Pb9 Cl2 132.3(12) 1_556 2_665 ? OH5 Pb9 Cl2 68.2(12) 2_666 2_665 ? Pb10 Pb9 Cl2 100.3(3) . . ? OH3 Pb9 Cl2 82.3(3) 2_665 . ? OH3 Pb9 Cl2 82.3(3) . . ? OH5 Pb9 Cl2 68.2(12) 1_556 . ? OH5 Pb9 Cl2 132.3(12) 2_666 . ? Cl2 Pb9 Cl2 159.5(7) 2_665 . ? Pb10 Pb9 Pb13 88.5(6) . . ? OH3 Pb9 Pb13 132.9(11) 2_665 . ? OH3 Pb9 Pb13 50.0(11) . . ? OH5 Pb9 Pb13 88.7(5) 1_556 . ? OH5 Pb9 Pb13 88.7(5) 2_666 . ? Cl2 Pb9 Pb13 90.26(11) 2_665 . ? Cl2 Pb9 Pb13 90.26(11) . . ? Pb10 Pb9 Pb13 88.5(6) . 1_455 ? OH3 Pb9 Pb13 50.0(11) 2_665 1_455 ? OH3 Pb9 Pb13 132.9(11) . 1_455 ? OH5 Pb9 Pb13 88.7(5) 1_556 1_455 ? OH5 Pb9 Pb13 88.7(5) 2_666 1_455 ? Cl2 Pb9 Pb13 90.26(11) 2_665 1_455 ? Cl2 Pb9 Pb13 90.26(11) . 1_455 ? Pb13 Pb9 Pb13 177.0(12) . 1_455 ? Pb10 Pb9 Pb2 72.92(11) . 1_556 ? OH3 Pb9 Pb2 131.1(4) 2_665 1_556 ? OH3 Pb9 Pb2 77.5(7) . 1_556 ? OH5 Pb9 Pb2 52.0(6) 1_556 1_556 ? OH5 Pb9 Pb2 96.7(9) 2_666 1_556 ? Cl2 Pb9 Pb2 137.04(9) 2_665 1_556 ? Cl2 Pb9 Pb2 51.15(17) . 1_556 ? Pb13 Pb9 Pb2 48.1(2) . 1_556 ? Pb13 Pb9 Pb2 130.8(3) 1_455 1_556 ? Pb10 Pb9 Pb2 72.92(10) . 1_456 ? OH3 Pb9 Pb2 77.5(7) 2_665 1_456 ? OH3 Pb9 Pb2 131.1(4) . 1_456 ? OH5 Pb9 Pb2 52.0(6) 1_556 1_456 ? OH5 Pb9 Pb2 96.7(9) 2_666 1_456 ? Cl2 Pb9 Pb2 137.04(9) 2_665 1_456 ? Cl2 Pb9 Pb2 51.15(17) . 1_456 ? Pb13 Pb9 Pb2 130.8(3) . 1_456 ? Pb13 Pb9 Pb2 48.1(2) 1_455 1_456 ? Pb2 Pb9 Pb2 82.75(9) 1_556 1_456 ? Pb10 Pb9 Pb2 72.92(10) . 2_666 ? OH3 Pb9 Pb2 77.5(7) 2_665 2_666 ? OH3 Pb9 Pb2 131.1(4) . 2_666 ? OH5 Pb9 Pb2 96.7(9) 1_556 2_666 ? OH5 Pb9 Pb2 52.0(6) 2_666 2_666 ? Cl2 Pb9 Pb2 51.15(17) 2_665 2_666 ? Cl2 Pb9 Pb2 137.04(9) . 2_666 ? Pb13 Pb9 Pb2 130.8(3) . 2_666 ? Pb13 Pb9 Pb2 48.1(2) 1_455 2_666 ? Pb2 Pb9 Pb2 145.8(2) 1_556 2_666 ? Pb2 Pb9 Pb2 87.35(9) 1_456 2_666 ? Pb10 Pb9 Pb2 72.92(10) . 2_766 ? OH3 Pb9 Pb2 131.1(4) 2_665 2_766 ? OH3 Pb9 Pb2 77.5(7) . 2_766 ? OH5 Pb9 Pb2 96.7(9) 1_556 2_766 ? OH5 Pb9 Pb2 52.0(6) 2_666 2_766 ? Cl2 Pb9 Pb2 51.15(17) 2_665 2_766 ? Cl2 Pb9 Pb2 137.04(9) . 2_766 ? Pb13 Pb9 Pb2 48.1(2) . 2_766 ? Pb13 Pb9 Pb2 130.8(3) 1_455 2_766 ? Pb2 Pb9 Pb2 87.35(9) 1_556 2_766 ? Pb2 Pb9 Pb2 145.8(2) 1_456 2_766 ? Pb2 Pb9 Pb2 82.75(9) 2_666 2_766 ? Pb9 Pb10 OH5 133.9(17) . 1_556 ? Pb9 Pb10 OH5 133.9(17) . 2_666 ? OH5 Pb10 OH5 92(3) 1_556 2_666 ? Pb9 Pb10 OH6 134(2) . 1_556 ? OH5 Pb10 OH6 43.6(19) 1_556 1_556 ? OH5 Pb10 OH6 76(2) 2_666 1_556 ? Pb9 Pb10 OH6 134(2) . 4_566 ? OH5 Pb10 OH6 76(2) 1_556 4_566 ? OH5 Pb10 OH6 43.6(19) 2_666 4_566 ? OH6 Pb10 OH6 40(3) 1_556 4_566 ? Pb9 Pb10 OH6 134(2) . 3_656 ? OH5 Pb10 OH6 43.6(19) 1_556 3_656 ? OH5 Pb10 OH6 76(2) 2_666 3_656 ? OH6 Pb10 OH6 79(4) 1_556 3_656 ? OH6 Pb10 OH6 92(4) 4_566 3_656 ? Pb9 Pb10 OH6 134(2) . 2_666 ? OH5 Pb10 OH6 76(2) 1_556 2_666 ? OH5 Pb10 OH6 43.6(19) 2_666 2_666 ? OH6 Pb10 OH6 92(4) 1_556 2_666 ? OH6 Pb10 OH6 79(4) 4_566 2_666 ? OH6 Pb10 OH6 40(3) 3_656 2_666 ? Pb9 Pb10 Pb13 73.9(8) . 1_455 ? OH5 Pb10 Pb13 101.1(6) 1_556 1_455 ? OH5 Pb10 Pb13 101.1(6) 2_666 1_455 ? OH6 Pb10 Pb13 143(2) 1_556 1_455 ? OH6 Pb10 Pb13 143(2) 4_566 1_455 ? OH6 Pb10 Pb13 65(2) 3_656 1_455 ? OH6 Pb10 Pb13 65(2) 2_666 1_455 ? Pb9 Pb10 Pb13 73.9(8) . . ? OH5 Pb10 Pb13 101.1(6) 1_556 . ? OH5 Pb10 Pb13 101.1(6) 2_666 . ? OH6 Pb10 Pb13 65(2) 1_556 . ? OH6 Pb10 Pb13 65(2) 4_566 . ? OH6 Pb10 Pb13 143(2) 3_656 . ? OH6 Pb10 Pb13 143(2) 2_666 . ? Pb13 Pb10 Pb13 147.8(16) 1_455 . ? Pb9 Pb10 Cl2 63.3(6) . 2_665 ? OH5 Pb10 Cl2 163(2) 1_556 2_665 ? OH5 Pb10 Cl2 70.6(16) 2_666 2_665 ? OH6 Pb10 Cl2 127.8(16) 1_556 2_665 ? OH6 Pb10 Cl2 90.5(16) 4_566 2_665 ? OH6 Pb10 Cl2 127.8(16) 3_656 2_665 ? OH6 Pb10 Cl2 90.5(16) 2_666 2_665 ? Pb13 Pb10 Cl2 82.9(5) 1_455 2_665 ? Pb13 Pb10 Cl2 82.9(5) . 2_665 ? Pb9 Pb10 Cl2 63.3(6) . . ? OH5 Pb10 Cl2 70.6(16) 1_556 . ? OH5 Pb10 Cl2 163(2) 2_666 . ? OH6 Pb10 Cl2 90.5(16) 1_556 . ? OH6 Pb10 Cl2 127.8(16) 4_566 . ? OH6 Pb10 Cl2 90.5(16) 3_656 . ? OH6 Pb10 Cl2 127.8(16) 2_666 . ? Pb13 Pb10 Cl2 82.9(5) 1_455 . ? Pb13 Pb10 Cl2 82.9(5) . . ? Cl2 Pb10 Cl2 126.7(13) 2_665 . ? Pb9 Pb10 Pb2 95.2(4) . 1_556 ? OH5 Pb10 Pb2 54.5(8) 1_556 1_556 ? OH5 Pb10 Pb2 117.1(13) 2_666 1_556 ? OH6 Pb10 Pb2 42.0(19) 1_556 1_556 ? OH6 Pb10 Pb2 75.1(16) 4_566 1_556 ? OH6 Pb10 Pb2 97.6(17) 3_656 1_556 ? OH6 Pb10 Pb2 128(2) 2_666 1_556 ? Pb13 Pb10 Pb2 133.4(2) 1_455 1_556 ? Pb13 Pb10 Pb2 50.4(2) . 1_556 ? Cl2 Pb10 Pb2 133.1(4) 2_665 1_556 ? Cl2 Pb10 Pb2 52.93(15) . 1_556 ? Pb9 Pb10 Pb2 95.2(4) . 2_666 ? OH5 Pb10 Pb2 117.1(13) 1_556 2_666 ? OH5 Pb10 Pb2 54.5(8) 2_666 2_666 ? OH6 Pb10 Pb2 128(2) 1_556 2_666 ? OH6 Pb10 Pb2 97.6(17) 4_566 2_666 ? OH6 Pb10 Pb2 75.1(16) 3_656 2_666 ? OH6 Pb10 Pb2 42.0(19) 2_666 2_666 ? Pb13 Pb10 Pb2 50.4(2) 1_455 2_666 ? Pb13 Pb10 Pb2 133.4(2) . 2_666 ? Cl2 Pb10 Pb2 52.93(15) 2_665 2_666 ? Cl2 Pb10 Pb2 133.1(4) . 2_666 ? Pb2 Pb10 Pb2 169.7(9) 1_556 2_666 ? Pb9 Pb10 Pb2 95.2(4) . 1_456 ? OH5 Pb10 Pb2 54.5(8) 1_556 1_456 ? OH5 Pb10 Pb2 117.1(13) 2_666 1_456 ? OH6 Pb10 Pb2 97.6(17) 1_556 1_456 ? OH6 Pb10 Pb2 128(2) 4_566 1_456 ? OH6 Pb10 Pb2 42.0(19) 3_656 1_456 ? OH6 Pb10 Pb2 75.1(16) 2_666 1_456 ? Pb13 Pb10 Pb2 50.4(2) 1_455 1_456 ? Pb13 Pb10 Pb2 133.4(2) . 1_456 ? Cl2 Pb10 Pb2 133.1(4) 2_665 1_456 ? Cl2 Pb10 Pb2 52.93(15) . 1_456 ? Pb2 Pb10 Pb2 87.05(10) 1_556 1_456 ? Pb2 Pb10 Pb2 92.03(11) 2_666 1_456 ? Pb9 Pb10 Pb2 95.2(4) . 2_766 ? OH5 Pb10 Pb2 117.1(13) 1_556 2_766 ? OH5 Pb10 Pb2 54.5(8) 2_666 2_766 ? OH6 Pb10 Pb2 75.1(16) 1_556 2_766 ? OH6 Pb10 Pb2 42.0(19) 4_566 2_766 ? OH6 Pb10 Pb2 128(2) 3_656 2_766 ? OH6 Pb10 Pb2 97.6(17) 2_666 2_766 ? Pb13 Pb10 Pb2 133.4(2) 1_455 2_766 ? Pb13 Pb10 Pb2 50.4(2) . 2_766 ? Cl2 Pb10 Pb2 52.93(15) 2_665 2_766 ? Cl2 Pb10 Pb2 133.1(4) . 2_766 ? Pb2 Pb10 Pb2 92.03(11) 1_556 2_766 ? Pb2 Pb10 Pb2 87.05(10) 2_666 2_766 ? Pb2 Pb10 Pb2 169.7(9) 1_456 2_766 ? Pb9 Pb10 Pb6 134.0(3) . 1_556 ? OH5 Pb10 Pb6 0.1(16) 1_556 1_556 ? OH5 Pb10 Pb6 92.0(19) 2_666 1_556 ? OH6 Pb10 Pb6 43.5(18) 1_556 1_556 ? OH6 Pb10 Pb6 76.2(18) 4_566 1_556 ? OH6 Pb10 Pb6 43.5(18) 3_656 1_556 ? OH6 Pb10 Pb6 76.2(18) 2_666 1_556 ? Pb13 Pb10 Pb6 101.1(5) 1_455 1_556 ? Pb13 Pb10 Pb6 101.1(5) . 1_556 ? Cl2 Pb10 Pb6 162.6(9) 2_665 1_556 ? Cl2 Pb10 Pb6 70.7(4) . 1_556 ? Pb2 Pb10 Pb6 54.58(19) 1_556 1_556 ? Pb2 Pb10 Pb6 117.0(6) 2_666 1_556 ? Pb2 Pb10 Pb6 54.58(19) 1_456 1_556 ? Pb2 Pb10 Pb6 117.0(6) 2_766 1_556 ? Pb9 Pb10 Pb6 134.0(3) . 2_666 ? OH5 Pb10 Pb6 92.0(19) 1_556 2_666 ? OH5 Pb10 Pb6 0.1(16) 2_666 2_666 ? OH6 Pb10 Pb6 76.2(18) 1_556 2_666 ? OH6 Pb10 Pb6 43.5(18) 4_566 2_666 ? OH6 Pb10 Pb6 76.2(18) 3_656 2_666 ? OH6 Pb10 Pb6 43.5(18) 2_666 2_666 ? Pb13 Pb10 Pb6 101.1(5) 1_455 2_666 ? Pb13 Pb10 Pb6 101.1(5) . 2_666 ? Cl2 Pb10 Pb6 70.7(4) 2_665 2_666 ? Cl2 Pb10 Pb6 162.6(9) . 2_666 ? Pb2 Pb10 Pb6 117.0(6) 1_556 2_666 ? Pb2 Pb10 Pb6 54.58(19) 2_666 2_666 ? Pb2 Pb10 Pb6 117.0(6) 1_456 2_666 ? Pb2 Pb10 Pb6 54.58(19) 2_766 2_666 ? Pb6 Pb10 Pb6 91.9(6) 1_556 2_666 ? Pb12 Pb11 OH4 49.0(10) . 1_655 ? Pb12 Pb11 OH4 49.0(10) . 2_665 ? OH4 Pb11 OH4 98(2) 1_655 2_665 ? Pb12 Pb11 Cl1 76.2(4) . . ? OH4 Pb11 Cl1 81.0(3) 1_655 . ? OH4 Pb11 Cl1 81.0(3) 2_665 . ? Pb12 Pb11 Cl1 76.2(4) . 2_765 ? OH4 Pb11 Cl1 81.0(3) 1_655 2_765 ? OH4 Pb11 Cl1 81.0(3) 2_665 2_765 ? Cl1 Pb11 Cl1 152.4(8) . 2_765 ? Pb12 Pb11 OH6 148.9(17) . 4_565 ? OH4 Pb11 OH6 152.0(17) 1_655 4_565 ? OH4 Pb11 OH6 104(2) 2_665 4_565 ? Cl1 Pb11 OH6 119.3(13) . 4_565 ? Cl1 Pb11 OH6 85.4(14) 2_765 4_565 ? Pb12 Pb11 OH6 148.9(17) . 3_755 ? OH4 Pb11 OH6 104(2) 1_655 3_755 ? OH4 Pb11 OH6 152.0(17) 2_665 3_755 ? Cl1 Pb11 OH6 85.4(14) . 3_755 ? Cl1 Pb11 OH6 119.3(13) 2_765 3_755 ? OH6 Pb11 OH6 62(3) 4_565 3_755 ? Pb12 Pb11 OH6 148.9(17) . . ? OH4 Pb11 OH6 152.0(17) 1_655 . ? OH4 Pb11 OH6 104(2) 2_665 . ? Cl1 Pb11 OH6 85.4(14) . . ? Cl1 Pb11 OH6 119.3(13) 2_765 . ? OH6 Pb11 OH6 34(3) 4_565 . ? OH6 Pb11 OH6 50(3) 3_755 . ? Pb12 Pb11 OH6 148.9(17) . 2_765 ? OH4 Pb11 OH6 104(2) 1_655 2_765 ? OH4 Pb11 OH6 152.0(17) 2_665 2_765 ? Cl1 Pb11 OH6 119.3(13) . 2_765 ? Cl1 Pb11 OH6 85.4(14) 2_765 2_765 ? OH6 Pb11 OH6 50(3) 4_565 2_765 ? OH6 Pb11 OH6 34(3) 3_755 2_765 ? OH6 Pb11 OH6 62(3) . 2_765 ? Pb12 Pb11 Mg 20.7(5) . 2_765 ? OH4 Pb11 Mg 28.3(11) 1_655 2_765 ? OH4 Pb11 Mg 69.8(11) 2_665 2_765 ? Cl1 Pb11 Mg 77.1(4) . 2_765 ? Cl1 Pb11 Mg 77.1(4) 2_765 2_765 ? OH6 Pb11 Mg 162.1(14) 4_565 2_765 ? OH6 Pb11 Mg 130.5(18) 3_755 2_765 ? OH6 Pb11 Mg 162.1(14) . 2_765 ? OH6 Pb11 Mg 130.5(18) 2_765 2_765 ? Pb12 Pb11 Mg 20.7(5) . . ? OH4 Pb11 Mg 69.8(11) 1_655 . ? OH4 Pb11 Mg 28.3(11) 2_665 . ? Cl1 Pb11 Mg 77.1(4) . . ? Cl1 Pb11 Mg 77.1(4) 2_765 . ? OH6 Pb11 Mg 130.5(18) 4_565 . ? OH6 Pb11 Mg 162.1(14) 3_755 . ? OH6 Pb11 Mg 130.5(18) . . ? OH6 Pb11 Mg 162.1(14) 2_765 . ? Mg Pb11 Mg 41.5(9) 2_765 . ? Pb12 Pb11 Pb6 108.34(11) . 2_665 ? OH4 Pb11 Pb6 134.5(3) 1_655 2_665 ? OH4 Pb11 Pb6 73.2(7) 2_665 2_665 ? Cl1 Pb11 Pb6 137.86(9) . 2_665 ? Cl1 Pb11 Pb6 53.8(2) 2_765 2_665 ? OH6 Pb11 Pb6 41.5(16) 4_565 2_665 ? OH6 Pb11 Pb6 102.2(16) 3_755 2_665 ? OH6 Pb11 Pb6 69.7(13) . 2_665 ? OH6 Pb11 Pb6 79.0(15) 2_765 2_665 ? Mg Pb11 Pb6 121.8(3) 2_765 2_665 ? Mg Pb11 Pb6 93.5(3) . 2_665 ? Pb12 Pb11 Pb6 108.34(11) . 1_655 ? OH4 Pb11 Pb6 73.2(7) 1_655 1_655 ? OH4 Pb11 Pb6 134.5(3) 2_665 1_655 ? Cl1 Pb11 Pb6 53.8(2) . 1_655 ? Cl1 Pb11 Pb6 137.86(9) 2_765 1_655 ? OH6 Pb11 Pb6 102.2(16) 4_565 1_655 ? OH6 Pb11 Pb6 41.5(16) 3_755 1_655 ? OH6 Pb11 Pb6 79.0(15) . 1_655 ? OH6 Pb11 Pb6 69.7(13) 2_765 1_655 ? Mg Pb11 Pb6 93.5(3) 2_765 1_655 ? Mg Pb11 Pb6 121.8(3) . 1_655 ? Pb6 Pb11 Pb6 143.3(2) 2_665 1_655 ? Pb12 Pb11 Pb6 108.34(11) . 2_765 ? OH4 Pb11 Pb6 73.2(7) 1_655 2_765 ? OH4 Pb11 Pb6 134.5(3) 2_665 2_765 ? Cl1 Pb11 Pb6 137.86(9) . 2_765 ? Cl1 Pb11 Pb6 53.8(2) 2_765 2_765 ? OH6 Pb11 Pb6 79.0(15) 4_565 2_765 ? OH6 Pb11 Pb6 69.7(13) 3_755 2_765 ? OH6 Pb11 Pb6 102.2(16) . 2_765 ? OH6 Pb11 Pb6 41.5(16) 2_765 2_765 ? Mg Pb11 Pb6 93.5(3) 2_765 2_765 ? Mg Pb11 Pb6 121.8(3) . 2_765 ? Pb6 Pb11 Pb6 81.97(9) 2_665 2_765 ? Pb6 Pb11 Pb6 86.65(11) 1_655 2_765 ? Pb12 Pb11 Pb6 108.34(11) . . ? OH4 Pb11 Pb6 134.5(3) 1_655 . ? OH4 Pb11 Pb6 73.2(7) 2_665 . ? Cl1 Pb11 Pb6 53.8(2) . . ? Cl1 Pb11 Pb6 137.86(9) 2_765 . ? OH6 Pb11 Pb6 69.7(13) 4_565 . ? OH6 Pb11 Pb6 79.0(15) 3_755 . ? OH6 Pb11 Pb6 41.5(16) . . ? OH6 Pb11 Pb6 102.2(16) 2_765 . ? Mg Pb11 Pb6 121.8(3) 2_765 . ? Mg Pb11 Pb6 93.5(3) . . ? Pb6 Pb11 Pb6 86.65(11) 2_665 . ? Pb6 Pb11 Pb6 81.97(9) 1_655 . ? Pb6 Pb11 Pb6 143.3(2) 2_765 . ? Pb11 Pb12 OH4 104.6(14) . 1_655 ? Pb11 Pb12 OH4 104.6(14) . 2_665 ? OH4 Pb12 OH4 151(3) 1_655 2_665 ? Pb11 Pb12 OH1 147.6(10) . 2_765 ? OH4 Pb12 OH1 77.7(12) 1_655 2_765 ? OH4 Pb12 OH1 77.7(12) 2_665 2_765 ? Pb11 Pb12 OH1 147.6(10) . . ? OH4 Pb12 OH1 77.7(12) 1_655 . ? OH4 Pb12 OH1 77.7(12) 2_665 . ? OH1 Pb12 OH1 65(2) 2_765 . ? Pb11 Pb12 Cl1 82.0(5) . . ? OH4 Pb12 Cl1 92.0(2) 1_655 . ? OH4 Pb12 Cl1 92.0(2) 2_665 . ? OH1 Pb12 Cl1 65.7(10) 2_765 . ? OH1 Pb12 Cl1 130.4(11) . . ? Pb11 Pb12 Cl1 82.0(5) . 2_765 ? OH4 Pb12 Cl1 92.0(2) 1_655 2_765 ? OH4 Pb12 Cl1 92.0(2) 2_665 2_765 ? OH1 Pb12 Cl1 130.4(11) 2_765 2_765 ? OH1 Pb12 Cl1 65.7(10) . 2_765 ? Cl1 Pb12 Cl1 163.9(9) . 2_765 ? Pb11 Pb12 Mg 151.9(6) . 2_765 ? OH4 Pb12 Mg 47.4(15) 1_655 2_765 ? OH4 Pb12 Mg 103.5(15) 2_665 2_765 ? OH1 Pb12 Mg 41.8(8) 2_765 2_765 ? OH1 Pb12 Mg 41.8(8) . 2_765 ? Cl1 Pb12 Mg 97.1(4) . 2_765 ? Cl1 Pb12 Mg 97.1(4) 2_765 2_765 ? Pb11 Pb12 Mg 151.9(6) . . ? OH4 Pb12 Mg 103.5(15) 1_655 . ? OH4 Pb12 Mg 47.4(15) 2_665 . ? OH1 Pb12 Mg 41.8(8) 2_765 . ? OH1 Pb12 Mg 41.8(8) . . ? Cl1 Pb12 Mg 97.1(4) . . ? Cl1 Pb12 Mg 97.1(4) 2_765 . ? Mg Pb12 Mg 56.1(13) 2_765 . ? Pb11 Pb12 Pb1 108.45(17) . 1_655 ? OH4 Pb12 Pb1 45.2(3) 1_655 1_655 ? OH4 Pb12 Pb1 123.1(8) 2_665 1_655 ? OH1 Pb12 Pb1 50.3(5) 2_765 1_655 ? OH1 Pb12 Pb1 96.0(8) . 1_655 ? Cl1 Pb12 Pb1 49.9(2) . 1_655 ? Cl1 Pb12 Pb1 137.05(16) 2_765 1_655 ? Mg Pb12 Pb1 54.3(3) 2_765 1_655 ? Mg Pb12 Pb1 91.4(5) . 1_655 ? Pb11 Pb12 Pb1 108.45(17) . 2_665 ? OH4 Pb12 Pb1 123.1(8) 1_655 2_665 ? OH4 Pb12 Pb1 45.2(3) 2_665 2_665 ? OH1 Pb12 Pb1 96.0(8) 2_765 2_665 ? OH1 Pb12 Pb1 50.3(5) . 2_665 ? Cl1 Pb12 Pb1 137.05(16) . 2_665 ? Cl1 Pb12 Pb1 49.9(2) 2_765 2_665 ? Mg Pb12 Pb1 91.4(5) 2_765 2_665 ? Mg Pb12 Pb1 54.3(3) . 2_665 ? Pb1 Pb12 Pb1 143.1(3) 1_655 2_665 ? Pb11 Pb12 Pb1 108.45(17) . 2_765 ? OH4 Pb12 Pb1 45.2(3) 1_655 2_765 ? OH4 Pb12 Pb1 123.1(8) 2_665 2_765 ? OH1 Pb12 Pb1 96.0(8) 2_765 2_765 ? OH1 Pb12 Pb1 50.3(5) . 2_765 ? Cl1 Pb12 Pb1 137.05(16) . 2_765 ? Cl1 Pb12 Pb1 49.9(2) 2_765 2_765 ? Mg Pb12 Pb1 54.3(3) 2_765 2_765 ? Mg Pb12 Pb1 91.4(5) . 2_765 ? Pb1 Pb12 Pb1 87.98(12) 1_655 2_765 ? Pb1 Pb12 Pb1 80.50(10) 2_665 2_765 ? Pb11 Pb12 Pb1 108.45(17) . . ? OH4 Pb12 Pb1 123.1(8) 1_655 . ? OH4 Pb12 Pb1 45.2(3) 2_665 . ? OH1 Pb12 Pb1 50.3(5) 2_765 . ? OH1 Pb12 Pb1 96.0(8) . . ? Cl1 Pb12 Pb1 49.9(2) . . ? Cl1 Pb12 Pb1 137.05(16) 2_765 . ? Mg Pb12 Pb1 91.4(5) 2_765 . ? Mg Pb12 Pb1 54.3(3) . . ? Pb1 Pb12 Pb1 80.50(10) 1_655 . ? Pb1 Pb12 Pb1 87.98(12) 2_665 . ? Pb1 Pb12 Pb1 143.1(3) 2_765 . ? OH3 Pb13 OH3 58(2) . 2_765 ? OH3 Pb13 Pb9 117.7(15) . 1_655 ? OH3 Pb13 Pb9 59.4(12) 2_765 1_655 ? OH3 Pb13 Pb9 59.4(12) . . ? OH3 Pb13 Pb9 117.7(15) 2_765 . ? Pb9 Pb13 Pb9 177.0(12) 1_655 . ? OH3 Pb13 Pb10 135.2(16) . 1_655 ? OH3 Pb13 Pb10 76.9(13) 2_765 1_655 ? Pb9 Pb13 Pb10 17.6(6) 1_655 1_655 ? Pb9 Pb13 Pb10 165.4(13) . 1_655 ? OH3 Pb13 Pb10 76.9(13) . . ? OH3 Pb13 Pb10 135.2(16) 2_765 . ? Pb9 Pb13 Pb10 165.4(13) 1_655 . ? Pb9 Pb13 Pb10 17.6(6) . . ? Pb10 Pb13 Pb10 147.8(16) 1_655 . ? OH3 Pb13 OH6 163.0(13) . 3_756 ? OH3 Pb13 OH6 123.4(19) 2_765 3_756 ? Pb9 Pb13 OH6 66.8(15) 1_655 3_756 ? Pb9 Pb13 OH6 116.0(17) . 3_756 ? Pb10 Pb13 OH6 50.3(16) 1_655 3_756 ? Pb10 Pb13 OH6 99.3(18) . 3_756 ? OH3 Pb13 OH6 163.0(13) . 2_766 ? OH3 Pb13 OH6 123.4(18) 2_765 2_766 ? Pb9 Pb13 OH6 66.8(15) 1_655 2_766 ? Pb9 Pb13 OH6 116.0(17) . 2_766 ? Pb10 Pb13 OH6 50.3(16) 1_655 2_766 ? Pb10 Pb13 OH6 99.3(18) . 2_766 ? OH6 Pb13 OH6 33(3) 3_756 2_766 ? OH3 Pb13 OH6 123.4(18) . 1_556 ? OH3 Pb13 OH6 163.0(13) 2_765 1_556 ? Pb9 Pb13 OH6 116.0(17) 1_655 1_556 ? Pb9 Pb13 OH6 66.8(15) . 1_556 ? Pb10 Pb13 OH6 99.3(18) 1_655 1_556 ? Pb10 Pb13 OH6 50.3(16) . 1_556 ? OH6 Pb13 OH6 49(3) 3_756 1_556 ? OH6 Pb13 OH6 61(3) 2_766 1_556 ? OH3 Pb13 OH6 123.4(19) . 4_566 ? OH3 Pb13 OH6 163.0(13) 2_765 4_566 ? Pb9 Pb13 OH6 116.0(17) 1_655 4_566 ? Pb9 Pb13 OH6 66.8(15) . 4_566 ? Pb10 Pb13 OH6 99.3(18) 1_655 4_566 ? Pb10 Pb13 OH6 50.3(16) . 4_566 ? OH6 Pb13 OH6 61(3) 3_756 4_566 ? OH6 Pb13 OH6 49(3) 2_766 4_566 ? OH6 Pb13 OH6 33(3) 1_556 4_566 ? OH3 Pb13 Pb2 109.0(4) . 1_556 ? OH3 Pb13 Pb2 109.0(4) 2_765 1_556 ? Pb9 Pb13 Pb2 90.5(2) 1_655 1_556 ? Pb9 Pb13 Pb2 90.5(2) . 1_556 ? Pb10 Pb13 Pb2 84.1(4) 1_655 1_556 ? Pb10 Pb13 Pb2 84.1(4) . 1_556 ? OH6 Pb13 Pb2 54.1(13) 3_756 1_556 ? OH6 Pb13 Pb2 86.8(14) 2_766 1_556 ? OH6 Pb13 Pb2 54.1(13) 1_556 1_556 ? OH6 Pb13 Pb2 86.8(14) 4_566 1_556 ? OH3 Pb13 Pb2 109.0(4) . 2_766 ? OH3 Pb13 Pb2 109.0(4) 2_765 2_766 ? Pb9 Pb13 Pb2 90.5(2) 1_655 2_766 ? Pb9 Pb13 Pb2 90.5(2) . 2_766 ? Pb10 Pb13 Pb2 84.1(4) 1_655 2_766 ? Pb10 Pb13 Pb2 84.1(4) . 2_766 ? OH6 Pb13 Pb2 86.8(14) 3_756 2_766 ? OH6 Pb13 Pb2 54.1(13) 2_766 2_766 ? OH6 Pb13 Pb2 86.8(14) 1_556 2_766 ? OH6 Pb13 Pb2 54.1(13) 4_566 2_766 ? Pb2 Pb13 Pb2 136.3(9) 1_556 2_766 ? OH3 Pb13 Pb3 55.4(6) . 2_765 ? OH3 Pb13 Pb3 55.4(6) 2_765 2_765 ? Pb9 Pb13 Pb3 89.0(4) 1_655 2_765 ? Pb9 Pb13 Pb3 89.0(4) . 2_765 ? Pb10 Pb13 Pb3 100.4(5) 1_655 2_765 ? Pb10 Pb13 Pb3 100.4(5) . 2_765 ? OH6 Pb13 Pb3 141.1(13) 3_756 2_765 ? OH6 Pb13 Pb3 110.0(13) 2_766 2_765 ? OH6 Pb13 Pb3 141.1(13) 1_556 2_765 ? OH6 Pb13 Pb3 110.0(13) 4_566 2_765 ? Pb2 Pb13 Pb3 161.3(8) 1_556 2_765 ? Pb2 Pb13 Pb3 62.34(17) 2_766 2_765 ? OH3 Pb13 Pb3 55.4(6) . . ? OH3 Pb13 Pb3 55.4(6) 2_765 . ? Pb9 Pb13 Pb3 89.0(4) 1_655 . ? Pb9 Pb13 Pb3 89.0(4) . . ? Pb10 Pb13 Pb3 100.4(5) 1_655 . ? Pb10 Pb13 Pb3 100.4(5) . . ? OH6 Pb13 Pb3 110.0(13) 3_756 . ? OH6 Pb13 Pb3 141.1(13) 2_766 . ? OH6 Pb13 Pb3 110.0(13) 1_556 . ? OH6 Pb13 Pb3 141.1(13) 4_566 . ? Pb2 Pb13 Pb3 62.34(17) 1_556 . ? Pb2 Pb13 Pb3 161.3(8) 2_766 . ? Pb3 Pb13 Pb3 99.0(6) 2_765 . ? Pb12 Cl1 Pb11 21.8(3) . . ? Pb12 Cl1 Pb4 138.9(7) . . ? Pb11 Cl1 Pb4 160.7(7) . . ? Pb12 Cl1 Pb1 90.4(5) . 1_655 ? Pb11 Cl1 Pb1 101.8(5) . 1_655 ? Pb4 Cl1 Pb1 69.1(3) . 1_655 ? Pb12 Cl1 Pb1 90.4(5) . . ? Pb11 Cl1 Pb1 101.8(5) . . ? Pb4 Cl1 Pb1 69.1(3) . . ? Pb1 Cl1 Pb1 115.2(5) 1_655 . ? Pb9 Cl2 Pb10 16.4(5) . . ? Pb9 Cl2 Pb7 137.0(6) . 1_556 ? Pb10 Cl2 Pb7 120.6(8) . 1_556 ? Pb9 Cl2 Pb2 87.8(3) . 1_556 ? Pb10 Cl2 Pb2 79.3(4) . 1_556 ? Pb7 Cl2 Pb2 70.6(3) 1_556 1_556 ? Pb9 Cl2 Pb2 87.8(3) . 1_456 ? Pb10 Cl2 Pb2 79.3(4) . 1_456 ? Pb7 Cl2 Pb2 70.6(3) 1_556 1_456 ? Pb2 Cl2 Pb2 116.0(4) 1_556 1_456 ? Pb2 Cl3 Pb2 114.4(5) 2_776 1_556 ? Pb2 Cl3 Pb3 172.1(5) 2_776 . ? Pb2 Cl3 Pb3 73.53(9) 1_556 . ? Pb2 Cl3 Pb3 73.53(9) 2_776 2_775 ? Pb2 Cl3 Pb3 172.1(5) 1_556 2_775 ? Pb3 Cl3 Pb3 98.6(5) . 2_775 ? Pb2 Cl3 Pb7 73.9(2) 2_776 1_656 ? Pb2 Cl3 Pb7 73.9(2) 1_556 1_656 ? Pb3 Cl3 Pb7 109.54(7) . 1_656 ? Pb3 Cl3 Pb7 109.54(7) 2_775 1_656 ? Pb2 Cl3 Pb7 73.9(2) 2_776 1_556 ? Pb2 Cl3 Pb7 73.9(2) 1_556 1_556 ? Pb3 Cl3 Pb7 109.54(7) . 1_556 ? Pb3 Cl3 Pb7 109.54(7) 2_775 1_556 ? Pb7 Cl3 Pb7 118.3(5) 1_656 1_556 ? Pb1 Cl4 Pb1 109.9(6) 2_675 . ? Pb1 Cl4 Pb6 176.4(6) 2_675 . ? Pb1 Cl4 Pb6 73.74(8) . . ? Pb1 Cl4 Pb6 73.74(8) 2_675 2_675 ? Pb1 Cl4 Pb6 176.4(6) . 2_675 ? Pb6 Cl4 Pb6 102.6(6) . 2_675 ? Pb1 Cl4 Pb4 72.2(3) 2_675 . ? Pb1 Cl4 Pb4 72.2(3) . . ? Pb6 Cl4 Pb4 109.42(6) . . ? Pb6 Cl4 Pb4 109.42(6) 2_675 . ? Pb1 Cl4 Pb4 72.2(3) 2_675 1_455 ? Pb1 Cl4 Pb4 72.2(3) . 1_455 ? Pb6 Cl4 Pb4 109.42(6) . 1_455 ? Pb6 Cl4 Pb4 109.42(6) 2_675 1_455 ? Pb4 Cl4 Pb4 115.7(6) . 1_455 ? OH3 Mg OH2 89(2) . . ? OH3 Mg OH2 89(2) . 2_665 ? OH2 Mg OH2 82(2) . 2_665 ? OH3 Mg OH1 95(2) . 2_765 ? OH2 Mg OH1 174(2) . 2_765 ? OH2 Mg OH1 94.6(10) 2_665 2_765 ? OH3 Mg OH1 95(2) . . ? OH2 Mg OH1 94.6(10) . . ? OH2 Mg OH1 174(2) 2_665 . ? OH1 Mg OH1 89(2) 2_765 . ? OH3 Mg OH4 179(3) . 2_665 ? OH2 Mg OH4 90(2) . 2_665 ? OH2 Mg OH4 90(2) 2_665 2_665 ? OH1 Mg OH4 86(2) 2_765 2_665 ? OH1 Mg OH4 86(2) . 2_665 ? OH3 Mg Mg 81.4(17) . 2_765 ? OH2 Mg Mg 138.4(12) . 2_765 ? OH2 Mg Mg 138.4(12) 2_665 2_765 ? OH1 Mg Mg 46.5(11) 2_765 2_765 ? OH1 Mg Mg 46.5(11) . 2_765 ? OH4 Mg Mg 99.4(14) 2_665 2_765 ? OH3 Mg Mg 98.6(17) . 2_665 ? OH2 Mg Mg 41.6(12) . 2_665 ? OH2 Mg Mg 41.6(12) 2_665 2_665 ? OH1 Mg Mg 133.5(11) 2_765 2_665 ? OH1 Mg Mg 133.5(11) . 2_665 ? OH4 Mg Mg 80.6(14) 2_665 2_665 ? Mg Mg Mg 180.000(4) 2_765 2_665 ? OH3 Mg Pb12 143(2) . . ? OH2 Mg Pb12 117(2) . . ? OH2 Mg Pb12 117(2) 2_665 . ? OH1 Mg Pb12 60.8(16) 2_765 . ? OH1 Mg Pb12 60.8(16) . . ? OH4 Mg Pb12 37.5(13) 2_665 . ? Mg Mg Pb12 61.9(6) 2_765 . ? Mg Mg Pb12 118.1(6) 2_665 . ? OH3 Mg Pb1 113.8(9) . 2_665 ? OH2 Mg Pb1 35.9(15) . 2_665 ? OH2 Mg Pb1 107.4(15) 2_665 2_665 ? OH1 Mg Pb1 143.5(19) 2_765 2_665 ? OH1 Mg Pb1 67.3(10) . 2_665 ? OH4 Mg Pb1 65.9(7) 2_665 2_665 ? Mg Mg Pb1 113.5(4) 2_765 2_665 ? Mg Mg Pb1 66.5(5) 2_665 2_665 ? Pb12 Mg Pb1 83.2(7) . 2_665 ? OH3 Mg Pb1 113.8(9) . . ? OH2 Mg Pb1 107.4(14) . . ? OH2 Mg Pb1 35.9(15) 2_665 . ? OH1 Mg Pb1 67.3(10) 2_765 . ? OH1 Mg Pb1 143.5(19) . . ? OH4 Mg Pb1 65.9(7) 2_665 . ? Mg Mg Pb1 113.5(5) 2_765 . ? Mg Mg Pb1 66.5(4) 2_665 . ? Pb12 Mg Pb1 83.2(7) . . ? Pb1 Mg Pb1 116.2(9) 2_665 . ? OH3 Mg Pb3 66.0(8) . . ? OH2 Mg Pb3 144(2) . . ? OH2 Mg Pb3 72.1(11) 2_665 . ? OH1 Mg Pb3 36.9(14) 2_765 . ? OH1 Mg Pb3 113.2(14) . . ? OH4 Mg Pb3 114.3(8) 2_665 . ? Mg Mg Pb3 67.0(5) 2_765 . ? Mg Mg Pb3 113.0(4) 2_665 . ? Pb12 Mg Pb3 97.3(6) . . ? Pb1 Mg Pb3 179.5(10) 2_665 . ? Pb1 Mg Pb3 63.60(3) . . ? Pb3 O1 Pb1 119.1(7) . . ? Pb3 O1 Pb5 115.1(17) . . ? Pb1 O1 Pb5 103.9(16) . . ? Pb3 O1 Pb4 100.5(15) . . ? Pb1 O1 Pb4 110.3(16) . . ? Pb5 O1 Pb4 107.5(6) . . ? Pb2 O2 Pb6 118.4(9) . . ? Pb2 O2 Pb8 104(2) . . ? Pb6 O2 Pb8 114(2) . . ? Pb2 O2 Pb7 114(2) . . ? Pb6 O2 Pb7 102(2) . . ? Pb8 O2 Pb7 104.5(7) . . ? Mg OH1 Mg 87(2) 2_765 . ? Mg OH1 Pb3 111.2(19) 2_765 2_765 ? Mg OH1 Pb3 111.2(19) . 2_765 ? Mg OH1 Pb12 77.4(17) 2_765 . ? Mg OH1 Pb12 77.4(17) . . ? Pb3 OH1 Pb12 168(2) 2_765 . ? Mg OH2 Mg 97(2) . 2_665 ? Mg OH2 Pb1 115(2) . 2_665 ? Mg OH2 Pb1 115(2) 2_665 2_665 ? Mg OH3 Pb13 159(3) . . ? Mg OH3 Pb9 130(2) . . ? Pb13 OH3 Pb9 70.6(12) . . ? Pb12 OH4 Mg 95(2) 1_455 2_665 ? Pb12 OH4 Pb11 26.4(7) 1_455 1_455 ? Mg OH4 Pb11 122(2) 2_665 1_455 ? OH6 OH5 OH6 134(6) . 3_655 ? OH6 OH5 Pb10 86(3) . 1_554 ? OH6 OH5 Pb10 86(3) 3_655 1_554 ? OH6 OH5 Pb6 94(3) . . ? OH6 OH5 Pb6 94(3) 3_655 . ? Pb10 OH5 Pb6 180(3) 1_554 . ? OH6 OH5 Pb9 91(3) . 1_554 ? OH6 OH5 Pb9 91(3) 3_655 1_554 ? Pb10 OH5 Pb9 14.0(9) 1_554 1_554 ? Pb6 OH5 Pb9 166(3) . 1_554 ? OH6 OH6 OH5 109(3) 4_565 . ? OH6 OH6 Pb10 70.2(15) 4_565 1_554 ? OH5 OH6 Pb10 51(3) . 1_554 ? OH6 OH6 Pb2 138.8(17) 4_565 . ? OH5 OH6 Pb2 93(3) . . ? Pb10 OH6 Pb2 101(3) 1_554 . ? OH6 OH6 Pb6 137.3(16) 4_565 . ? OH5 OH6 Pb6 49(3) . . ? Pb10 OH6 Pb6 100(2) 1_554 . ? Pb2 OH6 Pb6 83.3(17) . . ? OH6 OH6 Pb11 73.0(13) 4_565 . ? OH5 OH6 Pb11 133(5) . . ? Pb10 OH6 Pb11 140(3) 1_554 . ? Pb2 OH6 Pb11 117(3) . . ? Pb6 OH6 Pb11 97(3) . . ? OH6 OH6 Pb13 73.4(13) 4_565 1_554 ? OH5 OH6 Pb13 106(4) . 1_554 ? Pb10 OH6 Pb13 65(2) 1_554 1_554 ? Pb2 OH6 Pb13 67(2) . 1_554 ? Pb6 OH6 Pb13 141(3) . 1_554 ? Pb11 OH6 Pb13 119(2) . 1_554 ? _diffrn_measured_fraction_theta_max 0.963 _diffrn_reflns_theta_full 26.93 _diffrn_measured_fraction_theta_full 0.963 _refine_diff_density_max 5.918 _refine_diff_density_min -2.952 _refine_diff_density_rms 0.545