# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_shelxl _shelx_title ' siuk875m in P21/m N.1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 214.46 _exptl_crystal_F_000 442.89 _reflns_d_resolution_high 0.6202 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' '-x, -y, -z' 'x, -y-1/2, z' _cell_length_a 7.5764 _cell_length_b 5.9507 _cell_length_c 8.8050 _cell_angle_alpha 90.000 _cell_angle_beta 112.551 _cell_angle_gamma 90.000 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 1 0 0 33.49 19.44 12.56 o 2 0 0 4191.63 4261.04 87.88 o 3 0 0 5811.39 5629.49 133.88 o 4 0 0 9809.58 9900.21 142.11 o 5 0 0 45.31 47.24 6.40 o 6 0 0 757.85 683.65 18.92 o 7 0 0 1471.83 1405.42 31.26 o 8 0 0 220.76 259.83 24.64 o 9 0 0 571.66 565.21 78.34 o 10 0 0 228.58 173.57 29.74 o 11 0 0 9.89 40.23 28.00 o 1 1 0 729.94 690.63 7.01 o 2 1 0 238.65 216.37 5.38 o 3 1 0 157.19 136.29 3.75 o 4 1 0 2455.92 2385.26 23.06 o 5 1 0 14093.43 14587.00 114.49 o 6 1 0 175.07 151.00 9.43 o 7 1 0 261.23 208.34 11.79 o 8 1 0 1877.48 1901.18 38.85 o 9 1 0 938.15 917.63 29.58 o 10 1 0 5.84 7.42 14.73 o 11 1 0 1.63 14.35 18.11 o 0 2 0 38983.22 41799.98 477.26 o 1 2 0 1764.72 1835.20 17.36 o 2 2 0 4111.97 4472.47 36.96 o 3 2 0 1361.27 1317.83 16.36 o 4 2 0 116.13 110.21 5.63 o 5 2 0 238.39 220.62 8.18 o 6 2 0 396.44 385.33 11.51 o 7 2 0 493.48 444.00 13.81 o 8 2 0 1646.13 1552.81 37.61 o 9 2 0 222.39 223.63 19.59 o 10 2 0 874.75 874.16 39.47 o 11 2 0 53.22 49.89 18.59 o 1 3 0 386.07 379.23 8.97 o 2 3 0 222.25 217.65 6.35 o 3 3 0 432.58 451.58 10.26 o 4 3 0 1597.93 1570.11 20.91 o 5 3 0 10742.28 11373.54 102.13 o 6 3 0 146.40 126.15 9.21 o 7 3 0 122.57 121.88 11.76 o 8 3 0 1457.73 1478.30 35.78 o 9 3 0 816.35 791.28 30.16 o 10 3 0 6.65 7.66 16.01 o 0 4 0 45992.47 49280.95 483.10 o 1 4 0 21.80 21.62 2.91 o 2 4 0 1297.55 1277.93 14.99 o 3 4 0 3478.87 3652.45 37.33 o 4 4 0 3719.57 3851.58 45.67 o 5 4 0 74.86 73.99 8.47 o 6 4 0 404.33 389.23 15.78 o 7 4 0 934.18 871.98 24.08 o 8 4 0 169.85 141.66 18.14 o 9 4 0 400.03 398.66 25.96 o 10 4 0 147.49 142.15 21.94 o 1 5 0 100.68 94.69 5.79 o 2 5 0 110.85 113.79 6.91 o 3 5 0 285.26 284.50 9.36 o 4 5 0 991.81 948.92 19.97 o 5 5 0 5422.62 5571.70 65.09 o 6 5 0 63.08 69.35 11.50 o 7 5 0 119.02 107.02 14.63 o 8 5 0 835.97 864.72 27.27 o 9 5 0 403.06 411.15 27.57 o 0 6 0 7996.80 8259.60 156.04 o 1 6 0 483.98 478.70 12.42 o 2 6 0 304.36 284.46 12.37 o 3 6 0 512.66 473.88 14.21 o 4 6 0 53.80 61.77 19.31 o 5 6 0 63.20 52.10 12.36 o 6 6 0 73.25 72.77 14.65 o 7 6 0 167.08 171.52 19.37 o 8 6 0 688.43 714.51 30.78 o 1 7 0 44.04 47.15 9.63 o 2 7 0 80.72 81.09 9.55 o 3 7 0 310.48 262.90 16.05 o 4 7 0 393.19 377.14 19.70 o 5 7 0 2993.21 3161.47 53.39 o 6 7 0 52.18 49.59 17.27 o 7 7 0 9.77 12.07 18.39 o 0 8 0 6727.94 7553.95 184.82 o 1 8 0 12.13 13.63 11.00 o 2 8 0 231.66 240.34 15.16 o 3 8 0 902.58 925.43 28.80 o 4 8 0 594.29 529.69 23.66 o 5 8 0 53.42 45.73 17.50 o 6 8 0 107.60 149.13 20.84 o 1 9 0 5.85 1.89 16.36 o 2 9 0 22.89 38.65 28.51 o 3 9 0 109.64 61.30 17.28 o -11 0 1 489.80 514.51 105.67 o -10 0 1 1611.10 1610.69 58.40 o -9 0 1 145.67 113.60 23.34 o -8 0 1 173.23 175.19 21.02 o -7 0 1 7549.94 7668.36 103.62 o -6 0 1 91.47 94.12 13.78 o -5 0 1 3116.36 3061.52 115.10 o -4 0 1 37.53 33.93 3.27 o -3 0 1 24.36 17.96 5.17 o -2 0 1 303.59 307.04 7.51 o -1 0 1 338.87 372.25 7.84 o 0 0 1 601.01 639.10 13.48 o 1 0 1 446.11 371.23 6.94 o 2 0 1 7482.84 7726.51 118.02 o 3 0 1 19840.87 20358.88 285.82 o 4 0 1 296.75 280.16 28.77 o 5 0 1 2046.45 1865.15 32.79 o 6 0 1 397.95 367.71 22.69 o 7 0 1 1235.31 1193.92 55.94 o 8 0 1 12.77 19.26 17.38 o 9 0 1 129.77 155.21 36.29 o 10 0 1 672.98 696.90 59.20 o -11 1 1 151.44 174.90 27.81 o -10 1 1 368.01 338.46 22.97 o -9 1 1 1351.11 1394.95 41.86 o -8 1 1 48.43 38.53 9.22 o -7 1 1 1.76 15.23 5.87 o -6 1 1 499.12 463.82 13.23 o -5 1 1 6589.52 6649.65 55.99 o -4 1 1 15.81 14.51 2.46 o -3 1 1 1080.99 1068.33 11.72 o -2 1 1 40311.96 42866.19 317.82 o -1 1 1 565.32 598.46 6.25 o 0 1 1 850.68 843.65 8.58 o 1 1 1 3620.84 3854.95 37.40 o 2 1 1 6425.86 6456.01 65.81 o 3 1 1 21.20 26.29 6.14 o 4 1 1 149.62 141.29 5.92 o 5 1 1 423.26 383.27 12.10 o 6 1 1 951.99 866.19 26.31 o 7 1 1 1051.97 996.98 33.72 o 8 1 1 1999.59 1913.14 40.36 o 9 1 1 244.73 247.13 20.88 o 10 1 1 89.13 89.84 19.25 o -11 2 1 238.28 212.55 22.72 o -10 2 1 900.83 928.00 32.70 o -9 2 1 392.00 371.54 18.30 o -8 2 1 2.74 27.07 13.11 o -7 2 1 4535.83 4520.96 49.06 o -6 2 1 655.47 639.82 11.69 o -5 2 1 869.25 810.62 18.11 o -4 2 1 268.47 274.96 13.19 o -3 2 1 789.85 836.29 10.45 o -2 2 1 358.48 318.00 13.16 o -1 2 1 1786.30 1871.96 21.27 o 0 2 1 4420.60 4872.36 38.51 o 1 2 1 7712.42 8323.21 70.53 o 2 2 1 838.60 794.20 13.35 o 3 2 1 35316.02 38599.34 348.33 o 4 2 1 520.59 480.74 11.87 o 5 2 1 40.67 39.11 6.27 o 6 2 1 2058.04 2060.99 31.42 o 7 2 1 3988.11 4058.54 61.02 o 8 2 1 189.69 167.52 17.23 o 9 2 1 78.87 53.17 15.94 o 10 2 1 1187.32 1143.00 37.09 o -11 3 1 147.57 186.30 26.44 o -10 3 1 349.66 313.83 24.04 o -9 3 1 1124.90 1169.92 39.09 o -8 3 1 11.51 12.85 9.25 o -7 3 1 6.57 9.37 7.36 o -6 3 1 221.65 211.14 11.09 o -5 3 1 4942.44 5174.51 51.87 o -4 3 1 97.03 87.42 6.88 o -3 3 1 410.01 371.81 6.41 o -2 3 1 20769.72 22404.18 179.82 o -1 3 1 277.71 265.30 13.74 o 0 3 1 42.51 35.08 3.71 o 1 3 1 2603.28 2708.34 26.87 o 2 3 1 2309.24 2224.19 23.67 o 3 3 1 5.93 12.99 3.20 o 4 3 1 12.10 12.46 5.35 o 5 3 1 450.90 410.80 13.50 o 6 3 1 969.39 967.73 21.88 o 7 3 1 947.35 963.47 24.01 o 8 3 1 1669.24 1681.49 43.32 o 9 3 1 149.07 162.14 16.74 o 10 3 1 53.47 53.68 16.85 o -10 4 1 1022.82 1067.83 42.18 o -9 4 1 74.58 68.33 16.87 o -8 4 1 119.55 113.89 16.84 o -7 4 1 4506.05 4616.79 75.64 o -6 4 1 105.45 99.55 9.12 o -5 4 1 1749.31 1862.63 25.76 o -4 4 1 36.54 42.51 4.39 o -3 4 1 142.88 139.36 6.83 o -2 4 1 74.15 68.09 8.07 o -1 4 1 172.24 168.47 5.38 o 0 4 1 287.32 266.51 15.81 o 1 4 1 178.59 182.76 5.35 o 2 4 1 2972.96 3114.64 32.46 o 3 4 1 9281.57 9657.87 85.97 o 4 4 1 105.53 102.24 13.45 o 5 4 1 823.78 788.68 36.72 o 6 4 1 300.65 288.10 14.86 o 7 4 1 744.77 735.18 22.86 o 8 4 1 8.98 12.90 13.26 o 9 4 1 70.03 89.09 16.35 o -9 5 1 576.86 546.81 34.29 o -8 5 1 49.90 37.48 13.80 o -7 5 1 0.80 12.59 10.78 o -6 5 1 379.34 353.62 22.87 o -5 5 1 2457.31 2489.29 32.56 o -4 5 1 49.84 37.37 7.33 o -3 5 1 218.74 208.00 10.10 o -2 5 1 14430.23 15591.90 213.17 o -1 5 1 247.91 234.51 11.06 o 0 5 1 589.86 581.41 11.13 o 1 5 1 1124.42 1132.28 14.82 o 2 5 1 2041.73 1990.91 26.61 o 3 5 1 34.26 36.15 5.49 o 4 5 1 127.69 125.15 10.10 o 5 5 1 183.56 168.26 12.04 o 6 5 1 427.49 415.40 18.09 o 7 5 1 460.84 442.00 23.09 o 8 5 1 887.07 886.24 27.17 o 9 5 1 137.11 152.34 20.46 o -9 6 1 143.05 152.70 26.52 o -8 6 1 2.45 0.86 19.88 o -7 6 1 1637.61 1649.21 45.08 o -6 6 1 374.53 361.01 28.05 o -5 6 1 278.65 273.04 21.50 o -4 6 1 98.79 93.04 11.62 o -3 6 1 92.13 86.59 8.28 o -2 6 1 209.01 193.41 10.13 o -1 6 1 230.51 188.54 9.78 o 0 6 1 1218.28 1239.84 37.28 o 1 6 1 1479.98 1539.45 22.52 o 2 6 1 186.20 190.55 9.94 o 3 6 1 9007.83 9365.60 96.89 o 4 6 1 215.13 223.12 13.48 o 5 6 1 23.04 30.41 11.14 o 6 6 1 889.57 938.46 37.69 o 7 6 1 1397.94 1432.50 35.38 o 8 6 1 95.46 112.38 17.58 o -8 7 1 1.11 0.00 22.00 o -7 7 1 9.18 9.07 20.18 o -6 7 1 45.29 33.57 18.84 o -5 7 1 1308.69 1350.59 40.18 o -4 7 1 20.97 5.30 13.72 o -3 7 1 43.28 41.97 12.59 o -2 7 1 4593.56 4753.25 56.75 o -1 7 1 79.79 87.42 11.74 o 0 7 1 11.04 7.02 9.38 o 1 7 1 637.35 660.40 18.57 o 2 7 1 301.76 264.71 18.53 o 3 7 1 3.55 0.00 10.00 o 4 7 1 1.63 6.68 12.41 o 5 7 1 174.27 181.02 19.03 o 6 7 1 413.00 399.27 23.94 o 7 7 1 342.09 330.64 25.12 o -6 8 1 42.88 41.47 18.90 o -5 8 1 468.68 482.71 27.75 o -4 8 1 14.05 12.82 13.46 o -3 8 1 51.10 53.32 13.76 o -2 8 1 9.16 7.90 11.24 o -1 8 1 58.53 61.42 16.76 o 0 8 1 59.48 64.62 16.85 o 1 8 1 54.81 40.31 11.35 o 2 8 1 567.03 598.61 23.10 o 3 8 1 1975.80 1951.17 40.58 o 4 8 1 17.17 9.10 15.46 o 5 8 1 108.50 122.43 19.38 o -4 9 1 47.73 22.12 16.04 o -3 9 1 18.66 13.63 22.16 o -2 9 1 2790.85 3082.91 79.51 o -1 9 1 42.70 35.82 18.93 o 0 9 1 180.93 181.45 21.10 o 1 9 1 216.14 229.03 23.41 o 2 9 1 355.63 367.63 25.66 o 3 9 1 7.41 25.99 15.37 o -11 0 2 281.21 270.53 42.25 o -10 0 2 1.59 3.38 17.77 o -9 0 2 1.53 5.98 11.94 o -8 0 2 358.08 320.47 16.74 o -7 0 2 3468.58 3450.28 54.36 o -6 0 2 205.32 175.21 10.63 o -5 0 2 169.13 166.24 8.78 o -4 0 2 30424.16 32008.84 378.63 o -3 0 2 864.98 799.98 12.45 o -2 0 2 614.09 536.00 8.97 o -1 0 2 31.24 29.99 25.30 o 0 0 2 2263.82 2172.68 41.24 o 1 0 2 1446.17 1485.42 19.15 o 2 0 2 1816.68 1977.15 24.81 o 3 0 2 13.31 19.76 3.55 o 4 0 2 3068.98 3113.24 39.08 o 5 0 2 651.71 605.76 15.02 o 6 0 2 4400.05 4345.01 65.01 o 7 0 2 447.67 422.02 28.37 o 8 0 2 2.86 12.38 21.20 o 9 0 2 543.21 507.17 38.33 o 10 0 2 1182.56 1141.68 55.58 o -11 1 2 223.82 273.52 23.13 o -10 1 2 114.04 120.02 15.14 o -9 1 2 2501.74 2524.39 40.51 o -8 1 2 749.35 778.56 23.74 o -7 1 2 629.64 597.18 12.18 o -6 1 2 237.18 217.98 7.04 o -5 1 2 321.12 276.59 8.15 o -4 1 2 85.47 77.52 5.88 o -3 1 2 231.13 256.07 4.87 o -2 1 2 5610.94 6149.96 75.13 o -1 1 2 1438.57 1504.22 13.77 o 0 1 2 2285.28 2467.17 27.35 o 1 1 2 35337.00 37412.60 329.36 o 2 1 2 135.41 137.78 6.50 o 3 1 2 132.71 109.68 5.56 o 4 1 2 1853.24 1729.80 30.90 o 5 1 2 3612.45 3658.68 53.58 o 6 1 2 104.64 82.70 10.44 o 7 1 2 16.67 18.39 9.58 o 8 1 2 1454.51 1381.84 29.64 o 9 1 2 409.97 399.06 36.54 o 10 1 2 203.22 203.63 24.24 o -11 2 2 781.12 758.18 68.18 o -10 2 2 26.06 17.41 13.08 o -9 2 2 300.27 285.82 19.26 o -8 2 2 424.38 425.02 16.56 o -7 2 2 6162.22 6523.81 58.82 o -6 2 2 226.83 210.18 8.29 o -5 2 2 299.30 276.80 7.37 o -4 2 2 19709.13 21214.50 162.28 o -3 2 2 64.35 76.79 14.42 o -2 2 2 91.40 97.37 3.44 o -1 2 2 2009.73 2085.54 18.73 o 0 2 2 180.74 154.48 3.76 o 1 2 2 59.33 51.37 8.54 o 2 2 2 513.23 511.13 8.20 o 3 2 2 1617.41 1660.63 30.50 o 4 2 2 2236.33 2244.14 40.72 o 5 2 2 2988.87 3168.40 40.58 o 6 2 2 2810.21 2790.24 45.81 o 7 2 2 14.37 25.05 9.80 o 8 2 2 87.31 101.72 12.97 o 9 2 2 42.98 29.29 15.74 o 10 2 2 669.08 713.84 32.39 o -11 3 2 162.75 123.36 21.56 o -10 3 2 110.12 106.45 15.96 o -9 3 2 1998.12 2059.28 44.50 o -8 3 2 498.22 498.52 16.41 o -7 3 2 510.63 509.03 17.39 o -6 3 2 120.91 126.97 8.25 o -5 3 2 173.67 150.89 7.30 o -4 3 2 40.42 40.59 3.47 o -3 3 2 43.11 48.93 3.47 o -2 3 2 3398.81 3581.26 31.60 o -1 3 2 1228.74 1283.40 13.87 o 0 3 2 1659.42 1721.90 18.62 o 1 3 2 24015.29 26348.11 199.07 o 2 3 2 78.39 87.73 4.35 o 3 3 2 232.65 201.62 6.37 o 4 3 2 1316.00 1323.73 21.99 o 5 3 2 3216.88 3385.23 43.70 o 6 3 2 76.73 85.42 9.60 o 7 3 2 42.28 41.98 11.98 o 8 3 2 1118.48 1098.47 28.21 o 9 3 2 271.68 270.15 19.27 o -10 4 2 1.23 22.47 17.43 o -9 4 2 0.89 6.17 12.82 o -8 4 2 181.85 168.73 12.98 o -7 4 2 2060.52 2067.02 30.80 o -6 4 2 133.61 121.81 9.09 o -5 4 2 134.15 141.78 14.33 o -4 4 2 13348.16 14174.76 112.55 o -3 4 2 523.63 492.50 18.39 o -2 4 2 205.66 194.75 6.46 o -1 4 2 45.65 45.21 3.95 o 0 4 2 970.20 910.97 22.87 o 1 4 2 710.15 727.74 16.24 o 2 4 2 371.25 331.43 8.01 o 3 4 2 0.17 8.28 3.68 o 4 4 2 1803.30 1821.14 31.06 o 5 4 2 407.89 398.31 13.31 o 6 4 2 2699.27 2647.21 36.45 o 7 4 2 280.77 318.95 17.46 o 8 4 2 1.47 2.79 13.01 o 9 4 2 342.89 356.12 21.45 o -10 5 2 60.15 64.71 20.67 o -9 5 2 1197.05 1240.26 36.37 o -8 5 2 360.10 376.10 17.11 o -7 5 2 306.87 300.28 14.47 o -6 5 2 123.37 130.35 12.97 o -5 5 2 77.95 88.29 8.01 o -4 5 2 86.82 100.63 7.23 o -3 5 2 41.30 45.66 5.72 o -2 5 2 2138.33 2167.89 25.17 o -1 5 2 343.15 346.77 8.30 o 0 5 2 775.24 811.87 15.53 o 1 5 2 10059.09 10902.94 96.32 o 2 5 2 58.53 64.12 5.92 o 3 5 2 5.08 16.07 6.15 o 4 5 2 801.70 837.04 20.24 o 5 5 2 1382.95 1366.75 27.08 o 6 5 2 26.05 39.08 11.78 o 7 5 2 0.82 12.95 11.90 o 8 5 2 782.27 764.35 29.66 o -9 6 2 120.39 105.64 21.31 o -8 6 2 180.50 175.01 19.22 o -7 6 2 2150.74 2238.96 48.02 o -6 6 2 20.47 28.88 12.52 o -5 6 2 44.59 43.86 11.18 o -4 6 2 6890.20 7134.19 88.17 o -3 6 2 3.55 3.96 7.11 o -2 6 2 160.18 188.27 10.47 o -1 6 2 595.58 605.21 16.71 o 0 6 2 623.46 608.52 13.57 o 1 6 2 3.90 11.23 5.52 o 2 6 2 283.20 266.55 10.77 o 3 6 2 308.77 296.66 21.20 o 4 6 2 603.58 567.40 20.31 o 5 6 2 985.96 1010.11 43.52 o 6 6 2 1014.63 1009.10 27.92 o 7 6 2 4.11 7.77 14.21 o 8 6 2 30.45 56.10 17.53 o -8 7 2 124.65 136.08 23.92 o -7 7 2 189.71 156.35 21.88 o -6 7 2 24.75 26.00 17.58 o -5 7 2 20.32 28.50 15.69 o -4 7 2 16.37 18.18 12.96 o -3 7 2 2.06 8.08 9.45 o -2 7 2 859.50 915.74 35.87 o -1 7 2 339.37 347.42 13.78 o 0 7 2 410.35 409.75 21.61 o 1 7 2 5482.43 5759.61 63.97 o 2 7 2 23.99 19.50 8.26 o 3 7 2 74.11 50.86 10.92 o 4 7 2 376.46 349.36 44.53 o 5 7 2 1045.53 1035.89 29.22 o 6 7 2 10.00 21.97 15.68 o -6 8 2 30.56 32.32 21.64 o -5 8 2 30.51 48.31 19.87 o -4 8 2 2629.40 2860.95 60.16 o -3 8 2 116.87 116.07 15.63 o -2 8 2 42.95 42.11 15.91 o -1 8 2 23.49 39.10 15.64 o 0 8 2 169.48 173.17 15.42 o 1 8 2 143.99 146.86 13.44 o 2 8 2 42.38 49.39 13.43 o 3 8 2 0.80 11.92 12.86 o 4 8 2 509.27 511.06 25.98 o 5 8 2 107.94 107.21 20.63 o -4 9 2 30.97 14.48 19.14 o -3 9 2 8.84 18.08 22.90 o -2 9 2 409.81 423.21 35.11 o -1 9 2 73.67 37.36 18.02 o 0 9 2 138.09 145.36 26.94 o 1 9 2 1692.86 1692.62 80.17 o 2 9 2 11.18 12.41 15.61 o -12 0 3 4.94 0.00 21.33 o -11 0 3 572.30 539.41 37.95 o -10 0 3 411.89 478.08 126.58 o -9 0 3 107.90 107.65 21.23 o -8 0 3 1360.17 1384.33 42.91 o -7 0 3 47.90 39.82 8.02 o -6 0 3 2223.50 2093.18 29.40 o -5 0 3 59.40 47.25 5.74 o -4 0 3 12873.07 13595.70 138.87 o -3 0 3 305.31 336.70 14.71 o -2 0 3 58.54 88.35 23.41 o -1 0 3 39053.27 41999.38 527.80 o 0 0 3 1782.15 1915.97 27.79 o 1 0 3 1545.30 1513.70 22.44 o 2 0 3 3159.93 3107.08 65.10 o 3 0 3 8222.18 8609.48 92.59 o 4 0 3 94.62 82.48 18.46 o 5 0 3 114.62 95.36 7.87 o 6 0 3 2554.81 2545.45 45.11 o 7 0 3 750.26 689.42 52.14 o 8 0 3 683.21 681.88 39.17 o 9 0 3 193.91 148.03 36.89 o 10 0 3 18.12 19.43 28.60 o -11 1 3 0.67 2.71 16.20 o -10 1 3 116.24 103.45 14.80 o -9 1 3 3114.35 3225.32 61.97 o -8 1 3 264.68 241.49 11.29 o -7 1 3 1.70 7.28 4.44 o -6 1 3 15179.90 15711.92 124.18 o -5 1 3 157.93 148.56 5.01 o -4 1 3 294.45 295.18 6.07 o -3 1 3 730.90 717.35 9.42 o -2 1 3 6768.88 7473.54 63.86 o -1 1 3 1197.43 1290.04 21.53 o 0 1 3 43.58 41.01 4.29 o 1 1 3 449.71 405.56 6.28 o 2 1 3 2082.19 2027.86 20.24 o 3 1 3 2504.08 2456.97 25.32 o 4 1 3 8577.29 8794.68 67.93 o 5 1 3 218.90 199.48 8.93 o 6 1 3 8.20 11.60 7.19 o 7 1 3 134.44 123.93 12.70 o 8 1 3 1909.52 1860.44 51.50 o 9 1 3 3.18 19.37 19.42 o -11 2 3 1068.27 1098.76 31.23 o -10 2 3 10.11 22.94 12.80 o -9 2 3 616.01 621.86 48.05 o -8 2 3 66.84 54.37 8.52 o -7 2 3 158.78 149.02 9.20 o -6 2 3 35.82 41.35 4.82 o -5 2 3 164.60 152.76 6.23 o -4 2 3 3187.37 3261.80 31.46 o -3 2 3 405.87 393.13 8.73 o -2 2 3 3106.89 3243.51 28.15 o -1 2 3 31027.47 33238.64 350.33 o 0 2 3 32.38 36.11 3.42 o 1 2 3 379.12 330.70 6.06 o 2 2 3 313.47 286.11 7.32 o 3 2 3 7565.78 7677.76 69.73 o 4 2 3 304.18 270.57 9.74 o 5 2 3 98.18 92.59 8.71 o 6 2 3 802.81 746.02 20.17 o 7 2 3 780.83 782.99 25.50 o 8 2 3 129.75 133.65 20.90 o 9 2 3 239.81 181.33 23.30 o -11 3 3 2.56 12.81 15.46 o -10 3 3 59.45 56.89 14.37 o -9 3 3 2577.24 2720.96 56.00 o -8 3 3 280.10 261.93 13.26 o -7 3 3 5.80 6.89 6.88 o -6 3 3 9729.48 10320.49 86.26 o -5 3 3 100.40 98.08 5.54 o -4 3 3 66.89 74.59 5.70 o -3 3 3 445.36 408.86 7.66 o -2 3 3 2683.53 2660.49 32.23 o -1 3 3 676.51 706.65 10.92 o 0 3 3 7.54 11.48 2.38 o 1 3 3 234.56 223.96 6.92 o 2 3 3 1943.56 2029.11 21.58 o 3 3 3 1977.97 1954.20 22.00 o 4 3 3 6565.66 6809.26 65.93 o 5 3 3 149.08 161.39 11.85 o 6 3 3 2.24 2.27 9.24 o 7 3 3 84.69 72.75 12.76 o 8 3 3 1530.45 1570.27 33.97 o 9 3 3 1.76 20.66 15.69 o -10 4 3 265.09 305.26 20.76 o -9 4 3 77.33 83.16 12.86 o -8 4 3 722.14 743.11 20.05 o -7 4 3 42.97 47.93 8.98 o -6 4 3 1025.40 1027.31 25.32 o -5 4 3 37.38 41.22 4.90 o -4 4 3 6103.70 6226.07 52.88 o -3 4 3 29.68 35.84 3.74 o 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