data_OXO-MANGANI-LEAKEITE _publ_contact_author ; Roberta Oberti ; _publ_contact_author_email ; oberti@crystal.unipv.it ; loop_ _publ_author_name _publ_author_address 'Oberti R.' 'CNR-IGG, U.O.S. Pavia, Pavia, Italy' 'Zanetti A.' 'CNR-IGG, U.O.S. Pavia, Pavia, Italy' 'Boiocchi M.' 'Centro Grandi Strumenti, University of Pavia, Pavia, Italy' 'Hawthorne F.C.' 'Dep. Geological Sciences, University of Manitoba, Winnipeg, Canada' 'Ball N.A.' 'Dep. Geological Sciences, University of Manitoba, Winnipeg, Canada' _publ_section_title ; ? ; _audit_creation_method 'manually entered' _chemical_name_systematic ? _chemical_name_common ? _chemical_name_mineral ; OXO-MANGANI-LEAKEITE ; _chemical_compound_source ; Hoskins mine, Grenfell, Forbes Co, New South Wales, Australia (Australian Map Grid Reference 8530-039487) ; _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_analytical ; Al0.05 Ca0.06 Fe3+0.44 H0.64 Li0.58 K0.36 Mg1.60 Mn3+2.32 Na2.59 Zn0.01 O24 Si7.98 Ti0.03 ; _chemical_formula_sum 'Ca0.07 K0.35 Li0.33 Mg1.82 Mn2.85 Na2.58 O24 Si8' _chemical_formula_weight 887.32 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O2-' 'O2-' 0.0080 0.0060 'Hovesteydt, 1982' 'Si' 'Si' 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Si4+' 'Si4+' 0.0820 0.0710 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mg2+' 'Mg2+' 0.0490 0.0360 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Mn3+' 'Mn3+' 0.3370 0.7290 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Li+' 'Li+' 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Ca2+' 'Ca2+' 0.2260 0.3060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Na+' 'Na+' 0.0360 0.0250 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'K+' 'K+' 0.1790 0.2500 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting monoclinic _symmetry_space_group_name_H-M 'C 2/m' _symmetry_space_group_name_Hall '-C 2y' _symmetry_Int_Tables_number 12 loop_ _space_group_symop_operation_xyz 'x, y, z' 'x, -y, z' 'x+1/2, y+1/2, z' 'x+1/2, -y+1/2, z' '-x, -y, -z' '-x, y, -z' '-x+1/2, -y+1/2, -z' '-x+1/2, y+1/2, -z' _cell_length_a 9.875(5) _cell_length_b 17.873(9) _cell_length_c 5.295(2) _cell_angle_alpha 90 _cell_angle_beta 104.74(3) _cell_angle_gamma 90 _cell_volume 903.8(7) _cell_formula_units_Z 2 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 60 _cell_measurement_theta_min 2 _cell_measurement_theta_max 35 _exptl_crystal_description 'irreglular prism' _exptl_crystal_colour 'red orange' _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_density_diffrn 3.25 _exptl_crystal_F_000 868.8 _exptl_crystal_size_max 0.13 _exptl_crystal_size_mid 0.08 _exptl_crystal_size_min 0.07 _exptl_absorpt_coefficient_mu 2.86 _exptl_absorpt_correction_type psi-scan _exptl_absorpt_correction_T_min 0.85 _exptl_absorpt_correction_T_max 0.94 _exptl_absorpt_process_details ; North A.C.T., Phillips D.C. & Mathews F.S. (1968) Acta. Cryst. A24, 351 ; _diffrn_radiation_probe 'x-ray' _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'PHILIPS PW1100' _diffrn_measurement_method 'omega scans' _diffrn_standards_number 3 _diffrn_standards_interval_count 400 _diffrn_standards_decay_% 0 _diffrn_reflns_number 2664 _diffrn_reflns_av_R_equivalents 0.031 _diffrn_reflns_limit_h_min -13 _diffrn_reflns_limit_h_max 13 _diffrn_reflns_limit_k_min -25 _diffrn_reflns_limit_k_max 25 _diffrn_reflns_limit_l_min 0 _diffrn_reflns_limit_l_max 7 _diffrn_reflns_theta_min 2 _diffrn_reflns_theta_max 30 _diffrn_reflns_theta_full 30 _diffrn_measured_fraction_theta_max 1.000 _reflns_number_total 1371 _reflns_number_gt 769 _reflns_threshold_expression 'I > 3\s(I)' _reflns_special_details ; Refinement of F against reflections with F > 3sigma(F). The threshold expression (_gt) of I > 3sigma(I) corresponds to the cutoff used to discriminate between observed and unobserved reflections for refinement. The use of unitary weigth produces unusual values for the calculated weighted wR-factor (similar to R). ; _computing_data_collection 'local program' _computing_cell_refinement 'LAT routine of PW1100 diffractometer' _computing_data_reduction 'local program' _computing_structure_refinement 'ORFLS (Busing et al., 1962), modified' _refine_special_details ? _refine_ls_structure_factor_coef F _refine_ls_matrix_type full _refine_ls_weighting_scheme unit _refine_ls_extinction_method 'secondary isotropic' _refine_ls_extinction_expression 'Zachariasen, 1967' _refine_ls_extinction_coef 0.000009(1) _refine_ls_number_reflns 769 _refine_ls_number_parameters 121 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0647 _refine_ls_R_factor_gt 0.0201 _refine_ls_wR_factor_ref 0.0647 _refine_ls_wR_factor_gt 0.0203 _refine_ls_restrained_S_all 1.55 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group O1A O 0.11263(25) 0.08887(12) 0.21149(48) 0.0125(7) Uani 0.24(16) 1 d . . P . . O1B O2- 0.11263(25) 0.08887(12) 0.21149(48) 0.0125(7) Uani 0.76(16) 1 d . . P . . O2A O 0.11944(22) 0.16649(13) 0.72061(45) 0.0118(7) Uani 0.24(15) 1 d . . P . . O2B O2- 0.11944(22) 0.16649(13) 0.72061(45) 0.0118(7) Uani 0.76(15) 1 d . . P . . O3A O 0.10787(35) 0.0000 0.70332(69) 0.0137(10) Uani 0.01(10) 2 d S T P . . O3B O2- 0.10787(35) 0.0000 0.70332(69) 0.0137(10) Uani 0.99(10) 2 d S T P . . O4A O 0.35918(26) 0.24965(12) 0.79938(50) 0.0148(7) Uani 0.29(15) 1 d . . P . . O4B O2- 0.35918(26) 0.24965(12) 0.79938(50) 0.0148(7) Uani 0.71(15) 1 d . . P . . O5A O 0.34828(24) 0.12752(11) 0.08029(47) 0.0109(6) Uani 0.33(14) 1 d . . P . . O5B O2- 0.34828(24) 0.12752(11) 0.08029(47) 0.0109(6) Uani 0.67(14) 1 d . . P . . O6A O 0.34510(24) 0.11867(11) 0.58238(45) 0.0112(6) Uani 0.44(14) 1 d . . P . . O6B O2- 0.34510(24) 0.11867(11) 0.58238(45) 0.0112(6) Uani 0.56(14) 1 d . . P . . O7A O 0.33694(36) 0.0000 0.29630(69) 0.0156(10) Uani 0.40(11) 2 d S T P . . O7B O2- 0.33694(36) 0.0000 0.29630(69) 0.0156(10) Uani 0.60(11) 2 d S T P . . T1A Si 0.27993(9) 0.08588(4) 0.29089(18) 0.0070(2) Uani 0.78(13) 1 d . . P . . T1B Si4+ 0.27993(9) 0.08588(4) 0.29089(18) 0.0070(2) Uani 0.22(13) 1 d . . P . . T2A Si 0.28841(8) 0.17033(4) 0.79675(17) 0.0072(2) Uani 0.79(13) 1 d . . P . . T2B Si4+ 0.28841(8) 0.17033(4) 0.79675(17) 0.0072(2) Uani 0.21(13) 1 d . . P . . M1A Mg2+ 0.0000 0.08525(5) 0.5000 0.0089(3) Uani 0.421(7) 2 d S T P . . M1B Mn3+ 0.0000 0.08525(5) 0.5000 0.0089(3) Uani 0.579(7) 2 d S T P . . M2A Mg2+ 0.0000 0.18075(4) 0.0000 0.0078(2) Uani 0.156(6) 2 d S T P . . M2B Mn3+ 0.0000 0.18075(4) 0.0000 0.0078(2) Uani 0.844(6) 2 d S T P . . M3A Mg2+ 0.0000 0.0000 0.0000 0.0063(9) Uani 0.666(6) 4 d S T P . . M3B Li+ 0.0000 0.0000 0.0000 0.0063(9) Uani 0.334(6) 4 d S T P . . M4A Ca2+ 0.0000 0.27540(11) 0.5000 0.0165(10) Uani 0.033(13) 2 d S T P . . M4B Na+ 0.0000 0.27540(11) 0.5000 0.0165(7) Uani 0.967(13) 2 d S T P . . Aa Na+ 0.0000 0.5000 0.0000 0.0331(29) Uani 0.192(3) 4 d S T P . . AB K+ 0.0000 0.5000 0.0000 0.0331(29) Uani 0.104(3) 4 d S T P . . AMA Na+ 0.0437(5) 0.5000 0.0991(9) 0.0325(17) Uani 0.229(4) 2 d S T P . . AMB K+ 0.0437(5) 0.5000 0.0991(9) 0.0325(17) Uani 0.123(4) 2 d S T P . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 O1A 0.0102(11) 0.0154(11) 0.0111(13) -0.0034(8) 0.0014(9) -0.0013(8) O1B 0.0102(11) 0.0154(11) 0.0111(13) -0.0034(8) 0.0014(9) -0.0013(8) O2A 0.0083(10) 0.0163(11) 0.0098(12) 0.0009(8) 0.0006(8) 0.0026(8) O2B 0.0083(10) 0.0163(11) 0.0098(12) 0.0009(8) 0.0006(8) 0.0026(8) O3A 0.0131(15) 0.0119(16) 0.0151(18) 0.0000 0.0020(13) 0.0000 O3B 0.0131(15) 0.0119(16) 0.0151(18) 0.0000 0.0020(13) 0.0000 O4A 0.0234(12) 0.0079(10) 0.0162(12) -0.0036(9) 0.0106(10) -0.0004(8) O4B 0.0234(12) 0.0079(10) 0.0162(12) -0.0036(9) 0.0106(10) -0.0004(8) O5A 0.0103(9) 0.0133(10) 0.0090(10) 0.0004(8) 0.0020(8) 0.0034(8) O5B 0.0103(9) 0.0133(10) 0.0090(10) 0.0004(8) 0.0020(8) 0.0034(8) O6A 0.0098(9) 0.0151(10) 0.0076(9) 0.0014(8) -0.0002(7) -0.0021(8) O6B 0.0098(9) 0.0151(10) 0.0076(9) 0.0014(8) -0.0002(7) -0.0021(8) O7A 0.0185(16) 0.0058(13) 0.0213(18) 0.0000 0.0030(14) 0.0000 O7B 0.0185(16) 0.0058(13) 0.0213(18) 0.0000 0.0030(14) 0.0000 T1A 0.0071(4) 0.0060(3) 0.0071(4) -0.0006(3) 0.0004(3) -0.0004(3) T1B 0.0071(4) 0.0060(3) 0.0071(4) -0.0006(3) 0.0004(3) -0.0004(3) T2A 0.0077(4) 0.0070(3) 0.0065(4) -0.0004(3) 0.0008(3) 0.0012(3) T2B 0.0077(4) 0.0070(3) 0.0065(4) -0.0004(3) 0.0008(3) 0.0012(3) M1A 0.0091(5) 0.0112(5) 0.0066(5) 0.0000 0.0022(4) 0.0000 M1B 0.0091(5) 0.0112(5) 0.0066(5) 0.0000 0.0022(4) 0.0000 M2A 0.0072(4) 0.0076(3) 0.0082(4) 0.0000 0.0011(3) 0.0000 M2B 0.0072(4) 0.0076(3) 0.0082(4) 0.0000 0.0011(3) 0.0000 M3A 0.0073(14) 0.0042(13) 0.0055(16) 0.0000 -0.0020(10) 0.0000 M3B 0.0073(14) 0.0042(13) 0.0055(16) 0.0000 -0.0020(10) 0.0000 M4A 0.0185(11) 0.0141(11) 0.0206(13) 0.0000 0.0118(8) 0.0000 M4B 0.0185(11) 0.0141(11) 0.0206(13) 0.0000 0.0118(8) 0.0000 AA 0.0261(40) 0.0339(47) 0.0497(54) 0.0000 0.0287(40) 0.0000 AB 0.0261(40) 0.0339(47) 0.0497(54) 0.0000 0.0287(40) 0.0000 AMA 0.0372(28) 0.0303(26) 0.0346(28) 0.0000 0.0174(21) 0.0000 AMB 0.0372(28) 0.0303(26) 0.0346(28) 0.0000 0.0174(21) 0.0000 _geom_special_details ; Geometry data (distances and angles) are reported only for T, M and A sites flagged by the A suffix. All esds are estimated using the full covariance matrix. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag T1A O1A 1.599(3) . ? T1A O6A 1.623(3) . ? T1A O5A 1.624(2) . ? T1A O7A 1.633(2) . ? T2A O4A 1.579(2) . ? T2A O2A 1.615(2) . ? T2A O5A 1.654(3) 1_556 ? T2A O6A 1.667(2) . ? M1A O3A 2.008(2) . ? M1A O3A 2.008(2) 5_556 ? M1A O2A 2.040(2) . ? M1A O2A 2.040(2) 6_556 ? M1A O1A 2.107(3) . ? M1A O1A 2.107(3) 6_556 ? M2A O4A 1.964(3) 7_556 ? M2A O4A 1.964(3) 4_454 ? M2A O2A 2.129(2) 6_556 ? M2A O2A 2.129(2) 1_554 ? M2A O1A 2.134(3) 6 ? M2A O1A 2.134(3) . ? M3A O1A 2.093(2) . ? M3A O1A 2.093(2) 5 ? M3A O1A 2.093(2) 6 ? M3A O1A 2.093(2) 2 ? M3A O3A 2.110(4) 5_556 ? M3A O3A 2.110(4) 1_554 ? M4A O4A 2.402(3) 4_455 ? M4A O4A 2.402(3) 7_556 ? M4A O2A 2.417(3) 6_556 ? M4A O2A 2.417(3) . ? M4A O6A 2.541(3) 7_556 ? M4A O6A 2.541(3) 4_455 ? M4A O5A 2.915(3) 7_556 ? M4A O5A 2.915(3) 4_455 ? Aa O7A 2.518(4) 7 ? Aa O7A 2.518(4) 3_455 ? Aa O5A 2.819(2) 8 ? Aa O5A 2.819(2) 4_455 ? Aa O5A 2.819(2) 3_455 ? Aa O5A 2.819(2) 7 ? Aa O6A 3.163(2) 8_556 ? Aa O6A 3.163(2) 4_454 ? Aa O6A 3.163(2) 3_454 ? Aa O6A 3.163(2) 7_556 ? AMA O7A 2.519(9) 3_455 ? AMA O7A 2.651(10) 7 ? AMA O5A 2.784(5) 8 ? AMA O5A 2.784(5) 7 ? AMA O6A 2.758(6) 8_556 ? AMA O6A 2.758(6) 7_556 ? AMA O5A 2.972(6) 4_455 ? AMA O5A 2.972(6) 3_455 ? AMA O7A 3.118(9) 7_556 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag O1A T1A O6A 111.8(1) . . ? O1A T1A O5A 112.7(1) . . ? O6A T1A O5A 110.7(1) . . ? O1A T1A O7A 111.4(1) . . ? O6A T1A O7A 105.7(1) . . ? O5A T1A O7A 104.0(1) . . ? O4A T2A O2A 117.8(1) . . ? O4A T2A O5A 110.6(1) . 1_556 ? O2A T2A O5A 108.3(1) . 1_556 ? O4A T2A O6A 106.2(1) . . ? O2A T2A O6A 108.1(1) . . ? O5A T2A O6A 104.9(1) 1_556 . ? O3A M1A O3A 81.3(2) . 5_556 ? O3A M1A O2A 94.7(1) . . ? O3A M1A O2A 176.0(1) 5_556 . ? O3A M1A O2A 176.0(1) . 6_556 ? O3A M1A O2A 94.7(1) 5_556 6_556 ? O2A M1A O2A 89.3(1) . 6_556 ? O3A M1A O1A 96.1(1) . . ? O3A M1A O1A 86.6(1) 5_556 . ? O2A M1A O1A 93.3(1) . . ? O2A M1A O1A 84.1(1) 6_556 . ? O3A M1A O1A 86.6(1) . 6_556 ? O3A M1A O1A 96.1(1) 5_556 6_556 ? O2A M1A O1A 84.1(1) . 6_556 ? O2A M1A O1A 93.3(1) 6_556 6_556 ? O1A M1A O1A 176.5(1) . 6_556 ? O4A M2A O4A 101.4(1) 7_556 4_454 ? O4A M2A O2A 98.1(1) 7_556 6_556 ? O4A M2A O2A 90.6(1) 4_454 6_556 ? O4A M2A O2A 90.6(1) 7_556 1_554 ? O4A M2A O2A 98.1(1) 4_454 1_554 ? O2A M2A O2A 166.2(1) 6_556 1_554 ? O4A M2A O1A 166.9(1) 7_556 6 ? O4A M2A O1A 90.0(1) 4_454 6 ? O2A M2A O1A 88.0(1) 6_556 6 ? O2A M2A O1A 81.4(1) 1_554 6 ? O4A M2A O1A 90.0(1) 7_556 . ? O4A M2A O1A 166.9(1) 4_454 . ? O2A M2A O1A 81.4(1) 6_556 . ? O2A M2A O1A 88.0(1) 1_554 . ? O1A M2A O1A 79.4(1) 6 . ? O1A M3A O1A 180.0 . 5 ? O1A M3A O1A 81.3(1) . 6 ? O1A M3A O1A 98.7(1) 5 6 ? O1A M3A O1A 98.7(1) . 2 ? O1A M3A O1A 81.3(1) 5 2 ? O1A M3A O1A 180.0 6 2 ? O1A M3A O3A 84.4(1) . 5_556 ? O1A M3A O3A 95.6(1) 5 5_556 ? O1A M3A O3A 95.6(1) 6 5_556 ? O1A M3A O3A 84.4(1) 2 5_556 ? O1A M3A O3A 95.6(1) . 1_554 ? O1A M3A O3A 84.4(1) 5 1_554 ? O1A M3A O3A 84.4(1) 6 1_554 ? O1A M3A O3A 95.6(1) 2 1_554 ? O3A M3A O3A 180.0 5_556 1_554 ? O4A M4A O4A 158.5(1) 4_455 7_556 ? O4A M4A O2A 82.9(1) 4_455 6_556 ? O4A M4A O2A 79.9(1) 7_556 6_556 ? O4A M4A O2A 79.9(1) 4_455 . ? O4A M4A O2A 82.9(1) 7_556 . ? O2A M4A O2A 72.7(1) 6_556 . ? O4A M4A O6A 136.7(1) 4_455 7_556 ? O4A M4A O6A 63.3(1) 7_556 7_556 ? O2A M4A O6A 139.3(1) 6_556 7_556 ? O2A M4A O6A 116.2(1) . 7_556 ? O4A M4A O6A 63.3(1) 4_455 4_455 ? O4A M4A O6A 136.7(1) 7_556 4_455 ? O2A M4A O6A 116.2(1) 6_556 4_455 ? O2A M4A O6A 139.3(1) . 4_455 ? O6A M4A O6A 83.6(1) 7_556 4_455 ? O4A M4A O5A 83.1(1) 4_455 7_556 ? O4A M4A O5A 110.0(1) 7_556 7_556 ? O2A M4A O5A 160.1(1) 6_556 7_556 ? O2A M4A O5A 91.0(1) . 7_556 ? O6A M4A O5A 58.1(1) 7_556 7_556 ? O6A M4A O5A 68.9(1) 4_455 7_556 ? O4A M4A O5A 110.0(1) 4_455 4_455 ? O4A M4A O5A 83.1(1) 7_556 4_455 ? O2A M4A O5A 91.0(1) 6_556 4_455 ? O2A M4A O5A 160.1(1) . 4_455 ? O6A M4A O5A 68.9(1) 7_556 4_455 ? O6A M4A O5A 58.1(1) 4_455 4_455 ? O5A M4A O5A 107.0(1) 7_556 4_455 ? O7A Aa O7A 180.0 7 3_455 ? O7A Aa O5A 57.1(1) 7 8 ? O7A Aa O5A 122.9(1) 3_455 8 ? O7A Aa O5A 122.9(1) 7 4_455 ? O7A Aa O5A 57.1(1) 3_455 4_455 ? O5A Aa O5A 180.0 8 4_455 ? O7A Aa O5A 122.9(1) 7 3_455 ? O7A Aa O5A 57.1(1) 3_455 3_455 ? O5A Aa O5A 72.1(1) 8 3_455 ? O5A Aa O5A 107.9(1) 4_455 3_455 ? O7A Aa O5A 57.1(1) 7 7 ? O7A Aa O5A 122.9(1) 3_455 7 ? O5A Aa O5A 107.9(1) 8 7 ? O5A Aa O5A 72.1(1) 4_455 7 ? O5A Aa O5A 180.0 3_455 7 ? O7A Aa O6A 99.4(1) 7 8_556 ? O7A Aa O6A 80.6(1) 3_455 8_556 ? O5A Aa O6A 51.8(1) 8 8_556 ? O5A Aa O6A 128.2(1) 4_455 8_556 ? O5A Aa O6A 62.2(1) 3_455 8_556 ? O5A Aa O6A 117.8(1) 7 8_556 ? O7A Aa O6A 80.6(1) 7 4_454 ? O7A Aa O6A 99.4(1) 3_455 4_454 ? O5A Aa O6A 128.2(1) 8 4_454 ? O5A Aa O6A 51.8(1) 4_455 4_454 ? O5A Aa O6A 117.8(1) 3_455 4_454 ? O5A Aa O6A 62.2(1) 7 4_454 ? O6A Aa O6A 180.0 8_556 4_454 ? O7A Aa O6A 80.6(1) 7 3_454 ? O7A Aa O6A 99.4(1) 3_455 3_454 ? O5A Aa O6A 62.2(1) 8 3_454 ? O5A Aa O6A 117.8(1) 4_455 3_454 ? O5A Aa O6A 51.8(1) 3_455 3_454 ? O5A Aa O6A 128.2(1) 7 3_454 ? O6A Aa O6A 95.8(1) 8_556 3_454 ? O6A Aa O6A 84.2(1) 4_454 3_454 ? O7A Aa O6A 99.4(1) 7 7_556 ? O7A Aa O6A 80.6(1) 3_455 7_556 ? O5A Aa O6A 117.8(1) 8 7_556 ? O5A Aa O6A 62.2(1) 4_455 7_556 ? O5A Aa O6A 128.2(1) 3_455 7_556 ? O5A Aa O6A 51.8(1) 7 7_556 ? O6A Aa O6A 84.2(1) 8_556 7_556 ? O6A Aa O6A 95.8(1) 4_454 7_556 ? O6A Aa O6A 180.0 3_454 7_556 ? O7A AMA O7A 153.9(3) 3_455 7 ? O7A AMA O5A 124.3(2) 3_455 8 ? O7A AMA O5A 56.3(2) 7 8 ? O7A AMA O5A 124.3(2) 3_455 7 ? O7A AMA O5A 56.3(2) 7 7 ? O5A AMA O5A 109.9(3) 8 7 ? O7A AMA O6A 89.1(2) 3_455 8_556 ? O7A AMA O6A 107.2(2) 7 8_556 ? O5A AMA O6A 56.7(1) 8 8_556 ? O5A AMA O6A 135.3(3) 7 8_556 ? O7A AMA O6A 89.1(2) 3_455 7_556 ? O7A AMA O6A 107.2(2) 7 7_556 ? O5A AMA O6A 135.3(3) 8 7_556 ? O5A AMA O6A 56.7(1) 7 7_556 ? O6A AMA O6A 100.5(3) 8_556 7_556 ? O7A AMA O5A 55.0(2) 3_455 4_455 ? O7A AMA O5A 112.9(2) 7 4_455 ? O5A AMA O5A 156.7(3) 8 4_455 ? O5A AMA O5A 70.3(1) 7 4_455 ? O6A AMA O5A 139.9(3) 8_556 4_455 ? O6A AMA O5A 65.5(1) 7_556 4_455 ? O7A AMA O5A 55.0(2) 3_455 3_455 ? O7A AMA O5A 112.9(2) 7 3_455 ? O5A AMA O5A 70.3(1) 8 3_455 ? O5A AMA O5A 156.7(3) 7 3_455 ? O6A AMA O5A 65.5(1) 8_556 3_455 ? O6A AMA O5A 139.9(3) 7_556 3_455 ? O5A AMA O5A 100.2(3) 4_455 3_455 ? O7A AMA O7A 73.1(2) 3_455 7_556 ? O7A AMA O7A 133.1(3) 7 7_556 ? O5A AMA O7A 105.8(2) 8 7_556 ? O5A AMA O7A 105.8(2) 7 7_556 ? O6A AMA O7A 52.0(1) 8_556 7_556 ? O6A AMA O7A 52.0(1) 7_556 7_556 ? O5A AMA O7A 96.1(2) 4_455 7_556 ? O5A AMA O7A 96.1(2) 3_455 7_556 ? T1A O5A T2A 136.1(1) . 1_554 ? T1A O6A T2A 136.6(1) . . ? T1A O7A T1A 140.2(1) 2 . ? O6A O7A O6A 109.6(1) . 2 ? O5A O6A O5A 173.0(1) 1_556 . ? _refine_diff_density_max 0.433 _refine_diff_density_min -0.429 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_sigma 0 2 0 16.8 0.3 0 4 0 93.5 0.3 0 6 0 3.1 2.8 0 8 0 12.0 1.0 0 10 0 80.6 0.5 0 12 0 176.2 0.5 0 14 0 30.0 0.8 0 16 0 10.7 2.0 0 18 0 0.0 4.3 0 20 0 45.6 0.8 0 22 0 60.1 0.9 0 24 0 77.4 1.0 1 1 0 55.4 1.1 1 3 0 28.8 0.6 1 5 0 7.0 2.4 1 7 0 39.6 0.7 1 9 0 71.1 0.8 1 11 0 107.3 0.5 1 13 0 10.9 2.3 1 15 0 14.4 1.5 1 17 0 11.3 1.9 1 19 0 21.4 2.5 1 21 0 20.5 1.1 1 23 0 17.3 1.3 1 25 0 6.2 4.8 2 0 0 6.0 1.2 2 2 0 7.9 0.8 2 4 0 72.7 1.5 2 6 0 13.0 0.6 2 8 0 14.9 1.0 2 10 0 35.1 1.0 2 12 0 12.1 1.0 2 14 0 15.7 1.5 2 16 0 20.8 2.1 2 18 0 7.3 3.5 2 20 0 5.6 4.2 2 22 0 26.1 1.0 2 24 0 33.5 1.4 3 1 0 132.1 0.2 3 3 0 90.8 0.6 3 5 0 49.1 0.7 3 7 0 15.6 0.8 3 9 0 18.1 1.9 3 11 0 86.8 1.1 3 13 0 13.8 1.1 3 15 0 3.6 2.9 3 17 0 20.0 2.7 3 19 0 42.4 0.7 3 21 0 7.0 6.6 3 23 0 46.4 0.9 4 0 0 33.7 0.5 4 2 0 5.9 1.4 4 4 0 5.9 3.4 4 6 0 4.6 3.4 4 8 0 111.2 0.3 4 10 0 49.2 0.5 4 12 0 63.5 0.5 4 14 0 1.2 4.0 4 16 0 31.6 0.6 4 18 0 11.0 4.8 4 20 0 37.3 1.0 4 22 0 49.5 1.2 4 24 0 2.3 4.7 5 1 0 58.0 0.4 5 3 0 26.5 0.5 5 5 0 3.7 6.2 5 7 0 9.7 2.8 5 9 0 8.0 3.2 5 11 0 12.4 2.2 5 13 0 49.4 0.5 5 15 0 38.4 0.7 5 17 0 6.3 1.8 5 19 0 22.1 2.0 5 21 0 23.0 1.2 5 23 0 23.9 1.0 6 0 0 109.8 0.5 6 2 0 27.9 0.9 6 4 0 1.0 3.1 6 6 0 11.6 1.2 6 8 0 19.1 1.3 6 10 0 18.7 0.9 6 12 0 4.8 4.8 6 14 0 9.9 1.9 6 16 0 37.9 0.9 6 18 0 0.0 2.7 6 20 0 20.0 2.8 6 22 0 18.3 1.4 7 1 0 74.9 0.7 7 3 0 53.8 1.1 7 5 0 6.2 3.4 7 7 0 42.3 0.7 7 9 0 77.7 0.6 7 11 0 124.1 1.1 7 13 0 39.8 1.4 7 15 0 46.5 0.7 7 17 0 13.1 2.8 7 19 0 31.4 0.9 7 21 0 0.0 4.2 8 0 0 98.4 0.6 8 2 0 14.9 1.1 8 4 0 7.9 7.6 8 6 0 17.3 1.7 8 8 0 16.3 1.8 8 10 0 24.7 0.8 8 12 0 42.4 0.9 8 14 0 9.8 3.7 8 16 0 5.0 6.1 8 18 0 15.2 3.0 8 20 0 15.5 5.9 9 1 0 31.2 0.6 9 3 0 3.1 5.2 9 5 0 5.7 2.9 9 7 0 24.6 0.7 9 9 0 15.0 3.1 9 11 0 20.4 0.9 9 13 0 14.0 5.4 9 15 0 26.9 1.0 9 17 0 18.2 1.2 10 0 0 72.4 0.7 10 2 0 5.4 3.5 10 4 0 10.9 3.2 10 6 0 17.4 1.8 10 8 0 62.1 1.0 10 10 0 25.6 1.3 10 12 0 64.1 1.7 10 14 0 12.8 3.5 10 16 0 22.6 1.8 11 1 0 56.1 1.2 11 3 0 27.1 0.7 11 5 0 16.6 1.5 11 7 0 13.4 2.0 11 9 0 13.0 3.0 11 11 0 59.4 2.1 11 13 0 16.3 5.4 12 0 0 5.3 4.7 12 2 0 3.0 6.7 12 4 0 16.1 4.3 12 6 0 0.7 3.9 12 8 0 14.8 2.2 12 10 0 18.3 1.4 13 1 0 13.4 3.6 13 3 0 9.0 2.2 13 5 0 19.5 1.8 0 0 1 12.8 0.6 0 2 1 46.5 0.7 0 4 1 16.8 0.7 0 6 1 121.3 0.8 0 8 1 16.7 0.7 0 10 1 18.4 1.0 0 12 1 8.4 2.8 0 14 1 45.8 1.2 0 16 1 60.3 0.6 0 18 1 15.5 1.9 0 20 1 9.2 1.7 0 22 1 11.7 5.0 0 24 1 10.5 2.6 1 1 1 45.5 0.9 -1 1 1 19.2 0.3 1 3 1 129.4 0.7 -1 3 1 23.3 0.3 1 5 1 180.8 2.2 -1 5 1 31.4 0.6 1 7 1 64.7 0.4 -1 7 1 83.5 0.5 1 9 1 71.1 0.4 -1 9 1 64.9 0.7 1 11 1 15.2 0.7 -1 11 1 13.4 0.9 1 13 1 52.6 0.9 -1 13 1 4.1 3.5 1 15 1 43.7 0.5 -1 15 1 19.3 0.7 1 17 1 107.1 0.6 -1 17 1 19.2 0.9 1 19 1 20.9 1.9 -1 19 1 34.8 0.8 1 21 1 35.2 0.7 -1 21 1 42.1 1.2 1 23 1 9.3 3.2 -1 23 1 9.8 4.6 2 0 1 4.8 3.5 -2 0 1 12.9 0.7 2 2 1 60.1 0.4 -2 2 1 43.0 0.4 2 4 1 10.7 1.9 -2 4 1 14.4 0.7 2 6 1 149.7 2.2 -2 6 1 6.3 6.2 2 8 1 13.2 0.9 -2 8 1 8.2 3.0 2 10 1 42.7 0.9 -2 10 1 8.1 2.2 2 12 1 7.9 3.8 -2 12 1 11.6 1.1 2 14 1 9.8 1.2 -2 14 1 65.6 0.9 2 16 1 42.6 1.5 -2 16 1 51.0 1.0 2 18 1 12.6 2.5 -2 18 1 3.9 6.8 2 20 1 0.0 3.1 -2 20 1 5.2 3.7 2 22 1 27.4 1.5 -2 22 1 1.1 3.5 2 24 1 10.1 6.8 -2 24 1 10.4 3.3 3 1 1 7.5 1.0 -3 1 1 46.6 0.5 3 3 1 38.2 0.5 -3 3 1 110.4 1.0 3 5 1 91.3 0.6 -3 5 1 118.1 0.3 3 7 1 15.4 1.1 -3 7 1 31.1 0.7 3 9 1 9.2 4.5 -3 9 1 58.5 0.4 3 11 1 0.0 2.7 -3 11 1 28.5 0.9 3 13 1 1.2 3.7 -3 13 1 46.7 1.8 3 15 1 10.8 3.1 -3 15 1 24.9 0.8 3 17 1 24.4 1.0 -3 17 1 77.2 0.8 3 19 1 15.9 1.6 -3 19 1 5.8 3.4 3 21 1 17.0 3.9 -3 21 1 21.3 1.0 3 23 1 12.6 4.8 -3 23 1 5.9 4.5 4 0 1 3.9 2.9 -4 0 1 10.0 0.9 4 2 1 69.8 0.4 -4 2 1 55.4 0.4 4 4 1 16.9 1.9 -4 4 1 8.5 1.1 4 6 1 173.3 0.4 -4 6 1 72.3 0.6 4 8 1 29.4 0.6 -4 8 1 11.4 1.8 4 10 1 30.9 0.9 -4 10 1 49.4 0.5 4 12 1 4.0 4.3 -4 12 1 4.7 6.0 4 14 1 75.1 0.5 -4 14 1 0.0 3.0 4 16 1 57.9 1.0 -4 16 1 37.0 1.3 4 18 1 71.3 1.8 -4 18 1 0.0 2.7 4 20 1 14.5 1.3 -4 20 1 11.6 2.2 4 22 1 19.6 1.8 -4 22 1 23.1 1.7 -4 24 1 13.3 1.7 5 1 1 3.8 3.6 -5 1 1 7.9 7.5 5 3 1 20.4 1.1 -5 3 1 41.6 1.3 5 5 1 93.6 0.6 -5 5 1 41.0 1.1 5 7 1 32.5 0.6 -5 7 1 18.9 2.0 5 9 1 2.6 4.9 -5 9 1 4.6 4.8 5 11 1 7.5 3.2 -5 11 1 4.6 4.0 5 13 1 19.9 1.5 -5 13 1 11.8 2.2 5 15 1 8.1 1.8 -5 15 1 12.2 10.7 5 17 1 53.8 0.6 -5 17 1 14.5 1.4 5 19 1 1.4 4.0 -5 19 1 14.0 2.0 5 21 1 0.9 4.3 -5 21 1 8.5 5.4 -5 23 1 6.9 6.4 6 0 1 2.7 4.0 -6 0 1 2.8 4.1 6 2 1 14.0 0.8 -6 2 1 49.7 1.0 6 4 1 6.9 1.8 -6 4 1 8.2 1.5 6 6 1 51.0 0.8 -6 6 1 205.5 1.9 6 8 1 4.1 3.1 -6 8 1 30.5 1.1 6 10 1 24.7 0.8 -6 10 1 33.4 0.7 6 12 1 0.0 2.6 -6 12 1 5.8 3.4 6 14 1 5.0 3.2 -6 14 1 44.7 1.0 6 16 1 23.3 2.7 -6 16 1 56.0 1.3 6 18 1 58.0 0.8 -6 18 1 69.2 0.6 6 20 1 15.3 1.5 -6 20 1 19.5 1.4 -6 22 1 0.0 3.1 7 1 1 4.9 4.8 -7 1 1 10.1 1.5 7 3 1 36.4 0.8 -7 3 1 34.6 0.8 7 5 1 37.4 0.8 -7 5 1 117.4 0.7 7 7 1 7.6 3.0 -7 7 1 48.5 0.9 7 9 1 8.3 5.1 -7 9 1 16.5 1.1 7 11 1 15.0 4.4 -7 11 1 2.2 4.3 7 13 1 24.4 0.8 -7 13 1 21.3 1.5 7 15 1 19.2 1.9 -7 15 1 8.6 4.2 7 17 1 30.5 0.8 -7 17 1 72.1 2.0 7 19 1 2.5 6.1 -7 19 1 13.9 2.0 -7 21 1 0.0 3.8 8 0 1 8.6 2.0 -8 0 1 9.7 1.5 8 2 1 34.6 1.5 -8 2 1 8.3 2.5 8 4 1 6.8 2.5 -8 4 1 11.7 1.2 8 6 1 100.7 0.8 -8 6 1 11.1 1.6 8 8 1 20.5 1.6 -8 8 1 5.5 3.8 8 10 1 14.8 2.5 -8 10 1 19.3 0.9 8 12 1 11.7 2.3 -8 12 1 1.5 3.5 8 14 1 39.6 1.4 -8 14 1 11.5 1.8 8 16 1 38.9 0.9 -8 16 1 30.3 0.8 8 18 1 37.1 0.9 -8 18 1 30.5 0.8 -8 20 1 15.6 1.3 9 1 1 8.6 2.0 -9 1 1 6.7 6.8 9 3 1 2.9 4.7 -9 3 1 29.6 1.3 9 5 1 20.9 1.0 -9 5 1 46.7 0.5 9 7 1 8.6 1.8 -9 7 1 4.6 3.0 9 9 1 11.3 4.2 -9 9 1 13.1 1.3 9 11 1 7.0 2.9 -9 11 1 7.2 1.8 9 13 1 15.8 5.4 -9 13 1 7.0 2.0 9 15 1 7.4 4.8 -9 15 1 0.0 4.3 9 17 1 2.6 7.2 -9 17 1 28.0 1.2 -9 19 1 12.3 2.7 10 0 1 0.0 6.4 -10 0 1 0.0 5.4 10 2 1 3.8 3.4 -10 2 1 33.0 0.7 10 4 1 11.7 1.6 -10 4 1 13.7 4.0 10 6 1 20.2 1.4 -10 6 1 76.5 1.0 10 8 1 19.3 2.6 -10 8 1 13.9 1.5 10 10 1 15.8 3.2 -10 10 1 8.8 3.5 10 12 1 0.0 3.7 -10 12 1 1.9 5.0 10 14 1 16.2 1.6 -10 14 1 44.3 1.4 -10 16 1 40.3 0.9 11 1 1 4.9 5.4 -11 1 1 6.2 7.7 11 3 1 42.6 0.7 -11 3 1 9.6 8.2 11 5 1 81.5 1.1 -11 5 1 8.0 2.8 11 7 1 47.1 1.7 -11 7 1 17.2 1.1 11 9 1 31.4 0.9 -11 9 1 17.5 2.8 11 11 1 2.4 6.0 -11 11 1 7.3 3.1 -11 13 1 16.6 2.1 -11 15 1 0.0 4.6 12 0 1 0.0 6.0 -12 0 1 7.9 4.0 12 2 1 23.6 2.5 -12 2 1 14.2 6.4 12 4 1 19.0 2.4 -12 4 1 14.3 1.9 12 6 1 52.1 1.6 -12 6 1 5.7 5.4 12 8 1 1.4 5.0 -12 8 1 18.6 1.9 -12 10 1 18.1 1.7 -12 12 1 3.1 5.7 -13 1 1 0.0 3.9 -13 3 1 34.3 3.1 -13 5 1 55.4 0.7 -13 7 1 24.2 2.5 0 0 2 44.4 0.4 0 2 2 12.8 1.8 0 4 2 5.7 3.1 0 6 2 7.8 2.4 0 8 2 8.1 1.4 0 10 2 25.8 1.4 0 12 2 84.1 0.5 0 14 2 13.7 4.1 0 16 2 33.5 1.4 0 18 2 0.0 3.3 0 20 2 17.9 1.5 0 22 2 18.4 1.8 0 24 2 40.9 0.8 1 1 2 16.1 0.5 -1 1 2 24.4 0.5 1 3 2 5.5 1.9 -1 3 2 25.7 0.7 1 5 2 37.1 0.5 -1 5 2 25.1 0.4 1 7 2 47.6 0.5 -1 7 2 2.0 4.6 1 9 2 77.5 0.4 -1 9 2 10.4 2.0 1 11 2 114.8 0.5 -1 11 2 33.3 0.6 1 13 2 24.6 2.3 -1 13 2 35.5 1.3 1 15 2 23.9 1.0 -1 15 2 21.6 1.9 1 17 2 6.0 2.4 -1 17 2 9.6 2.9 1 19 2 31.6 1.0 -1 19 2 28.8 0.9 1 21 2 13.5 2.6 -1 21 2 13.9 1.5 1 23 2 33.8 3.3 -1 23 2 7.3 4.0 2 0 2 150.2 0.4 -2 0 2 233.8 0.4 2 2 2 17.3 0.7 -2 2 2 21.2 1.3 2 4 2 64.2 0.4 -2 4 2 45.8 1.2 2 6 2 1.2 3.0 -2 6 2 6.1 1.5 2 8 2 45.2 1.0 -2 8 2 91.3 0.4 2 10 2 44.7 1.2 -2 10 2 53.5 0.6 2 12 2 40.2 0.7 -2 12 2 178.5 1.5 2 14 2 12.8 0.9 -2 14 2 16.6 0.9 2 16 2 0.0 2.9 -2 16 2 26.6 1.0 2 18 2 8.5 3.6 -2 18 2 9.4 4.0 2 20 2 46.1 1.7 -2 20 2 23.0 0.8 2 22 2 41.7 0.9 -2 22 2 56.8 0.9 -2 24 2 42.1 1.4 3 1 2 3.9 3.0 -3 1 2 105.1 0.7 3 3 2 9.4 1.8 -3 3 2 85.2 0.7 3 5 2 9.7 2.2 -3 5 2 53.5 0.3 3 7 2 8.3 6.9 -3 7 2 4.1 2.3 3 9 2 1.1 2.8 -3 9 2 26.4 0.5 3 11 2 9.9 5.5 -3 11 2 73.0 0.4 3 13 2 39.8 1.8 -3 13 2 14.6 1.5 3 15 2 31.0 1.5 -3 15 2 5.8 6.2 3 17 2 5.7 8.6 -3 17 2 6.1 5.6 3 19 2 18.3 1.9 -3 19 2 34.7 0.9 3 21 2 16.0 1.4 -3 21 2 2.5 6.8 3 23 2 13.4 2.3 -3 23 2 27.1 0.9 4 0 2 100.1 0.5 -4 0 2 116.1 0.4 4 2 2 29.8 0.8 -4 2 2 9.1 1.2 4 4 2 51.5 1.1 -4 4 2 41.2 0.4 4 6 2 12.8 1.8 -4 6 2 8.4 4.1 4 8 2 42.3 1.4 -4 8 2 26.0 0.7 4 10 2 18.3 1.9 -4 10 2 32.8 0.6 4 12 2 81.8 1.3 -4 12 2 13.2 2.1 4 14 2 13.1 1.3 -4 14 2 5.7 5.7 4 16 2 4.6 6.4 -4 16 2 30.2 0.7 4 18 2 2.3 4.3 -4 18 2 5.7 5.7 4 20 2 0.0 2.9 -4 20 2 12.9 2.2 4 22 2 26.2 1.0 -4 22 2 21.4 1.0 5 1 2 146.5 0.6 -5 1 2 72.2 1.3 5 3 2 88.7 1.1 -5 3 2 30.3 0.8 5 5 2 30.3 0.5 -5 5 2 20.1 0.9 5 7 2 3.1 2.6 -5 7 2 30.7 0.6 5 9 2 37.3 1.3 -5 9 2 70.8 1.0 5 11 2 123.6 0.5 -5 11 2 128.0 1.2 5 13 2 30.0 1.3 -5 13 2 36.7 0.6 5 15 2 31.1 0.7 -5 15 2 30.5 1.9 5 17 2 1.9 4.0 -5 17 2 1.6 4.1 5 19 2 37.6 0.8 -5 19 2 20.7 1.2 5 21 2 9.1 10.6 -5 21 2 11.1 3.5 -5 23 2 42.4 2.4 6 0 2 75.1 0.6 -6 0 2 165.5 0.5 6 2 2 0.0 2.6 -6 2 2 6.5 2.0 6 4 2 9.8 2.6 -6 4 2 76.3 0.8 6 6 2 15.9 2.1 -6 6 2 0.8 3.7 6 8 2 18.1 0.9 -6 8 2 44.4 0.6 6 10 2 32.5 1.5 -6 10 2 57.8 1.0 6 12 2 28.2 1.0 -6 12 2 50.5 0.6 6 14 2 1.5 4.0 -6 14 2 3.9 5.7 6 16 2 2.2 5.9 -6 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11.9 2.3 -1 5 6 6.6 6.4 1 7 6 9.2 2.6 -1 7 6 10.6 3.7 1 9 6 16.2 3.6 -1 9 6 11.5 2.0 1 11 6 57.9 0.9 -1 11 6 5.7 6.9 1 13 6 8.9 4.9 -1 13 6 24.0 1.8 2 0 6 3.3 6.4 -2 0 6 100.2 0.8 2 2 6 2.1 5.6 -2 2 6 2.1 5.4 2 4 6 1.7 4.8 -2 4 6 12.4 2.2 2 6 6 2.4 6.2 -2 6 6 2.9 4.3 2 8 6 7.8 2.7 -2 8 6 17.7 1.9 2 10 6 12.3 2.3 -2 10 6 21.2 2.2 -2 12 6 57.1 0.7 -2 14 6 15.1 3.4 3 1 6 21.1 2.7 -3 1 6 60.8 0.9 3 3 6 16.3 1.5 -3 3 6 28.9 1.5 3 5 6 24.5 1.0 -3 5 6 10.1 4.0 3 7 6 3.3 6.0 -3 7 6 20.9 0.9 3 9 6 14.0 4.2 -3 9 6 42.8 0.8 -3 11 6 91.4 0.6 -3 13 6 34.2 1.7 4 0 6 83.4 0.9 -4 0 6 26.8 1.1 4 2 6 10.2 2.9 -4 2 6 14.4 2.2 4 4 6 29.2 2.3 -4 4 6 15.0 1.4 4 6 6 2.7 6.5 -4 6 6 3.1 4.8 -4 8 6 1.7 5.0 -4 10 6 18.4 1.5 -4 12 6 16.4 3.2 -4 14 6 9.0 3.9 5 1 6 38.7 0.9 -5 1 6 7.1 2.1 -5 3 6 3.4 3.6 -5 5 6 7.9 5.7 -5 7 6 5.6 5.9 -5 9 6 5.2 9.5 -5 11 6 18.9 2.1 -5 13 6 10.1 3.2 -6 0 6 57.8 0.9 -6 2 6 7.7 8.0 -6 4 6 12.1 3.8 -6 6 6 9.5 3.9 -6 8 6 56.1 0.7 -6 10 6 24.1 2.9 -6 12 6 50.8 1.4 -7 1 6 23.6 3.1 -7 3 6 21.1 1.2 -7 5 6 17.4 2.9 -7 7 6 9.6 9.6 -7 9 6 2.9 4.9 -7 11 6 19.4 2.0 -8 0 6 12.9 3.2 -8 2 6 8.7 4.5 -8 4 6 33.3 0.8 -8 6 6 0.0 3.5 -8 8 6 10.8 3.0 -8 10 6 0.0 4.1 -9 1 6 19.3 1.7 -9 3 6 16.2 3.9 -9 5 6 0.0 4.8 -9 7 6 12.6 4.1 -9 9 6 26.6 3.2 -10 0 6 96.8 0.9 -10 2 6 12.3 6.6 -10 4 6 31.4 1.0 -10 6 6 5.0 5.1 0 0 7 6.1 5.3 0 2 7 1.1 4.3 0 4 7 3.4 5.6 0 6 7 13.5 5.9 1 1 7 11.6 4.8 -1 1 7 1.6 5.1 1 3 7 29.6 2.6 -1 3 7 15.5 4.3 -1 5 7 36.0 1.0 -1 7 7 15.6 3.3 -2 0 7 7.9 3.2 -2 2 7 43.0 2.0 -2 4 7 8.8 2.9 -2 6 7 70.4 1.2 -2 8 7 15.7 2.5 -3 1 7 0.0 3.5 -3 3 7 10.9 2.2 -3 5 7 18.5 2.7 -3 7 7 6.8 8.2 -4 0 7 2.2 4.6 -4 2 7 8.0 2.5 -4 4 7 1.1 3.6 -4 6 7 19.7 1.1 -4 8 7 8.3 4.1 -5 1 7 9.0 6.2 -5 3 7 24.1 1.8 -5 5 7 42.4 1.1 -5 7 7 14.7 2.4 -6 0 7 0.0 5.0 -6 2 7 13.2 2.1 -6 4 7 0.0 2.9 -6 6 7 54.6 0.9 -7 1 7 1.3 4.5 -7 3 7 5.8 6.2 -7 5 7 10.5 5.0