data_veenite _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_melting_point ? _chemical_formula_moiety ? _chemical_formula_sum 'As7 Pb16 S40 Sb9' _chemical_formula_weight 6217.63 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _symmetry_cell_setting ? _symmetry_space_group_name_H-M ? loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, y+1/2, -z' _cell_length_a 8.4291(15) _cell_length_b 26.069(5) _cell_length_c 8.9618(16) _cell_angle_alpha 90.00 _cell_angle_beta 117.447(2) _cell_angle_gamma 90.00 _cell_volume 1747.6(5) _cell_formula_units_Z 1 _cell_measurement_temperature 300(2) _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _exptl_crystal_description ? _exptl_crystal_colour ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_density_meas ? _exptl_crystal_density_diffrn 5.908 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 2642 _exptl_absorpt_coefficient_mu 46.281 _exptl_absorpt_correction_type ? _exptl_absorpt_correction_T_min ? _exptl_absorpt_correction_T_max ? _exptl_absorpt_process_details ? _exptl_special_details ; ? ; _diffrn_ambient_temperature 300(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type ? _diffrn_measurement_method ? _diffrn_detector_area_resol_mean ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? _diffrn_reflns_number 14913 _diffrn_reflns_av_R_equivalents 0.0901 _diffrn_reflns_av_sigmaI/netI 0.0744 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -28 _diffrn_reflns_limit_k_max 28 _diffrn_reflns_limit_l_min -9 _diffrn_reflns_limit_l_max 9 _diffrn_reflns_theta_min 2.68 _diffrn_reflns_theta_max 23.28 _reflns_number_total 4973 _reflns_number_gt 3897 _reflns_threshold_expression >2sigma(I) _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_molecular_graphics ? _computing_publication_material ? _refine_special_details ; Refinement of F^2^ against ALL reflections. The weighted R-factor wR and goodness of fit S are based on F^2^, conventional R-factors R are based on F, with F set to zero for negative F^2^. The threshold expression of F^2^ > 2sigma(F^2^) is used only for calculating R-factors(gt) etc. and is not relevant to the choice of reflections for refinement. R-factors based on F^2^ are statistically about twice as large as those based on F, and R- factors based on ALL data will be even larger. ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0229P)^2^+0.0000P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _atom_sites_solution_hydrogens geom _refine_ls_hydrogen_treatment mixed _refine_ls_extinction_method none _refine_ls_extinction_coef ? _refine_ls_abs_structure_details 'Flack H D (1983), Acta Cryst. A39, 876-881' _refine_ls_abs_structure_Flack 0.056(9) _refine_ls_number_reflns 4973 _refine_ls_number_parameters 349 _refine_ls_number_restraints 1 _refine_ls_R_factor_all 0.0542 _refine_ls_R_factor_gt 0.0396 _refine_ls_wR_factor_ref 0.0822 _refine_ls_wR_factor_gt 0.0767 _refine_ls_goodness_of_fit_ref 0.951 _refine_ls_restrained_S_all 0.951 _refine_ls_shift/su_max 0.165 _refine_ls_shift/su_mean 0.002 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Sb5 Sb 0.5670(19) 0.0410(6) 0.8912(15) 0.0233(12) Uani 0.516(9) 1 d P . . Pb9 Pb 0.5614(11) 0.0410(3) 0.8526(9) 0.0233(12) Uani 0.484(9) 1 d P . . Pb8 Pb 0.27500(18) 0.42329(5) 0.79468(18) 0.0332(5) Uani 0.718(10) 1 d P . . Sb12 Sb 0.27500(18) 0.42329(5) 0.79468(18) 0.0332(5) Uani 0.282(10) 1 d P . . Pb7 Pb 0.8182(11) 0.4394(3) 0.3498(9) 0.0354(12) Uani 0.511(10) 1 d P . . Sb11 Sb 0.814(2) 0.4434(6) 0.3864(16) 0.0354(12) Uani 0.489(10) 1 d P . . As1 As 0.164(5) 0.3346(11) 0.015(3) 0.044(2) Uani 0.509(18) 1 d P . . Sb1 Sb 0.169(3) 0.3431(7) 0.047(2) 0.044(2) Uani 0.491(18) 1 d P . . As6 As 0.071(2) 0.0548(7) 0.862(3) 0.0041(18) Uani 0.538(15) 1 d P . . Sb6 Sb 0.0437(18) 0.0439(5) 0.8605(19) 0.0041(18) Uani 0.462(15) 1 d P . . Pb5 Pb 0.77923(17) 0.41873(5) 0.79527(17) 0.0353(5) Uani 0.954(10) 1 d P . . Sb9 Sb 0.77923(17) 0.41873(5) 0.79527(17) 0.0353(5) Uani 0.046(10) 1 d P . . Sb7 Sb 0.036(3) 0.0530(9) 0.306(3) 0.0307(12) Uani 0.485(10) 1 d P . . Pb10 Pb 0.0247(14) 0.0594(5) 0.3041(15) 0.0307(12) Uani 0.515(10) 1 d P . . Pb6 Pb 0.52608(16) 0.06244(5) 0.29870(17) 0.0310(5) Uani 0.865(10) 1 d P . . Sb10 Sb 0.52608(16) 0.06244(5) 0.29870(17) 0.0310(5) Uani 0.135(10) 1 d P . . Pb3 Pb 0.11436(16) 0.28789(5) 0.46217(16) 0.0376(3) Uani 1 1 d . . . Pb4 Pb 0.61162(16) 0.28496(5) 0.47421(16) 0.0385(3) Uani 1 1 d . . . Pb1 Pb 0.36300(17) 0.19117(5) 0.97388(16) 0.0394(4) Uani 1 1 d . . . Pb2 Pb 0.85929(17) 0.19444(5) 0.96302(16) 0.0400(4) Uani 1 1 d . . . Sb8 Sb 0.3046(3) 0.43630(10) 0.3590(3) 0.0407(6) Uani 1 1 d . . . As3 As 0.3916(4) 0.15066(11) 0.5304(3) 0.0194(6) Uani 1 1 d . . . As2 As 0.6551(3) 0.32811(11) 0.0534(3) 0.0185(7) Uani 1 1 d . . . Sb4 Sb 0.9088(3) 0.14823(8) 0.5391(2) 0.0334(5) Uani 1 1 d . . . S1 S 0.4883(9) 0.2129(3) 0.7195(9) 0.0284(18) Uani 1 1 d . . . S2 S 0.2313(8) 0.2682(3) 0.2011(8) 0.0188(16) Uani 1 1 d . . . S3 S 0.7795(7) 0.3054(3) 0.8865(7) 0.0215(14) Uani 1 1 d . . . S4 S 0.4288(8) 0.3802(3) 0.5916(8) 0.0180(15) Uani 1 1 d . . . S5 S 0.4436(7) 0.3903(3) 0.2162(7) 0.0258(15) Uani 1 1 d . . . S6 S 0.1220(8) 0.4943(3) 0.5403(8) 0.0207(15) Uani 1 1 d . . . S7 S 0.6775(8) 0.4967(3) 0.5506(9) 0.0252(17) Uani 1 1 d . . . S8 S 0.5733(8) 0.4877(3) 0.9434(9) 0.0237(16) Uani 1 1 d . . . S9 S 0.1149(9) 0.4925(3) 0.9495(9) 0.0227(15) Uani 1 1 d . . . S10 S 0.1805(8) 0.1033(3) 0.1015(8) 0.0231(17) Uani 1 1 d . . . S11 S 0.5278(7) 0.1770(2) 0.3789(7) 0.0174(13) Uani 1 1 d . . . S12 S 0.7841(7) 0.0990(2) 0.7314(7) 0.0219(14) Uani 1 1 d . . . S13 S 0.2003(7) 0.0989(2) 0.7261(7) 0.0187(13) Uani 1 1 d . . . S14 S 0.9804(9) 0.2262(3) 0.7056(8) 0.0219(16) Uani 1 1 d . . . S15 S 0.7431(8) 0.2600(3) 0.2266(8) 0.0187(15) Uani 1 1 d . . . S16 S 0.3622(7) 0.3050(2) 0.8886(7) 0.0177(13) Uani 1 1 d . . . S17 S 0.9117(8) 0.3707(3) 0.5851(9) 0.0199(15) Uani 1 1 d . . . S18 S 0.0309(7) 0.3904(2) 0.2250(7) 0.0210(14) Uani 1 1 d . . . S19 S 0.6623(8) 0.1135(3) 0.0925(8) 0.0203(16) Uani 1 1 d . . . S20 S 0.1065(7) 0.1804(3) 0.3805(7) 0.0212(14) Uani 1 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Sb5 0.0257(10) 0.0246(10) 0.023(3) -0.005(2) 0.015(2) -0.0019(7) Pb9 0.0257(10) 0.0246(10) 0.023(3) -0.005(2) 0.015(2) -0.0019(7) Pb8 0.0270(8) 0.0363(10) 0.0360(9) -0.0041(7) 0.0142(6) 0.0020(6) Sb12 0.0270(8) 0.0363(10) 0.0360(9) -0.0041(7) 0.0142(6) 0.0020(6) Pb7 0.0574(12) 0.0221(15) 0.028(3) -0.0077(17) 0.0211(19) -0.0020(10) Sb11 0.0574(12) 0.0221(15) 0.028(3) -0.0077(17) 0.0211(19) -0.0020(10) As1 0.101(3) 0.007(6) 0.005(6) -0.015(3) 0.007(5) -0.010(4) Sb1 0.101(3) 0.007(6) 0.005(6) -0.015(3) 0.007(5) -0.010(4) As6 0.002(4) 0.000(6) 0.0131(12) -0.001(3) 0.006(2) -0.016(3) Sb6 0.002(4) 0.000(6) 0.0131(12) -0.001(3) 0.006(2) -0.016(3) Pb5 0.0351(8) 0.0343(9) 0.0402(8) -0.0061(6) 0.0205(6) -0.0123(6) Sb9 0.0351(8) 0.0343(9) 0.0402(8) -0.0061(6) 0.0205(6) -0.0123(6) Sb7 0.0217(15) 0.041(3) 0.0298(10) -0.0029(15) 0.0122(10) -0.0015(15) Pb10 0.0217(15) 0.041(3) 0.0298(10) -0.0029(15) 0.0122(10) -0.0015(15) Pb6 0.0267(8) 0.0242(9) 0.0416(9) -0.0040(6) 0.0153(6) 0.0019(6) Sb10 0.0267(8) 0.0242(9) 0.0416(9) -0.0040(6) 0.0153(6) 0.0019(6) Pb3 0.0300(6) 0.0396(8) 0.0450(8) -0.0101(7) 0.0188(6) -0.0056(6) Pb4 0.0355(7) 0.0396(8) 0.0498(8) -0.0098(7) 0.0277(6) -0.0051(6) Pb1 0.0304(6) 0.0503(9) 0.0396(8) -0.0024(7) 0.0180(6) -0.0018(6) Pb2 0.0326(7) 0.0509(9) 0.0377(8) 0.0023(7) 0.0171(6) 0.0063(7) Sb8 0.0408(13) 0.0448(15) 0.0368(13) -0.0040(11) 0.0182(10) -0.0036(11) As3 0.0284(14) 0.0062(14) 0.0219(14) -0.0013(11) 0.0102(11) -0.0005(12) As2 0.0164(13) 0.0148(16) 0.0286(16) -0.0041(12) 0.0142(12) -0.0020(11) Sb4 0.0511(12) 0.0160(10) 0.0190(10) -0.0015(9) 0.0041(9) 0.0005(9) S1 0.029(4) 0.026(4) 0.023(4) -0.007(3) 0.005(3) -0.004(3) S2 0.027(3) 0.012(4) 0.023(4) 0.004(3) 0.016(3) 0.004(3) S3 0.024(3) 0.017(3) 0.020(3) 0.001(3) 0.007(3) 0.002(3) S4 0.020(3) 0.013(4) 0.017(3) 0.007(3) 0.006(2) 0.002(3) S5 0.024(3) 0.030(4) 0.028(4) -0.007(3) 0.016(3) -0.001(3) S6 0.019(3) 0.022(4) 0.023(4) 0.005(3) 0.011(3) 0.003(3) S7 0.023(3) 0.013(4) 0.037(4) 0.003(3) 0.012(3) -0.001(3) S8 0.020(3) 0.024(4) 0.029(4) 0.004(3) 0.013(3) 0.001(3) S9 0.030(4) 0.020(4) 0.025(4) -0.001(3) 0.019(3) 0.001(3) S10 0.019(3) 0.027(4) 0.019(4) 0.000(3) 0.005(3) 0.000(3) S11 0.015(3) 0.018(3) 0.027(3) 0.002(3) 0.016(3) 0.006(3) S12 0.023(3) 0.020(3) 0.024(3) 0.004(3) 0.012(3) 0.001(3) S13 0.012(3) 0.020(3) 0.024(3) 0.001(3) 0.008(2) 0.004(2) S14 0.028(3) 0.011(4) 0.019(4) 0.000(3) 0.004(3) -0.001(3) S15 0.019(3) 0.021(4) 0.023(4) 0.000(3) 0.015(3) 0.001(3) S16 0.022(3) 0.014(3) 0.019(3) -0.001(2) 0.010(2) 0.003(3) S17 0.021(3) 0.015(4) 0.027(4) 0.003(3) 0.014(3) 0.005(3) S18 0.017(3) 0.020(3) 0.027(3) -0.005(3) 0.011(2) -0.009(3) S19 0.026(3) 0.019(4) 0.019(3) -0.001(3) 0.012(3) 0.007(3) S20 0.020(3) 0.024(4) 0.021(3) 0.005(3) 0.010(3) 0.005(3) _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Sb5 S19 2.476(15) 1_556 ? Sb5 S9 2.702(16) 2_647 ? Sb5 S8 2.673(14) 2_647 ? Sb5 S12 3.179(14) . ? Sb5 S13 3.131(15) . ? Sb5 S7 3.707(14) 2_646 ? Sb5 Sb8 3.987(13) 2_646 ? Sb5 Sb11 3.95(2) 2_646 ? Sb5 Pb7 3.971(17) 2_646 ? Sb5 As3 4.049(14) . ? Sb5 S5 4.037(16) 2_646 ? Sb5 Sb10 3.864(10) 1_556 ? Pb9 S19 2.689(10) 1_556 ? Pb9 S9 2.779(11) 2_647 ? Pb9 S8 2.911(10) 2_647 ? Pb9 S12 2.979(10) . ? Pb9 S13 3.106(10) . ? Pb9 S7 3.427(11) 2_646 ? Pb9 Sb8 3.781(8) 2_646 ? Pb9 Sb11 3.853(18) 2_646 ? Pb9 Pb7 3.898(12) 2_646 ? Pb9 As3 3.841(9) . ? Pb9 S5 3.974(11) 2_646 ? Pb9 Sb10 4.181(7) 1_556 ? Pb8 S6 2.753(7) . ? Pb8 S8 2.798(7) . ? Pb8 S4 2.904(6) . ? Pb8 S9 2.954(7) . ? Pb8 S17 3.080(7) 1_455 ? Pb8 S16 3.193(6) . ? Pb8 As1 3.43(4) 1_556 ? Pb8 Sb1 3.48(2) 1_556 ? Pb8 S5 3.476(6) 1_556 ? Pb8 As2 3.867(3) 1_556 ? Pb8 Pb7 4.092(8) 1_455 ? Pb8 Sb8 4.039(3) . ? Pb7 S17 2.596(11) . ? Pb7 S6 2.737(10) 1_655 ? Pb7 S7 2.975(9) . ? Pb7 S18 2.818(9) 1_655 ? Pb7 S5 3.091(10) . ? Pb7 S8 3.490(11) 1_554 ? Pb7 As2 3.740(7) . ? Pb7 Sb6 3.789(17) 2_656 ? Pb7 As6 3.89(2) 2_656 ? Pb7 Sb5 3.971(17) 2_656 ? Pb7 Pb9 3.898(12) 2_656 ? Pb7 Pb10 4.169(14) 2_656 ? Sb11 S17 2.467(17) . ? Sb11 S6 2.663(17) 1_655 ? Sb11 S7 2.645(13) . ? Sb11 S18 3.124(13) 1_655 ? Sb11 S5 3.101(17) . ? Sb11 S8 3.713(16) 1_554 ? Sb11 As2 4.005(12) . ? Sb11 Sb6 3.95(2) 2_656 ? Sb11 As6 4.04(3) 2_656 ? Sb11 Sb5 3.95(2) 2_656 ? Sb11 Pb9 3.853(18) 2_656 ? Sb11 Pb10 3.901(17) 2_656 ? As1 S2 2.29(3) . ? As1 S5 2.64(3) . ? As1 S16 2.53(3) 1_554 ? As1 S18 2.98(3) . ? As1 S3 3.00(4) 1_454 ? As1 Sb12 3.43(4) 1_554 ? As1 Pb8 3.43(4) 1_554 ? As1 Sb8 3.820(17) . ? As1 Sb9 3.65(4) 1_454 ? As1 Pb5 3.65(4) 1_454 ? As1 S17 3.56(3) 1_454 ? As1 S14 3.76(2) 1_454 ? Sb1 S2 2.31(2) . ? Sb1 S5 2.44(2) . ? Sb1 S16 2.79(2) 1_554 ? Sb1 S18 2.674(19) . ? Sb1 S3 3.07(2) 1_454 ? Sb1 Sb12 3.48(2) 1_554 ? Sb1 Pb8 3.48(2) 1_554 ? Sb1 Sb8 3.479(14) . ? Sb1 Sb9 3.60(2) 1_454 ? Sb1 Pb5 3.60(2) 1_454 ? Sb1 S17 3.75(2) 1_454 ? Sb1 S14 4.083(16) 1_454 ? As6 S10 2.29(2) 1_556 ? As6 S12 2.44(2) 1_455 ? As6 S13 2.280(16) . ? As6 S9 3.226(16) 2_547 ? As6 S8 3.20(2) 2_647 ? As6 S6 3.56(2) 2_546 ? As6 Sb4 3.54(2) 1_455 ? As6 Pb7 3.89(2) 2_646 ? As6 Sb11 4.04(3) 2_646 ? As6 Sb8 4.209(13) 2_546 ? As6 Sb7 4.12(3) 1_556 ? As6 Pb10 4.16(2) 1_556 ? Sb6 S10 2.469(16) 1_556 ? Sb6 S12 2.420(16) 1_455 ? Sb6 S13 2.590(13) . ? Sb6 S9 2.930(14) 2_547 ? Sb6 S8 3.229(16) 2_647 ? Sb6 S6 3.449(16) 2_546 ? Sb6 Sb4 3.736(15) 1_455 ? Sb6 Pb7 3.789(17) 2_646 ? Sb6 Sb11 3.95(2) 2_646 ? Sb6 Sb8 3.878(12) 2_546 ? Sb6 Sb7 4.03(3) 1_556 ? Sb6 Pb10 4.072(19) 1_556 ? Pb5 S7 2.818(7) . ? Pb5 S4 2.845(6) . ? Pb5 S17 2.881(6) . ? Pb5 S3 3.065(7) . ? Pb5 S9 3.164(7) 1_655 ? Pb5 S8 3.183(7) . ? Pb5 S18 3.514(6) 1_656 ? Pb5 Sb1 3.60(2) 1_656 ? Pb5 As1 3.65(4) 1_656 ? Pb5 As2 3.776(3) 1_556 ? Sb7 S9 2.58(2) 2_546 ? Sb7 S7 2.60(2) 2_646 ? Sb7 S6 2.78(2) 2_546 ? Sb7 S10 2.93(2) . ? Sb7 S19 3.24(2) 1_455 ? Sb7 S20 3.39(2) . ? Sb7 S13 3.57(2) . ? Sb7 Sb4 3.71(2) 1_455 ? Sb7 As3 3.74(2) . ? Sb7 Sb11 3.76(3) 2_646 ? Sb7 Pb7 4.04(2) 2_646 ? Sb7 As6 4.12(3) 1_554 ? Pb10 S9 2.670(14) 2_546 ? Pb10 S7 2.767(12) 2_646 ? Pb10 S6 2.819(14) 2_546 ? Pb10 S10 2.921(13) . ? Pb10 S19 3.094(12) 1_455 ? Pb10 S20 3.234(14) . ? Pb10 S13 3.520(13) . ? Pb10 Sb4 3.556(11) 1_455 ? Pb10 As3 3.681(12) . ? Pb10 Sb11 3.901(17) 2_646 ? Pb10 Pb7 4.169(14) 2_646 ? Pb10 Pb9 4.158(14) 1_454 ? Pb6 S8 2.744(7) 2_646 ? Pb6 S10 2.828(6) . ? Pb6 S19 2.908(7) . ? Pb6 S11 3.070(6) . ? Pb6 S7 3.137(7) 2_646 ? Pb6 S6 3.176(7) 2_646 ? Pb6 S12 3.592(6) . ? Pb6 As3 3.613(3) . ? Pb6 Sb4 3.694(2) . ? Pb6 Sb5 3.864(10) 1_554 ? Pb6 Pb9 4.181(7) 1_554 ? Pb6 Sb6 4.180(14) 1_554 ? Pb3 S20 2.889(7) . ? Pb3 S15 2.947(7) 1_455 ? Pb3 S2 2.973(6) . ? Pb3 S17 3.245(6) 1_455 ? Pb3 S18 3.284(6) . ? Pb3 S14 3.301(7) 1_455 ? Pb3 S4 3.365(6) . ? Pb3 S16 3.436(6) . ? Pb3 S1 3.517(7) . ? Pb3 As2 4.054(3) 1_455 ? Pb3 Pb4 4.1435(13) . ? Pb3 As3 4.161(3) . ? Pb4 S11 2.931(6) . ? Pb4 S15 2.974(6) . ? Pb4 S2 3.037(7) . ? Pb4 S17 3.172(7) . ? Pb4 S14 3.220(7) . ? Pb4 S3 3.335(6) . ? Pb4 S4 3.337(7) . ? Pb4 S1 3.397(7) . ? Pb4 S5 3.446(7) . ? Pb4 As3 4.101(3) . ? Pb4 As2 4.111(3) . ? Pb1 S1 2.976(7) . ? Pb1 S19 3.021(6) 1_556 ? Pb1 S16 3.063(6) . ? Pb1 S13 3.130(6) . ? Pb1 S14 3.141(7) 1_455 ? Pb1 S10 3.246(7) 1_556 ? Pb1 S11 3.254(6) 1_556 ? Pb1 S2 3.390(6) 1_556 ? Pb1 S15 3.453(7) 1_556 ? Pb1 Sb4 4.164(2) 1_455 ? Pb1 Pb2 4.2027(15) 1_455 ? Pb1 As2 4.207(3) 1_556 ? Pb2 S1 2.912(7) . ? Pb2 S3 2.978(7) . ? Pb2 S14 3.036(7) . ? Pb2 S12 3.112(6) . ? Pb2 S19 3.215(7) 1_556 ? Pb2 S20 3.360(6) 1_656 ? Pb2 S10 3.378(7) 1_656 ? Pb2 S15 3.405(6) 1_556 ? Pb2 S2 3.452(7) 1_656 ? Pb2 As2 4.129(3) 1_556 ? Pb2 Sb4 4.186(2) . ? Pb2 Pb1 4.2027(15) 1_655 ? Sb8 S4 2.360(7) . ? Sb8 S18 2.374(6) . ? Sb8 S5 2.415(6) . ? Sb8 S6 3.098(7) . ? Sb8 S7 3.215(7) . ? Sb8 S9 3.573(7) 1_554 ? Sb8 Pb9 3.781(8) 2_656 ? Sb8 Sb5 3.987(13) 2_656 ? Sb8 As6 4.209(13) 2_556 ? Sb8 Sb6 3.878(12) 2_556 ? As3 S1 2.213(8) . ? As3 S11 2.252(6) . ? As3 S20 2.281(6) . ? As3 S13 3.179(6) . ? As3 S12 3.242(6) . ? As3 S10 3.628(7) . ? As2 S15 2.247(8) . ? As2 S3 2.265(6) 1_554 ? As2 S16 2.298(6) 1_554 ? As2 S5 3.214(6) . ? As2 S18 3.248(6) 1_655 ? As2 Sb9 3.776(3) 1_554 ? As2 Pb5 3.776(3) 1_554 ? As2 Sb12 3.867(3) 1_554 ? As2 Pb8 3.867(3) 1_554 ? As2 S4 3.916(7) 1_554 ? Sb4 S14 2.426(7) . ? Sb4 S13 2.589(6) 1_655 ? Sb4 S12 2.718(6) . ? Sb4 S20 2.772(6) 1_655 ? Sb4 S11 2.947(5) . ? Sb4 Pb10 3.556(11) 1_655 ? Sb4 Sb7 3.71(2) 1_655 ? Sb4 Sb6 3.736(15) 1_655 ? Sb4 As6 3.54(2) 1_655 ? Sb4 S19 3.673(7) . ? S1 As2 4.008(8) 1_556 ? S1 Sb4 4.695(7) 1_455 ? S2 Pb1 3.390(6) 1_554 ? S2 Pb2 3.452(7) 1_454 ? S2 As2 4.675(6) 1_455 ? S2 Pb5 5.511(6) 1_454 ? S2 Sb9 5.511(6) 1_454 ? S3 As2 2.265(6) 1_556 ? S3 Sb1 3.07(2) 1_656 ? S3 As1 3.00(4) 1_656 ? S3 Pb3 4.622(6) 1_656 ? S4 As2 3.916(7) 1_556 ? S4 Sb10 4.831(7) 2_656 ? S4 Pb6 4.831(7) 2_656 ? S5 Sb12 3.476(6) 1_554 ? S5 Pb8 3.476(6) 1_554 ? S5 Pb9 3.974(11) 2_656 ? S5 Sb5 4.037(16) 2_656 ? S6 Pb7 2.737(10) 1_455 ? S6 Sb11 2.663(17) 1_455 ? S6 Pb10 2.819(14) 2_556 ? S6 Sb7 2.78(2) 2_556 ? S6 Sb10 3.176(7) 2_656 ? S6 Pb6 3.176(7) 2_656 ? S6 Sb6 3.449(16) 2_556 ? S6 As6 3.56(2) 2_556 ? S6 Sb4 4.063(7) 2_656 ? S7 Sb7 2.60(2) 2_656 ? S7 Pb10 2.767(13) 2_656 ? S7 Sb10 3.137(7) 2_656 ? S7 Pb6 3.137(7) 2_656 ? S7 Sb5 3.707(14) 2_656 ? S7 Pb9 3.427(11) 2_656 ? S7 As3 4.072(8) 2_656 ? S8 Sb10 2.744(7) 2_656 ? S8 Pb6 2.744(7) 2_656 ? S8 Sb5 2.673(14) 2_657 ? S8 Pb9 2.911(10) 2_657 ? S8 Sb6 3.229(16) 2_657 ? S8 As6 3.20(2) 2_657 ? S8 Sb11 3.713(16) 1_556 ? S8 Pb7 3.490(11) 1_556 ? S9 Pb10 2.670(14) 2_556 ? S9 Sb7 2.58(2) 2_556 ? S9 Pb9 2.779(11) 2_657 ? S9 Sb5 2.702(16) 2_657 ? S9 As6 3.226(16) 2_557 ? S9 Sb6 2.930(14) 2_557 ? S9 Sb9 3.164(7) 1_455 ? S9 Pb5 3.164(7) 1_455 ? S9 Sb8 3.573(7) 1_556 ? S9 Sb1 3.97(2) 1_556 ? S10 Sb6 2.469(16) 1_554 ? S10 As6 2.29(2) 1_554 ? S10 Pb1 3.246(7) 1_554 ? S10 Pb2 3.378(7) 1_454 ? S10 Sb4 4.623(7) 1_454 ? S10 Sb5 4.740(14) 1_554 ? S10 Pb9 4.952(10) 1_554 ? S11 Pb1 3.254(6) 1_554 ? S11 Pb2 5.147(5) 1_454 ? S12 As6 2.44(2) 1_655 ? S12 Sb6 2.420(16) 1_655 ? S12 Sb8 4.319(7) 2_646 ? S12 Sb7 4.73(2) 1_656 ? S12 Pb10 4.683(13) 1_656 ? S13 Sb4 2.589(6) 1_455 ? S13 Pb7 4.204(10) 2_646 ? S13 Sb11 4.165(17) 2_646 ? S13 Sb10 4.668(6) 1_556 ? S14 Pb1 3.141(7) 1_655 ? S14 Pb3 3.301(7) 1_655 ? S14 Sb1 4.083(16) 1_656 ? S14 As1 3.76(2) 1_656 ? S14 Sb6 4.909(16) 1_655 ? S14 As6 4.64(2) 1_655 ? S14 As3 4.834(7) 1_655 ? S15 Pb3 2.947(7) 1_655 ? S15 Pb2 3.405(6) 1_554 ? S15 Pb1 3.453(7) 1_554 ? S15 Sb1 5.05(3) 1_655 ? S15 As1 5.12(4) 1_655 ? S16 As2 2.298(6) 1_556 ? S16 As1 2.53(3) 1_556 ? S16 Sb1 2.79(2) 1_556 ? S16 Pb4 4.697(6) 1_556 ? S17 Sb12 3.080(7) 1_655 ? S17 Pb8 3.080(7) 1_655 ? S17 Pb3 3.245(6) 1_655 ? S17 Sb1 3.75(2) 1_656 ? S17 As1 3.56(3) 1_656 ? S18 Pb7 2.818(9) 1_455 ? S18 Sb11 3.124(13) 1_455 ? S18 As2 3.248(6) 1_455 ? S18 Sb9 3.514(6) 1_454 ? S18 Pb5 3.514(6) 1_454 ? S18 As6 4.369(18) 2_556 ? S18 Sb6 4.068(15) 2_556 ? S19 Sb5 2.476(15) 1_554 ? S19 Pb9 2.689(10) 1_554 ? S19 Pb1 3.021(6) 1_554 ? S19 Pb10 3.094(12) 1_655 ? S19 Sb7 3.24(2) 1_655 ? S19 Pb2 3.215(7) 1_554 ? S19 As3 4.574(7) 1_554 ? S19 Sb6 4.981(13) 1_554 ? S19 As6 4.684(15) 1_554 ? S20 Sb4 2.772(6) 1_455 ? S20 Pb2 3.360(6) 1_454 ? S20 Pb1 5.029(5) 1_554 ? S20 As2 5.255(7) 1_455 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag S19 Sb5 S9 93.6(5) 1_556 2_647 ? S19 Sb5 S8 94.0(4) 1_556 2_647 ? S9 Sb5 S8 92.8(5) 2_647 2_647 ? S19 Sb5 S12 84.5(4) 1_556 . ? S9 Sb5 S12 79.8(4) 2_647 . ? S8 Sb5 S12 172.4(6) 2_647 . ? S19 Sb5 S13 84.0(4) 1_556 . ? S9 Sb5 S13 176.8(5) 2_647 . ? S8 Sb5 S13 85.4(4) 2_647 . ? S12 Sb5 S13 101.9(4) . . ? S19 Sb5 S7 148.2(6) 1_556 2_646 ? S9 Sb5 S7 110.3(4) 2_647 2_646 ? S8 Sb5 S7 105.1(5) 2_647 2_646 ? S12 Sb5 S7 79.6(3) . 2_646 ? S13 Sb5 S7 72.8(3) . 2_646 ? S19 Sb5 Sb8 148.3(5) 1_556 2_646 ? S9 Sb5 Sb8 61.0(3) 2_647 2_646 ? S8 Sb5 Sb8 105.1(5) 2_647 2_646 ? S12 Sb5 Sb8 73.2(2) . 2_646 ? S13 Sb5 Sb8 121.9(4) . 2_646 ? S7 Sb5 Sb8 49.23(18) 2_646 2_646 ? S19 Sb5 Sb11 147.8(5) 1_556 2_646 ? S9 Sb5 Sb11 110.6(5) 2_647 2_646 ? S8 Sb5 Sb11 64.8(4) 2_647 2_646 ? S12 Sb5 Sb11 119.5(4) . 2_646 ? S13 Sb5 Sb11 70.9(4) . 2_646 ? S7 Sb5 Sb11 40.2(2) 2_646 2_646 ? Sb8 Sb5 Sb11 63.8(3) 2_646 2_646 ? S19 Sb5 Pb7 144.6(5) 1_556 2_646 ? S9 Sb5 Pb7 109.8(5) 2_647 2_646 ? S8 Sb5 Pb7 59.6(3) 2_647 2_646 ? S12 Sb5 Pb7 124.7(4) . 2_646 ? S13 Sb5 Pb7 71.5(3) . 2_646 ? S7 Sb5 Pb7 45.4(2) 2_646 2_646 ? Sb8 Sb5 Pb7 66.6(2) 2_646 2_646 ? Sb11 Sb5 Pb7 5.2(2) 2_646 2_646 ? S19 Sb5 As3 85.4(4) 1_556 . ? S9 Sb5 As3 131.3(4) 2_647 . ? S8 Sb5 As3 135.9(5) 2_647 . ? S12 Sb5 As3 51.6(2) . . ? S13 Sb5 As3 50.6(2) . . ? S7 Sb5 As3 63.2(2) 2_646 . ? Sb8 Sb5 As3 97.4(2) 2_646 . ? Sb11 Sb5 As3 93.5(3) 2_646 . ? Pb7 Sb5 As3 97.5(3) 2_646 . ? S19 Sb5 S5 151.7(5) 1_556 2_646 ? S9 Sb5 S5 65.0(3) 2_647 2_646 ? S8 Sb5 S5 70.1(4) 2_647 2_646 ? S12 Sb5 S5 108.0(3) . 2_646 ? S13 Sb5 S5 116.6(4) . 2_646 ? S7 Sb5 S5 60.1(2) 2_646 2_646 ? Sb8 Sb5 S5 35.03(15) 2_646 2_646 ? Sb11 Sb5 S5 45.6(3) 2_646 2_646 ? Pb7 Sb5 S5 45.4(2) 2_646 2_646 ? As3 Sb5 S5 122.5(3) . 2_646 ? S19 Sb5 Sb10 48.8(2) 1_556 1_556 ? S9 Sb5 Sb10 93.9(3) 2_647 1_556 ? S8 Sb5 Sb10 45.2(2) 2_647 1_556 ? S12 Sb5 Sb10 132.7(4) . 1_556 ? S13 Sb5 Sb10 83.0(3) . 1_556 ? S7 Sb5 Sb10 143.8(4) 2_646 1_556 ? Sb8 Sb5 Sb10 142.8(4) 2_646 1_556 ? Sb11 Sb5 Sb10 106.7(3) 2_646 1_556 ? Pb7 Sb5 Sb10 101.7(3) 2_646 1_556 ? As3 Sb5 Sb10 119.6(4) . 1_556 ? S5 Sb5 Sb10 111.3(3) 2_646 1_556 ? S19 Pb9 S9 87.3(3) 1_556 2_647 ? S19 Pb9 S8 84.5(3) 1_556 2_647 ? S9 Pb9 S8 86.3(3) 2_647 2_647 ? S19 Pb9 S12 85.1(3) 1_556 . ? S9 Pb9 S12 82.3(3) 2_647 . ? S8 Pb9 S12 164.8(4) 2_647 . ? S19 Pb9 S13 81.1(3) 1_556 . ? S9 Pb9 S13 164.3(3) 2_647 . ? S8 Pb9 S13 82.0(3) 2_647 . ? S12 Pb9 S13 107.2(3) . . ? S19 Pb9 S7 153.6(4) 1_556 2_646 ? S9 Pb9 S7 116.5(3) 2_647 2_646 ? S8 Pb9 S7 107.0(3) 2_647 2_646 ? S12 Pb9 S7 87.1(2) . 2_646 ? S13 Pb9 S7 77.2(2) . 2_646 ? S19 Pb9 Sb8 148.3(3) 1_556 2_646 ? S9 Pb9 Sb8 63.9(2) 2_647 2_646 ? S8 Pb9 Sb8 105.3(3) 2_647 2_646 ? S12 Pb9 Sb8 78.44(19) . 2_646 ? S13 Pb9 Sb8 129.5(3) . 2_646 ? S7 Pb9 Sb8 52.69(15) 2_646 2_646 ? S19 Pb9 Sb11 141.7(4) 1_556 2_646 ? S9 Pb9 Sb11 111.6(4) 2_647 2_646 ? S8 Pb9 Sb11 64.9(3) 2_647 2_646 ? S12 Pb9 Sb11 128.9(3) . 2_646 ? S13 Pb9 Sb11 72.6(3) . 2_646 ? S7 Pb9 Sb11 42.1(2) 2_646 2_646 ? Sb8 Pb9 Sb11 66.6(3) 2_646 2_646 ? S19 Pb9 Pb7 137.6(3) 1_556 2_646 ? S9 Pb9 Pb7 110.0(3) 2_647 2_646 ? S8 Pb9 Pb7 59.6(2) 2_647 2_646 ? S12 Pb9 Pb7 134.1(3) . 2_646 ? S13 Pb9 Pb7 72.8(2) . 2_646 ? S7 Pb9 Pb7 47.39(18) 2_646 2_646 ? Sb8 Pb9 Pb7 69.34(18) 2_646 2_646 ? Sb11 Pb9 Pb7 5.3(2) 2_646 2_646 ? S19 Pb9 As3 87.1(3) 1_556 . ? S9 Pb9 As3 137.2(3) 2_647 . ? S8 Pb9 As3 135.2(3) 2_647 . ? S12 Pb9 As3 55.02(18) . . ? S13 Pb9 As3 53.19(17) . . ? S7 Pb9 As3 67.89(19) 2_646 . ? Sb8 Pb9 As3 104.72(17) 2_646 . ? Sb11 Pb9 As3 98.5(3) 2_646 . ? Pb7 Pb9 As3 102.4(2) 2_646 . ? S19 Pb9 S5 142.7(3) 1_556 2_646 ? S9 Pb9 S5 65.6(2) 2_647 2_646 ? S8 Pb9 S5 69.3(2) 2_647 2_646 ? S12 Pb9 S5 114.1(3) . 2_646 ? S13 Pb9 S5 119.0(3) . 2_646 ? S7 Pb9 S5 62.9(2) 2_646 2_646 ? Sb8 Pb9 S5 36.19(11) 2_646 2_646 ? Sb11 Pb9 S5 46.6(3) 2_646 2_646 ? Pb7 Pb9 S5 46.23(18) 2_646 2_646 ? As3 Pb9 S5 130.2(2) . 2_646 ? S19 Pb9 Sb10 43.72(17) 1_556 1_556 ? S9 Pb9 Sb10 86.1(2) 2_647 1_556 ? S8 Pb9 Sb10 40.81(17) 2_647 1_556 ? S12 Pb9 Sb10 128.0(3) . 1_556 ? S13 Pb9 Sb10 78.13(18) . 1_556 ? S7 Pb9 Sb10 141.9(3) 2_646 1_556 ? Sb8 Pb9 Sb10 138.2(2) 2_646 1_556 ? Sb11 Pb9 Sb10 102.6(2) 2_646 1_556 ? Pb7 Pb9 Sb10 97.52(18) 2_646 1_556 ? As3 Pb9 Sb10 116.9(2) . 1_556 ? S5 Pb9 Sb10 106.3(2) 2_646 1_556 ? S6 Pb8 S8 88.0(2) . . ? S6 Pb8 S4 85.13(19) . . ? S8 Pb8 S4 88.17(19) . . ? S6 Pb8 S9 80.63(18) . . ? S8 Pb8 S9 85.1(2) . . ? S4 Pb8 S9 164.43(19) . . ? S6 Pb8 S17 80.78(19) . 1_455 ? S8 Pb8 S17 168.63(18) . 1_455 ? S4 Pb8 S17 92.94(18) . 1_455 ? S9 Pb8 S17 90.99(18) . 1_455 ? S6 Pb8 S16 146.21(18) . . ? S8 Pb8 S16 114.02(18) . . ? S4 Pb8 S16 71.11(16) . . ? S9 Pb8 S16 124.47(17) . . ? S17 Pb8 S16 76.95(16) 1_455 . ? S6 Pb8 As1 141.3(7) . 1_556 ? S8 Pb8 As1 123.6(5) . 1_556 ? S4 Pb8 As1 114.6(4) . 1_556 ? S9 Pb8 As1 80.7(4) . 1_556 ? S17 Pb8 As1 66.0(5) 1_455 1_556 ? S16 Pb8 As1 44.7(5) . 1_556 ? S6 Pb8 Sb1 141.1(4) . 1_556 ? S8 Pb8 Sb1 119.6(3) . 1_556 ? S4 Pb8 Sb1 119.7(3) . 1_556 ? S9 Pb8 Sb1 75.7(3) . 1_556 ? S17 Pb8 Sb1 69.4(4) 1_455 1_556 ? S16 Pb8 Sb1 49.1(3) . 1_556 ? As1 Pb8 Sb1 5.7(4) 1_556 1_556 ? S6 Pb8 S5 150.16(18) . 1_556 ? S8 Pb8 S5 78.65(18) . 1_556 ? S4 Pb8 S5 120.55(16) . 1_556 ? S9 Pb8 S5 71.78(17) . 1_556 ? S17 Pb8 S5 110.27(16) 1_455 1_556 ? S16 Pb8 S5 62.95(15) . 1_556 ? As1 Pb8 S5 45.0(5) 1_556 1_556 ? Sb1 Pb8 S5 41.0(3) 1_556 1_556 ? S6 Pb8 As2 150.52(13) . 1_556 ? S8 Pb8 As2 77.59(16) . 1_556 ? S4 Pb8 As2 68.99(13) . 1_556 ? S9 Pb8 As2 122.82(15) . 1_556 ? S17 Pb8 As2 113.35(14) 1_455 1_556 ? S16 Pb8 As2 36.44(11) . 1_556 ? As1 Pb8 As2 66.0(6) 1_556 1_556 ? Sb1 Pb8 As2 67.4(4) 1_556 1_556 ? S5 Pb8 As2 51.59(11) 1_556 1_556 ? S6 Pb8 Pb7 41.67(18) . 1_455 ? S8 Pb8 Pb7 129.64(19) . 1_455 ? S4 Pb8 Pb7 85.43(16) . 1_455 ? S9 Pb8 Pb7 88.10(17) . 1_455 ? S17 Pb8 Pb7 39.35(17) 1_455 1_455 ? S16 Pb8 Pb7 110.77(15) . 1_455 ? As1 Pb8 Pb7 104.2(6) 1_556 1_455 ? Sb1 Pb8 Pb7 106.6(4) 1_556 1_455 ? S5 Pb8 Pb7 144.50(15) 1_556 1_455 ? As2 Pb8 Pb7 142.89(11) 1_556 1_455 ? S6 Pb8 Sb8 49.98(14) . . ? S8 Pb8 Sb8 88.16(15) . . ? S4 Pb8 Sb8 35.16(13) . . ? S9 Pb8 Sb8 130.36(15) . . ? S17 Pb8 Sb8 86.26(13) 1_455 . ? S16 Pb8 Sb8 103.10(11) . . ? As1 Pb8 Sb8 139.9(3) 1_556 . ? Sb1 Pb8 Sb8 145.6(2) 1_556 . ? S5 Pb8 Sb8 153.47(10) 1_556 . ? As2 Pb8 Sb8 103.31(6) 1_556 . ? Pb7 Pb8 Sb8 59.94(11) 1_455 . ? S17 Pb7 S6 90.5(3) . 1_655 ? S17 Pb7 S7 84.9(3) . . ? S6 Pb7 S7 83.1(3) 1_655 . ? S17 Pb7 S18 90.0(3) . 1_655 ? S6 Pb7 S18 84.3(3) 1_655 1_655 ? S7 Pb7 S18 166.3(4) . 1_655 ? S17 Pb7 S5 84.4(3) . . ? S6 Pb7 S5 162.4(3) 1_655 . ? S7 Pb7 S5 79.7(2) . . ? S18 Pb7 S5 112.5(3) 1_655 . ? S17 Pb7 S8 155.3(3) . 1_554 ? S6 Pb7 S8 113.3(3) 1_655 1_554 ? S7 Pb7 S8 103.9(3) . 1_554 ? S18 Pb7 S8 85.9(2) 1_655 1_554 ? S5 Pb7 S8 74.8(2) . 1_554 ? S17 Pb7 As2 85.2(2) . . ? S6 Pb7 As2 141.3(3) 1_655 . ? S7 Pb7 As2 134.5(3) . . ? S18 Pb7 As2 57.32(17) 1_655 . ? S5 Pb7 As2 55.15(17) . . ? S8 Pb7 As2 72.06(18) 1_554 . ? S17 Pb7 Sb6 148.5(4) . 2_656 ? S6 Pb7 Sb6 61.3(3) 1_655 2_656 ? S7 Pb7 Sb6 103.8(3) . 2_656 ? S18 Pb7 Sb6 74.4(3) 1_655 2_656 ? S5 Pb7 Sb6 126.7(3) . 2_656 ? S8 Pb7 Sb6 52.5(3) 1_554 2_656 ? As2 Pb7 Sb6 107.5(3) . 2_656 ? S17 Pb7 As6 151.4(4) . 2_656 ? S6 Pb7 As6 62.2(4) 1_655 2_656 ? S7 Pb7 As6 99.1(3) . 2_656 ? S18 Pb7 As6 79.5(3) 1_655 2_656 ? S5 Pb7 As6 124.2(4) . 2_656 ? S8 Pb7 As6 51.1(3) 1_554 2_656 ? As2 Pb7 As6 110.2(3) . 2_656 ? Sb6 Pb7 As6 5.2(3) 2_656 2_656 ? S17 Pb7 Sb5 140.2(3) . 2_656 ? S6 Pb7 Sb5 106.6(3) 1_655 2_656 ? S7 Pb7 Sb5 62.6(2) . 2_656 ? S18 Pb7 Sb5 126.6(3) 1_655 2_656 ? S5 Pb7 Sb5 68.4(3) . 2_656 ? S8 Pb7 Sb5 41.4(2) 1_554 2_656 ? As2 Pb7 Sb5 101.0(3) . 2_656 ? Sb6 Pb7 Sb5 67.1(3) 2_656 2_656 ? As6 Pb7 Sb5 62.5(3) 2_656 2_656 ? S17 Pb7 Pb9 136.3(3) . 2_656 ? S6 Pb7 Pb9 105.4(3) 1_655 2_656 ? S7 Pb7 Pb9 58.0(2) . 2_656 ? S18 Pb7 Pb9 131.2(3) 1_655 2_656 ? S5 Pb7 Pb9 68.2(2) . 2_656 ? S8 Pb7 Pb9 45.99(18) 1_554 2_656 ? As2 Pb7 Pb9 104.0(2) . 2_656 ? Sb6 Pb7 Pb9 69.8(2) 2_656 2_656 ? As6 Pb7 Pb9 65.0(3) 2_656 2_656 ? Sb5 Pb7 Pb9 4.6(2) 2_656 2_656 ? S17 Pb7 Pb10 92.3(3) . 2_656 ? S6 Pb7 Pb10 42.1(2) 1_655 2_656 ? S7 Pb7 Pb10 41.5(2) . 2_656 ? S18 Pb7 Pb10 126.4(3) 1_655 2_656 ? S5 Pb7 Pb10 121.1(3) . 2_656 ? S8 Pb7 Pb10 109.7(3) 1_554 2_656 ? As2 Pb7 Pb10 175.6(3) . 2_656 ? Sb6 Pb7 Pb10 76.4(3) 2_656 2_656 ? As6 Pb7 Pb10 73.5(4) 2_656 2_656 ? Sb5 Pb7 Pb10 78.6(3) 2_656 2_656 ? Pb9 Pb7 Pb10 75.4(2) 2_656 2_656 ? S17 Sb11 S6 95.1(6) . 1_655 ? S17 Sb11 S7 95.0(4) . . ? S6 Sb11 S7 91.2(4) 1_655 . ? S17 Sb11 S18 85.7(5) . 1_655 ? S6 Sb11 S18 79.8(4) 1_655 1_655 ? S7 Sb11 S18 170.9(6) . 1_655 ? S17 Sb11 S5 86.4(5) . . ? S6 Sb11 S5 175.8(5) 1_655 . ? S7 Sb11 S5 84.8(4) . . ? S18 Sb11 S5 104.3(4) 1_655 . ? S17 Sb11 S8 147.9(5) . 1_554 ? S6 Sb11 S8 108.7(5) 1_655 1_554 ? S7 Sb11 S8 105.5(5) . 1_554 ? S18 Sb11 S8 77.9(3) 1_655 1_554 ? S5 Sb11 S8 71.5(3) . 1_554 ? S17 Sb11 As2 81.2(4) . . ? S6 Sb11 As2 132.2(4) 1_655 . ? S7 Sb11 As2 136.6(5) . . ? S18 Sb11 As2 52.45(19) 1_655 . ? S5 Sb11 As2 51.9(2) . . ? S8 Sb11 As2 66.8(2) 1_554 . ? S17 Sb11 Sb6 145.8(6) . 2_656 ? S6 Sb11 Sb6 59.0(4) 1_655 2_656 ? S7 Sb11 Sb6 106.6(5) . 2_656 ? S18 Sb11 Sb6 69.0(3) 1_655 2_656 ? S5 Sb11 Sb6 121.1(5) . 2_656 ? S8 Sb11 Sb6 49.7(3) 1_554 2_656 ? As2 Sb11 Sb6 99.5(3) . 2_656 ? S17 Sb11 As6 150.0(6) . 2_656 ? S6 Sb11 As6 60.2(4) 1_655 2_656 ? S7 Sb11 As6 101.8(5) . 2_656 ? S18 Sb11 As6 74.0(3) 1_655 2_656 ? S5 Sb11 As6 119.5(5) . 2_656 ? S8 Sb11 As6 48.6(4) 1_554 2_656 ? As2 Sb11 As6 102.3(4) . 2_656 ? Sb6 Sb11 As6 5.1(3) 2_656 2_656 ? S17 Sb11 Sb5 148.4(6) . 2_656 ? S6 Sb11 Sb5 108.7(5) 1_655 2_656 ? S7 Sb11 Sb5 64.8(4) . 2_656 ? S18 Sb11 Sb5 118.2(4) 1_655 2_656 ? S5 Sb11 Sb5 68.6(4) . 2_656 ? S8 Sb11 Sb5 40.7(2) 1_554 2_656 ? As2 Sb11 Sb5 96.8(4) . 2_656 ? Sb6 Sb11 Sb5 65.7(3) 2_656 2_656 ? As6 Sb11 Sb5 61.4(3) 2_656 2_656 ? S17 Sb11 Pb9 145.4(5) . 2_656 ? S6 Sb11 Pb9 108.3(5) 1_655 2_656 ? S7 Sb11 Pb9 60.3(3) . 2_656 ? S18 Sb11 Pb9 122.7(4) 1_655 2_656 ? S5 Sb11 Pb9 68.7(4) . 2_656 ? S8 Sb11 Pb9 45.2(2) 1_554 2_656 ? As2 Sb11 Pb9 100.0(4) . 2_656 ? Sb6 Sb11 Pb9 68.5(3) 2_656 2_656 ? As6 Sb11 Pb9 64.0(3) 2_656 2_656 ? Sb5 Sb11 Pb9 4.6(2) 2_656 2_656 ? S17 Sb11 Pb10 101.0(4) . 2_656 ? S6 Sb11 Pb10 46.3(3) 1_655 2_656 ? S7 Sb11 Pb10 45.1(3) . 2_656 ? S18 Sb11 Pb10 125.9(5) 1_655 2_656 ? S5 Sb11 Pb10 129.6(4) . 2_656 ? S8 Sb11 Pb10 111.0(4) 1_554 2_656 ? As2 Sb11 Pb10 177.2(4) . 2_656 ? Sb6 Sb11 Pb10 77.8(4) 2_656 2_656 ? As6 Sb11 Pb10 75.0(4) 2_656 2_656 ? Sb5 Sb11 Pb10 82.1(4) 2_656 2_656 ? Pb9 Sb11 Pb10 79.1(3) 2_656 2_656 ? S2 As1 S5 94.2(11) . . ? S2 As1 S16 96.0(11) . 1_554 ? S5 As1 S16 84.9(12) . 1_554 ? S2 As1 S18 86.8(9) . . ? S5 As1 S18 77.1(4) . . ? S16 As1 S18 161.9(13) 1_554 . ? S2 As1 S3 86.9(12) . 1_454 ? S5 As1 S3 150.0(10) . 1_454 ? S16 As1 S3 124.9(7) 1_554 1_454 ? S18 As1 S3 73.1(9) . 1_454 ? S2 As1 Sb12 152.6(16) . 1_554 ? S5 As1 Sb12 68.4(8) . 1_554 ? S16 As1 Sb12 62.6(8) 1_554 1_554 ? S18 As1 Sb12 108.4(8) . 1_554 ? S3 As1 Sb12 118.9(10) 1_454 1_554 ? S2 As1 Pb8 152.6(16) . 1_554 ? S5 As1 Pb8 68.4(8) . 1_554 ? S16 As1 Pb8 62.6(8) 1_554 1_554 ? S18 As1 Pb8 108.4(8) . 1_554 ? S3 As1 Pb8 118.9(10) 1_454 1_554 ? Sb12 As1 Pb8 0.00(3) 1_554 1_554 ? S2 As1 Sb8 93.1(6) . . ? S5 As1 Sb8 38.8(3) . . ? S16 As1 Sb8 123.5(12) 1_554 . ? S18 As1 Sb8 38.4(2) . . ? S3 As1 Sb8 111.2(8) 1_454 . ? Sb12 As1 Sb8 86.1(6) 1_554 . ? Pb8 As1 Sb8 86.1(6) 1_554 . ? S2 As1 Sb9 134.9(15) . 1_454 ? S5 As1 Sb9 109.2(8) . 1_454 ? S16 As1 Sb9 123.3(10) 1_554 1_454 ? S18 As1 Sb9 63.0(6) . 1_454 ? S3 As1 Sb9 53.8(6) 1_454 1_454 ? Sb12 As1 Sb9 72.3(6) 1_554 1_454 ? Pb8 As1 Sb9 72.3(6) 1_554 1_454 ? Sb8 As1 Sb9 83.4(5) . 1_454 ? S2 As1 Pb5 134.9(15) . 1_454 ? S5 As1 Pb5 109.2(8) . 1_454 ? S16 As1 Pb5 123.3(10) 1_554 1_454 ? S18 As1 Pb5 63.0(6) . 1_454 ? S3 As1 Pb5 53.8(6) 1_454 1_454 ? Sb12 As1 Pb5 72.3(6) 1_554 1_454 ? Pb8 As1 Pb5 72.3(6) 1_554 1_454 ? Sb8 As1 Pb5 83.4(5) . 1_454 ? Sb9 As1 Pb5 0.00(5) 1_454 1_454 ? S2 As1 S17 144.3(10) . 1_454 ? S5 As1 S17 119.6(12) . 1_454 ? S16 As1 S17 77.7(6) 1_554 1_454 ? S18 As1 S17 110.0(10) . 1_454 ? S3 As1 S17 69.6(7) 1_454 1_454 ? Sb12 As1 S17 52.2(5) 1_554 1_454 ? Pb8 As1 S17 52.2(5) 1_554 1_454 ? Sb8 As1 S17 119.9(8) . 1_454 ? Sb9 As1 S17 47.1(4) 1_454 1_454 ? Pb5 As1 S17 47.1(4) 1_454 1_454 ? S2 As1 S14 81.3(7) . 1_454 ? S5 As1 S14 148.5(12) . 1_454 ? S16 As1 S14 64.8(4) 1_554 1_454 ? S18 As1 S14 133.3(13) . 1_454 ? S3 As1 S14 61.3(5) 1_454 1_454 ? Sb12 As1 S14 102.3(6) 1_554 1_454 ? Pb8 As1 S14 102.3(6) 1_554 1_454 ? Sb8 As1 S14 170.7(11) . 1_454 ? Sb9 As1 S14 95.3(7) 1_454 1_454 ? Pb5 As1 S14 95.3(7) 1_454 1_454 ? S17 As1 S14 64.2(4) 1_454 1_454 ? S2 Sb1 S5 99.4(8) . . ? S2 Sb1 S16 88.8(7) . 1_554 ? S5 Sb1 S16 83.5(8) . 1_554 ? S2 Sb1 S18 94.2(7) . . ? S5 Sb1 S18 86.8(4) . . ? S16 Sb1 S18 170.2(9) 1_554 . ? S2 Sb1 S3 84.8(7) . 1_454 ? S5 Sb1 S3 162.7(7) . 1_454 ? S16 Sb1 S3 113.4(5) 1_554 1_454 ? S18 Sb1 S3 76.2(6) . 1_454 ? S2 Sb1 Sb12 147.2(9) . 1_554 ? S5 Sb1 Sb12 69.3(6) . 1_554 ? S16 Sb1 Sb12 60.0(4) 1_554 1_554 ? S18 Sb1 Sb12 115.0(6) . 1_554 ? S3 Sb1 Sb12 115.3(6) 1_454 1_554 ? S2 Sb1 Pb8 147.2(9) . 1_554 ? S5 Sb1 Pb8 69.3(6) . 1_554 ? S16 Sb1 Pb8 60.0(4) 1_554 1_554 ? S18 Sb1 Pb8 115.0(6) . 1_554 ? S3 Sb1 Pb8 115.3(6) 1_454 1_554 ? Sb12 Sb1 Pb8 0.00(4) 1_554 1_554 ? S2 Sb1 Sb8 102.0(6) . . ? S5 Sb1 Sb8 43.9(3) . . ? S16 Sb1 Sb8 127.2(8) 1_554 . ? S18 Sb1 Sb8 43.0(2) . . ? S3 Sb1 Sb8 118.9(7) 1_454 . ? Sb12 Sb1 Sb8 90.9(5) 1_554 . ? Pb8 Sb1 Sb8 90.9(5) 1_554 . ? S2 Sb1 Sb9 136.8(10) . 1_454 ? S5 Sb1 Sb9 116.4(7) . 1_454 ? S16 Sb1 Sb9 117.2(6) 1_554 1_454 ? S18 Sb1 Sb9 66.3(5) . 1_454 ? S3 Sb1 Sb9 54.0(4) 1_454 1_454 ? Sb12 Sb1 Sb9 72.4(4) 1_554 1_454 ? Pb8 Sb1 Sb9 72.4(4) 1_554 1_454 ? Sb8 Sb1 Sb9 89.3(4) . 1_454 ? S2 Sb1 Pb5 136.8(10) . 1_454 ? S5 Sb1 Pb5 116.4(7) . 1_454 ? S16 Sb1 Pb5 117.2(6) 1_554 1_454 ? S18 Sb1 Pb5 66.3(5) . 1_454 ? S3 Sb1 Pb5 54.0(4) 1_454 1_454 ? Sb12 Sb1 Pb5 72.4(4) 1_554 1_454 ? Pb8 Sb1 Pb5 72.4(4) 1_554 1_454 ? Sb8 Sb1 Pb5 89.3(4) . 1_454 ? Sb9 Sb1 Pb5 0.00(5) 1_454 1_454 ? S2 Sb1 S17 132.9(6) . 1_454 ? S5 Sb1 S17 119.4(8) . 1_454 ? S16 Sb1 S17 71.6(4) 1_554 1_454 ? S18 Sb1 S17 112.4(7) . 1_454 ? S3 Sb1 S17 66.2(4) 1_454 1_454 ? Sb12 Sb1 S17 50.2(3) 1_554 1_454 ? Pb8 Sb1 S17 50.2(3) 1_554 1_454 ? Sb8 Sb1 S17 124.2(6) . 1_454 ? Sb9 Sb1 S17 46.1(3) 1_454 1_454 ? Pb5 Sb1 S17 46.1(3) 1_454 1_454 ? S2 Sb1 S14 73.8(4) . 1_454 ? S5 Sb1 S14 140.7(8) . 1_454 ? S16 Sb1 S14 58.1(3) 1_554 1_454 ? S18 Sb1 S14 131.8(8) . 1_454 ? S3 Sb1 S14 56.6(3) 1_454 1_454 ? Sb12 Sb1 S14 95.2(4) 1_554 1_454 ? Pb8 Sb1 S14 95.2(4) 1_554 1_454 ? Sb8 Sb1 S14 173.6(7) . 1_454 ? Sb9 Sb1 S14 90.7(4) 1_454 1_454 ? Pb5 Sb1 S14 90.7(4) 1_454 1_454 ? S17 Sb1 S14 59.4(3) 1_454 1_454 ? S10 As6 S12 94.0(8) 1_556 1_455 ? S10 As6 S13 97.9(5) 1_556 . ? S12 As6 S13 96.8(8) 1_455 . ? S10 As6 S9 82.4(6) 1_556 2_547 ? S12 As6 S9 82.8(5) 1_455 2_547 ? S13 As6 S9 179.4(10) . 2_547 ? S10 As6 S8 85.4(7) 1_556 2_647 ? S12 As6 S8 172.6(6) 1_455 2_647 ? S13 As6 S8 90.6(6) . 2_647 ? S9 As6 S8 89.9(5) 2_547 2_647 ? S10 As6 S6 172.6(9) 1_556 2_546 ? S12 As6 S6 80.5(5) 1_455 2_546 ? S13 As6 S6 78.0(6) . 2_546 ? S9 As6 S6 101.6(4) 2_547 2_546 ? S8 As6 S6 100.7(6) 2_647 2_546 ? S10 As6 Sb4 102.9(6) 1_556 1_455 ? S12 As6 Sb4 50.1(4) 1_455 1_455 ? S13 As6 Sb4 47.0(4) . 1_455 ? S9 As6 Sb4 132.6(6) 2_547 1_455 ? S8 As6 Sb4 137.2(5) 2_647 1_455 ? S6 As6 Sb4 69.8(4) 2_546 1_455 ? S10 As6 Pb7 143.3(8) 1_556 2_646 ? S12 As6 Pb7 122.7(7) 1_455 2_646 ? S13 As6 Pb7 81.4(6) . 2_646 ? S9 As6 Pb7 98.6(4) 2_547 2_646 ? S8 As6 Pb7 58.0(4) 2_647 2_646 ? S6 As6 Pb7 42.8(3) 2_546 2_646 ? Sb4 As6 Pb7 102.9(5) 1_455 2_646 ? S10 As6 Sb11 145.1(8) 1_556 2_646 ? S12 As6 Sb11 120.9(7) 1_455 2_646 ? S13 As6 Sb11 77.0(6) . 2_646 ? S9 As6 Sb11 103.0(5) 2_547 2_646 ? S8 As6 Sb11 60.4(4) 2_647 2_646 ? S6 As6 Sb11 40.4(3) 2_546 2_646 ? Sb4 As6 Sb11 98.4(5) 1_455 2_646 ? Pb7 As6 Sb11 4.8(2) 2_646 2_646 ? S10 As6 Sb8 137.5(6) 1_556 2_546 ? S12 As6 Sb8 75.9(4) 1_455 2_546 ? S13 As6 Sb8 124.0(7) . 2_546 ? S9 As6 Sb8 55.6(2) 2_547 2_546 ? S8 As6 Sb8 99.7(5) 2_647 2_546 ? S6 As6 Sb8 46.0(2) 2_546 2_546 ? Sb4 As6 Sb8 101.4(5) 1_455 2_546 ? Pb7 As6 Sb8 60.1(3) 2_646 2_546 ? Sb11 As6 Sb8 62.1(3) 2_646 2_546 ? S10 As6 Sb7 43.8(5) 1_556 1_556 ? S12 As6 Sb7 88.3(6) 1_455 1_556 ? S13 As6 Sb7 141.7(7) . 1_556 ? S9 As6 Sb7 38.7(4) 2_547 1_556 ? S8 As6 Sb7 86.2(6) 2_647 1_556 ? S6 As6 Sb7 140.1(4) 2_546 1_556 ? Sb4 As6 Sb7 128.6(7) 1_455 1_556 ? Pb7 As6 Sb7 126.9(6) 2_646 1_556 ? Sb11 As6 Sb7 131.7(6) 2_646 1_556 ? Sb8 As6 Sb7 94.1(4) 2_546 1_556 ? S10 As6 Pb10 42.6(4) 1_556 1_556 ? S12 As6 Pb10 86.2(6) 1_455 1_556 ? S13 As6 Pb10 140.4(7) . 1_556 ? S9 As6 Pb10 39.9(3) 2_547 1_556 ? S8 As6 Pb10 88.4(5) 2_647 1_556 ? S6 As6 Pb10 140.9(4) 2_546 1_556 ? Sb4 As6 Pb10 126.0(6) 1_455 1_556 ? Pb7 As6 Pb10 129.4(5) 2_646 1_556 ? Sb11 As6 Pb10 134.2(5) 2_646 1_556 ? Sb8 As6 Pb10 95.0(3) 2_546 1_556 ? Sb7 As6 Pb10 2.6(5) 1_556 1_556 ? S10 Sb6 S12 90.0(5) 1_556 1_455 ? S10 Sb6 S13 85.8(4) 1_556 . ? S12 Sb6 S13 89.5(5) 1_455 . ? S10 Sb6 S9 86.1(5) 1_556 2_547 ? S12 Sb6 S9 89.7(5) 1_455 2_547 ? S13 Sb6 S9 171.9(6) . 2_547 ? S10 Sb6 S8 82.1(4) 1_556 2_647 ? S12 Sb6 S8 170.5(5) 1_455 2_647 ? S13 Sb6 S8 84.7(4) . 2_647 ? S9 Sb6 S8 94.9(5) 2_547 2_647 ? S10 Sb6 S6 161.4(5) 1_556 2_546 ? S12 Sb6 S6 83.2(4) 1_455 2_546 ? S13 Sb6 S6 76.8(4) . 2_546 ? S9 Sb6 S6 111.1(4) 2_547 2_546 ? S8 Sb6 S6 102.7(5) 2_647 2_546 ? S10 Sb6 Sb4 94.1(4) 1_556 1_455 ? S12 Sb6 Sb4 46.6(3) 1_455 1_455 ? S13 Sb6 Sb4 43.8(3) . 1_455 ? S9 Sb6 Sb4 136.3(5) 2_547 1_455 ? S8 Sb6 Sb4 128.5(4) 2_647 1_455 ? S6 Sb6 Sb4 68.7(3) 2_546 1_455 ? S10 Sb6 Pb7 139.4(5) 1_556 2_646 ? S12 Sb6 Pb7 127.3(6) 1_455 2_646 ? S13 Sb6 Pb7 80.1(4) . 2_646 ? S9 Sb6 Pb7 106.7(4) 2_547 2_646 ? S8 Sb6 Pb7 59.0(3) 2_647 2_646 ? S6 Sb6 Pb7 44.1(2) 2_546 2_646 ? Sb4 Sb6 Pb7 101.2(4) 1_455 2_646 ? S10 Sb6 Sb11 139.9(6) 1_556 2_646 ? S12 Sb6 Sb11 124.5(6) 1_455 2_646 ? S13 Sb6 Sb11 75.9(4) . 2_646 ? S9 Sb6 Sb11 111.0(4) 2_547 2_646 ? S8 Sb6 Sb11 61.3(4) 2_647 2_646 ? S6 Sb6 Sb11 41.5(3) 2_546 2_646 ? Sb4 Sb6 Sb11 96.6(4) 1_455 2_646 ? Pb7 Sb6 Sb11 4.7(2) 2_646 2_646 ? S10 Sb6 Sb8 146.8(5) 1_556 2_546 ? S12 Sb6 Sb8 83.2(4) 1_455 2_546 ? S13 Sb6 Sb8 126.4(5) . 2_546 ? S9 Sb6 Sb8 61.5(2) 2_547 2_546 ? S8 Sb6 Sb8 106.3(4) 2_647 2_546 ? S6 Sb6 Sb8 49.6(2) 2_546 2_546 ? Sb4 Sb6 Sb8 104.2(4) 1_455 2_546 ? Pb7 Sb6 Sb8 64.0(3) 2_646 2_546 ? Sb11 Sb6 Sb8 65.8(3) 2_646 2_546 ? S10 Sb6 Sb7 46.4(4) 1_556 1_556 ? S12 Sb6 Sb7 90.9(5) 1_455 1_556 ? S13 Sb6 Sb7 132.3(6) . 1_556 ? S9 Sb6 Sb7 39.7(4) 2_547 1_556 ? S8 Sb6 Sb7 87.5(5) 2_647 1_556 ? S6 Sb6 Sb7 150.4(5) 2_546 1_556 ? Sb4 Sb6 Sb7 125.7(5) 1_455 1_556 ? Pb7 Sb6 Sb7 133.1(5) 2_646 1_556 ? Sb11 Sb6 Sb7 137.7(6) 2_646 1_556 ? Sb8 Sb6 Sb7 101.0(4) 2_546 1_556 ? S10 Sb6 Pb10 45.3(3) 1_556 1_556 ? S12 Sb6 Pb10 88.5(5) 1_455 1_556 ? S13 Sb6 Pb10 131.1(5) . 1_556 ? S9 Sb6 Pb10 40.9(3) 2_547 1_556 ? S8 Sb6 Pb10 89.6(4) 2_647 1_556 ? S6 Sb6 Pb10 151.0(4) 2_546 1_556 ? Sb4 Sb6 Pb10 123.1(4) 1_455 1_556 ? Pb7 Sb6 Pb10 135.7(4) 2_646 1_556 ? Sb11 Sb6 Pb10 140.4(5) 2_646 1_556 ? Sb8 Sb6 Pb10 101.9(3) 2_546 1_556 ? Sb7 Sb6 Pb10 2.6(5) 1_556 1_556 ? S7 Pb5 S4 84.37(19) . . ? S7 Pb5 S17 82.8(2) . . ? S4 Pb5 S17 91.58(19) . . ? S7 Pb5 S3 149.93(19) . . ? S4 Pb5 S3 72.76(17) . . ? S17 Pb5 S3 78.63(17) . . ? S7 Pb5 S9 77.97(17) . 1_655 ? S4 Pb5 S9 161.77(18) . 1_655 ? S17 Pb5 S9 90.67(18) . 1_655 ? S3 Pb5 S9 125.37(17) . 1_655 ? S7 Pb5 S8 83.57(19) . . ? S4 Pb5 S8 82.11(18) . . ? S17 Pb5 S8 165.52(18) . . ? S3 Pb5 S8 111.50(17) . . ? S9 Pb5 S8 91.38(18) 1_655 . ? S7 Pb5 S18 144.85(18) . 1_656 ? S4 Pb5 S18 123.57(16) . 1_656 ? S17 Pb5 S18 113.91(17) . 1_656 ? S3 Pb5 S18 65.13(15) . 1_656 ? S9 Pb5 S18 71.47(16) 1_655 1_656 ? S8 Pb5 S18 80.28(16) . 1_656 ? S7 Pb5 Sb1 138.2(4) . 1_656 ? S4 Pb5 Sb1 125.9(4) . 1_656 ? S17 Pb5 Sb1 69.7(3) . 1_656 ? S3 Pb5 Sb1 54.3(4) . 1_656 ? S9 Pb5 Sb1 71.6(4) 1_655 1_656 ? S8 Pb5 Sb1 124.4(3) . 1_656 ? S18 Pb5 Sb1 44.2(3) 1_656 1_656 ? S7 Pb5 As1 136.7(6) . 1_656 ? S4 Pb5 As1 122.4(5) . 1_656 ? S17 Pb5 As1 64.8(4) . 1_656 ? S3 Pb5 As1 52.2(6) . 1_656 ? S9 Pb5 As1 74.7(5) 1_655 1_656 ? S8 Pb5 As1 129.5(4) . 1_656 ? S18 Pb5 As1 49.2(3) 1_656 1_656 ? Sb1 Pb5 As1 5.5(4) 1_656 1_656 ? S7 Pb5 As2 148.99(13) . 1_556 ? S4 Pb5 As2 70.93(13) . 1_556 ? S17 Pb5 As2 115.40(15) . 1_556 ? S3 Pb5 As2 36.85(11) . 1_556 ? S9 Pb5 As2 123.86(14) 1_655 1_556 ? S8 Pb5 As2 74.91(14) . 1_556 ? S18 Pb5 As2 52.77(10) 1_656 1_556 ? Sb1 Pb5 As2 72.8(4) 1_656 1_556 ? As1 Pb5 As2 73.9(6) 1_656 1_556 ? S7 Pb5 Sb11 43.2(3) . . ? S4 Pb5 Sb11 87.8(3) . . ? S17 Pb5 Sb11 39.6(3) . . ? S3 Pb5 Sb11 115.0(2) . . ? S9 Pb5 Sb11 82.5(3) 1_655 . ? S8 Pb5 Sb11 126.6(3) . . ? S18 Pb5 Sb11 143.4(3) 1_656 . ? Sb1 Pb5 Sb11 103.8(4) 1_656 . ? As1 Pb5 Sb11 99.9(5) 1_656 . ? As2 Pb5 Sb11 148.1(2) 1_556 . ? S7 Pb5 Pb7 45.19(18) . . ? S4 Pb5 Pb7 87.03(17) . . ? S17 Pb5 Pb7 37.66(17) . . ? S3 Pb5 Pb7 112.80(15) . . ? S9 Pb5 Pb7 83.74(16) 1_655 . ? S8 Pb5 Pb7 128.49(17) . . ? S18 Pb5 Pb7 143.00(15) 1_656 . ? Sb1 Pb5 Pb7 102.5(3) 1_656 . ? As1 Pb5 Pb7 98.6(5) 1_656 . ? As2 Pb5 Pb7 146.09(12) 1_556 . ? Sb11 Pb5 Pb7 2.2(3) . . ? S9 Sb7 S7 93.5(7) 2_546 2_646 ? S9 Sb7 S6 87.2(7) 2_546 2_546 ? S7 Sb7 S6 89.5(7) 2_646 2_546 ? S9 Sb7 S10 84.1(6) 2_546 . ? S7 Sb7 S10 90.2(6) 2_646 . ? S6 Sb7 S10 171.3(9) 2_546 . ? S9 Sb7 S19 80.0(6) 2_546 1_455 ? S7 Sb7 S19 173.5(9) 2_646 1_455 ? S6 Sb7 S19 90.1(5) 2_546 1_455 ? S10 Sb7 S19 89.1(6) . 1_455 ? S9 Sb7 S20 138.2(8) 2_546 . ? S7 Sb7 S20 114.6(7) 2_646 . ? S6 Sb7 S20 121.5(7) 2_546 . ? S10 Sb7 S20 66.4(5) . . ? S19 Sb7 S20 70.9(5) 1_455 . ? S9 Sb7 S13 159.0(9) 2_546 . ? S7 Sb7 S13 81.2(6) 2_646 . ? S6 Sb7 S13 72.6(5) 2_546 . ? S10 Sb7 S13 116.0(7) . . ? S19 Sb7 S13 104.9(6) 1_455 . ? S20 Sb7 S13 61.0(4) . . ? S9 Sb7 Sb4 139.1(7) 2_546 1_455 ? S7 Sb7 Sb4 122.8(7) 2_646 1_455 ? S6 Sb7 Sb4 76.0(5) 2_546 1_455 ? S10 Sb7 Sb4 111.3(7) . 1_455 ? S19 Sb7 Sb4 63.4(4) 1_455 1_455 ? S20 Sb7 Sb4 45.7(3) . 1_455 ? S13 Sb7 Sb4 41.6(3) . 1_455 ? S9 Sb7 As3 147.2(7) 2_546 . ? S7 Sb7 As3 77.7(5) 2_646 . ? S6 Sb7 As3 123.8(7) 2_546 . ? S10 Sb7 As3 64.6(4) . . ? S19 Sb7 As3 107.8(6) 1_455 . ? S20 Sb7 As3 36.9(3) . . ? S13 Sb7 As3 51.5(3) . . ? Sb4 Sb7 As3 66.9(4) 1_455 . ? S9 Sb7 Sb11 92.7(7) 2_546 2_646 ? S7 Sb7 Sb11 44.6(4) 2_646 2_646 ? S6 Sb7 Sb11 45.0(4) 2_546 2_646 ? S10 Sb7 Sb11 134.6(6) . 2_646 ? S19 Sb7 Sb11 135.0(7) 1_455 2_646 ? S20 Sb7 Sb11 129.1(7) . 2_646 ? S13 Sb7 Sb11 69.2(5) . 2_646 ? Sb4 Sb7 Sb11 100.4(5) 1_455 2_646 ? As3 Sb7 Sb11 102.0(5) . 2_646 ? S9 Sb7 Pb7 94.7(7) 2_546 2_646 ? S7 Sb7 Pb7 47.4(4) 2_646 2_646 ? S6 Sb7 Pb7 42.5(4) 2_546 2_646 ? S10 Sb7 Pb7 137.5(6) . 2_646 ? S19 Sb7 Pb7 132.6(6) 1_455 2_646 ? S20 Sb7 Pb7 127.1(6) . 2_646 ? S13 Sb7 Pb7 66.8(4) . 2_646 ? Sb4 Sb7 Pb7 97.2(5) 1_455 2_646 ? As3 Sb7 Pb7 101.6(5) . 2_646 ? Sb11 Sb7 Pb7 3.4(3) 2_646 2_646 ? S9 Sb7 As6 51.5(4) 2_546 1_554 ? S7 Sb7 As6 91.2(6) 2_646 1_554 ? S6 Sb7 As6 138.6(8) 2_546 1_554 ? S10 Sb7 As6 32.7(3) . 1_554 ? S19 Sb7 As6 84.8(6) 1_455 1_554 ? S20 Sb7 As6 95.5(6) . 1_554 ? S13 Sb7 As6 148.1(7) . 1_554 ? Sb4 Sb7 As6 134.8(7) 1_455 1_554 ? As3 Sb7 As6 96.7(5) . 1_554 ? Sb11 Sb7 As6 124.6(7) 2_646 1_554 ? Pb7 Sb7 As6 127.9(6) 2_646 1_554 ? S9 Pb10 S7 87.9(4) 2_546 2_646 ? S9 Pb10 S6 84.6(4) 2_546 2_546 ? S7 Pb10 S6 85.5(4) 2_646 2_546 ? S9 Pb10 S10 82.8(4) 2_546 . ? S7 Pb10 S10 87.3(3) 2_646 . ? S6 Pb10 S10 165.7(5) 2_546 . ? S9 Pb10 S19 81.5(3) 2_546 1_455 ? S7 Pb10 S19 169.3(5) 2_646 1_455 ? S6 Pb10 S19 92.5(3) 2_546 1_455 ? S10 Pb10 S19 92.3(4) . 1_455 ? S9 Pb10 S20 141.7(5) 2_546 . ? S7 Pb10 S20 114.7(4) 2_646 . ? S6 Pb10 S20 125.6(4) 2_546 . ? S10 Pb10 S20 68.7(3) . . ? S19 Pb10 S20 74.9(3) 1_455 . ? S9 Pb10 S13 155.2(5) 2_546 . ? S7 Pb10 S13 80.0(3) 2_646 . ? S6 Pb10 S13 73.0(3) 2_546 . ? S10 Pb10 S13 117.8(4) . . ? S19 Pb10 S13 109.4(3) 1_455 . ? S20 Pb10 S13 62.9(3) . . ? S9 Pb10 Sb4 142.7(4) 2_546 1_455 ? S7 Pb10 Sb4 122.9(4) 2_646 1_455 ? S6 Pb10 Sb4 78.2(3) 2_546 1_455 ? S10 Pb10 Sb4 116.0(4) . 1_455 ? S19 Pb10 Sb4 66.6(2) 1_455 1_455 ? S20 Pb10 Sb4 47.90(19) . 1_455 ? S13 Pb10 Sb4 42.93(17) . 1_455 ? S9 Pb10 As3 145.1(4) 2_546 . ? S7 Pb10 As3 76.9(3) 2_646 . ? S6 Pb10 As3 124.4(4) 2_546 . ? S10 Pb10 As3 65.5(3) . . ? S19 Pb10 As3 112.6(4) 1_455 . ? S20 Pb10 As3 37.83(17) . . ? S13 Pb10 As3 52.3(2) . . ? Sb4 Pb10 As3 69.1(2) 1_455 . ? S9 Pb10 Sb11 88.3(4) 2_546 2_646 ? S7 Pb10 Sb11 42.7(3) 2_646 2_646 ? S6 Pb10 Sb11 43.1(3) 2_546 2_646 ? S10 Pb10 Sb11 129.6(4) . 2_646 ? S19 Pb10 Sb11 135.3(4) 1_455 2_646 ? S20 Pb10 Sb11 129.5(4) . 2_646 ? S13 Pb10 Sb11 68.1(3) . 2_646 ? Sb4 Pb10 Sb11 100.6(3) 1_455 2_646 ? As3 Pb10 Sb11 100.4(4) . 2_646 ? S9 Pb10 Pb7 90.4(4) 2_546 2_646 ? S7 Pb10 Pb7 45.4(3) 2_646 2_646 ? S6 Pb10 Pb7 40.6(2) 2_546 2_646 ? S10 Pb10 Pb7 132.6(4) . 2_646 ? S19 Pb10 Pb7 133.1(4) 1_455 2_646 ? S20 Pb10 Pb7 127.7(4) . 2_646 ? S13 Pb10 Pb7 65.7(2) . 2_646 ? Sb4 Pb10 Pb7 97.3(3) 1_455 2_646 ? As3 Pb10 Pb7 100.2(3) . 2_646 ? Sb11 Pb10 Pb7 3.4(3) 2_646 2_646 ? S9 Pb10 Pb9 41.3(2) 2_546 1_454 ? S7 Pb10 Pb9 129.1(4) 2_646 1_454 ? S6 Pb10 Pb9 89.0(3) 2_546 1_454 ? S10 Pb10 Pb9 86.0(3) . 1_454 ? S19 Pb10 Pb9 40.3(2) 1_455 1_454 ? S20 Pb10 Pb9 109.4(3) . 1_454 ? S13 Pb10 Pb9 145.1(3) . 1_454 ? Sb4 Pb10 Pb9 105.1(3) 1_455 1_454 ? As3 Pb10 Pb9 141.7(4) . 1_454 ? Sb11 Pb10 Pb9 117.7(4) 2_646 1_454 ? Pb7 Pb10 Pb9 118.1(3) 2_646 1_454 ? S8 Pb6 S10 85.5(2) 2_646 . ? S8 Pb6 S19 83.59(19) 2_646 . ? S10 Pb6 S19 91.44(19) . . ? S8 Pb6 S11 147.40(19) 2_646 . ? S10 Pb6 S11 70.85(18) . . ? S19 Pb6 S11 75.11(16) . . ? S8 Pb6 S7 85.66(19) 2_646 2_646 ? S10 Pb6 S7 82.23(18) . 2_646 ? S19 Pb6 S7 167.92(18) . 2_646 ? S11 Pb6 S7 112.04(16) . 2_646 ? S8 Pb6 S6 80.97(18) 2_646 2_646 ? S10 Pb6 S6 166.36(19) . 2_646 ? S19 Pb6 S6 89.14(17) . 2_646 ? S11 Pb6 S6 122.34(16) . 2_646 ? S7 Pb6 S6 94.61(18) 2_646 2_646 ? S8 Pb6 S12 148.70(18) 2_646 . ? S10 Pb6 S12 120.75(17) . . ? S19 Pb6 S12 110.14(16) . . ? S11 Pb6 S12 63.50(14) . . ? S7 Pb6 S12 81.93(16) 2_646 . ? S6 Pb6 S12 71.58(15) 2_646 . ? S8 Pb6 As3 147.56(13) 2_646 . ? S10 Pb6 As3 67.27(15) . . ? S19 Pb6 As3 113.23(14) . . ? S11 Pb6 As3 38.31(10) . . ? S7 Pb6 As3 73.83(13) 2_646 . ? S6 Pb6 As3 124.71(13) 2_646 . ? S12 Pb6 As3 53.47(10) . . ? S8 Pb6 Sb4 139.23(13) 2_646 . ? S10 Pb6 Sb4 120.48(16) . . ? S19 Pb6 Sb4 66.37(14) . . ? S11 Pb6 Sb4 50.65(10) . . ? S7 Pb6 Sb4 125.71(14) 2_646 . ? S6 Pb6 Sb4 72.06(13) 2_646 . ? S12 Pb6 Sb4 43.78(9) . . ? As3 Pb6 Sb4 72.57(6) . . ? S8 Pb6 Sb5 43.8(3) 2_646 1_554 ? S10 Pb6 Sb5 88.8(3) . 1_554 ? S19 Pb6 Sb5 39.8(3) . 1_554 ? S11 Pb6 Sb5 111.6(3) . 1_554 ? S7 Pb6 Sb5 129.3(3) 2_646 1_554 ? S6 Pb6 Sb5 82.9(2) 2_646 1_554 ? S12 Pb6 Sb5 141.7(2) . 1_554 ? As3 Pb6 Sb5 145.4(2) . 1_554 ? Sb4 Pb6 Sb5 101.8(2) . 1_554 ? S8 Pb6 Pb9 43.88(19) 2_646 1_554 ? S10 Pb6 Pb9 87.69(18) . 1_554 ? S19 Pb6 Pb9 39.71(18) . 1_554 ? S11 Pb6 Pb9 111.05(16) . 1_554 ? S7 Pb6 Pb9 129.24(18) 2_646 1_554 ? S6 Pb6 Pb9 84.06(17) 2_646 1_554 ? S12 Pb6 Pb9 142.48(15) . 1_554 ? As3 Pb6 Pb9 144.51(13) . 1_554 ? Sb4 Pb6 Pb9 102.17(13) . 1_554 ? Sb5 Pb6 Pb9 1.1(3) 1_554 1_554 ? S8 Pb6 Sb6 50.6(2) 2_646 1_554 ? S10 Pb6 Sb6 35.0(3) . 1_554 ? S19 Pb6 Sb6 87.4(2) . 1_554 ? S11 Pb6 Sb6 103.3(2) . 1_554 ? S7 Pb6 Sb6 81.6(2) 2_646 1_554 ? S6 Pb6 Sb6 131.5(2) 2_646 1_554 ? S12 Pb6 Sb6 152.6(2) . 1_554 ? As3 Pb6 Sb6 100.7(2) . 1_554 ? Sb4 Pb6 Sb6 145.88(19) . 1_554 ? Sb5 Pb6 Sb6 64.4(3) 1_554 1_554 ? Pb9 Pb6 Sb6 63.5(2) 1_554 1_554 ? S20 Pb3 S15 71.74(18) . 1_455 ? S20 Pb3 S2 67.07(17) . . ? S15 Pb3 S2 91.23(18) 1_455 . ? S20 Pb3 S17 141.00(16) . 1_455 ? S15 Pb3 S17 81.72(17) 1_455 1_455 ? S2 Pb3 S17 143.08(17) . 1_455 ? S20 Pb3 S18 130.74(15) . . ? S15 Pb3 S18 84.10(17) 1_455 . ? S2 Pb3 S18 71.38(16) . . ? S17 Pb3 S18 71.87(16) 1_455 . ? S20 Pb3 S14 73.72(16) . 1_455 ? S15 Pb3 S14 77.26(19) 1_455 1_455 ? S2 Pb3 S14 140.8(2) . 1_455 ? S17 Pb3 S14 72.90(17) 1_455 1_455 ? S18 Pb3 S14 142.03(15) . 1_455 ? S20 Pb3 S4 134.67(15) . . ? S15 Pb3 S4 146.16(18) 1_455 . ? S2 Pb3 S4 84.28(17) . . ? S17 Pb3 S4 82.05(16) 1_455 . ? S18 Pb3 S4 62.65(15) . . ? S14 Pb3 S4 125.16(16) 1_455 . ? S20 Pb3 S16 109.79(16) . . ? S15 Pb3 S16 136.82(16) 1_455 . ? S2 Pb3 S16 130.21(16) . . ? S17 Pb3 S16 71.44(15) 1_455 . ? S18 Pb3 S16 116.96(16) . . ? S14 Pb3 S16 63.00(15) 1_455 . ? S4 Pb3 S16 62.97(15) . . ? S20 Pb3 S1 62.37(16) . . ? S15 Pb3 S1 131.9(2) 1_455 . ? S2 Pb3 S1 84.15(17) . . ? S17 Pb3 S1 126.88(17) 1_455 . ? S18 Pb3 S1 137.43(15) . . ? S14 Pb3 S1 76.83(16) 1_455 . ? S4 Pb3 S1 81.12(16) . . ? S16 Pb3 S1 56.02(15) . . ? S20 Pb3 As2 96.96(12) . 1_455 ? S15 Pb3 As2 32.87(14) 1_455 1_455 ? S2 Pb3 As2 81.85(13) . 1_455 ? S17 Pb3 As2 72.65(13) 1_455 1_455 ? S18 Pb3 As2 51.25(10) . 1_455 ? S14 Pb3 As2 104.37(12) 1_455 1_455 ? S4 Pb3 As2 113.51(12) . 1_455 ? S16 Pb3 As2 144.04(10) . 1_455 ? S1 Pb3 As2 158.46(13) . 1_455 ? S20 Pb3 Pb4 83.89(11) . . ? S15 Pb3 Pb4 137.84(12) 1_455 . ? S2 Pb3 Pb4 47.06(13) . . ? S17 Pb3 Pb4 133.47(12) 1_455 . ? S18 Pb3 Pb4 86.79(9) . . ? S14 Pb3 Pb4 128.61(12) 1_455 . ? S4 Pb3 Pb4 51.51(11) . . ? S16 Pb3 Pb4 83.35(9) . . ? S1 Pb3 Pb4 51.87(12) . . ? As2 Pb3 Pb4 124.16(5) 1_455 . ? S20 Pb3 As3 31.69(11) . . ? S15 Pb3 As3 103.43(15) 1_455 . ? S2 Pb3 As3 66.42(13) . . ? S17 Pb3 As3 150.46(13) 1_455 . ? S18 Pb3 As3 137.17(11) . . ? S14 Pb3 As3 79.85(13) 1_455 . ? S4 Pb3 As3 105.32(12) . . ? S16 Pb3 As3 86.30(11) . . ? S1 Pb3 As3 32.13(12) . . ? As2 Pb3 As3 126.36(6) 1_455 . ? Pb4 Pb3 As3 59.18(4) . . ? S11 Pb4 S15 72.25(17) . . ? S11 Pb4 S2 66.67(16) . . ? S15 Pb4 S2 89.14(17) . . ? S11 Pb4 S17 144.89(15) . . ? S15 Pb4 S17 82.54(17) . . ? S2 Pb4 S17 138.29(18) . . ? S11 Pb4 S14 76.24(16) . . ? S15 Pb4 S14 78.19(19) . . ? S2 Pb4 S14 142.9(2) . . ? S17 Pb4 S14 74.94(17) . . ? S11 Pb4 S3 113.50(17) . . ? S15 Pb4 S3 138.43(16) . . ? S2 Pb4 S3 131.85(14) . . ? S17 Pb4 S3 70.76(16) . . ? S14 Pb4 S3 64.66(15) . . ? S11 Pb4 S4 136.20(14) . . ? S15 Pb4 S4 141.53(18) . . ? S2 Pb4 S4 83.79(16) . . ? S17 Pb4 S4 78.14(15) . . ? S14 Pb4 S4 126.87(17) . . ? S3 Pb4 S4 63.48(15) . . ? S11 Pb4 S1 63.48(16) . . ? S15 Pb4 S1 133.8(2) . . ? S2 Pb4 S1 85.30(17) . . ? S17 Pb4 S1 128.63(17) . . ? S14 Pb4 S1 79.20(16) . . ? S3 Pb4 S1 58.10(16) . . ? S4 Pb4 S1 83.32(17) . . ? S11 Pb4 S5 126.88(15) . . ? S15 Pb4 S5 81.53(17) . . ? S2 Pb4 S5 67.61(16) . . ? S17 Pb4 S5 70.75(16) . . ? S14 Pb4 S5 141.96(16) . . ? S3 Pb4 S5 116.70(16) . . ? S4 Pb4 S5 60.80(14) . . ? S1 Pb4 S5 136.13(15) . . ? S11 Pb4 As3 32.24(10) . . ? S15 Pb4 As3 104.49(14) . . ? S2 Pb4 As3 66.87(13) . . ? S17 Pb4 As3 154.64(14) . . ? S14 Pb4 As3 82.61(13) . . ? S3 Pb4 As3 89.16(12) . . ? S4 Pb4 As3 107.20(12) . . ? S1 Pb4 As3 32.65(13) . . ? S5 Pb4 As3 133.92(11) . . ? S11 Pb4 As2 96.13(11) . . ? S15 Pb4 As2 32.18(14) . . ? S2 Pb4 As2 78.88(11) . . ? S17 Pb4 As2 72.49(13) . . ? S14 Pb4 As2 104.67(12) . . ? S3 Pb4 As2 143.24(12) . . ? S4 Pb4 As2 109.58(12) . . ? S1 Pb4 As2 158.13(13) . . ? S5 Pb4 As2 49.39(10) . . ? As3 Pb4 As2 125.67(6) . . ? S11 Pb4 Pb3 84.55(9) . . ? S15 Pb4 Pb3 134.84(13) . . ? S2 Pb4 Pb3 45.77(11) . . ? S17 Pb4 Pb3 130.25(12) . . ? S14 Pb4 Pb3 133.64(12) . . ? S3 Pb4 Pb3 86.18(9) . . ? S4 Pb4 Pb3 52.12(10) . . ? S1 Pb4 Pb3 54.52(12) . . ? S5 Pb4 Pb3 82.53(9) . . ? As3 Pb4 Pb3 60.63(4) . . ? As2 Pb4 Pb3 119.21(5) . . ? S1 Pb1 S19 82.17(19) . 1_556 ? S1 Pb1 S16 65.46(18) . . ? S19 Pb1 S16 129.99(17) 1_556 . ? S1 Pb1 S13 78.30(18) . . ? S19 Pb1 S13 75.88(17) 1_556 . ? S16 Pb1 S13 128.15(15) . . ? S1 Pb1 S14 87.71(18) . 1_455 ? S19 Pb1 S14 149.36(18) 1_556 1_455 ? S16 Pb1 S14 69.17(17) . 1_455 ? S13 Pb1 S14 73.77(17) . 1_455 ? S1 Pb1 S10 142.90(19) . 1_556 ? S19 Pb1 S10 81.81(18) 1_556 1_556 ? S16 Pb1 S10 145.51(16) . 1_556 ? S13 Pb1 S10 65.41(16) . 1_556 ? S14 Pb1 S10 89.33(17) 1_455 1_556 ? S1 Pb1 S11 139.14(17) . 1_556 ? S19 Pb1 S11 70.94(15) 1_556 1_556 ? S16 Pb1 S11 109.81(16) . 1_556 ? S13 Pb1 S11 121.76(16) . 1_556 ? S14 Pb1 S11 130.28(15) 1_455 1_556 ? S10 Pb1 S11 63.58(16) 1_556 1_556 ? S1 Pb1 S2 132.6(2) . 1_556 ? S19 Pb1 S2 129.60(16) 1_556 1_556 ? S16 Pb1 S2 67.19(14) . 1_556 ? S13 Pb1 S2 136.38(15) . 1_556 ? S14 Pb1 S2 77.46(17) 1_455 1_556 ? S10 Pb1 S2 82.35(17) 1_556 1_556 ? S11 Pb1 S2 59.14(14) 1_556 1_556 ? S1 Pb1 S15 81.58(18) . 1_556 ? S19 Pb1 S15 75.27(18) 1_556 1_556 ? S16 Pb1 S15 63.57(16) . 1_556 ? S13 Pb1 S15 146.67(15) . 1_556 ? S14 Pb1 S15 131.8(2) 1_455 1_556 ? S10 Pb1 S15 125.64(17) 1_556 1_556 ? S11 Pb1 S15 62.46(15) 1_556 1_556 ? S2 Pb1 S15 76.11(15) 1_556 1_556 ? S1 Pb1 Sb4 80.35(14) . 1_455 ? S19 Pb1 Sb4 114.05(14) 1_556 1_455 ? S16 Pb1 Sb4 97.56(11) . 1_455 ? S13 Pb1 Sb4 38.39(10) . 1_455 ? S14 Pb1 Sb4 35.41(13) 1_455 1_455 ? S10 Pb1 Sb4 76.08(12) 1_556 1_455 ? S11 Pb1 Sb4 138.48(11) 1_556 1_455 ? S2 Pb1 Sb4 107.87(12) 1_556 1_455 ? S15 Pb1 Sb4 158.16(12) 1_556 1_455 ? S1 Pb1 Pb2 133.63(14) . 1_455 ? S19 Pb1 Pb2 133.85(13) 1_556 1_455 ? S16 Pb1 Pb2 95.08(10) . 1_455 ? S13 Pb1 Pb2 83.77(9) . 1_455 ? S14 Pb1 Pb2 46.09(13) 1_455 1_455 ? S10 Pb1 Pb2 52.03(12) 1_556 1_455 ? S11 Pb1 Pb2 86.30(9) 1_556 1_455 ? S2 Pb1 Pb2 52.77(11) 1_556 1_455 ? S15 Pb1 Pb2 128.81(11) 1_556 1_455 ? Sb4 Pb1 Pb2 60.03(4) 1_455 1_455 ? S1 Pb1 As2 65.24(14) . 1_556 ? S19 Pb1 As2 100.41(14) 1_556 1_556 ? S16 Pb1 As2 32.23(11) . 1_556 ? S13 Pb1 As2 143.46(11) . 1_556 ? S14 Pb1 As2 101.40(14) 1_455 1_556 ? S10 Pb1 As2 150.96(14) 1_556 1_556 ? S11 Pb1 As2 89.53(11) 1_556 1_556 ? S2 Pb1 As2 73.95(11) 1_556 1_556 ? S15 Pb1 As2 32.25(13) 1_556 1_556 ? Sb4 Pb1 As2 126.91(6) 1_455 1_556 ? Pb2 Pb1 As2 119.53(4) 1_455 1_556 ? S1 Pb2 S3 67.42(19) . . ? S1 Pb2 S14 90.36(19) . . ? S3 Pb2 S14 71.33(17) . . ? S1 Pb2 S12 79.30(18) . . ? S3 Pb2 S12 131.91(16) . . ? S14 Pb2 S12 75.35(18) . . ? S1 Pb2 S19 79.90(19) . 1_556 ? S3 Pb2 S19 128.43(15) . 1_556 ? S14 Pb2 S19 149.71(18) . 1_556 ? S12 Pb2 S19 74.69(16) . 1_556 ? S1 Pb2 S20 138.87(17) . 1_656 ? S3 Pb2 S20 108.69(17) . 1_656 ? S14 Pb2 S20 128.51(16) . 1_656 ? S12 Pb2 S20 119.14(17) . 1_656 ? S19 Pb2 S20 71.63(16) 1_556 1_656 ? S1 Pb2 S10 142.52(19) . 1_656 ? S3 Pb2 S10 145.62(16) . 1_656 ? S14 Pb2 S10 88.70(17) . 1_656 ? S12 Pb2 S10 64.25(16) . 1_656 ? S19 Pb2 S10 82.28(16) 1_556 1_656 ? S20 Pb2 S10 62.20(16) 1_656 1_656 ? S1 Pb2 S15 83.34(19) . 1_556 ? S3 Pb2 S15 64.22(16) . 1_556 ? S14 Pb2 S15 134.1(2) . 1_556 ? S12 Pb2 S15 145.98(15) . 1_556 ? S19 Pb2 S15 73.60(16) 1_556 1_556 ? S20 Pb2 S15 60.74(15) 1_656 1_556 ? S10 Pb2 S15 122.43(17) 1_656 1_556 ? S1 Pb2 S2 136.6(2) . 1_656 ? S3 Pb2 S2 69.23(15) . 1_656 ? S14 Pb2 S2 77.88(17) . 1_656 ? S12 Pb2 S2 134.84(14) . 1_656 ? S19 Pb2 S2 128.02(16) 1_556 1_656 ? S20 Pb2 S2 56.77(14) 1_656 1_656 ? S10 Pb2 S2 79.55(16) 1_656 1_656 ? S15 Pb2 S2 76.20(15) 1_556 1_656 ? S1 Pb2 As2 66.84(15) . 1_556 ? S3 Pb2 As2 32.30(11) . 1_556 ? S14 Pb2 As2 103.63(14) . 1_556 ? S12 Pb2 As2 146.13(12) . 1_556 ? S19 Pb2 As2 98.75(12) 1_556 1_556 ? S20 Pb2 As2 88.52(11) 1_656 1_556 ? S10 Pb2 As2 149.01(13) 1_656 1_556 ? S15 Pb2 As2 32.96(13) 1_556 1_556 ? S2 Pb2 As2 75.56(11) 1_656 1_556 ? S1 Pb2 Sb4 83.64(14) . . ? S3 Pb2 Sb4 100.21(11) . . ? S14 Pb2 Sb4 34.88(14) . . ? S12 Pb2 Sb4 40.47(11) . . ? S19 Pb2 Sb4 115.01(13) 1_556 . ? S20 Pb2 Sb4 135.17(10) 1_656 . ? S10 Pb2 Sb4 74.50(12) 1_656 . ? S15 Pb2 Sb4 162.75(13) 1_556 . ? S2 Pb2 Sb4 106.20(10) 1_656 . ? As2 Pb2 Sb4 130.23(6) 1_556 . ? S1 Pb2 Pb1 138.15(15) . 1_655 ? S3 Pb2 Pb1 98.26(11) . 1_655 ? S14 Pb2 Pb1 48.19(13) . 1_655 ? S12 Pb2 Pb1 83.80(10) . 1_655 ? S19 Pb2 Pb1 131.50(11) 1_556 1_655 ? S20 Pb2 Pb1 82.56(9) 1_656 1_655 ? S10 Pb2 Pb1 49.24(11) 1_656 1_655 ? S15 Pb2 Pb1 127.20(11) 1_556 1_655 ? S2 Pb2 Pb1 51.44(10) 1_656 1_655 ? As2 Pb2 Pb1 121.37(5) 1_556 1_655 ? Sb4 Pb2 Pb1 59.53(4) . 1_655 ? S4 Sb8 S18 93.8(2) . . ? S4 Sb8 S5 91.9(2) . . ? S18 Sb8 S5 94.4(2) . . ? S4 Sb8 S6 88.0(2) . . ? S18 Sb8 S6 84.81(19) . . ? S5 Sb8 S6 179.3(2) . . ? S4 Sb8 S7 84.6(2) . . ? S18 Sb8 S7 178.3(2) . . ? S5 Sb8 S7 86.1(2) . . ? S6 Sb8 S7 94.6(2) . . ? S4 Sb8 S9 165.4(2) . 1_554 ? S18 Sb8 S9 79.43(19) . 1_554 ? S5 Sb8 S9 75.87(19) . 1_554 ? S6 Sb8 S9 104.08(18) . 1_554 ? S7 Sb8 S9 102.25(17) . 1_554 ? S4 Sb8 Sb1 97.2(4) . . ? S18 Sb8 Sb1 50.1(4) . . ? S5 Sb8 Sb1 44.5(4) . . ? S6 Sb8 Sb1 134.8(4) . . ? S7 Sb8 Sb1 130.5(4) . . ? S9 Sb8 Sb1 68.5(4) 1_554 . ? S4 Sb8 As1 97.4(5) . . ? S18 Sb8 As1 51.4(6) . . ? S5 Sb8 As1 43.3(6) . . ? S6 Sb8 As1 136.0(6) . . ? S7 Sb8 As1 129.3(6) . . ? S9 Sb8 As1 68.2(5) 1_554 . ? Sb1 Sb8 As1 1.3(10) . . ? S4 Sb8 Pb9 141.0(2) . 2_656 ? S18 Sb8 Pb9 123.7(2) . 2_656 ? S5 Sb8 Pb9 76.3(2) . 2_656 ? S6 Sb8 Pb9 104.25(19) . 2_656 ? S7 Sb8 Pb9 57.98(19) . 2_656 ? S9 Sb8 Pb9 44.30(16) 1_554 2_656 ? Sb1 Sb8 Pb9 99.4(4) . 2_656 ? As1 Sb8 Pb9 98.5(5) . 2_656 ? S4 Sb8 Sb5 142.8(3) . 2_656 ? S18 Sb8 Sb5 120.8(3) . 2_656 ? S5 Sb8 Sb5 73.6(3) . 2_656 ? S6 Sb8 Sb5 106.8(2) . 2_656 ? S7 Sb8 Sb5 60.8(2) . 2_656 ? S9 Sb8 Sb5 41.4(2) 1_554 2_656 ? Sb1 Sb8 Sb5 95.7(4) . 2_656 ? As1 Sb8 Sb5 94.8(6) . 2_656 ? Pb9 Sb8 Sb5 3.7(3) 2_656 2_656 ? S4 Sb8 As6 143.3(3) . 2_556 ? S18 Sb8 As6 77.7(3) . 2_556 ? S5 Sb8 As6 124.0(3) . 2_556 ? S6 Sb8 As6 55.9(3) . 2_556 ? S7 Sb8 As6 103.3(3) . 2_556 ? S9 Sb8 As6 48.1(3) 1_554 2_556 ? Sb1 Sb8 As6 103.7(5) . 2_556 ? As1 Sb8 As6 104.1(6) . 2_556 ? Pb9 Sb8 As6 64.4(3) 2_656 2_556 ? Sb5 Sb8 As6 64.8(4) 2_656 2_556 ? S4 Sb8 Sb6 145.2(3) . 2_556 ? S18 Sb8 Sb6 77.1(3) . 2_556 ? S5 Sb8 Sb6 122.0(3) . 2_556 ? S6 Sb8 Sb6 58.0(3) . 2_556 ? S7 Sb8 Sb6 104.0(3) . 2_556 ? S9 Sb8 Sb6 46.1(2) 1_554 2_556 ? Sb1 Sb8 Sb6 101.9(4) . 2_556 ? As1 Sb8 Sb6 102.3(6) . 2_556 ? Pb9 Sb8 Sb6 63.6(3) 2_656 2_556 ? Sb5 Sb8 Sb6 63.7(3) 2_656 2_556 ? As6 Sb8 Sb6 2.1(5) 2_556 2_556 ? S1 As3 S11 97.3(3) . . ? S1 As3 S20 96.8(3) . . ? S11 As3 S20 103.4(2) . . ? S1 As3 S13 89.5(2) . . ? S11 As3 S13 172.5(2) . . ? S20 As3 S13 78.75(19) . . ? S1 As3 S12 87.6(2) . . ? S11 As3 S12 77.77(18) . . ? S20 As3 S12 175.3(2) . . ? S13 As3 S12 99.48(17) . . ? S1 As3 Pb6 143.5(2) . . ? S11 As3 Pb6 57.68(16) . . ? S20 As3 Pb6 113.71(18) . . ? S13 As3 Pb6 114.84(14) . . ? S12 As3 Pb6 62.92(12) . . ? S1 As3 S10 152.7(3) . . ? S11 As3 S10 66.54(19) . . ? S20 As3 S10 67.82(19) . . ? S13 As3 S10 108.33(16) . . ? S12 As3 S10 108.91(17) . . ? Pb6 As3 S10 45.98(11) . . ? S1 As3 Sb7 146.5(4) . . ? S11 As3 Sb7 112.8(4) . . ? S20 As3 Sb7 63.2(4) . . ? S13 As3 Sb7 61.5(3) . . ? S12 As3 Sb7 112.1(4) . . ? Pb6 As3 Sb7 69.0(3) . . ? S10 As3 Sb7 46.9(3) . . ? S1 As3 Pb10 144.6(3) . . ? S11 As3 Pb10 113.4(2) . . ? S20 As3 Pb10 60.4(3) . . ? S13 As3 Pb10 61.2(2) . . ? S12 As3 Pb10 114.9(2) . . ? Pb6 As3 Pb10 71.25(17) . . ? S10 As3 Pb10 47.1(2) . . ? Sb7 As3 Pb10 2.8(5) . . ? S1 As3 Sb5 92.1(3) . . ? S11 As3 Sb5 126.6(3) . . ? S20 As3 Sb5 127.4(3) . . ? S13 As3 Sb5 49.6(2) . . ? S12 As3 Sb5 50.2(2) . . ? Pb6 As3 Sb5 85.06(18) . . ? S10 As3 Sb5 115.2(2) . . ? Sb7 As3 Sb5 81.7(4) . . ? Pb10 As3 Sb5 83.6(3) . . ? S1 As3 Pb9 95.3(2) . . ? S11 As3 Pb9 124.3(2) . . ? S20 As3 Pb9 128.5(2) . . ? S13 As3 Pb9 51.48(15) . . ? S12 As3 Pb9 48.86(16) . . ? Pb6 As3 Pb9 81.45(12) . . ? S10 As3 Pb9 111.99(18) . . ? Sb7 As3 Pb9 80.0(4) . . ? Pb10 As3 Pb9 82.0(2) . . ? Sb5 As3 Pb9 3.6(3) . . ? S15 As2 S3 98.3(2) . 1_554 ? S15 As2 S16 98.7(2) . 1_554 ? S3 As2 S16 101.2(2) 1_554 1_554 ? S15 As2 S5 99.2(2) . . ? S3 As2 S5 162.5(2) 1_554 . ? S16 As2 S5 76.57(19) 1_554 . ? S15 As2 S18 97.4(2) . 1_655 ? S3 As2 S18 78.24(19) 1_554 1_655 ? S16 As2 S18 163.8(2) 1_554 1_655 ? S5 As2 S18 99.01(17) . 1_655 ? S15 As2 Sb9 145.18(18) . 1_554 ? S3 As2 Sb9 54.25(17) 1_554 1_554 ? S16 As2 Sb9 106.83(16) 1_554 1_554 ? S5 As2 Sb9 109.32(13) . 1_554 ? S18 As2 Sb9 59.47(11) 1_655 1_554 ? S15 As2 Pb5 145.18(18) . 1_554 ? S3 As2 Pb5 54.25(17) 1_554 1_554 ? S16 As2 Pb5 106.83(16) 1_554 1_554 ? S5 As2 Pb5 109.32(13) . 1_554 ? S18 As2 Pb5 59.47(11) 1_655 1_554 ? Sb9 As2 Pb5 0.00(3) 1_554 1_554 ? S15 As2 Sb11 100.8(3) . . ? S3 As2 Sb11 126.1(3) 1_554 . ? S16 As2 Sb11 124.6(3) 1_554 . ? S5 As2 Sb11 49.4(2) . . ? S18 As2 Sb11 49.7(2) 1_655 . ? Sb9 As2 Sb11 84.0(2) 1_554 . ? Pb5 As2 Sb11 84.0(2) 1_554 . ? S15 As2 Pb7 103.1(2) . . ? S3 As2 Pb7 122.7(2) 1_554 . ? S16 As2 Pb7 126.5(2) 1_554 . ? S5 As2 Pb7 52.11(17) . . ? S18 As2 Pb7 46.90(16) 1_655 . ? Sb9 As2 Pb7 80.50(13) 1_554 . ? Pb5 As2 Pb7 80.50(13) 1_554 . ? Sb11 As2 Pb7 3.6(3) . . ? S15 As2 Sb12 147.10(18) . 1_554 ? S3 As2 Sb12 106.23(17) 1_554 1_554 ? S16 As2 Sb12 55.61(16) 1_554 1_554 ? S5 As2 Sb12 57.92(12) . 1_554 ? S18 As2 Sb12 108.70(13) 1_655 1_554 ? Sb9 As2 Sb12 67.55(6) 1_554 1_554 ? Pb5 As2 Sb12 67.55(6) 1_554 1_554 ? Sb11 As2 Sb12 82.3(2) . 1_554 ? Pb7 As2 Sb12 81.95(15) . 1_554 ? S15 As2 Pb8 147.10(18) . 1_554 ? S3 As2 Pb8 106.23(17) 1_554 1_554 ? S16 As2 Pb8 55.61(16) 1_554 1_554 ? S5 As2 Pb8 57.92(12) . 1_554 ? S18 As2 Pb8 108.70(13) 1_655 1_554 ? Sb9 As2 Pb8 67.55(6) 1_554 1_554 ? Pb5 As2 Pb8 67.55(6) 1_554 1_554 ? Sb11 As2 Pb8 82.3(2) . 1_554 ? Pb7 As2 Pb8 81.95(15) . 1_554 ? Sb12 As2 Pb8 0.00(5) 1_554 1_554 ? S15 As2 S4 148.1(2) . 1_554 ? S3 As2 S4 62.67(18) 1_554 1_554 ? S16 As2 S4 63.64(17) 1_554 1_554 ? S5 As2 S4 101.71(16) . 1_554 ? S18 As2 S4 102.75(15) 1_655 1_554 ? Sb9 As2 S4 43.37(10) 1_554 1_554 ? Pb5 As2 S4 43.37(10) 1_554 1_554 ? Sb11 As2 S4 111.1(3) . 1_554 ? Pb7 As2 S4 108.80(18) . 1_554 ? Sb12 As2 S4 43.81(10) 1_554 1_554 ? Pb8 As2 S4 43.81(10) 1_554 1_554 ? S14 Sb4 S13 97.2(2) . 1_655 ? S14 Sb4 S12 93.7(2) . . ? S13 Sb4 S12 83.34(19) 1_655 . ? S14 Sb4 S20 91.4(2) . 1_655 ? S13 Sb4 S20 82.35(18) 1_655 1_655 ? S12 Sb4 S20 165.3(2) . 1_655 ? S14 Sb4 S11 89.6(2) . . ? S13 Sb4 S11 159.64(19) 1_655 . ? S12 Sb4 S11 77.07(17) . . ? S20 Sb4 S11 116.79(19) 1_655 . ? S14 Sb4 Pb10 148.3(3) . 1_655 ? S13 Sb4 Pb10 67.8(2) 1_655 1_655 ? S12 Sb4 Pb10 111.1(2) . 1_655 ? S20 Sb4 Pb10 59.9(2) 1_655 1_655 ? S11 Sb4 Pb10 114.3(2) . 1_655 ? S14 Sb4 Sb7 148.5(4) . 1_655 ? S13 Sb4 Sb7 66.3(3) 1_655 1_655 ? S12 Sb4 Sb7 109.8(4) . 1_655 ? S20 Sb4 Sb7 61.0(4) 1_655 1_655 ? S11 Sb4 Sb7 115.4(3) . 1_655 ? Pb10 Sb4 Sb7 1.8(5) 1_655 1_655 ? S14 Sb4 Sb6 103.5(3) . 1_655 ? S13 Sb4 Sb6 43.8(2) 1_655 1_655 ? S12 Sb4 Sb6 40.3(2) . 1_655 ? S20 Sb4 Sb6 125.0(3) 1_655 1_655 ? S11 Sb4 Sb6 115.9(2) . 1_655 ? Pb10 Sb4 Sb6 85.0(3) 1_655 1_655 ? Sb7 Sb4 Sb6 83.3(4) 1_655 1_655 ? S14 Sb4 As6 100.4(4) . 1_655 ? S13 Sb4 As6 40.1(3) 1_655 1_655 ? S12 Sb4 As6 43.5(3) . 1_655 ? S20 Sb4 As6 122.0(3) 1_655 1_655 ? S11 Sb4 As6 119.9(3) . 1_655 ? Pb10 Sb4 As6 85.8(4) 1_655 1_655 ? Sb7 Sb4 As6 84.1(5) 1_655 1_655 ? Sb6 Sb4 As6 4.8(4) 1_655 1_655 ? S14 Sb4 S19 137.1(2) . . ? S13 Sb4 S19 118.29(17) 1_655 . ? S12 Sb4 S19 112.62(18) . . ? S20 Sb4 S19 71.80(16) 1_655 . ? S11 Sb4 S19 65.79(14) . . ? Pb10 Sb4 S19 50.6(2) 1_655 . ? Sb7 Sb4 S19 52.1(3) 1_655 . ? Sb6 Sb4 S19 118.6(2) 1_655 . ? As6 Sb4 S19 122.1(3) 1_655 . ? S14 Sb4 Pb6 140.21(17) . . ? S13 Sb4 Pb6 112.93(15) 1_655 . ? S12 Sb4 Pb6 66.12(14) . . ? S20 Sb4 Pb6 117.00(14) 1_655 . ? S11 Sb4 Pb6 53.66(12) . . ? Pb10 Sb4 Pb6 70.42(18) 1_655 . ? Sb7 Sb4 Pb6 70.6(3) 1_655 . ? Sb6 Sb4 Pb6 83.26(19) 1_655 . ? As6 Sb4 Pb6 88.0(2) 1_655 . ? S19 Sb4 Pb6 46.51(11) . . ? As3 S1 Pb2 110.0(3) . . ? As3 S1 Pb1 108.1(3) . . ? Pb2 S1 Pb1 91.8(2) . . ? As3 S1 Pb4 91.4(2) . . ? Pb2 S1 Pb4 91.91(18) . . ? Pb1 S1 Pb4 157.4(3) . . ? As3 S1 Pb3 90.2(2) . . ? Pb2 S1 Pb3 155.7(3) . . ? Pb1 S1 Pb3 94.64(19) . . ? Pb4 S1 Pb3 73.61(15) . . ? As3 S1 As2 178.6(3) . 1_556 ? Pb2 S1 As2 71.25(15) . 1_556 ? Pb1 S1 As2 72.37(15) . 1_556 ? Pb4 S1 As2 87.85(17) . 1_556 ? Pb3 S1 As2 88.47(17) . 1_556 ? As3 S1 Sb5 59.7(2) . . ? Pb2 S1 Sb5 69.8(2) . . ? Pb1 S1 Sb5 67.2(2) . . ? Pb4 S1 Sb5 134.6(2) . . ? Pb3 S1 Sb5 134.0(3) . . ? As2 S1 Sb5 121.6(2) 1_556 . ? As3 S1 Pb9 56.1(2) . . ? Pb2 S1 Pb9 71.06(19) . . ? Pb1 S1 Pb9 70.63(17) . . ? Pb4 S1 Pb9 131.4(2) . . ? Pb3 S1 Pb9 133.1(2) . . ? As2 S1 Pb9 125.2(2) 1_556 . ? Sb5 S1 Pb9 3.9(2) . . ? As3 S1 Sb4 60.99(16) . 1_455 ? Pb2 S1 Sb4 141.8(2) . 1_455 ? Pb1 S1 Sb4 60.98(12) . 1_455 ? Pb4 S1 Sb4 123.77(18) . 1_455 ? Pb3 S1 Sb4 59.87(10) . 1_455 ? As2 S1 Sb4 118.52(16) 1_556 1_455 ? Sb5 S1 Sb4 74.7(2) . 1_455 ? Pb9 S1 Sb4 74.53(15) . 1_455 ? As3 S1 Sb4 63.62(17) . . ? Pb2 S1 Sb4 59.51(12) . . ? Pb1 S1 Sb4 139.9(2) . . ? Pb4 S1 Sb4 59.05(11) . . ? Pb3 S1 Sb4 123.30(18) . . ? As2 S1 Sb4 116.92(16) 1_556 . ? Sb5 S1 Sb4 76.18(18) . . ? Pb9 S1 Sb4 73.47(15) . . ? Sb4 S1 Sb4 124.55(16) 1_455 . ? Sb1 S2 As1 8.7(6) . . ? Sb1 S2 Pb3 105.0(5) . . ? As1 S2 Pb3 112.6(7) . . ? Sb1 S2 Pb4 103.1(6) . . ? As1 S2 Pb4 107.0(9) . . ? Pb3 S2 Pb4 87.16(17) . . ? Sb1 S2 Pb1 100.8(5) . 1_554 ? As1 S2 Pb1 92.8(6) . 1_554 ? Pb3 S2 Pb1 153.4(2) . 1_554 ? Pb4 S2 Pb1 93.05(16) . 1_554 ? Sb1 S2 Pb2 102.1(6) . 1_454 ? As1 S2 Pb2 97.0(8) . 1_454 ? Pb3 S2 Pb2 92.64(16) . 1_454 ? Pb4 S2 Pb2 154.0(2) . 1_454 ? Pb1 S2 Pb2 75.78(14) 1_554 1_454 ? Sb1 S2 As3 171.3(5) . . ? As1 S2 As3 175.0(10) . . ? Pb3 S2 As3 71.07(13) . . ? Pb4 S2 As3 69.28(13) . . ? Pb1 S2 As3 84.11(14) 1_554 . ? Pb2 S2 As3 86.06(14) 1_454 . ? Sb1 S2 Sb8 48.3(4) . . ? As1 S2 Sb8 56.8(4) . . ? Pb3 S2 Sb8 68.67(13) . . ? Pb4 S2 Sb8 70.73(13) . . ? Pb1 S2 Sb8 136.14(17) 1_554 . ? Pb2 S2 Sb8 132.99(17) 1_454 . ? As3 S2 Sb8 123.48(16) . . ? Sb1 S2 As2 62.3(6) . . ? As1 S2 As2 59.8(10) . . ? Pb3 S2 As2 138.5(2) . . ? Pb4 S2 As2 60.90(11) . . ? Pb1 S2 As2 61.15(9) 1_554 . ? Pb2 S2 As2 127.87(16) 1_454 . ? As3 S2 As2 115.13(14) . . ? Sb8 S2 As2 75.64(11) . . ? Sb1 S2 As2 68.2(6) . 1_455 ? As1 S2 As2 70.5(10) . 1_455 ? Pb3 S2 As2 59.13(11) . 1_455 ? Pb4 S2 As2 138.85(19) . 1_455 ? Pb1 S2 As2 127.80(18) 1_554 1_455 ? Pb2 S2 As2 58.79(10) 1_454 1_455 ? As3 S2 As2 114.51(14) . 1_455 ? Sb8 S2 As2 75.00(10) . 1_455 ? As2 S2 As2 130.26(15) . 1_455 ? Sb1 S2 Pb5 26.5(6) . 1_454 ? As1 S2 Pb5 28.0(10) . 1_454 ? Pb3 S2 Pb5 90.99(14) . 1_454 ? Pb4 S2 Pb5 125.56(18) . 1_454 ? Pb1 S2 Pb5 110.11(14) 1_554 1_454 ? Pb2 S2 Pb5 80.44(12) 1_454 1_454 ? As3 S2 Pb5 157.04(14) . 1_454 ? Sb8 S2 Pb5 58.26(8) . 1_454 ? As2 S2 Pb5 87.77(10) . 1_454 ? As2 S2 Pb5 42.54(6) 1_455 1_454 ? Sb1 S2 Sb9 26.5(6) . 1_454 ? As1 S2 Sb9 28.0(10) . 1_454 ? Pb3 S2 Sb9 90.99(14) . 1_454 ? Pb4 S2 Sb9 125.56(18) . 1_454 ? Pb1 S2 Sb9 110.11(14) 1_554 1_454 ? Pb2 S2 Sb9 80.44(12) 1_454 1_454 ? As3 S2 Sb9 157.04(14) . 1_454 ? Sb8 S2 Sb9 58.26(8) . 1_454 ? As2 S2 Sb9 87.77(10) . 1_454 ? As2 S2 Sb9 42.54(6) 1_455 1_454 ? Pb5 S2 Sb9 0.00(4) 1_454 1_454 ? As2 S3 Pb2 103.1(2) 1_556 . ? As2 S3 Sb1 109.2(4) 1_556 1_656 ? Pb2 S3 Sb1 97.1(4) . 1_656 ? As2 S3 As1 115.4(4) 1_556 1_656 ? Pb2 S3 As1 93.9(6) . 1_656 ? Sb1 S3 As1 6.4(6) 1_656 1_656 ? As2 S3 Pb5 88.9(2) 1_556 . ? Pb2 S3 Pb5 166.0(2) . . ? Sb1 S3 Pb5 71.7(4) 1_656 . ? As1 S3 Pb5 74.0(6) 1_656 . ? As2 S3 Pb4 133.2(2) 1_556 . ? Pb2 S3 Pb4 92.01(17) . . ? Sb1 S3 Pb4 112.6(4) 1_656 . ? As1 S3 Pb4 107.2(5) 1_656 . ? Pb5 S3 Pb4 84.87(14) . . ? As2 S3 Pb3 61.27(14) 1_556 1_656 ? Pb2 S3 Pb3 71.95(11) . 1_656 ? Sb1 S3 Pb3 62.6(4) 1_656 1_656 ? As1 S3 Pb3 66.5(5) 1_656 1_656 ? Pb5 S3 Pb3 108.55(16) . 1_656 ? Pb4 S3 Pb3 161.77(19) . 1_656 ? As2 S3 Pb1 58.21(14) 1_556 . ? Pb2 S3 Pb1 58.59(10) . . ? Sb1 S3 Pb1 143.5(4) 1_656 . ? As1 S3 Pb1 144.7(6) 1_656 . ? Pb5 S3 Pb1 135.33(16) . . ? Pb4 S3 Pb1 96.30(13) . . ? Pb3 S3 Pb1 82.90(9) 1_656 . ? As2 S3 Pb8 47.98(13) 1_556 . ? Pb2 S3 Pb8 136.06(16) . . ? Sb1 S3 Pb8 121.7(4) 1_656 . ? As1 S3 Pb8 126.5(5) 1_656 . ? Pb5 S3 Pb8 57.83(10) . . ? Pb4 S3 Pb8 91.24(12) . . ? Pb3 S3 Pb8 106.27(11) 1_656 . ? Pb1 S3 Pb8 77.51(8) . . ? As2 S3 Pb3 80.38(15) 1_556 . ? Pb2 S3 Pb3 97.90(15) . . ? Sb1 S3 Pb3 159.8(4) 1_656 . ? As1 S3 Pb3 157.5(6) 1_656 . ? Pb5 S3 Pb3 91.25(13) . . ? Pb4 S3 Pb3 53.51(8) . . ? Pb3 S3 Pb3 135.51(12) 1_656 . ? Pb1 S3 Pb3 56.69(6) . . ? Pb8 S3 Pb3 51.54(6) . . ? Sb8 S4 Pb5 104.8(2) . . ? Sb8 S4 Pb8 99.7(2) . . ? Pb5 S4 Pb8 95.3(2) . . ? Sb8 S4 Pb4 105.3(2) . . ? Pb5 S4 Pb4 88.36(16) . . ? Pb8 S4 Pb4 152.9(2) . . ? Sb8 S4 Pb3 100.4(2) . . ? Pb5 S4 Pb3 153.3(2) . . ? Pb8 S4 Pb3 89.10(15) . . ? Pb4 S4 Pb3 76.37(15) . . ? Sb8 S4 As2 161.8(3) . 1_556 ? Pb5 S4 As2 65.70(13) . 1_556 ? Pb8 S4 As2 67.20(13) . 1_556 ? Pb4 S4 As2 90.26(15) . 1_556 ? Pb3 S4 As2 92.24(15) . 1_556 ? Sb8 S4 Sb1 51.0(3) . . ? Pb5 S4 Sb1 128.5(4) . . ? Pb8 S4 Sb1 129.6(4) . . ? Pb4 S4 Sb1 63.7(3) . . ? Pb3 S4 Sb1 63.5(3) . . ? As2 S4 Sb1 147.1(3) 1_556 . ? Sb8 S4 As1 53.0(4) . . ? Pb5 S4 As1 128.0(5) . . ? Pb8 S4 As1 131.2(5) . . ? Pb4 S4 As1 61.5(4) . . ? Pb3 S4 As1 63.0(5) . . ? As2 S4 As1 145.2(4) 1_556 . ? Sb1 S4 As1 2.2(6) . . ? Sb8 S4 Sb10 62.05(16) . 2_656 ? Pb5 S4 Sb10 63.96(13) . 2_656 ? Pb8 S4 Sb10 60.52(12) . 2_656 ? Pb4 S4 Sb10 142.30(16) . 2_656 ? Pb3 S4 Sb10 138.49(16) . 2_656 ? As2 S4 Sb10 99.88(14) 1_556 2_656 ? Sb1 S4 Sb10 113.0(3) . 2_656 ? As1 S4 Sb10 114.9(4) . 2_656 ? Sb8 S4 Pb6 62.05(16) . 2_656 ? Pb5 S4 Pb6 63.96(13) . 2_656 ? Pb8 S4 Pb6 60.52(12) . 2_656 ? Pb4 S4 Pb6 142.30(16) . 2_656 ? Pb3 S4 Pb6 138.49(16) . 2_656 ? As2 S4 Pb6 99.88(14) 1_556 2_656 ? Sb1 S4 Pb6 113.0(3) . 2_656 ? As1 S4 Pb6 114.9(4) . 2_656 ? Sb10 S4 Pb6 0.00(4) 2_656 2_656 ? Sb8 S5 As1 98.0(7) . . ? Sb8 S5 Sb1 91.6(5) . . ? As1 S5 Sb1 6.4(11) . . ? Sb8 S5 Sb11 98.2(3) . . ? As1 S5 Sb11 163.5(7) . . ? Sb1 S5 Sb11 169.9(5) . . ? Sb8 S5 Pb7 104.4(2) . . ? As1 S5 Pb7 157.0(7) . . ? Sb1 S5 Pb7 163.2(5) . . ? Sb11 S5 Pb7 6.7(3) . . ? Sb8 S5 As2 175.6(3) . . ? As1 S5 As2 85.3(7) . . ? Sb1 S5 As2 91.6(5) . . ? Sb11 S5 As2 78.7(2) . . ? Pb7 S5 As2 72.74(18) . . ? Sb8 S5 Pb4 100.9(2) . . ? As1 S5 Pb4 89.0(7) . . ? Sb1 S5 Pb4 89.7(5) . . ? Sb11 S5 Pb4 90.9(3) . . ? Pb7 S5 Pb4 92.3(2) . . ? As2 S5 Pb4 76.14(14) . . ? Sb8 S5 Sb12 113.4(2) . 1_554 ? As1 S5 Sb12 66.6(7) . 1_554 ? Sb1 S5 Sb12 69.6(5) . 1_554 ? Sb11 S5 Sb12 103.8(3) . 1_554 ? Pb7 S5 Sb12 98.7(2) . 1_554 ? As2 S5 Sb12 70.49(13) . 1_554 ? Pb4 S5 Sb12 139.7(2) . 1_554 ? Sb8 S5 Pb8 113.4(2) . 1_554 ? As1 S5 Pb8 66.6(7) . 1_554 ? Sb1 S5 Pb8 69.6(5) . 1_554 ? Sb11 S5 Pb8 103.8(3) . 1_554 ? Pb7 S5 Pb8 98.7(2) . 1_554 ? As2 S5 Pb8 70.49(13) . 1_554 ? Pb4 S5 Pb8 139.7(2) . 1_554 ? Sb12 S5 Pb8 0.00(7) 1_554 1_554 ? Sb8 S5 Pb9 67.6(2) . 2_656 ? As1 S5 Pb9 119.6(8) . 2_656 ? Sb1 S5 Pb9 117.6(5) . 2_656 ? Sb11 S5 Pb9 64.6(3) . 2_656 ? Pb7 S5 Pb9 65.6(2) . 2_656 ? As2 S5 Pb9 113.37(19) . 2_656 ? Pb4 S5 Pb9 149.7(2) . 2_656 ? Sb12 S5 Pb9 67.47(16) 1_554 2_656 ? Pb8 S5 Pb9 67.47(16) 1_554 2_656 ? Sb8 S5 Sb5 71.3(2) . 2_656 ? As1 S5 Sb5 117.2(8) . 2_656 ? Sb1 S5 Sb5 115.6(6) . 2_656 ? Sb11 S5 Sb5 65.8(4) . 2_656 ? Pb7 S5 Sb5 66.2(3) . 2_656 ? As2 S5 Sb5 109.8(2) . 2_656 ? Pb4 S5 Sb5 153.2(3) . 2_656 ? Sb12 S5 Sb5 63.1(2) 1_554 2_656 ? Pb8 S5 Sb5 63.1(2) 1_554 2_656 ? Pb9 S5 Sb5 4.6(2) 2_656 2_656 ? Sb8 S5 Pb5 61.78(14) . . ? As1 S5 Pb5 137.5(7) . . ? Sb1 S5 Pb5 133.3(5) . . ? Sb11 S5 Pb5 55.1(2) . . ? Pb7 S5 Pb5 61.19(16) . . ? As2 S5 Pb5 113.86(16) . . ? Pb4 S5 Pb5 62.04(9) . . ? Sb12 S5 Pb5 154.21(19) 1_554 . ? Pb8 S5 Pb5 154.21(19) 1_554 . ? Pb9 S5 Pb5 88.47(16) 2_656 . ? Sb5 S5 Pb5 92.6(2) 2_656 . ? Pb7 S6 Sb11 7.5(3) 1_455 1_455 ? Pb7 S6 Pb8 96.4(3) 1_455 . ? Sb11 S6 Pb8 93.8(4) 1_455 . ? Pb7 S6 Pb10 97.2(3) 1_455 2_556 ? Sb11 S6 Pb10 90.7(4) 1_455 2_556 ? Pb8 S6 Pb10 98.0(3) . 2_556 ? Pb7 S6 Sb7 94.2(5) 1_455 2_556 ? Sb11 S6 Sb7 87.5(5) 1_455 2_556 ? Pb8 S6 Sb7 96.2(5) . 2_556 ? Pb10 S6 Sb7 3.8(6) 2_556 2_556 ? Pb7 S6 Sb8 88.0(2) 1_455 . ? Sb11 S6 Sb8 94.9(3) 1_455 . ? Pb8 S6 Sb8 87.12(18) . . ? Pb10 S6 Sb8 172.1(3) 2_556 . ? Sb7 S6 Sb8 175.8(5) 2_556 . ? Pb7 S6 Sb10 170.1(3) 1_455 2_656 ? Sb11 S6 Sb10 175.2(4) 1_455 2_656 ? Pb8 S6 Sb10 90.97(18) . 2_656 ? Pb10 S6 Sb10 88.2(3) 2_556 2_656 ? Sb7 S6 Sb10 91.6(5) 2_556 2_656 ? Sb8 S6 Sb10 85.74(15) . 2_656 ? Pb7 S6 Pb6 170.1(3) 1_455 2_656 ? Sb11 S6 Pb6 175.2(4) 1_455 2_656 ? Pb8 S6 Pb6 90.97(18) . 2_656 ? Pb10 S6 Pb6 88.2(3) 2_556 2_656 ? Sb7 S6 Pb6 91.6(5) 2_556 2_656 ? Sb8 S6 Pb6 85.74(15) . 2_656 ? Sb10 S6 Pb6 0.00(7) 2_656 2_656 ? Pb7 S6 Sb6 74.5(3) 1_455 2_556 ? Sb11 S6 Sb6 79.5(4) 1_455 2_556 ? Pb8 S6 Sb6 157.7(3) . 2_556 ? Pb10 S6 Sb6 103.3(4) 2_556 2_556 ? Sb7 S6 Sb6 104.7(5) 2_556 2_556 ? Sb8 S6 Sb6 72.4(2) . 2_556 ? Sb10 S6 Sb6 96.2(3) 2_656 2_556 ? Pb6 S6 Sb6 96.2(3) 2_656 2_556 ? Pb7 S6 As6 75.0(4) 1_455 2_556 ? Sb11 S6 As6 79.3(5) 1_455 2_556 ? Pb8 S6 As6 162.9(4) . 2_556 ? Pb10 S6 As6 97.7(4) 2_556 2_556 ? Sb7 S6 As6 99.1(5) 2_556 2_556 ? Sb8 S6 As6 78.0(3) . 2_556 ? Sb10 S6 As6 96.2(4) 2_656 2_556 ? Pb6 S6 As6 96.2(4) 2_656 2_556 ? Sb6 S6 As6 5.6(3) 2_556 2_556 ? Pb7 S6 Sb4 116.2(3) 1_455 2_656 ? Sb11 S6 Sb4 115.7(4) 1_455 2_656 ? Pb8 S6 Sb4 141.0(2) . 2_656 ? Pb10 S6 Sb4 59.0(3) 2_556 2_656 ? Sb7 S6 Sb4 62.4(5) 2_556 2_656 ? Sb8 S6 Sb4 113.42(18) . 2_656 ? Sb10 S6 Sb4 59.88(12) 2_656 2_656 ? Pb6 S6 Sb4 59.88(12) 2_656 2_656 ? Sb6 S6 Sb4 59.0(3) 2_556 2_656 ? As6 S6 Sb4 54.8(3) 2_556 2_656 ? Sb7 S7 Pb10 2.1(8) 2_656 2_656 ? Sb7 S7 Pb5 98.1(5) 2_656 . ? Pb10 S7 Pb5 100.1(3) 2_656 . ? Sb7 S7 Sb11 91.6(6) 2_656 . ? Pb10 S7 Sb11 92.2(5) 2_656 . ? Pb5 S7 Sb11 90.0(4) . . ? Sb7 S7 Pb7 92.6(5) 2_656 . ? Pb10 S7 Pb7 93.0(3) 2_656 . ? Pb5 S7 Pb7 92.6(3) . . ? Sb11 S7 Pb7 2.9(5) . . ? Sb7 S7 Sb10 92.6(5) 2_656 2_656 ? Pb10 S7 Sb10 91.9(3) 2_656 2_656 ? Pb5 S7 Sb10 95.2(2) . 2_656 ? Sb11 S7 Sb10 172.8(4) . 2_656 ? Pb7 S7 Sb10 170.0(3) . 2_656 ? Sb7 S7 Pb6 92.6(5) 2_656 2_656 ? Pb10 S7 Pb6 91.9(3) 2_656 2_656 ? Pb5 S7 Pb6 95.2(2) . 2_656 ? Sb11 S7 Pb6 172.8(4) . 2_656 ? Pb7 S7 Pb6 170.0(3) . 2_656 ? Sb10 S7 Pb6 0.00(4) 2_656 2_656 ? Sb7 S7 Sb8 175.0(6) 2_656 . ? Pb10 S7 Sb8 173.0(4) 2_656 . ? Pb5 S7 Sb8 86.23(18) . . ? Sb11 S7 Sb8 90.9(4) . . ? Pb7 S7 Sb8 89.7(2) . . ? Sb10 S7 Sb8 84.45(15) 2_656 . ? Pb6 S7 Sb8 84.45(15) 2_656 . ? Sb7 S7 Sb5 106.6(6) 2_656 2_656 ? Pb10 S7 Sb5 104.8(4) 2_656 2_656 ? Pb5 S7 Sb5 151.2(3) . 2_656 ? Sb11 S7 Sb5 74.9(4) . 2_656 ? Pb7 S7 Sb5 72.0(3) . 2_656 ? Sb10 S7 Sb5 98.3(3) 2_656 2_656 ? Pb6 S7 Sb5 98.3(3) 2_656 2_656 ? Sb8 S7 Sb5 69.9(3) . 2_656 ? Sb7 S7 Pb9 107.0(5) 2_656 2_656 ? Pb10 S7 Pb9 105.2(3) 2_656 2_656 ? Pb5 S7 Pb9 152.1(3) . 2_656 ? Sb11 S7 Pb9 77.6(4) . 2_656 ? Pb7 S7 Pb9 74.7(3) . 2_656 ? Sb10 S7 Pb9 95.6(2) 2_656 2_656 ? Pb6 S7 Pb9 95.6(2) 2_656 2_656 ? Sb8 S7 Pb9 69.3(2) . 2_656 ? Sb5 S7 Pb9 2.7(3) 2_656 2_656 ? Sb7 S7 As3 63.7(5) 2_656 2_656 ? Pb10 S7 As3 61.7(3) 2_656 2_656 ? Pb5 S7 As3 144.8(2) . 2_656 ? Sb11 S7 As3 118.8(4) . 2_656 ? Pb7 S7 As3 116.8(3) . 2_656 ? Sb10 S7 As3 58.45(12) 2_656 2_656 ? Pb6 S7 As3 58.45(12) 2_656 2_656 ? Sb8 S7 As3 111.30(18) . 2_656 ? Sb5 S7 As3 62.5(3) 2_656 2_656 ? Pb9 S7 As3 60.90(18) 2_656 2_656 ? Sb10 S8 Pb6 0.00(4) 2_656 2_656 ? Sb10 S8 Pb8 99.8(2) 2_656 . ? Pb6 S8 Pb8 99.8(2) 2_656 . ? Sb10 S8 Sb5 91.0(4) 2_656 2_657 ? Pb6 S8 Sb5 91.0(4) 2_656 2_657 ? Pb8 S8 Sb5 92.6(4) . 2_657 ? Sb10 S8 Pb9 95.3(3) 2_656 2_657 ? Pb6 S8 Pb9 95.3(3) 2_656 2_657 ? Pb8 S8 Pb9 93.5(2) . 2_657 ? Sb5 S8 Pb9 4.6(4) 2_657 2_657 ? Sb10 S8 Pb5 95.60(19) 2_656 . ? Pb6 S8 Pb5 95.60(19) 2_656 . ? Pb8 S8 Pb5 90.3(2) . . ? Sb5 S8 Pb5 172.2(4) 2_657 . ? Pb9 S8 Pb5 167.7(3) 2_657 . ? Sb10 S8 Sb6 88.4(3) 2_656 2_657 ? Pb6 S8 Sb6 88.4(3) 2_656 2_657 ? Pb8 S8 Sb6 170.1(3) . 2_657 ? Sb5 S8 Sb6 92.8(4) 2_657 2_657 ? Pb9 S8 Sb6 91.3(3) 2_657 2_657 ? Pb5 S8 Sb6 83.3(3) . 2_657 ? Sb10 S8 As6 84.9(4) 2_656 2_657 ? Pb6 S8 As6 84.9(4) 2_656 2_657 ? Pb8 S8 As6 175.3(4) . 2_657 ? Sb5 S8 As6 87.4(5) 2_657 2_657 ? Pb9 S8 As6 86.3(4) 2_657 2_657 ? Pb5 S8 As6 89.0(3) . 2_657 ? Sb6 S8 As6 6.5(3) 2_657 2_657 ? Sb10 S8 Sb11 152.1(3) 2_656 1_556 ? Pb6 S8 Sb11 152.1(3) 2_656 1_556 ? Pb8 S8 Sb11 104.6(3) . 1_556 ? Sb5 S8 Sb11 74.5(4) 2_657 1_556 ? Pb9 S8 Sb11 69.9(3) 2_657 1_556 ? Pb5 S8 Sb11 97.8(3) . 1_556 ? Sb6 S8 Sb11 69.0(4) 2_657 1_556 ? As6 S8 Sb11 71.0(5) 2_657 1_556 ? Sb10 S8 Pb7 154.1(3) 2_656 1_556 ? Pb6 S8 Pb7 154.1(3) 2_656 1_556 ? Pb8 S8 Pb7 104.5(2) . 1_556 ? Sb5 S8 Pb7 79.0(3) 2_657 1_556 ? Pb9 S8 Pb7 74.4(2) 2_657 1_556 ? Pb5 S8 Pb7 93.3(2) . 1_556 ? Sb6 S8 Pb7 68.5(3) 2_657 1_556 ? As6 S8 Pb7 70.9(4) 2_657 1_556 ? Sb11 S8 Pb7 4.5(3) 1_556 1_556 ? Pb10 S9 Sb7 3.7(7) 2_556 2_556 ? Pb10 S9 Pb9 99.4(4) 2_556 2_657 ? Sb7 S9 Pb9 103.1(5) 2_556 2_657 ? Pb10 S9 Sb5 94.9(4) 2_556 2_657 ? Sb7 S9 Sb5 98.4(6) 2_556 2_657 ? Pb9 S9 Sb5 6.6(3) 2_657 2_657 ? Pb10 S9 Pb8 96.7(3) 2_556 . ? Sb7 S9 Pb8 95.9(5) 2_556 . ? Pb9 S9 Pb8 92.9(2) 2_657 . ? Sb5 S9 Pb8 88.7(3) 2_657 . ? Pb10 S9 As6 89.3(5) 2_556 2_557 ? Sb7 S9 As6 89.8(6) 2_556 2_557 ? Pb9 S9 As6 90.5(5) 2_657 2_557 ? Sb5 S9 As6 95.2(5) 2_657 2_557 ? Pb8 S9 As6 172.5(5) . 2_557 ? Pb10 S9 Sb6 93.2(4) 2_556 2_557 ? Sb7 S9 Sb6 93.7(6) 2_556 2_557 ? Pb9 S9 Sb6 89.9(4) 2_657 2_557 ? Sb5 S9 Sb6 94.9(4) 2_657 2_557 ? Pb8 S9 Sb6 169.1(4) . 2_557 ? As6 S9 Sb6 3.9(6) 2_557 2_557 ? Pb10 S9 Sb9 94.1(3) 2_556 1_455 ? Sb7 S9 Sb9 90.4(5) 2_556 1_455 ? Pb9 S9 Sb9 166.5(3) 2_657 1_455 ? Sb5 S9 Sb9 170.2(4) 2_657 1_455 ? Pb8 S9 Sb9 86.19(18) . 1_455 ? As6 S9 Sb9 89.0(4) 2_557 1_455 ? Sb6 S9 Sb9 88.6(3) 2_557 1_455 ? Pb10 S9 Pb5 94.1(3) 2_556 1_455 ? Sb7 S9 Pb5 90.4(5) 2_556 1_455 ? Pb9 S9 Pb5 166.5(3) 2_657 1_455 ? Sb5 S9 Pb5 170.2(4) 2_657 1_455 ? Pb8 S9 Pb5 86.19(18) . 1_455 ? As6 S9 Pb5 89.0(4) 2_557 1_455 ? Sb6 S9 Pb5 88.6(3) 2_557 1_455 ? Sb9 S9 Pb5 0.00(5) 1_455 1_455 ? Pb10 S9 Sb8 162.8(4) 2_556 1_556 ? Sb7 S9 Sb8 165.0(6) 2_556 1_556 ? Pb9 S9 Sb8 71.8(2) 2_657 1_556 ? Sb5 S9 Sb8 77.5(3) 2_657 1_556 ? Pb8 S9 Sb8 98.45(19) . 1_556 ? As6 S9 Sb8 76.3(4) 2_557 1_556 ? Sb6 S9 Sb8 72.5(3) 2_557 1_556 ? Sb9 S9 Sb8 94.93(17) 1_455 1_556 ? Pb5 S9 Sb8 94.93(17) 1_455 1_556 ? Pb10 S9 Sb1 142.0(4) 2_556 1_556 ? Sb7 S9 Sb1 138.9(6) 2_556 1_556 ? Pb9 S9 Sb1 109.1(4) 2_657 1_556 ? Sb5 S9 Sb1 111.0(5) 2_657 1_556 ? Pb8 S9 Sb1 58.2(3) . 1_556 ? As6 S9 Sb1 114.4(5) 2_557 1_556 ? Sb6 S9 Sb1 111.0(5) 2_557 1_556 ? Sb9 S9 Sb1 59.2(4) 1_455 1_556 ? Pb5 S9 Sb1 59.2(4) 1_455 1_556 ? Sb8 S9 Sb1 54.6(2) 1_556 1_556 ? Sb6 S10 As6 7.6(6) 1_554 1_554 ? Sb6 S10 Pb6 104.0(4) 1_554 . ? As6 S10 Pb6 103.3(6) 1_554 . ? Sb6 S10 Sb7 96.0(6) 1_554 . ? As6 S10 Sb7 103.6(6) 1_554 . ? Pb6 S10 Sb7 92.6(4) . . ? Sb6 S10 Pb10 97.8(4) 1_554 . ? As6 S10 Pb10 105.4(5) 1_554 . ? Pb6 S10 Pb10 95.3(3) . . ? Sb7 S10 Pb10 3.7(6) . . ? Sb6 S10 Pb1 103.9(4) 1_554 1_554 ? As6 S10 Pb1 96.3(4) 1_554 1_554 ? Pb6 S10 Pb1 88.13(17) . 1_554 ? Sb7 S10 Pb1 159.3(5) . 1_554 ? Pb10 S10 Pb1 156.5(4) . 1_554 ? Sb6 S10 Pb2 98.5(4) 1_554 1_454 ? As6 S10 Pb2 97.8(6) 1_554 1_454 ? Pb6 S10 Pb2 156.2(3) . 1_454 ? Sb7 S10 Pb2 92.9(4) . 1_454 ? Pb10 S10 Pb2 89.4(3) . 1_454 ? Pb1 S10 Pb2 78.73(16) 1_554 1_454 ? Sb6 S10 As3 160.6(4) 1_554 . ? As6 S10 As3 166.2(6) 1_554 . ? Pb6 S10 As3 66.75(14) . . ? Sb7 S10 As3 68.5(5) . . ? Pb10 S10 As3 67.4(3) . . ? Pb1 S10 As3 93.03(18) 1_554 . ? Pb2 S10 As3 93.94(18) 1_454 . ? Sb6 S10 Sb4 53.7(4) 1_554 1_454 ? As6 S10 Sb4 48.2(5) 1_554 1_454 ? Pb6 S10 Sb4 128.80(19) . 1_454 ? Sb7 S10 Sb4 130.8(4) . 1_454 ? Pb10 S10 Sb4 129.7(3) . 1_454 ? Pb1 S10 Sb4 60.96(11) 1_554 1_454 ? Pb2 S10 Sb4 60.74(11) 1_454 1_454 ? As3 S10 Sb4 145.5(2) . 1_454 ? Sb6 S10 Sb5 64.3(4) 1_554 1_554 ? As6 S10 Sb5 59.3(5) 1_554 1_554 ? Pb6 S10 Sb5 54.59(19) . 1_554 ? Sb7 S10 Sb5 130.8(5) . 1_554 ? Pb10 S10 Sb5 134.5(4) . 1_554 ? Pb1 S10 Sb5 65.0(2) 1_554 1_554 ? Pb2 S10 Sb5 132.6(2) 1_454 1_554 ? As3 S10 Sb5 116.5(2) . 1_554 ? Sb4 S10 Sb5 74.88(19) 1_454 1_554 ? Sb6 S10 Pb9 62.5(4) 1_554 1_554 ? As6 S10 Pb9 57.3(5) 1_554 1_554 ? Pb6 S10 Pb9 57.51(15) . 1_554 ? Sb7 S10 Pb9 132.5(5) . 1_554 ? Pb10 S10 Pb9 136.2(3) . 1_554 ? Pb1 S10 Pb9 64.03(15) 1_554 1_554 ? Pb2 S10 Pb9 129.9(2) 1_454 1_554 ? As3 S10 Pb9 119.06(18) . 1_554 ? Sb4 S10 Pb9 71.97(13) 1_454 1_554 ? Sb5 S10 Pb9 2.9(2) 1_554 1_554 ? As3 S11 Pb4 103.8(2) . . ? As3 S11 Sb4 111.9(2) . . ? Pb4 S11 Sb4 92.31(16) . . ? As3 S11 Pb6 84.0(2) . . ? Pb4 S11 Pb6 167.58(18) . . ? Sb4 S11 Pb6 75.70(14) . . ? As3 S11 Pb1 129.3(2) . 1_554 ? Pb4 S11 Pb1 97.92(17) . 1_554 ? Sb4 S11 Pb1 112.42(15) . 1_554 ? Pb6 S11 Pb1 84.02(14) . 1_554 ? As3 S11 Pb2 64.08(15) . . ? Pb4 S11 Pb2 69.00(11) . . ? Sb4 S11 Pb2 61.66(11) . . ? Pb6 S11 Pb2 106.97(15) . . ? Pb1 S11 Pb2 164.50(17) 1_554 . ? As3 S11 Pb3 59.07(13) . . ? Pb4 S11 Pb3 58.40(9) . . ? Sb4 S11 Pb3 140.95(18) . . ? Pb6 S11 Pb3 133.67(14) . . ? Pb1 S11 Pb3 97.85(12) 1_554 . ? Pb2 S11 Pb3 82.57(9) . . ? As3 S11 Sb7 42.9(3) . . ? Pb4 S11 Sb7 136.5(3) . . ? Sb4 S11 Sb7 123.0(3) . . ? Pb6 S11 Sb7 55.4(2) . . ? Pb1 S11 Sb7 91.4(3) 1_554 . ? Pb2 S11 Sb7 103.8(3) . . ? Pb3 S11 Sb7 78.3(2) . . ? As3 S11 Pb10 42.29(18) . . ? Pb4 S11 Pb10 134.45(19) . . ? Sb4 S11 Pb10 125.0(2) . . ? Pb6 S11 Pb10 57.47(16) . . ? Pb1 S11 Pb10 91.17(18) 1_554 . ? Pb2 S11 Pb10 103.91(17) . . ? Pb3 S11 Pb10 76.20(14) . . ? Sb7 S11 Pb10 2.1(4) . . ? As3 S11 Pb2 76.78(14) . 1_454 ? Pb4 S11 Pb2 99.36(13) . 1_454 ? Sb4 S11 Pb2 163.47(17) . 1_454 ? Pb6 S11 Pb2 91.77(12) . 1_454 ? Pb1 S11 Pb2 54.58(8) 1_554 1_454 ? Pb2 S11 Pb2 133.69(10) . 1_454 ? Pb3 S11 Pb2 55.49(6) . 1_454 ? Sb7 S11 Pb2 53.4(2) . 1_454 ? Pb10 S11 Pb2 51.82(14) . 1_454 ? As3 S11 As2 148.0(2) . . ? Pb4 S11 As2 50.49(9) . . ? Sb4 S11 As2 90.33(12) . . ? Pb6 S11 As2 125.08(14) . . ? Pb1 S11 As2 52.57(9) 1_554 . ? Pb2 S11 As2 112.05(12) . . ? Pb3 S11 As2 89.08(10) . . ? Sb7 S11 As2 140.0(3) . . ? Pb10 S11 As2 138.90(18) . . ? Pb2 S11 As2 88.15(9) 1_454 . ? As6 S12 Sb6 8.6(4) 1_655 1_655 ? As6 S12 Sb4 86.5(4) 1_655 . ? Sb6 S12 Sb4 93.1(4) 1_655 . ? As6 S12 Pb9 103.8(4) 1_655 . ? Sb6 S12 Pb9 96.1(4) 1_655 . ? Sb4 S12 Pb9 164.5(3) . . ? As6 S12 Sb5 102.1(5) 1_655 . ? Sb6 S12 Sb5 94.8(4) 1_655 . ? Sb4 S12 Sb5 168.9(3) . . ? Pb9 S12 Sb5 4.8(4) . . ? As6 S12 Pb2 101.9(5) 1_655 . ? Sb6 S12 Pb2 107.1(4) 1_655 . ? Sb4 S12 Pb2 91.52(18) . . ? Pb9 S12 Pb2 97.6(2) . . ? Sb5 S12 Pb2 93.6(3) . . ? As6 S12 As3 174.9(5) 1_655 . ? Sb6 S12 As3 168.1(4) 1_655 . ? Sb4 S12 As3 92.63(18) . . ? Pb9 S12 As3 76.1(2) . . ? Sb5 S12 As3 78.2(3) . . ? Pb2 S12 As3 83.15(15) . . ? As6 S12 Pb6 111.4(5) 1_655 . ? Sb6 S12 Pb6 108.8(4) 1_655 . ? Sb4 S12 Pb6 70.10(13) . . ? Pb9 S12 Pb6 95.1(2) . . ? Sb5 S12 Pb6 99.9(3) . . ? Pb2 S12 Pb6 140.2(2) . . ? As3 S12 Pb6 63.60(12) . . ? As6 S12 Sb8 70.9(4) 1_655 2_646 ? Sb6 S12 Sb8 63.0(3) 1_655 2_646 ? Sb4 S12 Sb8 115.38(18) . 2_646 ? Pb9 S12 Sb8 59.05(19) . 2_646 ? Sb5 S12 Sb8 62.1(3) . 2_646 ? Pb2 S12 Sb8 150.99(18) . 2_646 ? As3 S12 Sb8 105.03(16) . 2_646 ? Pb6 S12 Sb8 64.55(10) . 2_646 ? As6 S12 Sb7 60.7(5) 1_655 1_656 ? Sb6 S12 Sb7 58.4(4) 1_655 1_656 ? Sb4 S12 Sb7 134.3(3) . 1_656 ? Pb9 S12 Sb7 61.1(3) . 1_656 ? Sb5 S12 Sb7 56.8(4) . 1_656 ? Pb2 S12 Sb7 68.0(3) . 1_656 ? As3 S12 Sb7 122.8(3) . 1_656 ? Pb6 S12 Sb7 148.4(3) . 1_656 ? Sb8 S12 Sb7 84.6(3) 2_646 1_656 ? As6 S12 Pb10 62.5(5) 1_655 1_656 ? Sb6 S12 Pb10 60.4(4) 1_655 1_656 ? Sb4 S12 Pb10 134.5(2) . 1_656 ? Pb9 S12 Pb10 61.0(2) . 1_656 ? Sb5 S12 Pb10 56.6(3) . 1_656 ? Pb2 S12 Pb10 65.98(19) . 1_656 ? As3 S12 Pb10 121.06(19) . 1_656 ? Pb6 S12 Pb10 149.9(2) . 1_656 ? Sb8 S12 Pb10 86.50(19) 2_646 1_656 ? Sb7 S12 Pb10 2.3(4) 1_656 1_656 ? Sb6 S13 As6 4.5(8) . . ? Sb6 S13 Sb4 92.3(4) . 1_455 ? As6 S13 Sb4 93.0(6) . 1_455 ? Sb6 S13 Sb5 96.8(5) . . ? As6 S13 Sb5 96.6(6) . . ? Sb4 S13 Sb5 168.8(3) 1_455 . ? Sb6 S13 Pb9 100.7(4) . . ? As6 S13 Pb9 100.9(6) . . ? Sb4 S13 Pb9 162.9(3) 1_455 . ? Sb5 S13 Pb9 6.0(3) . . ? Sb6 S13 Pb1 104.2(4) . . ? As6 S13 Pb1 99.8(5) . . ? Sb4 S13 Pb1 92.97(18) 1_455 . ? Sb5 S13 Pb1 91.2(3) . . ? Pb9 S13 Pb1 94.5(2) . . ? Sb6 S13 As3 171.2(4) . . ? As6 S13 As3 174.9(6) . . ? Sb4 S13 As3 90.19(18) 1_455 . ? Sb5 S13 As3 79.8(3) . . ? Pb9 S13 As3 75.33(19) . . ? Pb1 S13 As3 84.09(15) . . ? Sb6 S13 Pb10 106.6(4) . . ? As6 S13 Pb10 111.0(5) . . ? Sb4 S13 Pb10 69.3(2) 1_455 . ? Sb5 S13 Pb10 101.6(3) . . ? Pb9 S13 Pb10 96.1(3) . . ? Pb1 S13 Pb10 144.8(3) . . ? As3 S13 Pb10 66.5(2) . . ? Sb6 S13 Sb7 105.8(5) . . ? As6 S13 Sb7 110.2(6) . . ? Sb4 S13 Sb7 72.1(3) 1_455 . ? Sb5 S13 Sb7 98.9(4) . . ? Pb9 S13 Sb7 93.5(4) . . ? Pb1 S13 Sb7 146.8(4) . . ? As3 S13 Sb7 67.0(4) . . ? Pb10 S13 Sb7 3.0(5) . . ? Sb6 S13 Pb7 62.6(4) . 2_646 ? As6 S13 Pb7 66.2(6) . 2_646 ? Sb4 S13 Pb7 115.7(2) 1_455 2_646 ? Sb5 S13 Pb7 63.6(3) . 2_646 ? Pb9 S13 Pb7 62.3(2) . 2_646 ? Pb1 S13 Pb7 147.8(2) . 2_646 ? As3 S13 Pb7 108.74(18) . 2_646 ? Pb10 S13 Pb7 64.6(2) . 2_646 ? Sb7 S13 Pb7 62.0(4) . 2_646 ? Sb6 S13 Sb11 67.0(4) . 2_646 ? As6 S13 Sb11 70.8(5) . 2_646 ? Sb4 S13 Sb11 114.4(3) 1_455 2_646 ? Sb5 S13 Sb11 63.8(4) . 2_646 ? Pb9 S13 Sb11 62.0(3) . 2_646 ? Pb1 S13 Sb11 151.0(3) . 2_646 ? As3 S13 Sb11 104.2(2) . 2_646 ? Pb10 S13 Sb11 60.3(3) . 2_646 ? Sb7 S13 Sb11 57.6(4) . 2_646 ? Pb7 S13 Sb11 4.90(19) 2_646 2_646 ? Sb6 S13 Sb10 62.9(3) . 1_556 ? As6 S13 Sb10 59.7(5) . 1_556 ? Sb4 S13 Sb10 135.60(18) 1_455 1_556 ? Sb5 S13 Sb10 55.3(2) . 1_556 ? Pb9 S13 Sb10 61.23(16) . 1_556 ? Pb1 S13 Sb10 62.16(10) . 1_556 ? As3 S13 Sb10 120.12(15) . 1_556 ? Pb10 S13 Sb10 149.8(3) . 1_556 ? Sb7 S13 Sb10 146.9(4) . 1_556 ? Pb7 S13 Sb10 86.31(14) 2_646 1_556 ? Sb11 S13 Sb10 90.3(2) 2_646 1_556 ? Sb4 S14 Pb2 99.4(2) . . ? Sb4 S14 Pb1 96.0(2) . 1_655 ? Pb2 S14 Pb1 85.72(17) . 1_655 ? Sb4 S14 Pb4 96.3(2) . . ? Pb2 S14 Pb4 93.22(18) . . ? Pb1 S14 Pb4 167.7(3) 1_655 . ? Sb4 S14 Pb3 93.8(2) . 1_655 ? Pb2 S14 Pb3 166.5(3) . 1_655 ? Pb1 S14 Pb3 95.97(18) 1_655 1_655 ? Pb4 S14 Pb3 82.25(16) . 1_655 ? Sb4 S14 Sb1 170.3(4) . 1_656 ? Pb2 S14 Sb1 77.6(4) . 1_656 ? Pb1 S14 Sb1 74.7(4) 1_655 1_656 ? Pb4 S14 Sb1 93.1(4) . 1_656 ? Pb3 S14 Sb1 89.8(4) 1_655 1_656 ? Sb4 S14 As1 170.0(6) . 1_656 ? Pb2 S14 As1 79.3(6) . 1_656 ? Pb1 S14 As1 74.0(6) 1_655 1_656 ? Pb4 S14 As1 93.7(6) . 1_656 ? Pb3 S14 As1 88.2(6) 1_655 1_656 ? Sb1 S14 As1 1.8(9) 1_656 1_656 ? Sb4 S14 Sb6 47.7(2) . 1_655 ? Pb2 S14 Sb6 63.4(2) . 1_655 ? Pb1 S14 Sb6 64.09(19) 1_655 1_655 ? Pb4 S14 Sb6 126.1(2) . 1_655 ? Pb3 S14 Sb6 129.3(2) 1_655 1_655 ? Sb1 S14 Sb6 123.8(4) 1_656 1_655 ? As1 S14 Sb6 124.5(5) 1_656 1_655 ? Sb4 S14 As6 48.6(3) . 1_655 ? Pb2 S14 As6 64.9(3) . 1_655 ? Pb1 S14 As6 61.4(2) 1_655 1_655 ? Pb4 S14 As6 129.0(3) . 1_655 ? Pb3 S14 As6 127.6(3) 1_655 1_655 ? Sb1 S14 As6 122.7(4) 1_656 1_655 ? As1 S14 As6 123.2(6) 1_656 1_655 ? Sb6 S14 As6 2.9(3) 1_655 1_655 ? Sb4 S14 As3 58.11(14) . 1_655 ? Pb2 S14 As3 132.7(2) . 1_655 ? Pb1 S14 As3 59.56(11) 1_655 1_655 ? Pb4 S14 As3 127.48(18) . 1_655 ? Pb3 S14 As3 57.92(11) 1_655 1_655 ? Sb1 S14 As3 117.2(4) 1_656 1_655 ? As1 S14 As3 115.6(6) 1_656 1_655 ? Sb6 S14 As3 72.36(19) 1_655 1_655 ? As6 S14 As3 70.3(3) 1_655 1_655 ? Sb4 S14 As3 62.39(15) . . ? Pb2 S14 As3 59.08(12) . . ? Pb1 S14 As3 131.5(2) 1_655 . ? Pb4 S14 As3 56.49(11) . . ? Pb3 S14 As3 126.26(17) 1_655 . ? Sb1 S14 As3 122.0(4) 1_656 . ? As1 S14 As3 123.7(6) 1_656 . ? Sb6 S14 As3 70.27(18) 1_655 . ? As6 S14 As3 73.2(2) 1_655 . ? As3 S14 As3 120.45(16) 1_655 . ? Sb4 S14 Pb5 148.4(2) . . ? Pb2 S14 Pb5 84.43(15) . . ? Pb1 S14 Pb5 115.60(17) 1_655 . ? Pb4 S14 Pb5 52.10(10) . . ? Pb3 S14 Pb5 82.73(14) 1_655 . ? Sb1 S14 Pb5 41.0(3) 1_656 . ? As1 S14 Pb5 41.6(6) 1_656 . ? Sb6 S14 Pb5 147.8(2) 1_655 . ? As6 S14 Pb5 149.1(3) 1_655 . ? As3 S14 Pb5 137.55(15) 1_655 . ? As3 S14 Pb5 94.55(12) . . ? As2 S15 Pb3 101.7(2) . 1_655 ? As2 S15 Pb4 103.0(2) . . ? Pb3 S15 Pb4 92.83(19) 1_655 . ? As2 S15 Pb2 91.5(2) . 1_554 ? Pb3 S15 Pb2 94.07(16) 1_655 1_554 ? Pb4 S15 Pb2 162.3(2) . 1_554 ? As2 S15 Pb1 92.7(2) . 1_554 ? Pb3 S15 Pb1 162.9(3) 1_655 1_554 ? Pb4 S15 Pb1 92.91(16) . 1_554 ? Pb2 S15 Pb1 76.16(14) 1_554 1_554 ? As2 S15 Sb4 177.2(3) . . ? Pb3 S15 Sb4 75.82(15) 1_655 . ? Pb4 S15 Sb4 75.90(14) . . ? Pb2 S15 Sb4 90.05(16) 1_554 . ? Pb1 S15 Sb4 89.97(16) 1_554 . ? As2 S15 As1 56.6(5) . . ? Pb3 S15 As1 137.7(3) 1_655 . ? Pb4 S15 As1 62.8(3) . . ? Pb2 S15 As1 119.9(3) 1_554 . ? Pb1 S15 As1 58.7(3) 1_554 . ? Sb4 S15 As1 124.3(4) . . ? As2 S15 Sb1 57.1(3) . . ? Pb3 S15 Sb1 134.1(3) 1_655 . ? Pb4 S15 Sb1 59.5(2) . . ? Pb2 S15 Sb1 123.7(2) 1_554 . ? Pb1 S15 Sb1 62.1(2) 1_554 . ? Sb4 S15 Sb1 123.7(3) . . ? As1 S15 Sb1 4.0(3) . . ? As2 S15 Sb11 52.7(2) . . ? Pb3 S15 Sb11 66.9(2) 1_655 . ? Pb4 S15 Sb11 67.04(19) . . ? Pb2 S15 Sb11 130.6(2) 1_554 . ? Pb1 S15 Sb11 130.1(3) 1_554 . ? Sb4 S15 Sb11 124.6(2) . . ? As1 S15 Sb11 71.7(4) . . ? Sb1 S15 Sb11 68.6(3) . . ? As2 S15 Pb7 49.68(18) . . ? Pb3 S15 Pb7 67.01(17) 1_655 . ? Pb4 S15 Pb7 70.66(16) . . ? Pb2 S15 Pb7 126.99(18) 1_554 . ? Pb1 S15 Pb7 130.1(2) 1_554 . ? Sb4 S15 Pb7 127.62(19) . . ? As1 S15 Pb7 72.2(4) . . ? Sb1 S15 Pb7 69.2(3) . . ? Sb11 S15 Pb7 3.8(2) . . ? As2 S15 Sb1 59.8(3) . 1_655 ? Pb3 S15 Sb1 56.4(2) 1_655 1_655 ? Pb4 S15 Sb1 135.1(2) . 1_655 ? Pb2 S15 Sb1 61.30(18) 1_554 1_655 ? Pb1 S15 Sb1 126.5(2) 1_554 1_655 ? Sb4 S15 Sb1 119.1(3) . 1_655 ? As1 S15 Sb1 116.5(5) . 1_655 ? Sb1 S15 Sb1 116.7(4) . 1_655 ? Sb11 S15 Sb1 70.7(2) . 1_655 ? Pb7 S15 Sb1 67.4(2) . 1_655 ? As2 S15 As1 60.5(4) . 1_655 ? Pb3 S15 As1 58.9(3) 1_655 1_655 ? Pb4 S15 As1 139.0(3) . 1_655 ? Pb2 S15 As1 57.5(2) 1_554 1_655 ? Pb1 S15 As1 123.1(3) 1_554 1_655 ? Sb4 S15 As1 118.6(4) . 1_655 ? As1 S15 As1 117.1(7) . 1_655 ? Sb1 S15 As1 117.6(4) . 1_655 ? Sb11 S15 As1 74.2(3) . 1_655 ? Pb7 S15 As1 70.9(3) . 1_655 ? Sb1 S15 As1 3.9(3) 1_655 1_655 ? As2 S16 As1 111.5(7) 1_556 1_556 ? As2 S16 Sb1 106.6(5) 1_556 1_556 ? As1 S16 Sb1 5.0(11) 1_556 1_556 ? As2 S16 Pb1 102.5(2) 1_556 . ? As1 S16 Pb1 96.4(8) 1_556 . ? Sb1 S16 Pb1 98.8(5) 1_556 . ? As2 S16 Pb8 87.96(19) 1_556 . ? As1 S16 Pb8 72.7(8) 1_556 . ? Sb1 S16 Pb8 70.9(5) 1_556 . ? Pb1 S16 Pb8 167.25(19) . . ? As2 S16 Pb3 132.2(2) 1_556 . ? As1 S16 Pb3 110.4(7) 1_556 . ? Sb1 S16 Pb3 114.4(5) 1_556 . ? Pb1 S16 Pb3 94.73(16) . . ? Pb8 S16 Pb3 83.34(13) . . ? As2 S16 Pb4 61.05(14) 1_556 1_556 ? As1 S16 Pb4 65.3(7) 1_556 1_556 ? Sb1 S16 Pb4 62.5(4) 1_556 1_556 ? Pb1 S16 Pb4 70.44(11) . 1_556 ? Pb8 S16 Pb4 109.38(14) . 1_556 ? Pb3 S16 Pb4 163.30(18) . 1_556 ? As2 S16 Pb2 57.70(13) 1_556 . ? As1 S16 Pb2 145.4(8) 1_556 . ? Sb1 S16 Pb2 143.9(5) 1_556 . ? Pb1 S16 Pb2 59.34(9) . . ? Pb8 S16 Pb2 133.36(15) . . ? Pb3 S16 Pb2 96.86(12) . . ? Pb4 S16 Pb2 82.39(9) 1_556 . ? As2 S16 Pb5 46.82(13) 1_556 . ? As1 S16 Pb5 123.9(7) 1_556 . ? Sb1 S16 Pb5 119.9(5) 1_556 . ? Pb1 S16 Pb5 134.56(15) . . ? Pb8 S16 Pb5 58.16(9) . . ? Pb3 S16 Pb5 90.28(11) . . ? Pb4 S16 Pb5 105.54(11) 1_556 . ? Pb2 S16 Pb5 75.22(8) . . ? As2 S16 Pb4 79.18(15) 1_556 . ? As1 S16 Pb4 160.2(8) 1_556 . ? Sb1 S16 Pb4 161.0(5) 1_556 . ? Pb1 S16 Pb4 97.43(13) . . ? Pb8 S16 Pb4 91.67(12) . . ? Pb3 S16 Pb4 54.31(7) . . ? Pb4 S16 Pb4 133.17(12) 1_556 . ? Pb2 S16 Pb4 54.43(6) . . ? Pb5 S16 Pb4 51.08(6) . . ? Sb11 S17 Pb7 7.6(3) . . ? Sb11 S17 Pb5 92.2(3) . . ? Pb7 S17 Pb5 99.6(3) . . ? Sb11 S17 Sb12 90.3(4) . 1_655 ? Pb7 S17 Sb12 91.9(3) . 1_655 ? Pb5 S17 Sb12 89.07(19) . 1_655 ? Sb11 S17 Pb8 90.3(4) . 1_655 ? Pb7 S17 Pb8 91.9(3) . 1_655 ? Pb5 S17 Pb8 89.07(19) . 1_655 ? Sb12 S17 Pb8 0.00(7) 1_655 1_655 ? Sb11 S17 Pb4 111.3(4) . . ? Pb7 S17 Pb4 109.4(3) . . ? Pb5 S17 Pb4 91.01(16) . . ? Sb12 S17 Pb4 158.4(3) 1_655 . ? Pb8 S17 Pb4 158.4(3) 1_655 . ? Sb11 S17 Pb3 108.5(3) . 1_655 ? Pb7 S17 Pb3 101.1(2) . 1_655 ? Pb5 S17 Pb3 159.1(3) . 1_655 ? Sb12 S17 Pb3 88.40(15) 1_655 1_655 ? Pb8 S17 Pb3 88.40(15) 1_655 1_655 ? Pb4 S17 Pb3 83.88(17) . 1_655 ? Sb11 S17 Sb1 140.8(5) . 1_656 ? Pb7 S17 Sb1 146.4(4) . 1_656 ? Pb5 S17 Sb1 64.1(3) . 1_656 ? Sb12 S17 Sb1 60.4(4) 1_655 1_656 ? Pb8 S17 Sb1 60.4(4) 1_655 1_656 ? Pb4 S17 Sb1 100.5(4) . 1_656 ? Pb3 S17 Sb1 96.9(3) 1_655 1_656 ? Sb11 S17 As1 144.8(6) . 1_656 ? Pb7 S17 As1 150.1(6) . 1_656 ? Pb5 S17 As1 68.1(5) . 1_656 ? Sb12 S17 As1 61.8(6) 1_655 1_656 ? Pb8 S17 As1 61.8(6) 1_655 1_656 ? Pb4 S17 As1 98.4(6) . 1_656 ? Pb3 S17 As1 92.6(5) 1_655 1_656 ? Sb1 S17 As1 4.6(6) 1_656 1_656 ? Sb11 S17 As2 64.9(3) . . ? Pb7 S17 As2 58.5(2) . . ? Pb5 S17 As2 132.60(19) . . ? Sb12 S17 As2 129.13(18) 1_655 . ? Pb8 S17 As2 129.13(18) 1_655 . ? Pb4 S17 As2 63.72(12) . . ? Pb3 S17 As2 62.25(12) 1_655 . ? Sb1 S17 As2 153.8(3) 1_656 . ? As1 S17 As2 149.3(4) 1_656 . ? Sb11 S17 Sb8 59.6(4) . . ? Pb7 S17 Sb8 63.4(2) . . ? Pb5 S17 Sb8 57.94(11) . . ? Sb12 S17 Sb8 131.08(19) 1_655 . ? Pb8 S17 Sb8 131.08(19) 1_655 . ? Pb4 S17 Sb8 65.38(11) . . ? Pb3 S17 Sb8 135.24(19) 1_655 . ? Sb1 S17 Sb8 119.3(4) 1_656 . ? As1 S17 Sb8 122.2(6) 1_656 . ? As2 S17 Sb8 74.84(11) . . ? Sb8 S18 Sb1 86.9(5) . . ? Sb8 S18 As1 90.2(7) . . ? Sb1 S18 As1 3.3(11) . . ? Sb8 S18 Pb7 102.6(3) . 1_455 ? Sb1 S18 Pb7 168.0(5) . 1_455 ? As1 S18 Pb7 165.1(7) . 1_455 ? Sb8 S18 Sb11 100.5(3) . 1_455 ? Sb1 S18 Sb11 171.4(6) . 1_455 ? As1 S18 Sb11 168.3(8) . 1_455 ? Pb7 S18 Sb11 3.6(4) 1_455 1_455 ? Sb8 S18 As2 178.0(2) . 1_455 ? Sb1 S18 As2 94.8(5) . 1_455 ? As1 S18 As2 91.5(7) . 1_455 ? Pb7 S18 As2 75.8(2) 1_455 1_455 ? Sb11 S18 As2 77.9(3) 1_455 1_455 ? Sb8 S18 Pb3 102.4(2) . . ? Sb1 S18 Pb3 89.4(5) . . ? As1 S18 Pb3 88.9(7) . . ? Pb7 S18 Pb3 95.6(2) 1_455 . ? Sb11 S18 Pb3 93.2(3) 1_455 . ? As2 S18 Pb3 76.72(14) 1_455 . ? Sb8 S18 Sb9 113.8(2) . 1_454 ? Sb1 S18 Sb9 69.5(5) . 1_454 ? As1 S18 Sb9 67.8(7) . 1_454 ? Pb7 S18 Sb9 99.6(2) 1_455 1_454 ? Sb11 S18 Sb9 103.2(3) 1_455 1_454 ? As2 S18 Sb9 67.76(12) 1_455 1_454 ? Pb3 S18 Sb9 136.16(19) . 1_454 ? Sb8 S18 Pb5 113.8(2) . 1_454 ? Sb1 S18 Pb5 69.5(5) . 1_454 ? As1 S18 Pb5 67.8(7) . 1_454 ? Pb7 S18 Pb5 99.6(2) 1_455 1_454 ? Sb11 S18 Pb5 103.2(3) 1_455 1_454 ? As2 S18 Pb5 67.76(12) 1_455 1_454 ? Pb3 S18 Pb5 136.16(19) . 1_454 ? Sb9 S18 Pb5 0.00(7) 1_454 1_454 ? Sb8 S18 As6 70.3(3) . 2_556 ? Sb1 S18 As6 116.8(6) . 2_556 ? As1 S18 As6 117.8(7) . 2_556 ? Pb7 S18 As6 61.1(3) 1_455 2_556 ? Sb11 S18 As6 62.6(4) 1_455 2_556 ? As2 S18 As6 109.7(3) 1_455 2_556 ? Pb3 S18 As6 151.6(3) . 2_556 ? Sb9 S18 As6 68.2(3) 1_454 2_556 ? Pb5 S18 As6 68.2(3) 1_454 2_556 ? Sb8 S18 Sb6 68.3(3) . 2_556 ? Sb1 S18 Sb6 114.4(5) . 2_556 ? As1 S18 Sb6 115.6(7) . 2_556 ? Pb7 S18 Sb6 63.8(3) 1_455 2_556 ? Sb11 S18 Sb6 65.2(4) 1_455 2_556 ? As2 S18 Sb6 111.7(3) 1_455 2_556 ? Pb3 S18 Sb6 153.0(3) . 2_556 ? Sb9 S18 Sb6 67.9(2) 1_454 2_556 ? Pb5 S18 Sb6 67.9(2) 1_454 2_556 ? As6 S18 Sb6 2.8(4) 2_556 2_556 ? Sb8 S18 Pb8 60.91(13) . . ? Sb1 S18 Pb8 130.7(5) . . ? As1 S18 Pb8 133.1(7) . . ? Pb7 S18 Pb8 61.21(19) 1_455 . ? Sb11 S18 Pb8 57.6(3) 1_455 . ? As2 S18 Pb8 117.15(15) 1_455 . ? Pb3 S18 Pb8 65.31(10) . . ? Sb9 S18 Pb8 155.32(18) 1_454 . ? Pb5 S18 Pb8 155.32(18) 1_454 . ? As6 S18 Pb8 88.0(3) 2_556 . ? Sb6 S18 Pb8 88.7(2) 2_556 . ? Sb5 S19 Pb9 5.5(4) 1_554 1_554 ? Sb5 S19 Pb6 91.4(4) 1_554 . ? Pb9 S19 Pb6 96.6(3) 1_554 . ? Sb5 S19 Pb1 108.5(4) 1_554 1_554 ? Pb9 S19 Pb1 106.5(3) 1_554 1_554 ? Pb6 S19 Pb1 91.14(16) . 1_554 ? Sb5 S19 Pb10 89.8(4) 1_554 1_655 ? Pb9 S19 Pb10 91.7(3) 1_554 1_655 ? Pb6 S19 Pb10 88.3(3) . 1_655 ? Pb1 S19 Pb10 161.7(3) 1_554 1_655 ? Sb5 S19 Sb7 87.7(5) 1_554 1_655 ? Pb9 S19 Sb7 89.6(5) 1_554 1_655 ? Pb6 S19 Sb7 88.0(4) . 1_655 ? Pb1 S19 Sb7 163.9(5) 1_554 1_655 ? Pb10 S19 Sb7 2.2(6) 1_655 1_655 ? Sb5 S19 Pb2 106.6(3) 1_554 1_554 ? Pb9 S19 Pb2 101.4(3) 1_554 1_554 ? Pb6 S19 Pb2 161.9(3) . 1_554 ? Pb1 S19 Pb2 85.37(17) 1_554 1_554 ? Pb10 S19 Pb2 89.6(3) 1_655 1_554 ? Sb7 S19 Pb2 90.5(4) 1_655 1_554 ? Sb5 S19 Sb4 144.4(4) 1_554 . ? Pb9 S19 Sb4 148.9(3) 1_554 . ? Pb6 S19 Sb4 67.12(13) . . ? Pb1 S19 Sb4 100.33(17) 1_554 . ? Pb10 S19 Sb4 62.7(2) 1_655 . ? Sb7 S19 Sb4 64.5(4) 1_655 . ? Pb2 S19 Sb4 96.00(18) 1_554 . ? Sb5 S19 As3 61.9(3) 1_554 1_554 ? Pb9 S19 As3 57.0(2) 1_554 1_554 ? Pb6 S19 As3 130.8(2) . 1_554 ? Pb1 S19 As3 63.80(12) 1_554 1_554 ? Pb10 S19 As3 128.5(3) 1_655 1_554 ? Sb7 S19 As3 127.4(4) 1_655 1_554 ? Pb2 S19 As3 62.73(12) 1_554 1_554 ? Sb4 S19 As3 153.2(2) . 1_554 ? Sb5 S19 Sb6 59.5(4) 1_554 1_554 ? Pb9 S19 Sb6 61.7(3) 1_554 1_554 ? Pb6 S19 Sb6 57.0(2) . 1_554 ? Pb1 S19 Sb6 63.5(2) 1_554 1_554 ? Pb10 S19 Sb6 129.6(3) 1_655 1_554 ? Sb7 S19 Sb6 127.9(5) 1_655 1_554 ? Pb2 S19 Sb6 134.7(2) 1_554 1_554 ? Sb4 S19 Sb6 120.2(2) . 1_554 ? As3 S19 Sb6 73.9(2) 1_554 1_554 ? Sb5 S19 As6 60.5(4) 1_554 1_554 ? Pb9 S19 As6 62.4(3) 1_554 1_554 ? Pb6 S19 As6 58.7(3) . 1_554 ? Pb1 S19 As6 61.2(3) 1_554 1_554 ? Pb10 S19 As6 132.1(4) 1_655 1_554 ? Sb7 S19 As6 130.4(5) 1_655 1_554 ? Pb2 S19 As6 132.5(3) 1_554 1_554 ? Sb4 S19 As6 120.9(3) . 1_554 ? As3 S19 As6 72.2(3) 1_554 1_554 ? Sb6 S19 As6 2.5(4) 1_554 1_554 ? As3 S20 Sb4 108.3(2) . 1_455 ? As3 S20 Pb3 106.6(2) . . ? Sb4 S20 Pb3 96.46(18) 1_455 . ? As3 S20 Sb7 79.9(4) . . ? Sb4 S20 Sb7 73.3(4) 1_455 . ? Pb3 S20 Sb7 169.4(4) . . ? As3 S20 Pb10 81.8(3) . . ? Sb4 S20 Pb10 72.1(2) 1_455 . ? Pb3 S20 Pb10 167.8(3) . . ? Sb7 S20 Pb10 2.0(5) . . ? As3 S20 Pb2 129.6(2) . 1_454 ? Sb4 S20 Pb2 113.14(18) 1_455 1_454 ? Pb3 S20 Pb2 96.11(17) . 1_454 ? Sb7 S20 Pb2 85.6(4) . 1_454 ? Pb10 S20 Pb2 84.7(2) . 1_454 ? As3 S20 Pb1 63.07(15) . . ? Sb4 S20 Pb1 60.88(11) 1_455 . ? Pb3 S20 Pb1 73.31(12) . . ? Sb7 S20 Pb1 103.2(4) . . ? Pb10 S20 Pb1 103.8(2) . . ? Pb2 S20 Pb1 166.34(17) 1_454 . ? As3 S20 Pb4 58.71(15) . . ? Sb4 S20 Pb4 141.05(19) 1_455 . ? Pb3 S20 Pb4 59.28(10) . . ? Sb7 S20 Pb4 130.8(3) . . ? Pb10 S20 Pb4 132.6(2) . . ? Pb2 S20 Pb4 100.26(13) 1_454 . ? Pb1 S20 Pb4 81.99(9) . . ? As3 S20 Pb6 41.54(13) . . ? Sb4 S20 Pb6 121.55(19) 1_455 . ? Pb3 S20 Pb6 134.43(16) . . ? Sb7 S20 Pb6 55.8(3) . . ? Pb10 S20 Pb6 57.60(19) . . ? Pb2 S20 Pb6 91.22(12) 1_454 . ? Pb1 S20 Pb6 102.35(10) . . ? Pb4 S20 Pb6 75.15(8) . . ? As3 S20 Pb1 75.99(15) . 1_554 ? Sb4 S20 Pb1 161.7(2) 1_455 1_554 ? Pb3 S20 Pb1 99.33(14) . 1_554 ? Sb7 S20 Pb1 90.3(4) . 1_554 ? Pb10 S20 Pb1 91.3(2) . 1_554 ? Pb2 S20 Pb1 55.96(8) 1_454 1_554 ? Pb1 S20 Pb1 133.16(12) . 1_554 ? Pb4 S20 Pb1 56.73(6) . 1_554 ? Pb6 S20 Pb1 50.01(6) . 1_554 ? As3 S20 As2 150.8(2) . 1_455 ? Sb4 S20 As2 93.20(14) 1_455 1_455 ? Pb3 S20 As2 49.97(10) . 1_455 ? Sb7 S20 As2 126.3(4) . 1_455 ? Pb10 S20 As2 124.6(2) . 1_455 ? Pb2 S20 As2 51.76(9) 1_454 1_455 ? Pb1 S20 As2 114.92(12) . 1_455 ? Pb4 S20 As2 92.14(11) . 1_455 ? Pb6 S20 As2 138.56(11) . 1_455 ? Pb1 S20 As2 89.85(9) 1_554 1_455 ? _diffrn_measured_fraction_theta_max 0.991 _diffrn_reflns_theta_full 23.28 _diffrn_measured_fraction_theta_full 0.991 _refine_diff_density_max 1.492 _refine_diff_density_min -1.955 _refine_diff_density_rms 0.293