data_chovanite _audit_creation_method SHELXL-97 _chemical_name_systematic ; ? ; _chemical_name_mineral 'chovanite' _chemical_compound_source 'Pollone mine, Italy' _chemical_formula_sum 'As4.33 O1.92 Pb53.14 S144 Sb58.53' _chemical_formula_weight 23108.90 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source 'As' 'As' 0.0499 2.0058 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'O' 'O' 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Pb' 'Pb' -3.3944 10.1111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'S' 'S' 0.1246 0.1234 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 'Sb' 'Sb' -0.5866 1.5461 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' _space_group_crystal_system monoclinic _space_group_IT_number 12 _space_group_name_H-M_alt 'C 2/m' _space_group_name_Hall '-C 2y' _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, y, -z' 'x+1/2, y+1/2, z' '-x+1/2, y+1/2, -z' '-x, -y, -z' 'x, -y, z' '-x+1/2, -y+1/2, -z' 'x+1/2, -y+1/2, z' _cell_length_a 48.076(4) _cell_length_b 4.1021(4) _cell_length_c 34.050(3) _cell_angle_alpha 90 _cell_angle_beta 106.266(4) _cell_angle_gamma 90 _cell_volume 6446.3(10) _cell_formula_units_Z 1 _cell_measurement_temperature 293(2) _cell_measurement_reflns_used 8966 _cell_measurement_theta_min 2.781 _cell_measurement_theta_max 33.695 _exptl_crystal_description prismatic _exptl_crystal_colour black _exptl_crystal_size_max 0.290 _exptl_crystal_size_mid 0.030 _exptl_crystal_size_min 0.017 _exptl_crystal_density_meas 'not measured' _exptl_crystal_density_diffrn 5.953 _exptl_crystal_density_method 'not measured' _exptl_crystal_F_000 9804.7 _exptl_absorpt_coefficient_mu 42.293 _exptl_absorpt_correction_type 'multi-scan' _exptl_absorpt_correction_T_min 0.232 _exptl_absorpt_correction_T_max 0.482 _exptl_absorpt_process_details '(SADABS; Sheldrick 1996)' _exptl_special_details ; ? ; _diffrn_ambient_temperature 293(2) _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_type MoK\a _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_monochromator graphite _diffrn_measurement_device_type 'Bruker Smart Breeze' _diffrn_reflns_number 26250 _diffrn_reflns_av_unetI/netI 0.0593 _diffrn_reflns_av_R_equivalents 0.0302 _diffrn_reflns_limit_h_min -72 _diffrn_reflns_limit_h_max 53 _diffrn_reflns_limit_k_min -6 _diffrn_reflns_limit_k_max 3 _diffrn_reflns_limit_l_min -52 _diffrn_reflns_limit_l_max 52 _diffrn_reflns_theta_min 1.214 _diffrn_reflns_theta_max 33.920 _diffrn_reflns_theta_full 25.242 _diffrn_measured_fraction_theta_max 0.894 _diffrn_measured_fraction_theta_full 0.993 _diffrn_reflns_Laue_measured_fraction_max 0.894 _diffrn_reflns_Laue_measured_fraction_full 0.993 _diffrn_reflns_point_group_measured_fraction_max 0.894 _diffrn_reflns_point_group_measured_fraction_full 0.993 _reflns_number_total 13061 _reflns_number_gt 8734 _reflns_threshold_expression 'I > 2\s(I)' _reflns_Friedel_coverage 0.000 _reflns_Friedel_fraction_max . _reflns_Friedel_fraction_full . _reflns_special_details ; Reflections were merged by SHELXL according to the crystal class for the calculation of statistics and refinement. _reflns_Friedel_fraction is defined as the number of unique Friedel pairs measured divided by the number that would be possible theoretically, ignoring centric projections and systematic absences. ; _computing_data_collection 'Apex2 (Bruker AXS Inc., 2004)' _computing_cell_refinement 'Apex2 (Bruker AXS Inc., 2004)' _computing_data_reduction 'Apex2 (Bruker AXS Inc., 2004)' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _refine_special_details ; ? ; _refine_ls_structure_factor_coef Fsqd _refine_ls_matrix_type full _refine_ls_weighting_scheme calc _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0326P)^2^+506.0154P] where P=(Fo^2^+2Fc^2^)/3' _atom_sites_solution_primary ? _atom_sites_solution_secondary ? _atom_sites_solution_hydrogens . _refine_ls_hydrogen_treatment undef _refine_ls_extinction_method none _refine_ls_extinction_coef . _refine_ls_number_reflns 13061 _refine_ls_number_parameters 422 _refine_ls_number_restraints 0 _refine_ls_R_factor_all 0.0934 _refine_ls_R_factor_gt 0.0553 _refine_ls_wR_factor_ref 0.1199 _refine_ls_wR_factor_gt 0.1043 _refine_ls_goodness_of_fit_ref 1.018 _refine_ls_restrained_S_all 1.018 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Pb1 Pb 0.02447(6) 0.5000 0.16820(8) 0.0331(5) Uani 0.482(5) 2 d S T P . . Sb1 Sb 0.01459(9) 0.5000 0.15733(13) 0.0331(5) Uani 0.518(5) 2 d S T P . . Pb2 Pb 0.04371(2) 0.0000 0.38156(2) 0.02794(14) Uani 1 2 d S T P . . Pb3 Pb 0.08635(2) 0.5000 0.09886(3) 0.03947(19) Uani 1 2 d S T P . . Pb4 Pb 0.11283(2) 0.0000 0.31777(2) 0.02477(13) Uani 1 2 d S T P . . Pb5 Pb 0.13469(2) 0.0000 0.45437(2) 0.02769(14) Uani 1 2 d S T P . . Pb6 Pb 0.17026(2) 0.0000 0.12053(2) 0.02765(14) Uani 1 2 d S T P . . Pb7A Pb 0.17519(10) 0.0000 0.24628(8) 0.0334(5) Uani 0.737(12) 2 d S T P . . Pb7B Pb 0.18404(18) 0.0000 0.2515(2) 0.0334(5) Uani 0.263(12) 2 d S T P . . Pb8 Pb 0.28404(2) 0.5000 0.29644(2) 0.03925(19) Uani 1 2 d S T P . . Pb9 Pb 0.32385(2) 0.5000 0.42095(2) 0.02288(13) Uani 1 2 d S T P . . Pb10 Pb 0.34859(2) 0.5000 0.01036(2) 0.02950(15) Uani 1 2 d S T P . . Pb11 Pb 0.36446(2) 0.5000 0.14463(2) 0.03025(15) Uani 1 2 d S T P . . Pb12a Pb 0.36796(5) 0.5000 0.27231(8) 0.0246(5) Uani 0.587(8) 2 d S T P . . Sb12b Sb 0.36358(12) 0.5000 0.28269(17) 0.0246(5) Uani 0.413(8) 2 d S T P . . Pb13 Pb 0.45444(2) 0.5000 0.33214(2) 0.02259(13) Uani 1 2 d S T P . . Sb3 Sb 0.00981(9) 0.0000 0.05694(11) 0.0474(6) Uani 0.771(6) 2 d S T P . . Pb14 Pb 0.00238(15) 0.0000 0.0479(2) 0.0474(6) Uani 0.229(6) 2 d S T P . . Sb4 Sb 0.03224(4) 0.5000 0.26914(5) 0.0510(7) Uani 0.870(18) 2 d S T P . . As4 As 0.03224(4) 0.5000 0.26914(5) 0.0510(7) Uani 0.130(18) 2 d S T P . . Sb5 Sb 0.07531(3) 0.5000 0.50225(4) 0.0415(4) Uani 1 2 d S T P . . Sb6 Sb 0.09154(5) 0.5000 0.20820(7) 0.0257(4) Uani 0.518(3) 2 d S T P . . Sb7 Sb 0.10458(6) 0.5000 0.20146(8) 0.0257(4) Uani 0.482(3) 2 d S T P . . Sb8 Sb 0.18533(4) 0.5000 0.38825(5) 0.0365(6) Uani 0.522(17) 2 d S T P . . As8 As 0.18533(4) 0.5000 0.38825(5) 0.0365(6) Uani 0.478(17) 2 d S T P . . Sb9 Sb 0.22388(3) 0.5000 0.06070(7) 0.0590(5) Uani 1 2 d S T P . . Sb10 Sb 0.24038(4) 0.5000 0.18655(5) 0.0586(7) Uani 0.899(19) 2 d S T P . . As10 As 0.24038(4) 0.5000 0.18655(5) 0.0586(7) Uani 0.101(19) 2 d S T P . . Sb11 Sb 0.24315(4) 0.0000 0.36652(5) 0.0443(4) Uani 1 2 d S T P . . Sb12 Sb 0.28260(4) 0.0000 0.49214(6) 0.0478(6) Uani 0.864(18) 2 d S T P . . As12 As 0.28260(4) 0.0000 0.49214(6) 0.0478(6) Uani 0.136(18) 2 d S T P . . Sb13 Sb 0.29345(3) 0.0000 0.06778(5) 0.0391(3) Uani 1 2 d S T P . . Sb14 Sb 0.30685(3) 0.0000 0.19743(5) 0.0485(7) Uani 0.762(18) 2 d S T P . . As14 As 0.30685(3) 0.0000 0.19743(5) 0.0485(7) Uani 0.238(18) 2 d S T P . . Sb15 Sb 0.39733(3) 0.0000 0.38557(4) 0.0413(3) Uani 1 2 d S T P . . Sb16 Sb 0.4268(3) 0.5000 0.0103(3) 0.0416(9) Uani 0.456(18) 2 d S T P . . Sb61 Sb 0.43117(19) 0.403(4) 0.0071(2) 0.0416(9) Uani 0.272(9) 1 d . . P . . Pb15 Pb 0.44021(8) 0.5000 0.10895(9) 0.0306(6) Uani 0.572(9) 2 d S T P . . Sb17 Sb 0.4419(2) 0.5000 0.1190(2) 0.0306(6) Uani 0.428(9) 2 d S T P . . Sb18 Sb 0.48866(4) 0.0000 0.44285(5) 0.0460(4) Uani 1 2 d S T P . . Sb20 Sb 0.45163(3) 0.0000 0.22253(3) 0.0426(4) Uani 0.585(9) 2 d S T P . . Pb16 Pb 0.45163(3) 0.0000 0.22253(3) 0.0426(4) Uani 0.415(9) 2 d S T P . . S1 S 0.00596(9) 0.0000 0.29358(13) 0.0334(12) Uani 1 2 d S T P . . S2 S 0.03996(9) 0.5000 0.02942(12) 0.0297(10) Uani 1 2 d S T P . . S3 S 0.04611(9) 0.0000 0.12062(12) 0.0221(8) Uani 1 2 d S T P . . S4 S 0.06640(10) 0.0000 0.23727(13) 0.0452(16) Uani 1 2 d S T P . . S5 S 0.06931(8) 0.5000 0.33170(11) 0.0175(7) Uani 1 2 d S T P . . S6 S 0.08537(8) 0.5000 0.43695(11) 0.0187(7) Uani 1 2 d S T P . . S7 S 0.11057(9) 0.0000 0.52841(12) 0.0313(11) Uani 1 2 d S T P . . S8 S 0.12606(10) 0.0000 0.17564(14) 0.0390(13) Uani 1 2 d S T P . . S9 S 0.13696(8) 0.5000 0.38838(11) 0.0181(7) Uani 1 2 d S T P . . S10 S 0.13640(9) 0.5000 0.26722(12) 0.0231(8) Uani 1 2 d S T P . . S11 S 0.17264(9) 0.5000 0.05504(12) 0.0212(8) Uani 1 2 d S T P . . S12 S 0.17758(10) 0.0000 0.34108(14) 0.056(2) Uani 1 2 d S T P . . S13 S 0.18854(10) 0.5000 0.18288(13) 0.0264(9) Uani 1 2 d S T P . . S14 S 0.21360(11) 0.0000 -0.00086(15) 0.0465(16) Uani 1 2 d S T P . . S15 S 0.23035(10) 0.0000 0.12147(14) 0.0473(17) Uani 1 2 d S T P . . S16 S 0.22990(15) 0.5000 0.31393(17) 0.0513(16) Uani 1 2 d S T P . . S17 S 0.24609(12) 0.0000 0.23638(16) 0.073(3) Uani 1 2 d S T P . . S18 S 0.26706(10) 0.5000 0.43247(14) 0.0420(15) Uani 1 2 d S T P . . S19 S 0.29396(8) 0.0000 0.35931(12) 0.0208(8) Uani 1 2 d S T P . . S20 S 0.29916(11) 0.5000 0.54763(14) 0.054(2) Uani 1 2 d S T P . . S21 S 0.30092(11) 0.5000 0.12115(16) 0.0474(16) Uani 1 2 d S T P . . S22 S 0.32493(10) 0.0000 0.27348(15) 0.0481(17) Uani 1 2 d S T P . . S23 S 0.33113(9) 0.0000 0.48473(12) 0.0210(8) Uani 1 2 d S T P . . S24 S 0.34437(9) 0.0000 0.07255(12) 0.0214(8) Uani 1 2 d S T P . . S25 S 0.35652(9) 0.0000 0.19849(13) 0.0243(8) Uani 1 2 d S T P . . S26 S 0.36081(9) 0.5000 0.35605(13) 0.0316(11) Uani 1 2 d S T P . . S27 S 0.39215(9) 0.5000 -0.05715(13) 0.0265(9) Uani 1 2 d S T P . . S28 S 0.40317(12) 0.0000 0.03348(18) 0.074(3) Uani 1 2 d S T P . . S29 S 0.40924(8) 0.0000 0.31967(12) 0.0188(7) Uani 1 2 d S T P . . S30 S 0.41770(9) 0.0000 0.14780(12) 0.0282(10) Uani 1 2 d S T P . . S31 S 0.42030(10) 0.5000 0.23630(15) 0.0359(11) Uani 1 2 d S T P . . S32 S 0.44512(10) 0.5000 0.41190(13) 0.0379(13) Uani 1 2 d S T P . . S33 S 0.48134(9) 0.0000 0.08867(12) 0.0262(9) Uani 1 2 d S T P . . S34 S 0.48531(9) 0.5000 0.17960(13) 0.0276(9) Uani 1 2 d S T P . . S35 S 0.49747(9) 0.0000 0.37594(12) 0.0204(8) Uani 1 2 d S T P . . S36 S 0.52826(11) 0.5000 0.46726(15) 0.0444(15) Uani 1 2 d S T P . . O O 0.3072(7) -0.5000 0.2175(10) 0.050 Uiso 0.48(3) 2 d S U . . . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Pb1 0.0238(12) 0.0465(8) 0.0308(12) 0.000 0.0104(8) 0.000 Sb1 0.0238(12) 0.0465(8) 0.0308(12) 0.000 0.0104(8) 0.000 Pb2 0.0216(3) 0.0203(3) 0.0427(4) 0.000 0.0103(3) 0.000 Pb3 0.0279(4) 0.0409(5) 0.0491(4) 0.000 0.0099(3) 0.000 Pb4 0.0284(3) 0.0204(3) 0.0272(3) 0.000 0.0105(2) 0.000 Pb5 0.0323(3) 0.0195(3) 0.0260(3) 0.000 -0.0006(3) 0.000 Pb6 0.0257(3) 0.0250(3) 0.0305(3) 0.000 0.0049(3) 0.000 Pb7A 0.0332(14) 0.0258(4) 0.0407(7) 0.000 0.0092(9) 0.000 Pb7B 0.0332(14) 0.0258(4) 0.0407(7) 0.000 0.0092(9) 0.000 Pb8 0.0589(5) 0.0270(4) 0.0257(3) 0.000 0.0017(3) 0.000 Pb9 0.0256(3) 0.0203(3) 0.0234(3) 0.000 0.0078(2) 0.000 Pb10 0.0293(3) 0.0278(4) 0.0292(3) 0.000 0.0045(3) 0.000 Pb11 0.0373(4) 0.0241(3) 0.0364(3) 0.000 0.0219(3) 0.000 Pb12a 0.0252(8) 0.0206(5) 0.0246(10) 0.000 0.0014(5) 0.000 Sb12b 0.0252(8) 0.0206(5) 0.0246(10) 0.000 0.0014(5) 0.000 Pb13 0.0222(3) 0.0181(3) 0.0281(3) 0.000 0.0080(2) 0.000 Sb3 0.0276(16) 0.0906(14) 0.0180(14) 0.000 -0.0034(10) 0.000 Pb14 0.0276(16) 0.0906(14) 0.0180(14) 0.000 -0.0034(10) 0.000 Sb4 0.0546(11) 0.0381(10) 0.0392(9) 0.000 -0.0213(7) 0.000 As4 0.0546(11) 0.0381(10) 0.0392(9) 0.000 -0.0213(7) 0.000 Sb5 0.0366(7) 0.0658(11) 0.0275(6) 0.000 0.0179(5) 0.000 Sb6 0.0228(10) 0.0297(9) 0.0239(8) 0.000 0.0054(7) 0.000 Sb7 0.0228(10) 0.0297(9) 0.0239(8) 0.000 0.0054(7) 0.000 Sb8 0.0379(9) 0.0447(11) 0.0338(9) 0.000 0.0215(7) 0.000 As8 0.0379(9) 0.0447(11) 0.0338(9) 0.000 0.0215(7) 0.000 Sb9 0.0240(7) 0.0205(7) 0.1331(17) 0.000 0.0230(8) 0.000 Sb10 0.0726(14) 0.0336(10) 0.0461(10) 0.000 -0.0219(8) 0.000 As10 0.0726(14) 0.0336(10) 0.0461(10) 0.000 -0.0219(8) 0.000 Sb11 0.0672(10) 0.0290(8) 0.0545(8) 0.000 0.0465(8) 0.000 Sb12 0.0581(11) 0.0295(9) 0.0755(13) 0.000 0.0514(9) 0.000 As12 0.0581(11) 0.0295(9) 0.0755(13) 0.000 0.0514(9) 0.000 Sb13 0.0275(6) 0.0281(7) 0.0631(9) 0.000 0.0150(6) 0.000 Sb14 0.0190(7) 0.0874(16) 0.0387(9) 0.000 0.0074(6) 0.000 As14 0.0190(7) 0.0874(16) 0.0387(9) 0.000 0.0074(6) 0.000 Sb15 0.0498(8) 0.0485(9) 0.0323(6) 0.000 0.0229(6) 0.000 Sb16 0.054(3) 0.040(5) 0.0408(12) 0.000 0.0305(15) 0.000 Sb61 0.054(3) 0.040(5) 0.0408(12) 0.000 0.0305(15) 0.000 Pb15 0.0267(7) 0.0419(6) 0.0247(14) 0.000 0.0096(11) 0.000 Sb17 0.0267(7) 0.0419(6) 0.0247(14) 0.000 0.0096(11) 0.000 Sb18 0.0646(10) 0.0451(9) 0.0425(7) 0.000 0.0386(7) 0.000 Sb20 0.0664(9) 0.0350(7) 0.0368(6) 0.000 0.0314(5) 0.000 Pb16 0.0664(9) 0.0350(7) 0.0368(6) 0.000 0.0314(5) 0.000 S1 0.0188(19) 0.062(4) 0.0201(18) 0.000 0.0060(15) 0.000 S2 0.024(2) 0.044(3) 0.0196(17) 0.000 0.0044(15) 0.000 S3 0.0206(18) 0.024(2) 0.0211(17) 0.000 0.0058(14) 0.000 S4 0.021(2) 0.098(5) 0.0192(18) 0.000 0.0083(16) 0.000 S5 0.0147(16) 0.0178(18) 0.0192(16) 0.000 0.0034(13) 0.000 S6 0.0194(17) 0.0211(19) 0.0157(15) 0.000 0.0051(13) 0.000 S7 0.0207(19) 0.056(3) 0.0185(17) 0.000 0.0069(15) 0.000 S8 0.023(2) 0.070(4) 0.0225(19) 0.000 0.0049(16) 0.000 S9 0.0185(17) 0.0190(19) 0.0182(16) 0.000 0.0074(13) 0.000 S10 0.030(2) 0.020(2) 0.0209(17) 0.000 0.0103(15) 0.000 S11 0.0221(18) 0.0175(19) 0.0242(18) 0.000 0.0070(15) 0.000 S12 0.017(2) 0.135(7) 0.0174(19) 0.000 0.0062(16) 0.000 S13 0.039(2) 0.017(2) 0.0273(19) 0.000 0.0157(18) 0.000 S14 0.025(2) 0.085(5) 0.031(2) 0.000 0.0107(19) 0.000 S15 0.021(2) 0.095(5) 0.024(2) 0.000 0.0048(17) 0.000 S16 0.067(4) 0.061(4) 0.039(3) 0.000 0.037(3) 0.000 S17 0.023(2) 0.164(9) 0.027(2) 0.000 0.0006(19) 0.000 S18 0.021(2) 0.081(5) 0.026(2) 0.000 0.0102(17) 0.000 S19 0.0187(17) 0.022(2) 0.0200(16) 0.000 0.0034(14) 0.000 S20 0.024(2) 0.119(6) 0.020(2) 0.000 0.0068(17) 0.000 S21 0.029(2) 0.085(5) 0.031(2) 0.000 0.0121(19) 0.000 S22 0.023(2) 0.095(5) 0.031(2) 0.000 0.0156(19) 0.000 S23 0.0251(19) 0.0143(18) 0.0215(17) 0.000 0.0029(15) 0.000 S24 0.0230(19) 0.020(2) 0.0252(18) 0.000 0.0130(15) 0.000 S25 0.026(2) 0.025(2) 0.0261(19) 0.000 0.0147(16) 0.000 S26 0.023(2) 0.051(3) 0.0238(19) 0.000 0.0116(16) 0.000 S27 0.0207(19) 0.034(3) 0.0247(18) 0.000 0.0069(15) 0.000 S28 0.025(3) 0.160(9) 0.034(3) 0.000 0.003(2) 0.000 S29 0.0200(17) 0.0167(18) 0.0218(17) 0.000 0.0090(14) 0.000 S30 0.023(2) 0.042(3) 0.0197(17) 0.000 0.0063(15) 0.000 S31 0.026(2) 0.052(3) 0.035(2) 0.000 0.0163(19) 0.000 S32 0.023(2) 0.073(4) 0.0200(18) 0.000 0.0089(16) 0.000 S33 0.024(2) 0.033(2) 0.0192(17) 0.000 0.0036(15) 0.000 S34 0.0187(18) 0.041(3) 0.0245(18) 0.000 0.0080(15) 0.000 S35 0.0224(18) 0.0151(18) 0.0237(17) 0.000 0.0065(15) 0.000 S36 0.025(2) 0.080(5) 0.027(2) 0.000 0.0059(18) 0.000 _geom_special_details ; All esds (except the esd in the dihedral angle between two l.s. planes) are estimated using the full covariance matrix. The cell esds are taken into account individually in the estimation of esds in distances, angles and torsion angles; correlations between esds in cell parameters are only used when they are defined by crystal symmetry. An approximate (isotropic) treatment of cell esds is used for estimating esds involving l.s. planes. ; loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 _geom_bond_publ_flag Pb1 Sb1 0.514(3) . ? Pb1 S34 2.883(3) 3_445 ? Pb1 S34 2.883(3) 3_455 ? Pb1 S33 2.913(5) 3_455 ? Pb1 S3 2.976(3) 1_565 ? Pb1 S3 2.976(3) . ? Pb1 Sb6 3.129(4) . ? Pb1 S4 3.338(4) 1_565 ? Pb1 S4 3.338(4) . ? Pb1 Sb4 3.352(3) . ? Pb1 S30 4.984(5) 3_455 ? Pb1 S2 4.985(5) . ? Sb1 S33 2.435(6) 3_455 ? Sb1 S34 2.713(4) 3_445 ? Sb1 S34 2.713(4) 3_455 ? Sb1 S3 3.021(4) 1_565 ? Sb1 S3 3.021(4) . ? Sb1 S4 3.745(5) . ? Sb1 S4 3.745(5) 1_565 ? Sb1 S30 4.578(6) 3_455 ? Sb1 S33 4.770(3) 3_445 ? Sb1 S33 4.770(3) 3_465 ? Sb1 S2 4.841(6) . ? Pb2 S35 2.991(3) 3_445 ? Pb2 S35 2.991(3) 3_455 ? Pb2 S1 3.037(4) . ? Pb2 S6 3.108(3) 1_545 ? Pb2 S6 3.108(3) . ? Pb2 S5 3.127(3) 1_545 ? Pb2 S5 3.127(3) . ? Pb2 S36 3.206(5) 3_445 ? Pb2 S9 4.876(3) 1_545 ? Pb2 S9 4.876(3) . ? Pb2 S1 5.104(3) 1_545 ? Pb2 S1 5.104(3) 1_565 ? Pb3 S2 2.759(4) . ? Pb3 S27 2.849(3) 7 ? Pb3 S27 2.849(3) 7_565 ? Pb3 S3 3.050(3) . ? Pb3 S3 3.050(3) 1_565 ? Pb3 Sb7 3.355(3) . ? Pb3 S8 3.448(4) . ? Pb3 S8 3.448(4) 1_565 ? Pb3 S28 4.672(6) 7 ? Pb3 S11 4.786(4) . ? Pb3 S2 4.943(2) 1_545 ? Pb3 S2 4.943(2) 1_565 ? Pb4 S12 2.989(5) . ? Pb4 S4 3.011(5) . ? Pb4 S5 3.060(3) . ? Pb4 S5 3.060(3) 1_545 ? Pb4 S10 3.089(3) . ? Pb4 S10 3.090(3) 1_545 ? Pb4 S9 3.126(3) 1_545 ? Pb4 S9 3.126(3) . ? Pb4 S1 4.970(4) . ? Pb4 S6 5.042(3) . ? Pb4 S6 5.042(3) 1_545 ? Pb4 S8 5.054(5) . ? Pb5 S23 3.049(3) 7_556 ? Pb5 S23 3.049(3) 7_546 ? Pb5 S7 3.056(4) . ? Pb5 S6 3.065(3) . ? Pb5 S6 3.065(3) 1_545 ? Pb5 S9 3.067(3) 1_545 ? Pb5 S9 3.067(3) . ? Pb5 S20 3.200(5) 7_556 ? Pb5 S12 4.857(5) . ? Pb5 S5 4.917(3) . ? Pb5 S5 4.917(3) 1_545 ? Pb5 S7 5.115(3) 1_565 ? Pb6 S15 2.880(5) . ? Pb6 S13 2.905(3) 1_545 ? Pb6 S13 2.905(3) . ? Pb6 S11 3.055(3) . ? Pb6 S11 3.055(3) 1_545 ? Pb6 S27 3.168(4) 7 ? Pb6 S8 3.205(5) . ? Pb6 S17 4.560(5) . ? Pb6 S15 5.012(3) 1_565 ? Pb6 S15 5.012(3) 1_545 ? Pb6 S14 5.123(5) . ? Pb6 S27 5.183(3) 7_545 ? Pb7A S8 2.860(6) . ? Pb7A S10 2.990(4) 1_545 ? Pb7A S10 2.990(4) . ? Pb7A S13 3.171(4) . ? Pb7A S13 3.171(4) 1_545 ? Pb7A S12 3.197(5) . ? Pb7A S17 3.518(7) . ? Pb7A S16 3.611(7) 1_545 ? Pb7A S16 3.611(7) . ? Pb7A S8 5.001(4) 1_545 ? Pb7A S8 5.001(4) 1_565 ? Pb7A S4 5.153(6) . ? Pb7B S12 3.153(9) . ? Pb7B S13 3.160(6) . ? Pb7B S13 3.160(6) 1_545 ? Pb7B S17 3.165(10) . ? Pb7B S8 3.225(9) . ? Pb7B S10 3.229(7) 1_545 ? Pb7B S10 3.230(7) . ? Pb7B S16 3.312(8) 1_545 ? Pb7B S16 3.312(8) . ? Pb7B S12 5.174(5) 1_565 ? Pb7B S12 5.174(5) 1_545 ? Pb7B S17 5.181(6) 1_565 ? Pb8 S16 2.828(6) . ? Pb8 S19 2.906(3) 1_565 ? Pb8 S19 2.906(3) . ? Pb8 S22 3.089(3) . ? Pb8 S22 3.089(4) 1_565 ? Pb8 S17 3.103(4) . ? Pb8 S17 3.103(4) 1_565 ? Pb8 O 3.18(3) 1_565 ? Pb8 S26 3.680(4) . ? Pb8 S18 4.923(5) . ? Pb8 S16 4.982(3) 1_545 ? Pb8 S16 4.982(3) 1_565 ? Pb9 S18 2.865(5) . ? Pb9 S23 2.936(3) . ? Pb9 S23 2.936(3) 1_565 ? Pb9 S19 2.998(3) . ? Pb9 S19 2.998(3) 1_565 ? Pb9 S7 3.141(4) 7_556 ? Pb9 S26 3.200(4) . ? Pb9 S20 4.784(5) . ? Pb9 S16 4.945(7) . ? Pb9 S18 5.004(3) 1_545 ? Pb9 S18 5.004(3) 1_565 ? Pb9 S7 5.167(3) 7_566 ? Pb10 S14 2.915(5) 7 ? Pb10 S11 2.989(3) 7 ? Pb10 S11 2.989(3) 7_565 ? Pb10 S24 2.995(3) . ? Pb10 S24 2.995(3) 1_565 ? Pb10 S28 3.249(4) . ? Pb10 S28 3.249(4) 1_565 ? Pb10 S27 3.517(4) . ? Pb10 S21 4.932(5) . ? Pb10 S15 5.001(5) 7 ? Pb10 S14 5.033(3) 7_545 ? Pb10 S14 5.033(3) 7_565 ? Pb11 S25 2.847(3) . ? Pb11 S25 2.847(3) 1_565 ? Pb11 S21 2.933(5) . ? Pb11 S24 3.136(3) 1_565 ? Pb11 S24 3.136(3) . ? Pb11 S30 3.258(3) 1_565 ? Pb11 S30 3.258(3) . ? Pb11 S31 3.501(5) . ? Pb11 O 4.19(3) 1_565 ? Pb11 S21 5.043(3) 1_545 ? Pb11 S21 5.043(3) 1_565 ? Pb11 S28 5.093(6) . ? Pb12a S22 2.921(4) 1_565 ? Pb12a S22 2.921(4) . ? Pb12a S26 2.966(5) . ? Pb12a S29 2.992(3) . ? Pb12a S29 2.992(3) 1_565 ? Pb12a O 2.99(3) 1_565 ? Pb12a S31 3.092(5) . ? Pb12a S25 3.171(4) 1_565 ? Pb12a S25 3.171(4) . ? Pb12a S26 5.062(3) 1_565 ? Pb12a S26 5.062(3) 1_545 ? Pb12a O 5.08(2) 1_575 ? Sb12b S26 2.538(7) . ? Sb12b S22 2.726(5) 1_565 ? Sb12b S22 2.726(5) . ? Sb12b O 2.98(3) 1_565 ? Sb12b S29 3.010(5) . ? Sb12b S29 3.010(5) 1_565 ? Sb12b S25 3.464(6) 1_565 ? Sb12b S25 3.464(6) . ? Sb12b S31 3.513(8) . ? Sb12b S26 4.824(4) 1_565 ? Sb12b S26 4.824(4) 1_545 ? Sb12b S32 5.006(7) . ? Pb13 S32 2.874(4) . ? Pb13 S29 2.931(3) 1_565 ? Pb13 S29 2.931(3) . ? Pb13 S35 2.997(3) 1_565 ? Pb13 S35 2.997(3) . ? Pb13 S1 3.111(4) 3 ? Pb13 S31 3.216(5) . ? Pb13 S26 4.794(4) . ? Pb13 S36 4.961(5) . ? Pb13 S32 5.008(3) 1_565 ? Pb13 S32 5.008(3) 1_545 ? Pb13 S1 5.148(3) 3_565 ? Sb3 S3 2.372(5) . ? Sb3 S2 2.819(4) . ? Sb3 S2 2.819(4) 1_545 ? Sb3 S33 2.842(4) 3_445 ? Sb3 S33 2.842(4) 3_455 ? Sb3 Pb14 3.450(7) 5 ? Sb3 S2 3.826(5) 5 ? Sb3 S2 3.826(5) 5_565 ? Sb3 S34 4.646(6) 3_445 ? Sb3 S27 4.711(6) 7 ? Sb3 S3 4.739(3) 1_565 ? Sb3 S3 4.739(3) 1_545 ? Pb14 S3 2.764(7) . ? Pb14 S33 2.819(7) 3_455 ? Pb14 S33 2.819(7) 3_445 ? Pb14 S2 2.916(7) . ? Pb14 S2 2.916(7) 1_545 ? Pb14 Pb14 3.202(15) 5 ? Pb14 Sb61 3.338(11) 3_445 ? Pb14 Sb61 3.338(11) 8_455 ? Pb14 Sb3 3.450(7) 5 ? Pb14 Sb16 3.498(15) 3_445 ? Pb14 S2 3.503(6) 5 ? Pb14 S2 3.503(6) 5_565 ? Sb4 S5 2.363(4) . ? Sb4 S1 2.662(3) . ? Sb4 S1 2.662(3) 1_565 ? Sb4 S4 3.013(4) . ? Sb4 S4 3.013(4) 1_565 ? Sb4 S34 3.839(4) 3_445 ? Sb4 S34 3.839(4) 3_455 ? Sb4 S35 4.408(4) 3_455 ? Sb4 S5 4.7342(19) 1_565 ? Sb4 S5 4.7342(19) 1_545 ? Sb4 S10 5.026(5) . ? Sb5 S6 2.404(4) . ? Sb5 S7 2.651(3) . ? Sb5 S7 2.651(3) 1_565 ? Sb5 S36 3.039(4) 3_445 ? Sb5 S36 3.039(4) 3_455 ? Sb5 S32 3.915(4) 7_566 ? Sb5 S32 3.915(4) 7_556 ? Sb5 S23 4.395(4) 7_556 ? Sb5 S6 4.755(2) 1_545 ? Sb5 S6 4.755(2) 1_565 ? Sb5 S35 4.846(4) 3_455 ? Sb5 S26 5.350(4) 7_566 ? Sb6 Sb7 0.725(3) . ? Sb6 S10 2.502(5) . ? Sb6 S4 2.705(3) 1_565 ? Sb6 S4 2.705(3) . ? Sb6 S8 3.036(4) . ? Sb6 S8 3.036(4) 1_565 ? Sb6 S3 3.771(4) . ? Sb6 S3 3.771(4) 1_565 ? Sb6 S5 4.620(5) . ? Sb6 S10 4.805(3) 1_565 ? Sb6 S10 4.805(2) 1_545 ? Sb7 S10 2.331(5) . ? Sb7 S8 2.560(3) . ? Sb7 S8 2.560(3) 1_565 ? Sb7 S4 3.212(4) 1_565 ? Sb7 S4 3.212(4) . ? Sb7 S3 3.918(4) . ? Sb7 S3 3.918(4) 1_565 ? Sb7 S13 4.257(5) . ? Sb7 S10 4.718(2) 1_565 ? Sb7 S10 4.718(2) 1_545 ? Sb8 S9 2.326(4) . ? Sb8 S12 2.567(3) . ? Sb8 S12 2.567(3) 1_565 ? Sb8 S20 2.936(4) 7_566 ? Sb8 S20 2.936(4) 7_556 ? Sb8 S16 3.746(5) . ? Sb8 S18 3.794(5) . ? Sb8 S10 4.133(4) . ? Sb8 S23 4.610(4) 7_556 ? Sb8 S9 4.716(2) 1_545 ? Sb8 S9 4.716(2) 1_565 ? Sb8 S5 5.367(4) . ? Sb9 S11 2.417(4) . ? Sb9 S15 2.868(4) 1_565 ? Sb9 S15 2.868(4) . ? Sb9 S14 2.875(4) 1_565 ? Sb9 S14 2.875(4) . ? Sb9 S21 3.699(5) . ? Sb9 S14 4.077(5) 7 ? Sb9 S11 4.761(2) 1_545 ? Sb9 S11 4.761(2) 1_565 ? Sb9 S24 4.797(5) 7 ? Sb9 S13 4.915(5) . ? Sb9 S21 5.524(4) 1_565 ? Sb10 S13 2.460(5) . ? Sb10 S17 2.627(4) 1_565 ? Sb10 S17 2.627(4) . ? Sb10 S15 2.958(4) . ? Sb10 S15 2.958(4) 1_565 ? Sb10 O 3.09(3) 1_565 ? Sb10 S21 4.130(6) . ? Sb10 S16 4.505(5) . ? Sb10 S11 4.742(4) . ? Sb10 S22 4.770(5) . ? Sb10 S22 4.770(5) 1_565 ? Sb10 S13 4.783(3) 1_545 ? Sb11 S19 2.523(4) . ? Sb11 S16 2.679(4) . ? Sb11 S16 2.679(4) 1_545 ? Sb11 S18 3.021(4) . ? Sb11 S18 3.021(4) 1_545 ? Sb11 S12 3.026(5) . ? Sb11 S20 4.002(5) 7_556 ? Sb11 S17 4.473(6) . ? Sb11 S19 4.816(2) 1_565 ? Sb11 S19 4.816(2) 1_545 ? Sb11 S23 4.955(4) . ? Sb11 S12 5.097(3) 1_545 ? Sb12 S23 2.416(4) . ? Sb12 S20 2.751(3) 1_545 ? Sb12 S20 2.751(3) . ? Sb12 S18 2.836(3) 1_545 ? Sb12 S18 2.836(3) . ? Sb12 S20 3.782(5) 7_556 ? Sb12 S18 3.965(5) 7_556 ? Sb12 S19 4.705(4) . ? Sb12 S23 4.761(2) 1_565 ? Sb12 S23 4.761(2) 1_545 ? Sb12 S9 4.764(4) 7_556 ? Sb12 S20 5.580(4) 7_546 ? Sb13 S24 2.408(4) . ? Sb13 S21 2.697(3) 1_545 ? Sb13 S21 2.697(3) . ? Sb13 S14 3.014(4) 7_545 ? Sb13 S14 3.014(4) 7 ? Sb13 S14 3.895(5) . ? Sb13 S15 3.956(5) . ? Sb13 S25 4.631(5) . ? Sb13 S24 4.756(2) 1_565 ? Sb13 S24 4.756(2) 1_545 ? Sb13 S11 4.896(4) 7 ? Sb13 O 5.36(3) . ? Sb14 O 2.160(10) . ? Sb14 O 2.160(10) 1_565 ? Sb14 S25 2.378(4) . ? Sb14 S22 2.490(5) . ? Sb14 S21 3.259(4) . ? Sb14 S21 3.259(4) 1_545 ? Sb14 S17 3.530(6) . ? Sb14 S15 3.858(5) . ? Sb14 S25 4.742(2) 1_565 ? Sb14 S25 4.742(2) 1_545 ? Sb14 S22 4.799(3) 1_565 ? Sb14 S22 4.799(3) 1_545 ? Sb15 S29 2.466(4) . ? Sb15 S26 2.704(3) . ? Sb15 S26 2.704(3) 1_545 ? Sb15 S32 3.022(4) 1_545 ? Sb15 S32 3.023(4) . ? Sb15 S7 3.682(4) 7_556 ? Sb15 S7 3.682(4) 7_546 ? Sb15 S22 4.386(5) . ? Sb15 S29 4.786(2) 1_545 ? Sb15 S29 4.786(2) 1_565 ? Sb15 S19 4.796(4) . ? Sb15 S35 4.916(4) . ? Sb16 Sb61 0.477(7) 6_565 ? Sb16 S27 2.429(7) . ? Sb16 S28 2.573(11) 1_565 ? Sb16 S28 2.574(11) . ? Sb16 S2 3.131(13) 7_565 ? Sb16 S2 3.131(13) 7 ? Sb16 Pb15 3.239(10) . ? Sb16 Pb14 3.499(15) 3 ? Sb16 S33 3.780(7) 1_565 ? Sb16 S33 3.780(7) . ? Sb16 S27 4.767(4) 1_545 ? Sb16 S27 4.767(4) 1_565 ? Sb61 Sb61 0.80(3) 6_565 ? Sb61 S28 2.456(16) . ? Sb61 S27 2.482(8) . ? Sb61 S2 2.678(9) 7 ? Sb61 S28 3.049(11) 1_565 ? Sb61 S2 3.230(16) 7_565 ? Sb61 Sb61 3.31(3) 6 ? Sb61 Pb14 3.338(11) 3 ? Sb61 Pb15 3.396(7) . ? Sb61 S33 3.538(10) . ? Sb61 S33 3.972(12) 1_565 ? Sb61 S27 4.442(14) 1_545 ? Pb15 S34 2.751(5) . ? Pb15 S30 2.816(4) 1_565 ? Pb15 S30 2.816(4) . ? Pb15 S33 3.059(4) 1_565 ? Pb15 S33 3.059(4) . ? Pb15 S28 3.379(5) 1_565 ? Pb15 S28 3.379(5) . ? Pb15 Sb61 3.396(7) 6_565 ? Pb15 S31 4.695(6) . ? Pb15 S24 4.876(5) . ? Sb17 S34 2.492(9) . ? Sb17 S30 2.676(7) 1_565 ? Sb17 S30 2.676(7) . ? Sb17 S33 3.157(8) 1_565 ? Sb17 S33 3.157(8) . ? Sb17 S28 3.620(8) 1_565 ? Sb17 S28 3.620(8) . ? Sb17 S31 4.400(9) . ? Sb17 S34 4.800(5) 1_565 ? Sb17 S34 4.800(5) 1_545 ? Sb17 S24 4.952(10) . ? Sb17 S24 4.952(10) 1_565 ? Sb18 S35 2.431(4) . ? Sb18 S36 2.763(3) . ? Sb18 S36 2.763(3) 1_545 ? Sb18 S32 2.909(3) . ? Sb18 S32 2.909(3) 1_545 ? Sb18 S36 3.954(4) 5_666 ? Sb18 S36 3.954(4) 5_656 ? Sb18 S6 4.709(4) 3_545 ? Sb18 S35 4.768(2) 1_545 ? Sb18 S35 4.768(2) 1_565 ? Sb18 S29 4.817(4) . ? Sb18 S32 5.476(4) 5_666 ? Sb20 S30 2.610(4) . ? Sb20 S31 2.663(3) 1_545 ? Sb20 S31 2.663(3) . ? Sb20 S34 3.208(3) . ? Sb20 S34 3.208(3) 1_545 ? Sb20 S1 3.653(4) 3 ? Sb20 S1 3.653(4) 3_545 ? Sb20 S29 4.344(4) . ? Sb20 S25 4.414(4) . ? Sb20 S30 4.862(2) 1_545 ? Sb20 S30 4.862(2) 1_565 ? Sb20 S35 5.069(4) . ? S1 As4 2.662(3) 1_545 ? S1 Sb4 2.662(3) 1_545 ? S1 Pb13 3.111(4) 3_445 ? S1 S35 3.589(5) 3_455 ? S1 S35 3.589(5) 3_445 ? S1 S5 3.599(5) 1_545 ? S1 S5 3.599(5) . ? S1 Pb16 3.653(4) 3_445 ? S1 Sb20 3.653(4) 3_445 ? S2 Sb61 2.678(9) 4 ? S2 Sb61 2.678(9) 7 ? S2 Sb3 2.819(4) 1_565 ? S2 Pb14 2.915(7) 1_565 ? S2 Sb16 3.130(13) 7_565 ? S2 Sb16 3.130(13) 7 ? S2 Sb61 3.230(16) 7_565 ? S2 Sb61 3.230(16) 4_545 ? S2 Pb14 3.503(6) 5 ? S3 Pb1 2.976(3) 1_545 ? S3 Sb1 3.021(4) 1_545 ? S3 Pb3 3.050(3) 1_545 ? S3 S33 3.632(5) 3_445 ? S3 S33 3.632(5) 3_455 ? S3 S2 3.664(5) 1_545 ? S4 Sb6 2.705(3) 1_545 ? S4 As4 3.013(4) 1_545 ? S4 Sb4 3.013(4) 1_545 ? S4 Sb7 3.212(4) 1_545 ? S4 Pb1 3.338(4) 1_545 ? S5 Pb4 3.060(3) 1_565 ? S5 Pb2 3.126(3) 1_565 ? S5 S9 3.285(5) . ? S5 S6 3.448(5) . ? S5 S1 3.599(5) 1_565 ? S5 S4 3.783(5) 1_565 ? S6 Pb5 3.065(3) 1_565 ? S6 Pb2 3.108(3) 1_565 ? S6 S9 3.344(5) . ? S6 S7 3.641(4) 1_565 ? S6 S7 3.641(4) . ? S6 S36 3.795(5) 3_445 ? S6 S36 3.795(5) 3_455 ? S6 S6 4.1021(4) 1_565 ? S7 Sb5 2.651(3) 1_545 ? S7 Pb9 3.142(4) 7_556 ? S7 S23 3.601(5) 7_556 ? S7 S23 3.601(5) 7_546 ? S7 S6 3.641(4) 1_545 ? S7 Sb15 3.682(4) 7_556 ? S7 Sb15 3.682(4) 7_546 ? S7 S26 3.787(6) 7_556 ? S7 S32 3.788(6) 7_556 ? S8 Sb7 2.560(3) 1_545 ? S8 Sb6 3.036(4) 1_545 ? S8 Pb3 3.448(4) 1_545 ? S8 S13 3.588(5) 1_545 ? S8 S13 3.588(5) . ? S8 S10 3.648(5) 1_545 ? S9 Pb5 3.067(3) 1_565 ? S9 Pb4 3.126(3) 1_565 ? S9 S12 3.518(5) 1_565 ? S9 S12 3.518(5) . ? S9 S20 3.826(5) 7_566 ? S9 S20 3.826(5) 7_556 ? S10 Pb7A 2.990(4) 1_565 ? S10 Pb4 3.090(3) 1_565 ? S10 Pb7B 3.230(7) 1_565 ? S10 S12 3.415(5) 1_565 ? S10 S12 3.415(5) . ? S10 S8 3.648(5) 1_565 ? S11 Pb10 2.989(3) 7 ? S11 Pb10 2.989(3) 7_565 ? S11 Pb6 3.055(3) 1_565 ? S11 S15 3.675(5) 1_565 ? S11 S15 3.675(5) . ? S11 S14 3.716(5) 1_565 ? S11 S14 3.716(5) . ? S11 S27 3.747(5) 7 ? S11 S27 3.747(5) 7_565 ? S11 S28 4.026(7) 7 ? S12 As8 2.567(3) 1_545 ? S12 Sb8 2.567(3) 1_545 ? S12 S10 3.415(5) 1_545 ? S12 S9 3.518(5) 1_545 ? S13 Pb6 2.905(3) 1_565 ? S13 Pb7B 3.160(6) 1_565 ? S13 Pb7A 3.171(4) 1_565 ? S13 S17 3.515(6) 1_565 ? S13 S17 3.515(6) . ? S13 S8 3.588(5) 1_565 ? S14 Sb9 2.875(4) 1_545 ? S14 Pb10 2.915(5) 7 ? S14 Sb13 3.014(4) 7_545 ? S14 Sb13 3.014(4) 7 ? S14 S11 3.716(5) 1_545 ? S14 S24 3.758(5) 7_545 ? S14 S24 3.758(5) 7 ? S14 S21 3.958(7) 7 ? S14 S15 4.015(7) . ? S15 Sb9 2.868(4) 1_545 ? S15 As10 2.958(4) 1_545 ? S15 Sb10 2.958(4) 1_545 ? S15 S11 3.675(5) 1_545 ? S15 S17 3.771(7) . ? S16 Sb11 2.679(4) 1_565 ? S16 Pb7B 3.312(8) 1_565 ? S16 S12 3.562(6) 1_565 ? S16 S17 3.597(6) 1_565 ? S16 S17 3.597(6) . ? S16 Pb7A 3.611(7) 1_565 ? S16 S19 3.662(7) 1_565 ? S17 As10 2.627(4) 1_545 ? S17 Sb10 2.627(4) 1_545 ? S17 Pb8 3.103(4) 1_545 ? S17 S13 3.515(6) 1_545 ? S18 As12 2.836(3) 1_565 ? S18 Sb12 2.836(3) 1_565 ? S18 Sb11 3.021(4) 1_565 ? S18 S23 3.713(5) 1_565 ? S18 S23 3.713(5) . ? S18 S19 3.727(5) 1_565 ? S18 S19 3.727(5) . ? S18 S20 3.791(7) . ? S19 Pb8 2.906(3) 1_545 ? S19 Pb9 2.998(3) 1_545 ? S19 S22 3.633(6) . ? S19 S16 3.662(7) 1_545 ? S19 S18 3.727(5) 1_545 ? S19 S26 3.840(5) 1_545 ? S19 S26 3.840(5) . ? S20 As12 2.751(3) 1_565 ? S20 Sb12 2.751(3) 1_565 ? S20 As8 2.936(4) 7_566 ? S20 Sb8 2.936(4) 7_566 ? S20 As8 2.936(4) 7_556 ? S20 Sb8 2.936(4) 7_556 ? S20 Pb5 3.200(5) 7_556 ? S20 S23 3.605(5) 1_565 ? S20 S23 3.605(5) . ? S20 S12 3.638(6) 7_556 ? S21 Sb13 2.697(3) 1_565 ? S21 O 3.21(3) 1_565 ? S21 As14 3.259(4) 1_565 ? S21 Sb14 3.259(4) 1_565 ? S21 S24 3.639(5) 1_565 ? S21 S24 3.639(5) . ? S21 S25 3.787(6) 1_565 ? S22 Sb12b 2.726(5) 1_545 ? S22 O 2.77(2) 1_565 ? S22 O 2.77(2) . ? S22 Pb12a 2.921(4) 1_545 ? S22 Pb8 3.089(3) 1_545 ? S22 S25 3.316(6) . ? S22 S26 3.517(5) 1_545 ? S23 Pb9 2.936(3) 1_545 ? S23 Pb5 3.049(3) 7_556 ? S23 Pb5 3.049(3) 7_546 ? S23 S7 3.601(5) 7_556 ? S23 S7 3.601(5) 7_546 ? S23 S20 3.605(5) 1_545 ? S23 S18 3.713(5) 1_545 ? S24 Pb10 2.995(3) 1_545 ? S24 Pb11 3.136(3) 1_545 ? S24 S28 3.445(7) . ? S24 S21 3.639(5) 1_545 ? S24 S30 3.733(6) . ? S24 S14 3.758(5) 7_545 ? S24 S14 3.758(5) 7 ? S24 S24 4.1021(4) 1_565 ? S25 Pb11 2.847(3) 1_545 ? S25 Pb12a 3.171(4) 1_545 ? S25 O 3.33(3) 1_565 ? S25 O 3.33(3) . ? S25 Sb12b 3.464(6) 1_545 ? S25 S31 3.613(5) 1_545 ? S26 Sb15 2.704(3) 1_565 ? S26 S22 3.517(5) 1_565 ? S26 S29 3.575(5) . ? S26 S29 3.575(5) 1_565 ? S26 S7 3.787(6) 7_556 ? S27 Sb61 2.482(8) 6_565 ? S27 Pb3 2.849(3) 7 ? S27 Pb3 2.849(3) 7_565 ? S27 Pb6 3.168(4) 7 ? S27 S28 3.619(6) 1_565 ? S27 S28 3.619(6) . ? S27 S2 3.745(5) 7_565 ? S27 S2 3.745(5) 7 ? S27 S11 3.747(5) 7 ? S28 Sb61 2.456(16) 6 ? S28 Sb16 2.574(11) 1_545 ? S28 Sb61 3.049(11) 6_565 ? S28 Sb61 3.049(11) 1_545 ? S28 Pb10 3.249(4) 1_545 ? S28 Pb15 3.379(5) 1_545 ? S28 S27 3.619(6) 1_545 ? S29 Pb13 2.931(3) 1_545 ? S29 Pb12a 2.992(3) 1_545 ? S29 Sb12b 3.010(5) 1_545 ? S29 S26 3.575(5) 1_545 ? S29 S31 3.660(5) . ? S29 S31 3.660(5) 1_545 ? S29 S32 3.743(5) 1_545 ? S30 Sb17 2.676(7) 1_545 ? S30 Pb15 2.816(4) 1_545 ? S30 Pb11 3.258(3) 1_545 ? S30 S31 3.618(5) 1_545 ? S30 S31 3.618(5) . ? S30 S34 3.738(5) . ? S31 Pb16 2.663(3) 1_565 ? S31 Sb20 2.663(3) 1_565 ? S31 S25 3.613(5) 1_565 ? S31 S30 3.618(5) 1_565 ? S32 Sb18 2.909(3) 1_565 ? S32 Sb15 3.023(4) 1_565 ? S32 S35 3.710(5) 1_565 ? S32 S35 3.710(5) . ? S32 S29 3.743(5) 1_565 ? S32 S7 3.788(6) 7_556 ? S32 S36 3.912(7) . ? S32 Sb5 3.915(4) 7_566 ? S33 Sb1 2.434(6) 3_545 ? S33 Pb14 2.819(7) 3_545 ? S33 Pb14 2.819(7) 3 ? S33 Sb3 2.842(4) 3 ? S33 Sb3 2.842(4) 3_545 ? S33 Pb1 2.913(5) 3_545 ? S33 Pb15 3.059(4) 1_545 ? S33 Sb17 3.157(8) 1_545 ? S33 Sb61 3.538(10) 6 ? S34 Sb1 2.713(4) 3 ? S34 Sb1 2.713(4) 3_545 ? S34 Pb1 2.883(3) 3 ? S34 Pb1 2.883(3) 3_545 ? S34 Pb16 3.208(3) 1_565 ? S34 Sb20 3.208(3) 1_565 ? S34 S33 3.674(5) 1_565 ? S35 Pb2 2.991(3) 3 ? S35 Pb2 2.991(3) 3_545 ? S35 Pb13 2.997(3) 1_545 ? S35 S1 3.589(5) 3_545 ? S35 S1 3.589(5) 3 ? S35 S36 3.673(5) . ? S35 S36 3.673(5) 1_545 ? S35 S32 3.710(5) 1_545 ? S35 S35 4.1021(4) 1_565 ? S36 Sb18 2.763(3) 1_565 ? S36 Sb5 3.039(4) 3 ? S36 Sb5 3.039(4) 3_545 ? S36 Pb2 3.206(5) 3 ? S36 S35 3.672(5) 1_565 ? S36 S6 3.795(5) 3 ? S36 S6 3.795(5) 3_545 ? S36 S7 3.922(6) 3 ? S36 S32 3.952(6) 5_666 ? O As14 2.160(10) 1_545 ? O Sb14 2.160(10) 1_545 ? O S22 2.77(2) 1_545 ? O Sb12b 2.98(3) 1_545 ? O Pb12a 2.99(3) 1_545 ? O As10 3.09(3) 1_545 ? O Sb10 3.09(3) 1_545 ? O Pb8 3.18(3) 1_545 ? O S21 3.21(3) 1_545 ? loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 _geom_angle_publ_flag Sb1 Pb1 S34 65.8(4) . 3_445 ? Sb1 Pb1 S34 65.8(4) . 3_455 ? S34 Pb1 S34 90.71(13) 3_445 3_455 ? Sb1 Pb1 S33 19.4(6) . 3_455 ? S34 Pb1 S33 78.67(12) 3_445 3_455 ? S34 Pb1 S33 78.67(12) 3_455 3_455 ? Sb1 Pb1 S3 90.1(5) . 1_565 ? S34 Pb1 S3 154.77(15) 3_445 1_565 ? S34 Pb1 S3 85.64(9) 3_455 1_565 ? S33 Pb1 S3 76.13(11) 3_455 1_565 ? Sb1 Pb1 S3 90.1(5) . . ? S34 Pb1 S3 85.64(9) 3_445 . ? S34 Pb1 S3 154.77(15) 3_455 . ? S33 Pb1 S3 76.13(11) 3_455 . ? S3 Pb1 S3 87.13(12) 1_565 . ? Sb1 Pb1 Sb6 161.0(7) . . ? S34 Pb1 Sb6 125.00(10) 3_445 . ? S34 Pb1 Sb6 125.00(10) 3_455 . ? S33 Pb1 Sb6 141.53(12) 3_455 . ? S3 Pb1 Sb6 76.25(10) 1_565 . ? S3 Pb1 Sb6 76.25(10) . . ? Sb1 Pb1 S4 139.6(2) . 1_565 ? S34 Pb1 S4 129.08(13) 3_445 1_565 ? S34 Pb1 S4 75.89(10) 3_455 1_565 ? S33 Pb1 S4 141.90(6) 3_455 1_565 ? S3 Pb1 S4 74.10(10) 1_565 1_565 ? S3 Pb1 S4 124.95(13) . 1_565 ? Sb6 Pb1 S4 49.32(8) . 1_565 ? Sb1 Pb1 S4 139.6(2) . . ? S34 Pb1 S4 75.89(10) 3_445 . ? S34 Pb1 S4 129.08(13) 3_455 . ? S33 Pb1 S4 141.90(6) 3_455 . ? S3 Pb1 S4 124.95(13) 1_565 . ? S3 Pb1 S4 74.10(10) . . ? Sb6 Pb1 S4 49.32(8) . . ? S4 Pb1 S4 75.81(11) 1_565 . ? Sb1 Pb1 Sb4 123.6(7) . . ? S34 Pb1 Sb4 75.60(10) 3_445 . ? S34 Pb1 Sb4 75.60(10) 3_455 . ? S33 Pb1 Sb4 143.04(12) 3_455 . ? S3 Pb1 Sb4 127.06(9) 1_565 . ? S3 Pb1 Sb4 127.06(9) . . ? Sb6 Pb1 Sb4 75.43(8) . . ? S4 Pb1 Sb4 53.54(8) 1_565 . ? S4 Pb1 Sb4 53.53(8) . . ? Sb1 Pb1 S30 36.0(6) . 3_455 ? S34 Pb1 S30 48.15(7) 3_445 3_455 ? S34 Pb1 S30 48.15(7) 3_455 3_455 ? S33 Pb1 S30 55.47(11) 3_455 3_455 ? S3 Pb1 S30 115.31(10) 1_565 3_455 ? S3 Pb1 S30 115.31(10) . 3_455 ? Sb6 Pb1 S30 162.99(9) . 3_455 ? S4 Pb1 S30 119.56(9) 1_565 3_455 ? S4 Pb1 S30 119.55(9) . 3_455 ? Sb4 Pb1 S30 87.57(7) . 3_455 ? Sb1 Pb1 S2 70.8(6) . . ? S34 Pb1 S2 113.84(10) 3_445 . ? S34 Pb1 S2 113.84(10) 3_455 . ? S33 Pb1 S2 51.35(10) 3_455 . ? S3 Pb1 S2 46.87(7) 1_565 . ? S3 Pb1 S2 46.87(7) . . ? Sb6 Pb1 S2 90.19(8) . . ? S4 Pb1 S2 116.53(9) 1_565 . ? S4 Pb1 S2 116.54(9) . . ? Sb4 Pb1 S2 165.61(10) . . ? S30 Pb1 S2 106.82(9) 3_455 . ? Pb1 Sb1 S33 156.5(7) . 3_455 ? Pb1 Sb1 S34 104.2(4) . 3_445 ? S33 Sb1 S34 90.91(16) 3_455 3_445 ? Pb1 Sb1 S34 104.2(4) . 3_455 ? S33 Sb1 S34 90.91(16) 3_455 3_455 ? S34 Sb1 S34 98.23(18) 3_445 3_455 ? Pb1 Sb1 S3 80.1(5) . 1_565 ? S33 Sb1 S3 82.72(15) 3_455 1_565 ? S34 Sb1 S3 171.31(18) 3_445 1_565 ? S34 Sb1 S3 87.82(9) 3_455 1_565 ? Pb1 Sb1 S3 80.1(5) . . ? S33 Sb1 S3 82.72(15) 3_455 . ? S34 Sb1 S3 87.82(9) 3_445 . ? S34 Sb1 S3 171.31(18) 3_455 . ? S3 Sb1 S3 85.52(15) 1_565 . ? Pb1 Sb1 S4 35.3(2) . . ? S33 Sb1 S4 145.30(7) 3_455 . ? S34 Sb1 S4 70.99(12) 3_445 . ? S34 Sb1 S4 120.16(17) 3_455 . ? S3 Sb1 S4 111.35(15) 1_565 . ? S3 Sb1 S4 67.68(11) . . ? Pb1 Sb1 S4 35.3(2) . 1_565 ? S33 Sb1 S4 145.30(7) 3_455 1_565 ? S34 Sb1 S4 120.16(17) 3_445 1_565 ? S34 Sb1 S4 70.99(12) 3_455 1_565 ? S3 Sb1 S4 67.68(11) 1_565 1_565 ? S3 Sb1 S4 111.35(15) . 1_565 ? S4 Sb1 S4 66.43(10) . 1_565 ? Pb1 Sb1 S30 140.2(7) . 3_455 ? S33 Sb1 S30 63.29(14) 3_455 3_455 ? S34 Sb1 S30 54.73(10) 3_445 3_455 ? S34 Sb1 S30 54.73(10) 3_455 3_455 ? S3 Sb1 S30 126.08(11) 1_565 3_455 ? S3 Sb1 S30 126.09(11) . 3_455 ? S4 Sb1 S30 120.53(11) . 3_455 ? S4 Sb1 S30 120.53(11) 1_565 3_455 ? Pb1 Sb1 S33 117.92(17) . 3_445 ? S33 Sb1 S33 59.31(6) 3_455 3_445 ? S34 Sb1 S33 50.06(10) 3_445 3_445 ? S34 Sb1 S33 131.16(15) 3_455 3_445 ? S3 Sb1 S33 121.28(13) 1_565 3_445 ? S3 Sb1 S33 49.57(9) . 3_445 ? S4 Sb1 S33 87.05(6) . 3_445 ? S4 Sb1 S33 152.96(10) 1_565 3_445 ? S30 Sb1 S33 76.74(8) 3_455 3_445 ? Pb1 Sb1 S33 117.92(17) . 3_465 ? S33 Sb1 S33 59.31(6) 3_455 3_465 ? S34 Sb1 S33 131.16(15) 3_445 3_465 ? S34 Sb1 S33 50.06(10) 3_455 3_465 ? S3 Sb1 S33 49.56(9) 1_565 3_465 ? S3 Sb1 S33 121.27(13) . 3_465 ? S4 Sb1 S33 152.96(10) . 3_465 ? S4 Sb1 S33 87.05(6) 1_565 3_465 ? S30 Sb1 S33 76.74(8) 3_455 3_465 ? S33 Sb1 S33 118.62(12) 3_445 3_465 ? Pb1 Sb1 S2 103.5(7) . . ? S33 Sb1 S2 53.07(14) 3_455 . ? S34 Sb1 S2 122.18(12) 3_445 . ? S34 Sb1 S2 122.18(12) 3_455 . ? S3 Sb1 S2 49.14(9) 1_565 . ? S3 Sb1 S2 49.14(9) . . ? S4 Sb1 S2 111.72(11) . . ? S4 Sb1 S2 111.72(11) 1_565 . ? S30 Sb1 S2 116.36(11) 3_455 . ? S33 Sb1 S2 72.14(7) 3_445 . ? S33 Sb1 S2 72.14(7) 3_465 . ? S35 Pb2 S35 86.58(11) 3_445 3_455 ? S35 Pb2 S1 73.08(9) 3_445 . ? S35 Pb2 S1 73.08(9) 3_455 . ? S35 Pb2 S6 85.83(8) 3_445 1_545 ? S35 Pb2 S6 146.35(10) 3_455 1_545 ? S1 Pb2 S6 134.75(6) . 1_545 ? S35 Pb2 S6 146.35(10) 3_445 . ? S35 Pb2 S6 85.83(8) 3_455 . ? S1 Pb2 S6 134.75(6) . . ? S6 Pb2 S6 82.59(9) 1_545 . ? S35 Pb2 S5 85.07(8) 3_445 1_545 ? S35 Pb2 S5 144.45(10) 3_455 1_545 ? S1 Pb2 S5 71.43(9) . 1_545 ? S6 Pb2 S5 67.16(9) 1_545 1_545 ? S6 Pb2 S5 118.53(9) . 1_545 ? S35 Pb2 S5 144.46(10) 3_445 . ? S35 Pb2 S5 85.07(8) 3_455 . ? S1 Pb2 S5 71.43(9) . . ? S6 Pb2 S5 118.53(9) 1_545 . ? S6 Pb2 S5 67.16(9) . . ? S5 Pb2 S5 81.99(9) 1_545 . ? S35 Pb2 S36 72.59(10) 3_445 3_445 ? S35 Pb2 S36 72.59(10) 3_455 3_445 ? S1 Pb2 S36 132.15(12) . 3_445 ? S6 Pb2 S36 73.86(9) 1_545 3_445 ? S6 Pb2 S36 73.86(9) . 3_445 ? S5 Pb2 S36 136.14(6) 1_545 3_445 ? S5 Pb2 S36 136.14(6) . 3_445 ? S35 Pb2 S9 111.81(6) 3_445 1_545 ? S35 Pb2 S9 161.51(6) 3_455 1_545 ? S1 Pb2 S9 109.53(9) . 1_545 ? S6 Pb2 S9 42.76(8) 1_545 1_545 ? S6 Pb2 S9 79.69(7) . 1_545 ? S5 Pb2 S9 41.70(7) 1_545 1_545 ? S5 Pb2 S9 78.77(6) . 1_545 ? S36 Pb2 S9 113.63(9) 3_445 1_545 ? S35 Pb2 S9 161.51(6) 3_445 . ? S35 Pb2 S9 111.81(6) 3_455 . ? S1 Pb2 S9 109.53(9) . . ? S6 Pb2 S9 79.69(7) 1_545 . ? S6 Pb2 S9 42.76(8) . . ? S5 Pb2 S9 78.77(6) 1_545 . ? S5 Pb2 S9 41.70(7) . . ? S36 Pb2 S9 113.63(9) 3_445 . ? S9 Pb2 S9 49.75(4) 1_545 . ? S35 Pb2 S1 43.59(8) 3_445 1_545 ? S35 Pb2 S1 112.20(8) 3_455 1_545 ? S1 Pb2 S1 53.49(4) . 1_545 ? S6 Pb2 S1 83.60(6) 1_545 1_545 ? S6 Pb2 S1 161.68(8) . 1_545 ? S5 Pb2 S1 44.22(8) 1_545 1_545 ? S5 Pb2 S1 109.74(7) . 1_545 ? S36 Pb2 S1 113.53(6) 3_445 1_545 ? S9 Pb2 S1 82.00(5) 1_545 1_545 ? S9 Pb2 S1 122.48(6) . 1_545 ? S35 Pb2 S1 112.20(8) 3_445 1_565 ? S35 Pb2 S1 43.59(8) 3_455 1_565 ? S1 Pb2 S1 53.49(4) . 1_565 ? S6 Pb2 S1 161.69(8) 1_545 1_565 ? S6 Pb2 S1 83.60(6) . 1_565 ? S5 Pb2 S1 109.74(7) 1_545 1_565 ? S5 Pb2 S1 44.22(8) . 1_565 ? S36 Pb2 S1 113.53(6) 3_445 1_565 ? S9 Pb2 S1 122.48(6) 1_545 1_565 ? S9 Pb2 S1 82.00(5) . 1_565 ? S1 Pb2 S1 106.97(8) 1_545 1_565 ? S2 Pb3 S27 83.78(11) . 7 ? S2 Pb3 S27 83.78(11) . 7_565 ? S27 Pb3 S27 92.11(13) 7 7_565 ? S2 Pb3 S3 78.03(10) . . ? S27 Pb3 S3 88.87(8) 7 . ? S27 Pb3 S3 161.58(11) 7_565 . ? S2 Pb3 S3 78.03(10) . 1_565 ? S27 Pb3 S3 161.57(11) 7 1_565 ? S27 Pb3 S3 88.88(8) 7_565 1_565 ? S3 Pb3 S3 84.52(11) . 1_565 ? S2 Pb3 Sb7 143.62(11) . . ? S27 Pb3 Sb7 119.59(8) 7 . ? S27 Pb3 Sb7 119.59(8) 7_565 . ? S3 Pb3 Sb7 75.26(8) . . ? S3 Pb3 Sb7 75.26(8) 1_565 . ? S2 Pb3 S8 142.45(5) . . ? S27 Pb3 S8 75.45(10) 7 . ? S27 Pb3 S8 127.25(11) 7_565 . ? S3 Pb3 S8 70.73(10) . . ? S3 Pb3 S8 118.03(10) 1_565 . ? Sb7 Pb3 S8 44.18(7) . . ? S2 Pb3 S8 142.45(5) . 1_565 ? S27 Pb3 S8 127.24(11) 7 1_565 ? S27 Pb3 S8 75.44(10) 7_565 1_565 ? S3 Pb3 S8 118.03(10) . 1_565 ? S3 Pb3 S8 70.73(10) 1_565 1_565 ? Sb7 Pb3 S8 44.18(7) . 1_565 ? S8 Pb3 S8 73.00(9) . 1_565 ? S2 Pb3 S28 56.84(11) . 7 ? S27 Pb3 S28 50.72(7) 7 7 ? S27 Pb3 S28 50.72(7) 7_565 7 ? S3 Pb3 S28 118.77(8) . 7 ? S3 Pb3 S28 118.78(8) 1_565 7 ? Sb7 Pb3 S28 159.53(9) . 7 ? S8 Pb3 S28 123.02(9) . 7 ? S8 Pb3 S28 123.02(9) 1_565 7 ? S2 Pb3 S11 107.22(11) . . ? S27 Pb3 S11 51.49(7) 7 . ? S27 Pb3 S11 51.49(7) 7_565 . ? S3 Pb3 S11 137.73(5) . . ? S3 Pb3 S11 137.73(5) 1_565 . ? Sb7 Pb3 S11 109.16(7) . . ? S8 Pb3 S11 83.82(9) . . ? S8 Pb3 S11 83.81(9) 1_565 . ? S28 Pb3 S11 50.37(8) 7 . ? S2 Pb3 S2 56.08(4) . 1_545 ? S27 Pb3 S2 48.86(9) 7 1_545 ? S27 Pb3 S2 122.48(9) 7_565 1_545 ? S3 Pb3 S2 47.64(8) . 1_545 ? S3 Pb3 S2 116.25(8) 1_565 1_545 ? Sb7 Pb3 S2 116.70(5) . 1_545 ? S8 Pb3 S2 87.07(6) . 1_545 ? S8 Pb3 S2 159.39(6) 1_565 1_545 ? S28 Pb3 S2 72.23(6) 7 1_545 ? S11 Pb3 S2 99.51(6) . 1_545 ? S2 Pb3 S2 56.08(4) . 1_565 ? S27 Pb3 S2 122.48(9) 7 1_565 ? S27 Pb3 S2 48.86(9) 7_565 1_565 ? S3 Pb3 S2 116.25(8) . 1_565 ? S3 Pb3 S2 47.64(8) 1_565 1_565 ? Sb7 Pb3 S2 116.70(5) . 1_565 ? S8 Pb3 S2 159.39(6) . 1_565 ? S8 Pb3 S2 87.07(6) 1_565 1_565 ? S28 Pb3 S2 72.23(6) 7 1_565 ? S11 Pb3 S2 99.51(6) . 1_565 ? S2 Pb3 S2 112.16(8) 1_545 1_565 ? S12 Pb4 S4 133.86(12) . . ? S12 Pb4 S5 131.70(7) . . ? S4 Pb4 S5 77.08(9) . . ? S12 Pb4 S5 131.70(7) . 1_545 ? S4 Pb4 S5 77.08(9) . 1_545 ? S5 Pb4 S5 84.16(10) . 1_545 ? S12 Pb4 S10 68.33(10) . . ? S4 Pb4 S10 77.70(10) . . ? S5 Pb4 S10 90.84(8) . . ? S5 Pb4 S10 154.76(10) 1_545 . ? S12 Pb4 S10 68.33(10) . 1_545 ? S4 Pb4 S10 77.70(10) . 1_545 ? S5 Pb4 S10 154.77(10) . 1_545 ? S5 Pb4 S10 90.85(8) 1_545 1_545 ? S10 Pb4 S10 83.19(10) . 1_545 ? S12 Pb4 S9 70.20(9) . 1_545 ? S4 Pb4 S9 136.13(6) . 1_545 ? S5 Pb4 S9 116.30(9) . 1_545 ? S5 Pb4 S9 64.13(9) 1_545 1_545 ? S10 Pb4 S9 138.51(10) . 1_545 ? S10 Pb4 S9 82.99(8) 1_545 1_545 ? S12 Pb4 S9 70.20(9) . . ? S4 Pb4 S9 136.13(6) . . ? S5 Pb4 S9 64.13(9) . . ? S5 Pb4 S9 116.30(9) 1_545 . ? S10 Pb4 S9 82.99(8) . . ? S10 Pb4 S9 138.51(10) 1_545 . ? S9 Pb4 S9 82.01(9) 1_545 . ? S12 Pb4 S1 174.39(10) . . ? S4 Pb4 S1 51.75(10) . . ? S5 Pb4 S1 46.04(5) . . ? S5 Pb4 S1 46.04(5) 1_545 . ? S10 Pb4 S1 115.53(8) . . ? S10 Pb4 S1 115.53(8) 1_545 . ? S9 Pb4 S1 105.73(8) 1_545 . ? S9 Pb4 S1 105.74(8) . . ? S12 Pb4 S6 105.92(9) . . ? S4 Pb4 S6 115.98(9) . . ? S5 Pb4 S6 42.10(8) . . ? S5 Pb4 S6 78.66(7) 1_545 . ? S10 Pb4 S6 113.45(5) . . ? S10 Pb4 S6 159.73(6) 1_545 . ? S9 Pb4 S6 76.84(6) 1_545 . ? S9 Pb4 S6 40.40(8) . . ? S1 Pb4 S6 69.01(6) . . ? S12 Pb4 S6 105.92(9) . 1_545 ? S4 Pb4 S6 115.98(9) . 1_545 ? S5 Pb4 S6 78.66(7) . 1_545 ? S5 Pb4 S6 42.10(8) 1_545 1_545 ? S10 Pb4 S6 159.73(6) . 1_545 ? S10 Pb4 S6 113.45(5) 1_545 1_545 ? S9 Pb4 S6 40.40(8) 1_545 1_545 ? S9 Pb4 S6 76.84(6) . 1_545 ? S1 Pb4 S6 69.01(6) . 1_545 ? S6 Pb4 S6 48.01(4) . 1_545 ? S12 Pb4 S8 81.56(10) . . ? S4 Pb4 S8 52.30(10) . . ? S5 Pb4 S8 115.04(8) . . ? S5 Pb4 S8 115.04(8) 1_545 . ? S10 Pb4 S8 45.77(6) . . ? S10 Pb4 S8 45.77(6) 1_545 . ? S9 Pb4 S8 128.12(7) 1_545 . ? S9 Pb4 S8 128.12(7) . . ? S1 Pb4 S8 104.05(7) . . ? S6 Pb4 S8 154.44(3) . . ? S6 Pb4 S8 154.44(3) 1_545 . ? S23 Pb5 S23 84.53(10) 7_556 7_546 ? S23 Pb5 S7 72.29(10) 7_556 . ? S23 Pb5 S7 72.29(10) 7_546 . ? S23 Pb5 S6 85.52(8) 7_556 . ? S23 Pb5 S6 145.30(11) 7_546 . ? S7 Pb5 S6 73.02(9) . . ? S23 Pb5 S6 145.30(11) 7_556 1_545 ? S23 Pb5 S6 85.52(8) 7_546 1_545 ? S7 Pb5 S6 73.02(9) . 1_545 ? S6 Pb5 S6 84.02(10) . 1_545 ? S23 Pb5 S9 145.59(11) 7_556 1_545 ? S23 Pb5 S9 85.72(8) 7_546 1_545 ? S7 Pb5 S9 134.76(6) . 1_545 ? S6 Pb5 S9 119.36(9) . 1_545 ? S6 Pb5 S9 66.11(9) 1_545 1_545 ? S23 Pb5 S9 85.72(8) 7_556 . ? S23 Pb5 S9 145.59(11) 7_546 . ? S7 Pb5 S9 134.76(6) . . ? S6 Pb5 S9 66.11(9) . . ? S6 Pb5 S9 119.36(9) 1_545 . ? S9 Pb5 S9 83.95(9) 1_545 . ? S23 Pb5 S20 70.42(10) 7_556 7_556 ? S23 Pb5 S20 70.42(10) 7_546 7_556 ? S7 Pb5 S20 128.79(12) . 7_556 ? S6 Pb5 S20 135.68(6) . 7_556 ? S6 Pb5 S20 135.68(6) 1_545 7_556 ? S9 Pb5 S20 75.22(9) 1_545 7_556 ? S9 Pb5 S20 75.21(9) . 7_556 ? S23 Pb5 S12 105.79(9) 7_556 . ? S23 Pb5 S12 105.79(9) 7_546 . ? S7 Pb5 S12 177.30(10) . . ? S6 Pb5 S12 108.90(8) . . ? S6 Pb5 S12 108.90(8) 1_545 . ? S9 Pb5 S12 46.20(6) 1_545 . ? S9 Pb5 S12 46.20(6) . . ? S20 Pb5 S12 48.51(10) 7_556 . ? S23 Pb5 S5 113.06(5) 7_556 . ? S23 Pb5 S5 162.32(5) 7_546 . ? S7 Pb5 S5 113.63(8) . . ? S6 Pb5 S5 44.00(8) . . ? S6 Pb5 S5 80.73(6) 1_545 . ? S9 Pb5 S5 78.59(7) 1_545 . ? S9 Pb5 S5 40.90(8) . . ? S20 Pb5 S5 112.62(9) 7_556 . ? S12 Pb5 S5 68.77(7) . . ? S23 Pb5 S5 162.32(5) 7_556 1_545 ? S23 Pb5 S5 113.06(5) 7_546 1_545 ? S7 Pb5 S5 113.63(8) . 1_545 ? S6 Pb5 S5 80.73(7) . 1_545 ? S6 Pb5 S5 44.00(8) 1_545 1_545 ? S9 Pb5 S5 40.90(8) 1_545 1_545 ? S9 Pb5 S5 78.59(7) . 1_545 ? S20 Pb5 S5 112.62(9) 7_556 1_545 ? S12 Pb5 S5 68.77(7) . 1_545 ? S5 Pb5 S5 49.31(4) . 1_545 ? S23 Pb5 S7 43.85(8) 7_556 1_565 ? S23 Pb5 S7 110.96(7) 7_546 1_565 ? S7 Pb5 S7 53.32(4) . 1_565 ? S6 Pb5 S7 44.67(8) . 1_565 ? S6 Pb5 S7 111.24(7) 1_545 1_565 ? S9 Pb5 S7 163.13(7) 1_545 1_565 ? S9 Pb5 S7 83.35(6) . 1_565 ? S20 Pb5 S7 111.98(6) 7_556 1_565 ? S12 Pb5 S7 126.63(4) . 1_565 ? S5 Pb5 S7 84.55(5) . 1_565 ? S5 Pb5 S7 125.03(6) 1_545 1_565 ? S15 Pb6 S13 83.96(11) . 1_545 ? S15 Pb6 S13 83.96(11) . . ? S13 Pb6 S13 89.81(12) 1_545 . ? S15 Pb6 S11 76.45(10) . . ? S13 Pb6 S11 160.35(12) 1_545 . ? S13 Pb6 S11 89.65(8) . . ? S15 Pb6 S11 76.45(10) . 1_545 ? S13 Pb6 S11 89.65(8) 1_545 1_545 ? S13 Pb6 S11 160.35(12) . 1_545 ? S11 Pb6 S11 84.34(10) . 1_545 ? S15 Pb6 S27 139.76(12) . 7 ? S13 Pb6 S27 122.19(10) 1_545 7 ? S13 Pb6 S27 122.19(10) . 7 ? S11 Pb6 S27 74.02(9) . 7 ? S11 Pb6 S27 74.02(9) 1_545 7 ? S15 Pb6 S8 145.19(13) . . ? S13 Pb6 S8 71.73(10) 1_545 . ? S13 Pb6 S8 71.73(10) . . ? S11 Pb6 S8 126.43(8) . . ? S11 Pb6 S8 126.43(8) 1_545 . ? S27 Pb6 S8 75.05(11) 7 . ? S15 Pb6 S17 55.53(12) . . ? S13 Pb6 S17 50.43(8) 1_545 . ? S13 Pb6 S17 50.43(8) . . ? S11 Pb6 S17 116.56(9) . . ? S11 Pb6 S17 116.56(9) 1_545 . ? S27 Pb6 S17 164.70(11) 7 . ? S8 Pb6 S17 89.65(11) . . ? S15 Pb6 S15 54.93(5) . 1_565 ? S13 Pb6 S15 121.15(10) 1_545 1_565 ? S13 Pb6 S15 50.34(9) . 1_565 ? S11 Pb6 S15 46.84(8) . 1_565 ? S11 Pb6 S15 114.51(8) 1_545 1_565 ? S27 Pb6 S15 116.02(6) 7 1_565 ? S8 Pb6 S15 118.15(6) . 1_565 ? S17 Pb6 S15 71.02(6) . 1_565 ? S15 Pb6 S15 54.93(5) . 1_545 ? S13 Pb6 S15 50.34(9) 1_545 1_545 ? S13 Pb6 S15 121.15(10) . 1_545 ? S11 Pb6 S15 114.51(8) . 1_545 ? S11 Pb6 S15 46.84(8) 1_545 1_545 ? S27 Pb6 S15 116.02(6) 7 1_545 ? S8 Pb6 S15 118.15(6) . 1_545 ? S17 Pb6 S15 71.02(6) . 1_545 ? S15 Pb6 S15 109.85(9) 1_565 1_545 ? S15 Pb6 S14 51.37(11) . . ? S13 Pb6 S14 118.78(9) 1_545 . ? S13 Pb6 S14 118.78(9) . . ? S11 Pb6 S14 45.93(6) . . ? S11 Pb6 S14 45.93(6) 1_545 . ? S27 Pb6 S14 88.39(10) 7 . ? S8 Pb6 S14 163.44(10) . . ? S17 Pb6 S14 106.90(9) . . ? S15 Pb6 S14 68.98(6) 1_565 . ? S15 Pb6 S14 68.98(6) 1_545 . ? S15 Pb6 S27 117.81(6) . 7_545 ? S13 Pb6 S27 76.52(8) 1_545 7_545 ? S13 Pb6 S27 152.17(10) . 7_545 ? S11 Pb6 S27 111.29(7) . 7_545 ? S11 Pb6 S27 45.60(8) 1_545 7_545 ? S27 Pb6 S27 52.32(4) 7 7_545 ? S8 Pb6 S27 80.93(7) . 7_545 ? S17 Pb6 S27 126.12(4) . 7_545 ? S15 Pb6 S27 156.33(7) 1_565 7_545 ? S15 Pb6 S27 67.69(6) 1_545 7_545 ? S14 Pb6 S27 89.02(6) . 7_545 ? S8 Pb7A S10 77.13(15) . 1_545 ? S8 Pb7A S10 77.12(15) . . ? S10 Pb7A S10 86.64(15) 1_545 . ? S8 Pb7A S13 72.81(12) . . ? S10 Pb7A S13 149.86(19) 1_545 . ? S10 Pb7A S13 88.70(9) . . ? S8 Pb7A S13 72.81(12) . 1_545 ? S10 Pb7A S13 88.70(9) 1_545 1_545 ? S10 Pb7A S13 149.86(19) . 1_545 ? S13 Pb7A S13 80.60(11) . 1_545 ? S8 Pb7A S12 129.54(19) . . ? S10 Pb7A S12 66.91(10) 1_545 . ? S10 Pb7A S12 66.91(10) . . ? S13 Pb7A S12 136.91(9) . . ? S13 Pb7A S12 136.92(9) 1_545 . ? S8 Pb7A S17 120.89(14) . . ? S10 Pb7A S17 135.13(10) 1_545 . ? S10 Pb7A S17 135.13(10) . . ? S13 Pb7A S17 63.16(12) . . ? S13 Pb7A S17 63.16(12) 1_545 . ? S12 Pb7A S17 109.56(17) . . ? S8 Pb7A S16 144.97(7) . 1_545 ? S10 Pb7A S16 81.36(11) 1_545 1_545 ? S10 Pb7A S16 128.99(13) . 1_545 ? S13 Pb7A S16 123.47(18) . 1_545 ? S13 Pb7A S16 79.44(12) 1_545 1_545 ? S12 Pb7A S16 62.75(11) . 1_545 ? S17 Pb7A S16 60.58(13) . 1_545 ? S8 Pb7A S16 144.97(7) . . ? S10 Pb7A S16 128.99(13) 1_545 . ? S10 Pb7A S16 81.36(11) . . ? S13 Pb7A S16 79.44(12) . . ? S13 Pb7A S16 123.47(18) 1_545 . ? S12 Pb7A S16 62.75(11) . . ? S17 Pb7A S16 60.58(13) . . ? S16 Pb7A S16 69.23(15) 1_545 . ? S8 Pb7A S8 55.11(6) . 1_545 ? S10 Pb7A S8 46.35(9) 1_545 1_545 ? S10 Pb7A S8 115.80(15) . 1_545 ? S13 Pb7A S8 111.19(10) . 1_545 ? S13 Pb7A S8 45.60(10) 1_545 1_545 ? S12 Pb7A S8 111.36(8) . 1_545 ? S17 Pb7A S8 107.08(8) . 1_545 ? S16 Pb7A S8 90.14(7) 1_545 1_545 ? S16 Pb7A S8 159.12(12) . 1_545 ? S8 Pb7A S8 55.11(6) . 1_565 ? S10 Pb7A S8 115.81(15) 1_545 1_565 ? S10 Pb7A S8 46.36(9) . 1_565 ? S13 Pb7A S8 45.60(10) . 1_565 ? S13 Pb7A S8 111.19(10) 1_545 1_565 ? S12 Pb7A S8 111.36(8) . 1_565 ? S17 Pb7A S8 107.08(8) . 1_565 ? S16 Pb7A S8 159.12(12) 1_545 1_565 ? S16 Pb7A S8 90.14(7) . 1_565 ? S8 Pb7A S8 110.23(12) 1_545 1_565 ? S8 Pb7A S4 50.55(13) . . ? S10 Pb7A S4 47.44(9) 1_545 . ? S10 Pb7A S4 47.44(9) . . ? S13 Pb7A S4 110.80(13) . . ? S13 Pb7A S4 110.80(13) 1_545 . ? S12 Pb7A S4 78.99(12) . . ? S17 Pb7A S4 171.44(12) . . ? S16 Pb7A S4 125.73(10) 1_545 . ? S16 Pb7A S4 125.73(10) . . ? S8 Pb7A S4 68.69(8) 1_545 . ? S8 Pb7A S4 68.69(8) 1_565 . ? S12 Pb7B S13 139.53(10) . . ? S12 Pb7B S13 139.53(10) . 1_545 ? S13 Pb7B S13 80.9(2) . 1_545 ? S12 Pb7B S17 120.6(3) . . ? S13 Pb7B S17 67.52(18) . . ? S13 Pb7B S17 67.52(18) 1_545 . ? S12 Pb7B S8 118.5(3) . . ? S13 Pb7B S8 68.37(18) . . ? S13 Pb7B S8 68.37(18) 1_545 . ? S17 Pb7B S8 120.8(3) . . ? S12 Pb7B S10 64.69(16) . 1_545 ? S13 Pb7B S10 137.2(3) . 1_545 ? S13 Pb7B S10 84.79(13) 1_545 1_545 ? S17 Pb7B S10 140.48(11) . 1_545 ? S8 Pb7B S10 68.83(18) . 1_545 ? S12 Pb7B S10 64.69(16) . . ? S13 Pb7B S10 84.79(13) . . ? S13 Pb7B S10 137.2(3) 1_545 . ? S17 Pb7B S10 140.48(11) . . ? S8 Pb7B S10 68.83(18) . . ? S10 Pb7B S10 78.9(2) 1_545 . ? S12 Pb7B S16 66.83(17) . 1_545 ? S13 Pb7B S16 134.9(3) . 1_545 ? S13 Pb7B S16 84.36(14) 1_545 1_545 ? S17 Pb7B S16 67.42(19) . 1_545 ? S8 Pb7B S16 141.71(12) . 1_545 ? S10 Pb7B S16 82.85(14) 1_545 1_545 ? S10 Pb7B S16 131.5(3) . 1_545 ? S12 Pb7B S16 66.83(17) . . ? S13 Pb7B S16 84.35(14) . . ? S13 Pb7B S16 134.9(3) 1_545 . ? S17 Pb7B S16 67.42(19) . . ? S8 Pb7B S16 141.71(12) . . ? S10 Pb7B S16 131.5(3) 1_545 . ? S10 Pb7B S16 82.85(14) . . ? S16 Pb7B S16 76.5(2) 1_545 . ? S12 Pb7B S12 52.46(8) . 1_565 ? S13 Pb7B S12 87.08(7) . 1_565 ? S13 Pb7B S12 168.00(16) 1_545 1_565 ? S17 Pb7B S12 108.09(15) . 1_565 ? S8 Pb7B S12 106.91(15) . 1_565 ? S10 Pb7B S12 104.06(18) 1_545 1_565 ? S10 Pb7B S12 40.17(10) . 1_565 ? S16 Pb7B S12 104.55(19) 1_545 1_565 ? S16 Pb7B S12 43.04(12) . 1_565 ? S12 Pb7B S12 52.46(8) . 1_545 ? S13 Pb7B S12 168.00(16) . 1_545 ? S13 Pb7B S12 87.08(7) 1_545 1_545 ? S17 Pb7B S12 108.09(15) . 1_545 ? S8 Pb7B S12 106.91(15) . 1_545 ? S10 Pb7B S12 40.17(10) 1_545 1_545 ? S10 Pb7B S12 104.06(18) . 1_545 ? S16 Pb7B S12 43.04(12) 1_545 1_545 ? S16 Pb7B S12 104.55(19) . 1_545 ? S12 Pb7B S12 104.91(15) 1_565 1_545 ? S12 Pb7B S17 108.14(15) . 1_565 ? S13 Pb7B S17 41.63(12) . 1_565 ? S13 Pb7B S17 106.27(19) 1_545 1_565 ? S17 Pb7B S17 52.35(9) . 1_565 ? S8 Pb7B S17 108.25(14) . 1_565 ? S10 Pb7B S17 166.92(17) 1_545 1_565 ? S10 Pb7B S17 88.19(7) . 1_565 ? S16 Pb7B S17 104.8(2) 1_545 1_565 ? S16 Pb7B S17 43.54(11) . 1_565 ? S12 Pb7B S17 64.02(8) 1_565 1_565 ? S12 Pb7B S17 144.83(19) 1_545 1_565 ? S16 Pb8 S19 79.38(12) . 1_565 ? S16 Pb8 S19 79.38(12) . . ? S19 Pb8 S19 89.79(11) 1_565 . ? S16 Pb8 S22 137.88(6) . . ? S19 Pb8 S22 132.09(12) 1_565 . ? S19 Pb8 S22 74.52(10) . . ? S16 Pb8 S22 137.88(6) . 1_565 ? S19 Pb8 S22 74.52(10) 1_565 1_565 ? S19 Pb8 S22 132.08(12) . 1_565 ? S22 Pb8 S22 83.20(12) . 1_565 ? S16 Pb8 S17 74.50(14) . . ? S19 Pb8 S17 153.75(13) 1_565 . ? S19 Pb8 S17 87.93(9) . . ? S22 Pb8 S17 72.11(12) . . ? S22 Pb8 S17 124.78(13) 1_565 . ? S16 Pb8 S17 74.50(14) . 1_565 ? S19 Pb8 S17 87.93(9) 1_565 1_565 ? S19 Pb8 S17 153.76(13) . 1_565 ? S22 Pb8 S17 124.78(13) . 1_565 ? S22 Pb8 S17 72.11(12) 1_565 1_565 ? S17 Pb8 S17 82.75(13) . 1_565 ? S16 Pb8 O 137.5(6) . 1_565 ? S19 Pb8 O 126.7(3) 1_565 1_565 ? S19 Pb8 O 126.7(3) . 1_565 ? S22 Pb8 O 52.3(3) . 1_565 ? S22 Pb8 O 52.3(3) 1_565 1_565 ? S17 Pb8 O 74.0(4) . 1_565 ? S17 Pb8 O 74.0(4) 1_565 1_565 ? S16 Pb8 S26 136.37(14) . . ? S19 Pb8 S26 70.21(9) 1_565 . ? S19 Pb8 S26 70.21(9) . . ? S22 Pb8 S26 61.88(10) . . ? S22 Pb8 S26 61.88(10) 1_565 . ? S17 Pb8 S26 132.63(9) . . ? S17 Pb8 S26 132.63(9) 1_565 . ? O Pb8 S26 86.1(6) 1_565 . ? S16 Pb8 S18 52.91(13) . . ? S19 Pb8 S18 48.95(7) 1_565 . ? S19 Pb8 S18 48.95(7) . . ? S22 Pb8 S18 121.54(9) . . ? S22 Pb8 S18 121.54(9) 1_565 . ? S17 Pb8 S18 113.46(11) . . ? S17 Pb8 S18 113.46(11) 1_565 . ? O Pb8 S18 169.6(6) 1_565 . ? S26 Pb8 S18 83.46(9) . . ? S16 Pb8 S16 55.42(6) . 1_545 ? S19 Pb8 S16 118.45(9) 1_565 1_545 ? S19 Pb8 S16 46.71(10) . 1_545 ? S22 Pb8 S16 82.78(8) . 1_545 ? S22 Pb8 S16 165.38(8) 1_565 1_545 ? S17 Pb8 S16 45.90(11) . 1_545 ? S17 Pb8 S16 113.11(11) 1_565 1_545 ? O Pb8 S16 114.8(3) 1_565 1_545 ? S26 Pb8 S16 114.26(8) . 1_545 ? S18 Pb8 S16 69.98(6) . 1_545 ? S16 Pb8 S16 55.42(6) . 1_565 ? S19 Pb8 S16 46.71(10) 1_565 1_565 ? S19 Pb8 S16 118.46(9) . 1_565 ? S22 Pb8 S16 165.38(8) . 1_565 ? S22 Pb8 S16 82.79(8) 1_565 1_565 ? S17 Pb8 S16 113.11(11) . 1_565 ? S17 Pb8 S16 45.90(11) 1_565 1_565 ? O Pb8 S16 114.8(3) 1_565 1_565 ? S26 Pb8 S16 114.26(8) . 1_565 ? S18 Pb8 S16 69.98(6) . 1_565 ? S16 Pb8 S16 110.83(11) 1_545 1_565 ? S18 Pb9 S23 79.59(10) . . ? S18 Pb9 S23 79.59(10) . 1_565 ? S23 Pb9 S23 88.62(11) . 1_565 ? S18 Pb9 S19 78.91(10) . . ? S23 Pb9 S19 88.53(8) . . ? S23 Pb9 S19 158.48(11) 1_565 . ? S18 Pb9 S19 78.91(10) . 1_565 ? S23 Pb9 S19 158.48(11) . 1_565 ? S23 Pb9 S19 88.53(8) 1_565 1_565 ? S19 Pb9 S19 86.34(10) . 1_565 ? S18 Pb9 S7 140.64(12) . 7_556 ? S23 Pb9 S7 72.58(9) . 7_556 ? S23 Pb9 S7 72.58(9) 1_565 7_556 ? S19 Pb9 S7 126.50(8) . 7_556 ? S19 Pb9 S7 126.50(8) 1_565 7_556 ? S18 Pb9 S26 146.03(12) . . ? S23 Pb9 S26 122.46(9) . . ? S23 Pb9 S26 122.46(9) 1_565 . ? S19 Pb9 S26 76.49(10) . . ? S19 Pb9 S26 76.49(10) 1_565 . ? S7 Pb9 S26 73.33(11) 7_556 . ? S18 Pb9 S20 52.40(11) . . ? S23 Pb9 S20 48.79(7) . . ? S23 Pb9 S20 48.79(7) 1_565 . ? S19 Pb9 S20 116.10(8) . . ? S19 Pb9 S20 116.10(8) 1_565 . ? S7 Pb9 S20 88.24(10) 7_556 . ? S26 Pb9 S20 161.57(10) . . ? S18 Pb9 S16 52.57(11) . . ? S23 Pb9 S16 116.11(8) . . ? S23 Pb9 S16 116.11(8) 1_565 . ? S19 Pb9 S16 47.50(6) . . ? S19 Pb9 S16 47.50(6) 1_565 . ? S7 Pb9 S16 166.79(10) 7_556 . ? S26 Pb9 S16 93.46(10) . . ? S20 Pb9 S16 104.97(8) . . ? S18 Pb9 S18 55.07(4) . 1_545 ? S23 Pb9 S18 47.46(9) . 1_545 ? S23 Pb9 S18 117.99(8) 1_565 1_545 ? S19 Pb9 S18 47.85(9) . 1_545 ? S19 Pb9 S18 116.79(8) 1_565 1_545 ? S7 Pb9 S18 116.28(6) 7_556 1_545 ? S26 Pb9 S18 118.35(6) . 1_545 ? S20 Pb9 S18 69.55(6) . 1_545 ? S16 Pb9 S18 69.64(6) . 1_545 ? S18 Pb9 S18 55.07(4) . 1_565 ? S23 Pb9 S18 117.99(8) . 1_565 ? S23 Pb9 S18 47.46(9) 1_565 1_565 ? S19 Pb9 S18 116.80(8) . 1_565 ? S19 Pb9 S18 47.85(9) 1_565 1_565 ? S7 Pb9 S18 116.28(6) 7_556 1_565 ? S26 Pb9 S18 118.35(6) . 1_565 ? S20 Pb9 S18 69.55(6) . 1_565 ? S16 Pb9 S18 69.64(6) . 1_565 ? S18 Pb9 S18 110.14(9) 1_545 1_565 ? S18 Pb9 S7 118.04(6) . 7_566 ? S23 Pb9 S7 111.87(8) . 7_566 ? S23 Pb9 S7 42.55(9) 1_565 7_566 ? S19 Pb9 S7 154.81(9) . 7_566 ? S19 Pb9 S7 79.54(7) 1_565 7_566 ? S7 Pb9 S7 52.56(4) 7_556 7_566 ? S26 Pb9 S7 79.96(7) . 7_566 ? S20 Pb9 S7 88.93(6) . 7_566 ? S16 Pb9 S7 126.29(4) . 7_566 ? S18 Pb9 S7 156.94(7) 1_545 7_566 ? S18 Pb9 S7 67.56(6) 1_565 7_566 ? S14 Pb10 S11 77.98(10) 7 7 ? S14 Pb10 S11 77.98(10) 7 7_565 ? S11 Pb10 S11 86.66(11) 7 7_565 ? S14 Pb10 S24 78.94(11) 7 . ? S11 Pb10 S24 88.86(8) 7 . ? S11 Pb10 S24 156.92(11) 7_565 . ? S14 Pb10 S24 78.93(11) 7 1_565 ? S11 Pb10 S24 156.92(11) 7 1_565 ? S11 Pb10 S24 88.87(8) 7_565 1_565 ? S24 Pb10 S24 86.43(10) . 1_565 ? S14 Pb10 S28 139.50(7) 7 . ? S11 Pb10 S28 80.29(10) 7 . ? S11 Pb10 S28 134.25(13) 7_565 . ? S24 Pb10 S28 66.82(12) . . ? S24 Pb10 S28 118.10(12) 1_565 . ? S14 Pb10 S28 139.50(7) 7 1_565 ? S11 Pb10 S28 134.25(13) 7 1_565 ? S11 Pb10 S28 80.29(10) 7_565 1_565 ? S24 Pb10 S28 118.10(12) . 1_565 ? S24 Pb10 S28 66.83(12) 1_565 1_565 ? S28 Pb10 S28 78.30(13) . 1_565 ? S14 Pb10 S27 135.02(12) 7 . ? S11 Pb10 S27 69.79(9) 7 . ? S11 Pb10 S27 69.79(9) 7_565 . ? S24 Pb10 S27 129.25(7) . . ? S24 Pb10 S27 129.25(7) 1_565 . ? S28 Pb10 S27 64.53(11) . . ? S28 Pb10 S27 64.53(11) 1_565 . ? S14 Pb10 S21 53.36(12) 7 . ? S11 Pb10 S21 115.78(8) 7 . ? S11 Pb10 S21 115.78(8) 7_565 . ? S24 Pb10 S21 47.26(6) . . ? S24 Pb10 S21 47.26(6) 1_565 . ? S28 Pb10 S21 109.36(11) . . ? S28 Pb10 S21 109.36(11) 1_565 . ? S27 Pb10 S21 171.62(9) . . ? S14 Pb10 S15 53.39(11) 7 7 ? S11 Pb10 S15 46.87(6) 7 7 ? S11 Pb10 S15 46.87(6) 7_565 7 ? S24 Pb10 S15 116.74(8) . 7 ? S24 Pb10 S15 116.74(8) 1_565 7 ? S28 Pb10 S15 125.16(10) . 7 ? S28 Pb10 S15 125.16(10) 1_565 7 ? S27 Pb10 S15 81.63(9) . 7 ? S21 Pb10 S15 106.75(8) . 7 ? S14 Pb10 S14 54.60(5) 7 7_545 ? S11 Pb10 S14 47.16(9) 7 7_545 ? S11 Pb10 S14 116.02(8) 7_565 7_545 ? S24 Pb10 S14 47.99(9) . 7_545 ? S24 Pb10 S14 116.55(8) 1_565 7_545 ? S28 Pb10 S14 85.75(8) . 7_545 ? S28 Pb10 S14 162.77(9) 1_565 7_545 ? S27 Pb10 S14 114.19(6) . 7_545 ? S21 Pb10 S14 69.77(6) . 7_545 ? S15 Pb10 S14 69.79(6) 7 7_545 ? S14 Pb10 S14 54.60(5) 7 7_565 ? S11 Pb10 S14 116.02(8) 7 7_565 ? S11 Pb10 S14 47.16(9) 7_565 7_565 ? S24 Pb10 S14 116.55(8) . 7_565 ? S24 Pb10 S14 47.99(9) 1_565 7_565 ? S28 Pb10 S14 162.77(9) . 7_565 ? S28 Pb10 S14 85.75(8) 1_565 7_565 ? S27 Pb10 S14 114.19(6) . 7_565 ? S21 Pb10 S14 69.77(6) . 7_565 ? S15 Pb10 S14 69.79(6) 7 7_565 ? S14 Pb10 S14 109.20(9) 7_545 7_565 ? S25 Pb11 S25 92.16(12) . 1_565 ? S25 Pb11 S21 81.85(11) . . ? S25 Pb11 S21 81.85(11) 1_565 . ? S25 Pb11 S24 155.19(11) . 1_565 ? S25 Pb11 S24 88.02(8) 1_565 1_565 ? S21 Pb11 S24 73.61(10) . 1_565 ? S25 Pb11 S24 88.02(8) . . ? S25 Pb11 S24 155.19(11) 1_565 . ? S21 Pb11 S24 73.61(10) . . ? S24 Pb11 S24 81.69(10) 1_565 . ? S25 Pb11 S30 132.68(11) . 1_565 ? S25 Pb11 S30 76.76(9) 1_565 1_565 ? S21 Pb11 S30 139.25(6) . 1_565 ? S24 Pb11 S30 71.40(9) 1_565 1_565 ? S24 Pb11 S30 120.30(10) . 1_565 ? S25 Pb11 S30 76.76(9) . . ? S25 Pb11 S30 132.68(11) 1_565 . ? S21 Pb11 S30 139.25(6) . . ? S24 Pb11 S30 120.30(10) 1_565 . ? S24 Pb11 S30 71.40(9) . . ? S30 Pb11 S30 78.04(10) 1_565 . ? S25 Pb11 S31 68.49(10) . . ? S25 Pb11 S31 68.49(10) 1_565 . ? S21 Pb11 S31 136.30(13) . . ? S24 Pb11 S31 133.55(7) 1_565 . ? S24 Pb11 S31 133.55(7) . . ? S30 Pb11 S31 64.62(9) 1_565 . ? S30 Pb11 S31 64.62(9) . . ? S25 Pb11 O 52.4(2) . 1_565 ? S25 Pb11 O 52.4(2) 1_565 1_565 ? S21 Pb11 O 49.8(5) . 1_565 ? S24 Pb11 O 110.7(3) 1_565 1_565 ? S24 Pb11 O 110.7(3) . 1_565 ? S30 Pb11 O 128.4(3) 1_565 1_565 ? S30 Pb11 O 128.4(3) . 1_565 ? S31 Pb11 O 86.5(5) . 1_565 ? S25 Pb11 S21 48.06(10) . 1_545 ? S25 Pb11 S21 120.24(9) 1_565 1_545 ? S21 Pb11 S21 54.44(5) . 1_545 ? S24 Pb11 S21 111.58(8) 1_565 1_545 ? S24 Pb11 S21 45.88(8) . 1_545 ? S30 Pb11 S21 162.32(7) 1_565 1_545 ? S30 Pb11 S21 85.90(7) . 1_545 ? S31 Pb11 S21 114.87(6) . 1_545 ? O Pb11 S21 68.0(2) 1_565 1_545 ? S25 Pb11 S21 120.24(9) . 1_565 ? S25 Pb11 S21 48.06(10) 1_565 1_565 ? S21 Pb11 S21 54.44(5) . 1_565 ? S24 Pb11 S21 45.88(8) 1_565 1_565 ? S24 Pb11 S21 111.58(8) . 1_565 ? S30 Pb11 S21 85.90(7) 1_565 1_565 ? S30 Pb11 S21 162.32(7) . 1_565 ? S31 Pb11 S21 114.87(6) . 1_565 ? O Pb11 S21 68.0(2) 1_565 1_565 ? S21 Pb11 S21 108.87(10) 1_545 1_565 ? S25 Pb11 S28 109.35(7) . . ? S25 Pb11 S28 155.71(7) 1_565 . ? S21 Pb11 S28 111.52(11) . . ? S24 Pb11 S28 77.20(7) 1_565 . ? S24 Pb11 S28 41.55(9) . . ? S30 Pb11 S28 80.27(8) 1_565 . ? S30 Pb11 S28 47.46(9) . . ? S31 Pb11 S28 108.30(9) . . ? O Pb11 S28 151.3(2) 1_565 . ? S21 Pb11 S28 83.44(7) 1_545 . ? S21 Pb11 S28 122.75(7) 1_565 . ? S22 Pb12a S22 89.20(15) 1_565 . ? S22 Pb12a S26 73.37(13) 1_565 . ? S22 Pb12a S26 73.36(13) . . ? S22 Pb12a S29 147.06(16) 1_565 . ? S22 Pb12a S29 82.92(10) . . ? S26 Pb12a S29 73.73(10) . . ? S22 Pb12a S29 82.92(10) 1_565 1_565 ? S22 Pb12a S29 147.06(16) . 1_565 ? S26 Pb12a S29 73.74(10) . 1_565 ? S29 Pb12a S29 86.55(11) . 1_565 ? S22 Pb12a O 55.8(4) 1_565 1_565 ? S22 Pb12a O 55.8(4) . 1_565 ? S26 Pb12a O 104.1(7) . 1_565 ? S29 Pb12a O 136.06(12) . 1_565 ? S29 Pb12a O 136.06(12) 1_565 1_565 ? S22 Pb12a S31 131.55(9) 1_565 . ? S22 Pb12a S31 131.55(9) . . ? S26 Pb12a S31 135.03(14) . . ? S29 Pb12a S31 73.93(11) . . ? S29 Pb12a S31 73.93(11) 1_565 . ? O Pb12a S31 120.9(7) 1_565 . ? S22 Pb12a S25 65.82(11) 1_565 1_565 ? S22 Pb12a S25 119.91(13) . 1_565 ? S26 Pb12a S25 136.14(8) . 1_565 ? S29 Pb12a S25 144.32(14) . 1_565 ? S29 Pb12a S25 85.72(9) 1_565 1_565 ? O Pb12a S25 65.4(5) 1_565 1_565 ? S31 Pb12a S25 70.45(12) . 1_565 ? S22 Pb12a S25 119.91(13) 1_565 . ? S22 Pb12a S25 65.82(11) . . ? S26 Pb12a S25 136.14(8) . . ? S29 Pb12a S25 85.72(9) . . ? S29 Pb12a S25 144.32(14) 1_565 . ? O Pb12a S25 65.4(5) 1_565 . ? S31 Pb12a S25 70.45(12) . . ? S25 Pb12a S25 80.61(11) 1_565 . ? S22 Pb12a S26 42.54(11) 1_565 1_565 ? S22 Pb12a S26 113.65(11) . 1_565 ? S26 Pb12a S26 54.13(5) . 1_565 ? S29 Pb12a S26 113.04(9) . 1_565 ? S29 Pb12a S26 43.98(8) 1_565 1_565 ? O Pb12a S26 98.2(4) 1_565 1_565 ? S31 Pb12a S26 114.49(7) . 1_565 ? S25 Pb12a S26 84.16(6) 1_565 1_565 ? S25 Pb12a S26 161.20(9) . 1_565 ? S22 Pb12a S26 113.66(11) 1_565 1_545 ? S22 Pb12a S26 42.55(11) . 1_545 ? S26 Pb12a S26 54.13(5) . 1_545 ? S29 Pb12a S26 43.98(8) . 1_545 ? S29 Pb12a S26 113.04(9) 1_565 1_545 ? O Pb12a S26 98.2(4) 1_565 1_545 ? S31 Pb12a S26 114.49(7) . 1_545 ? S25 Pb12a S26 161.20(9) 1_565 1_545 ? S25 Pb12a S26 84.16(6) . 1_545 ? S26 Pb12a S26 108.26(9) 1_565 1_545 ? S22 Pb12a O 26.0(4) 1_565 1_575 ? S22 Pb12a O 103.6(3) . 1_575 ? S26 Pb12a O 98.3(4) . 1_575 ? S29 Pb12a O 168.0(3) . 1_575 ? S29 Pb12a O 82.6(3) 1_565 1_575 ? O Pb12a O 53.9(3) 1_565 1_575 ? S31 Pb12a O 107.6(4) . 1_575 ? S25 Pb12a O 39.8(4) 1_565 1_575 ? S25 Pb12a O 106.1(3) . 1_575 ? S26 Pb12a O 55.2(3) 1_565 1_575 ? S26 Pb12a O 137.6(4) 1_545 1_575 ? S26 Sb12b S22 83.8(2) . 1_565 ? S26 Sb12b S22 83.8(2) . . ? S22 Sb12b S22 97.6(2) 1_565 . ? S26 Sb12b O 116.4(7) . 1_565 ? S22 Sb12b O 57.8(3) 1_565 1_565 ? S22 Sb12b O 57.8(3) . 1_565 ? S26 Sb12b S29 79.72(16) . . ? S22 Sb12b S29 162.6(3) 1_565 . ? S22 Sb12b S29 85.94(10) . . ? O Sb12b S29 135.66(17) 1_565 . ? S26 Sb12b S29 79.72(16) . 1_565 ? S22 Sb12b S29 85.94(10) 1_565 1_565 ? S22 Sb12b S29 162.6(3) . 1_565 ? O Sb12b S29 135.66(18) 1_565 1_565 ? S29 Sb12b S29 85.90(17) . 1_565 ? S26 Sb12b S25 142.61(10) . 1_565 ? S22 Sb12b S25 63.48(13) 1_565 1_565 ? S22 Sb12b S25 116.4(2) . 1_565 ? O Sb12b S25 61.7(5) 1_565 1_565 ? S29 Sb12b S25 129.8(2) . 1_565 ? S29 Sb12b S25 80.43(12) 1_565 1_565 ? S26 Sb12b S25 142.61(10) . . ? S22 Sb12b S25 116.4(2) 1_565 . ? S22 Sb12b S25 63.49(13) . . ? O Sb12b S25 61.7(5) 1_565 . ? S29 Sb12b S25 80.43(12) . . ? S29 Sb12b S25 129.8(2) 1_565 . ? S25 Sb12b S25 72.62(14) 1_565 . ? S26 Sb12b S31 134.7(2) . . ? S22 Sb12b S31 122.55(16) 1_565 . ? S22 Sb12b S31 122.55(16) . . ? O Sb12b S31 108.9(7) 1_565 . ? S29 Sb12b S31 67.75(14) . . ? S29 Sb12b S31 67.75(14) 1_565 . ? S25 Sb12b S31 62.37(14) 1_565 . ? S25 Sb12b S31 62.37(14) . . ? S26 Sb12b S26 58.25(8) . 1_565 ? S22 Sb12b S26 45.81(12) 1_565 1_565 ? S22 Sb12b S26 125.6(2) . 1_565 ? O Sb12b S26 103.5(3) 1_565 1_565 ? S29 Sb12b S26 119.05(16) . 1_565 ? S29 Sb12b S26 47.68(9) 1_565 1_565 ? S25 Sb12b S26 85.10(6) 1_565 1_565 ? S25 Sb12b S26 157.17(13) . 1_565 ? S31 Sb12b S26 111.74(10) . 1_565 ? S26 Sb12b S26 58.25(7) . 1_545 ? S22 Sb12b S26 125.6(2) 1_565 1_545 ? S22 Sb12b S26 45.81(12) . 1_545 ? O Sb12b S26 103.5(3) 1_565 1_545 ? S29 Sb12b S26 47.68(9) . 1_545 ? S29 Sb12b S26 119.05(16) 1_565 1_545 ? S25 Sb12b S26 157.17(13) 1_565 1_545 ? S25 Sb12b S26 85.10(6) . 1_545 ? S31 Sb12b S26 111.74(10) . 1_545 ? S26 Sb12b S26 116.50(15) 1_565 1_545 ? S26 Sb12b S32 51.63(15) . . ? S22 Sb12b S32 116.22(16) 1_565 . ? S22 Sb12b S32 116.22(16) . . ? O Sb12b S32 168.0(7) 1_565 . ? S29 Sb12b S32 48.14(10) . . ? S29 Sb12b S32 48.14(10) 1_565 . ? S25 Sb12b S32 126.77(14) 1_565 . ? S25 Sb12b S32 126.77(14) . . ? S31 Sb12b S32 83.10(14) . . ? S26 Sb12b S32 70.94(8) 1_565 . ? S26 Sb12b S32 70.94(8) 1_545 . ? S32 Pb13 S29 80.29(10) . 1_565 ? S32 Pb13 S29 80.29(10) . . ? S29 Pb13 S29 88.80(11) 1_565 . ? S32 Pb13 S35 78.36(10) . 1_565 ? S29 Pb13 S35 88.48(8) 1_565 1_565 ? S29 Pb13 S35 158.63(11) . 1_565 ? S32 Pb13 S35 78.36(10) . . ? S29 Pb13 S35 158.64(11) 1_565 . ? S29 Pb13 S35 88.49(8) . . ? S35 Pb13 S35 86.37(10) 1_565 . ? S32 Pb13 S1 138.77(12) . 3 ? S29 Pb13 S1 125.76(8) 1_565 3 ? S29 Pb13 S1 125.76(8) . 3 ? S35 Pb13 S1 71.94(9) 1_565 3 ? S35 Pb13 S1 71.94(9) . 3 ? S32 Pb13 S31 142.05(12) . . ? S29 Pb13 S31 72.90(9) 1_565 . ? S29 Pb13 S31 72.90(9) . . ? S35 Pb13 S31 126.16(8) 1_565 . ? S35 Pb13 S31 126.15(8) . . ? S1 Pb13 S31 79.18(11) 3 . ? S32 Pb13 S26 55.74(10) . . ? S29 Pb13 S26 48.03(6) 1_565 . ? S29 Pb13 S26 48.03(6) . . ? S35 Pb13 S26 117.74(8) 1_565 . ? S35 Pb13 S26 117.75(8) . . ? S1 Pb13 S26 165.48(9) 3 . ? S31 Pb13 S26 86.31(10) . . ? S32 Pb13 S36 51.97(11) . . ? S29 Pb13 S36 116.30(8) 1_565 . ? S29 Pb13 S36 116.30(8) . . ? S35 Pb13 S36 47.45(6) 1_565 . ? S35 Pb13 S36 47.45(6) . . ? S1 Pb13 S36 86.80(10) 3 . ? S31 Pb13 S36 165.98(10) . . ? S26 Pb13 S36 107.72(8) . . ? S32 Pb13 S32 54.99(4) . 1_565 ? S29 Pb13 S32 47.95(8) 1_565 1_565 ? S29 Pb13 S32 118.44(8) . 1_565 ? S35 Pb13 S32 47.45(8) 1_565 1_565 ? S35 Pb13 S32 116.41(8) . 1_565 ? S1 Pb13 S32 115.57(6) 3 1_565 ? S31 Pb13 S32 116.90(6) . 1_565 ? S26 Pb13 S32 71.16(6) . 1_565 ? S36 Pb13 S32 69.30(6) . 1_565 ? S32 Pb13 S32 54.99(4) . 1_545 ? S29 Pb13 S32 118.44(8) 1_565 1_545 ? S29 Pb13 S32 47.95(8) . 1_545 ? S35 Pb13 S32 116.41(8) 1_565 1_545 ? S35 Pb13 S32 47.45(8) . 1_545 ? S1 Pb13 S32 115.57(6) 3 1_545 ? S31 Pb13 S32 116.90(6) . 1_545 ? S26 Pb13 S32 71.16(6) . 1_545 ? S36 Pb13 S32 69.30(6) . 1_545 ? S32 Pb13 S32 109.98(8) 1_565 1_545 ? S32 Pb13 S1 117.03(6) . 3_565 ? S29 Pb13 S1 78.21(7) 1_565 3_565 ? S29 Pb13 S1 155.59(8) . 3_565 ? S35 Pb13 S1 42.89(8) 1_565 3_565 ? S35 Pb13 S1 110.97(8) . 3_565 ? S1 Pb13 S1 52.82(4) 3 3_565 ? S31 Pb13 S1 83.48(7) . 3_565 ? S26 Pb13 S1 125.80(4) . 3_565 ? S36 Pb13 S1 88.07(6) . 3_565 ? S32 Pb13 S1 66.93(6) 1_565 3_565 ? S32 Pb13 S1 155.97(7) 1_545 3_565 ? S3 Sb3 S2 89.36(15) . . ? S3 Sb3 S2 89.36(15) . 1_545 ? S2 Sb3 S2 93.37(17) . 1_545 ? S3 Sb3 S33 87.81(14) . 3_445 ? S2 Sb3 S33 177.14(19) . 3_445 ? S2 Sb3 S33 87.05(9) 1_545 3_445 ? S3 Sb3 S33 87.81(14) . 3_455 ? S2 Sb3 S33 87.05(9) . 3_455 ? S2 Sb3 S33 177.13(19) 1_545 3_455 ? S33 Sb3 S33 92.39(17) 3_445 3_455 ? S3 Sb3 Pb14 144.47(18) . 5 ? S2 Sb3 Pb14 67.08(9) . 5 ? S2 Sb3 Pb14 67.08(9) 1_545 5 ? S33 Sb3 Pb14 115.64(16) 3_445 5 ? S33 Sb3 Pb14 115.64(16) 3_455 5 ? S3 Sb3 S2 147.58(5) . 5 ? S2 Sb3 S2 113.81(12) . 5 ? S2 Sb3 S2 67.89(14) 1_545 5 ? S33 Sb3 S2 68.97(11) 3_445 5 ? S33 Sb3 S2 114.51(15) 3_455 5 ? Pb14 Sb3 S2 46.89(13) 5 5 ? S3 Sb3 S2 147.58(5) . 5_565 ? S2 Sb3 S2 67.89(14) . 5_565 ? S2 Sb3 S2 113.81(12) 1_545 5_565 ? S33 Sb3 S2 114.51(15) 3_445 5_565 ? S33 Sb3 S2 68.97(11) 3_455 5_565 ? Pb14 Sb3 S2 46.89(13) 5 5_565 ? S2 Sb3 S2 64.83(9) 5 5_565 ? S3 Sb3 S34 59.01(13) . 3_445 ? S2 Sb3 S34 125.61(10) . 3_445 ? S2 Sb3 S34 125.60(10) 1_545 3_445 ? S33 Sb3 S34 52.26(9) 3_445 3_445 ? S33 Sb3 S34 52.26(9) 3_455 3_445 ? Pb14 Sb3 S34 156.53(17) 5 3_445 ? S2 Sb3 S34 115.43(11) 5 3_445 ? S2 Sb3 S34 115.43(11) 5_565 3_445 ? S3 Sb3 S27 61.26(14) . 7 ? S2 Sb3 S27 52.64(10) . 7 ? S2 Sb3 S27 52.64(10) 1_545 7 ? S33 Sb3 S27 125.99(11) 3_445 7 ? S33 Sb3 S27 125.99(11) 3_455 7 ? Pb14 Sb3 S27 83.20(11) 5 7 ? S2 Sb3 S27 114.28(11) 5 7 ? S2 Sb3 S27 114.28(11) 5_565 7 ? S34 Sb3 S27 120.27(11) 3_445 7 ? S3 Sb3 S3 59.96(6) . 1_565 ? S2 Sb3 S3 50.54(9) . 1_565 ? S2 Sb3 S3 128.63(14) 1_545 1_565 ? S33 Sb3 S3 127.28(13) 3_445 1_565 ? S33 Sb3 S3 49.92(9) 3_455 1_565 ? Pb14 Sb3 S3 114.04(5) 5 1_565 ? S2 Sb3 S3 152.45(9) 5 1_565 ? S2 Sb3 S3 87.62(5) 5_565 1_565 ? S34 Sb3 S3 75.06(7) 3_445 1_565 ? S27 Sb3 S3 76.08(7) 7 1_565 ? S3 Sb3 S3 59.96(6) . 1_545 ? S2 Sb3 S3 128.63(14) . 1_545 ? S2 Sb3 S3 50.54(9) 1_545 1_545 ? S33 Sb3 S3 49.92(9) 3_445 1_545 ? S33 Sb3 S3 127.28(13) 3_455 1_545 ? Pb14 Sb3 S3 114.04(5) 5 1_545 ? S2 Sb3 S3 87.62(5) 5 1_545 ? S2 Sb3 S3 152.45(9) 5_565 1_545 ? S34 Sb3 S3 75.06(7) 3_445 1_545 ? S27 Sb3 S3 76.08(7) 7 1_545 ? S3 Sb3 S3 119.92(11) 1_565 1_545 ? S3 Pb14 S33 81.14(19) . 3_455 ? S3 Pb14 S33 81.14(19) . 3_445 ? S33 Pb14 S33 93.4(3) 3_455 3_445 ? S3 Pb14 S2 80.29(18) . . ? S33 Pb14 S2 85.63(10) 3_455 . ? S33 Pb14 S2 161.3(3) 3_445 . ? S3 Pb14 S2 80.29(18) . 1_545 ? S33 Pb14 S2 161.3(3) 3_455 1_545 ? S33 Pb14 S2 85.63(10) 3_445 1_545 ? S2 Pb14 S2 89.4(3) . 1_545 ? S3 Pb14 Pb14 137.0(4) . 5 ? S33 Pb14 Pb14 124.64(18) 3_455 5 ? S33 Pb14 Pb14 124.64(18) 3_445 5 ? S2 Pb14 Pb14 69.7(2) . 5 ? S2 Pb14 Pb14 69.7(2) 1_545 5 ? S3 Pb14 Sb61 143.8(3) . 3_445 ? S33 Pb14 Sb61 79.9(3) 3_455 3_445 ? S33 Pb14 Sb61 69.5(3) 3_445 3_445 ? S2 Pb14 Sb61 128.3(3) . 3_445 ? S2 Pb14 Sb61 116.9(2) 1_545 3_445 ? Pb14 Pb14 Sb61 78.7(3) 5 3_445 ? S3 Pb14 Sb61 143.8(3) . 8_455 ? S33 Pb14 Sb61 69.5(3) 3_455 8_455 ? S33 Pb14 Sb61 79.9(3) 3_445 8_455 ? S2 Pb14 Sb61 116.9(2) . 8_455 ? S2 Pb14 Sb61 128.3(3) 1_545 8_455 ? Pb14 Pb14 Sb61 78.7(3) 5 8_455 ? Sb61 Pb14 Sb61 13.7(5) 3_445 8_455 ? S3 Pb14 Sb3 142.5(3) . 5 ? S33 Pb14 Sb3 121.96(17) 3_455 5 ? S33 Pb14 Sb3 121.96(17) 3_445 5 ? S2 Pb14 Sb3 73.34(16) . 5 ? S2 Pb14 Sb3 73.35(16) 1_545 5 ? Pb14 Pb14 Sb3 5.45(16) 5 5 ? Sb61 Pb14 Sb3 73.3(2) 3_445 5 ? Sb61 Pb14 Sb3 73.3(2) 8_455 5 ? S3 Pb14 Sb16 141.2(4) . 3_445 ? S33 Pb14 Sb16 72.6(2) 3_455 3_445 ? S33 Pb14 Sb16 72.6(2) 3_445 3_445 ? S2 Pb14 Sb16 124.34(18) . 3_445 ? S2 Pb14 Sb16 124.34(18) 1_545 3_445 ? Pb14 Pb14 Sb16 81.8(3) 5 3_445 ? Sb61 Pb14 Sb16 7.53(16) 3_445 3_445 ? Sb61 Pb14 Sb16 7.53(16) 8_455 3_445 ? Sb3 Pb14 Sb16 76.3(3) 5 3_445 ? S3 Pb14 S2 144.03(7) . 5 ? S33 Pb14 S2 125.7(2) 3_455 5 ? S33 Pb14 S2 74.40(13) 3_445 5 ? S2 Pb14 S2 121.0(2) . 5 ? S2 Pb14 S2 72.02(16) 1_545 5 ? Pb14 Pb14 S2 51.30(14) 5 5 ? Sb61 Pb14 S2 46.00(19) 3_445 5 ? Sb61 Pb14 S2 56.3(3) 8_455 5 ? Sb3 Pb14 S2 47.82(13) 5 5 ? Sb16 Pb14 S2 53.11(17) 3_445 5 ? S3 Pb14 S2 144.03(7) . 5_565 ? S33 Pb14 S2 74.40(13) 3_455 5_565 ? S33 Pb14 S2 125.7(2) 3_445 5_565 ? S2 Pb14 S2 72.01(16) . 5_565 ? S2 Pb14 S2 121.0(2) 1_545 5_565 ? Pb14 Pb14 S2 51.30(14) 5 5_565 ? Sb61 Pb14 S2 56.3(3) 3_445 5_565 ? Sb61 Pb14 S2 46.00(19) 8_455 5_565 ? Sb3 Pb14 S2 47.82(13) 5 5_565 ? Sb16 Pb14 S2 53.11(17) 3_445 5_565 ? S2 Pb14 S2 71.67(14) 5 5_565 ? S5 Sb4 S1 91.28(12) . . ? S5 Sb4 S1 91.28(12) . 1_565 ? S1 Sb4 S1 100.81(16) . 1_565 ? S5 Sb4 S4 88.58(12) . . ? S1 Sb4 S4 86.70(9) . . ? S1 Sb4 S4 172.50(11) 1_565 . ? S5 Sb4 S4 88.58(12) . 1_565 ? S1 Sb4 S4 172.50(11) . 1_565 ? S1 Sb4 S4 86.70(9) 1_565 1_565 ? S4 Sb4 S4 85.80(13) . 1_565 ? S5 Sb4 Pb1 139.78(13) . . ? S1 Sb4 Pb1 113.22(9) . . ? S1 Sb4 Pb1 113.22(9) 1_565 . ? S4 Sb4 Pb1 63.01(9) . . ? S4 Sb4 Pb1 63.01(9) 1_565 . ? S5 Sb4 S34 147.43(4) . 3_445 ? S1 Sb4 S34 67.16(10) . 3_445 ? S1 Sb4 S34 115.79(11) 1_565 3_445 ? S4 Sb4 S34 66.96(10) . 3_445 ? S4 Sb4 S34 109.63(11) 1_565 3_445 ? Pb1 Sb4 S34 46.66(6) . 3_445 ? S5 Sb4 S34 147.43(4) . 3_455 ? S1 Sb4 S34 115.79(11) . 3_455 ? S1 Sb4 S34 67.16(10) 1_565 3_455 ? S4 Sb4 S34 109.63(11) . 3_455 ? S4 Sb4 S34 66.96(10) 1_565 3_455 ? Pb1 Sb4 S34 46.66(6) . 3_455 ? S34 Sb4 S34 64.58(7) 3_445 3_455 ? S5 Sb4 S35 67.72(11) . 3_455 ? S1 Sb4 S35 54.48(8) . 3_455 ? S1 Sb4 S35 54.48(8) 1_565 3_455 ? S4 Sb4 S35 131.92(7) . 3_455 ? S4 Sb4 S35 131.92(7) 1_565 3_455 ? Pb1 Sb4 S35 152.50(8) . 3_455 ? S34 Sb4 S35 112.39(8) 3_445 3_455 ? S34 Sb4 S35 112.39(8) 3_455 3_455 ? S5 Sb4 S5 60.05(4) . 1_565 ? S1 Sb4 S5 132.75(11) . 1_565 ? S1 Sb4 S5 48.97(9) 1_565 1_565 ? S4 Sb4 S5 125.28(10) . 1_565 ? S4 Sb4 S5 52.98(8) 1_565 1_565 ? Pb1 Sb4 S5 112.41(5) . 1_565 ? S34 Sb4 S5 152.08(6) 3_445 1_565 ? S34 Sb4 S5 87.58(5) 3_455 1_565 ? S35 Sb4 S5 79.09(6) 3_455 1_565 ? S5 Sb4 S5 60.05(4) . 1_545 ? S1 Sb4 S5 48.96(9) . 1_545 ? S1 Sb4 S5 132.75(11) 1_565 1_545 ? S4 Sb4 S5 52.98(8) . 1_545 ? S4 Sb4 S5 125.27(10) 1_565 1_545 ? Pb1 Sb4 S5 112.41(5) . 1_545 ? S34 Sb4 S5 87.58(5) 3_445 1_545 ? S34 Sb4 S5 152.08(6) 3_455 1_545 ? S35 Sb4 S5 79.09(6) 3_455 1_545 ? S5 Sb4 S5 120.10(8) 1_565 1_545 ? S5 Sb4 S10 60.62(11) . . ? S1 Sb4 S10 124.47(9) . . ? S1 Sb4 S10 124.47(9) 1_565 . ? S4 Sb4 S10 49.45(8) . . ? S4 Sb4 S10 49.45(8) 1_565 . ? Pb1 Sb4 S10 79.16(7) . . ? S34 Sb4 S10 110.84(8) 3_445 . ? S34 Sb4 S10 110.84(8) 3_455 . ? S35 Sb4 S10 128.34(7) 3_455 . ? S5 Sb4 S10 75.82(5) 1_565 . ? S5 Sb4 S10 75.82(5) 1_545 . ? S6 Sb5 S7 92.03(11) . . ? S6 Sb5 S7 92.02(11) . 1_565 ? S7 Sb5 S7 101.37(15) . 1_565 ? S6 Sb5 S36 87.59(12) . 3_445 ? S7 Sb5 S36 86.86(9) . 3_445 ? S7 Sb5 S36 171.77(10) 1_565 3_445 ? S6 Sb5 S36 87.59(12) . 3_455 ? S7 Sb5 S36 171.77(10) . 3_455 ? S7 Sb5 S36 86.86(9) 1_565 3_455 ? S36 Sb5 S36 84.91(13) 3_445 3_455 ? S6 Sb5 S32 148.01(4) . 7_566 ? S7 Sb5 S32 115.15(11) . 7_566 ? S7 Sb5 S32 67.32(10) 1_565 7_566 ? S36 Sb5 S32 109.36(11) 3_445 7_566 ? S36 Sb5 S32 67.93(10) 3_455 7_566 ? S6 Sb5 S32 148.01(4) . 7_556 ? S7 Sb5 S32 67.32(10) . 7_556 ? S7 Sb5 S32 115.15(11) 1_565 7_556 ? S36 Sb5 S32 67.93(10) 3_445 7_556 ? S36 Sb5 S32 109.36(11) 3_455 7_556 ? S32 Sb5 S32 63.19(7) 7_566 7_556 ? S6 Sb5 S23 68.16(11) . 7_556 ? S7 Sb5 S23 54.97(8) . 7_556 ? S7 Sb5 S23 54.97(8) 1_565 7_556 ? S36 Sb5 S23 131.92(8) 3_445 7_556 ? S36 Sb5 S23 131.92(8) 3_455 7_556 ? S32 Sb5 S23 112.86(8) 7_566 7_556 ? S32 Sb5 S23 112.86(8) 7_556 7_556 ? S6 Sb5 S6 59.62(4) . 1_545 ? S7 Sb5 S6 49.49(9) . 1_545 ? S7 Sb5 S6 133.26(10) 1_565 1_545 ? S36 Sb5 S6 52.87(9) 3_445 1_545 ? S36 Sb5 S6 124.13(9) 3_455 1_545 ? S32 Sb5 S6 151.75(6) 7_566 1_545 ? S32 Sb5 S6 88.67(5) 7_556 1_545 ? S23 Sb5 S6 79.16(5) 7_556 1_545 ? S6 Sb5 S6 59.62(4) . 1_565 ? S7 Sb5 S6 133.27(10) . 1_565 ? S7 Sb5 S6 49.49(9) 1_565 1_565 ? S36 Sb5 S6 124.13(9) 3_445 1_565 ? S36 Sb5 S6 52.87(9) 3_455 1_565 ? S32 Sb5 S6 88.67(5) 7_566 1_565 ? S32 Sb5 S6 151.75(6) 7_556 1_565 ? S23 Sb5 S6 79.16(5) 7_556 1_565 ? S6 Sb5 S6 119.25(8) 1_545 1_565 ? S6 Sb5 S35 58.98(11) . 3_455 ? S7 Sb5 S35 124.08(8) . 3_455 ? S7 Sb5 S35 124.08(8) 1_565 3_455 ? S36 Sb5 S35 49.24(8) 3_445 3_455 ? S36 Sb5 S35 49.24(8) 3_455 3_455 ? S32 Sb5 S35 111.70(8) 7_566 3_455 ? S32 Sb5 S35 111.70(8) 7_556 3_455 ? S23 Sb5 S35 127.13(7) 7_556 3_455 ? S6 Sb5 S35 74.89(5) 1_545 3_455 ? S6 Sb5 S35 74.89(5) 1_565 3_455 ? S6 Sb5 S26 128.37(10) . 7_566 ? S7 Sb5 S26 80.91(9) . 7_566 ? S7 Sb5 S26 41.31(9) 1_565 7_566 ? S36 Sb5 S26 142.06(10) 3_445 7_566 ? S36 Sb5 S26 105.73(8) 3_455 7_566 ? S32 Sb5 S26 47.65(8) 7_566 7_566 ? S32 Sb5 S26 74.22(7) 7_556 7_566 ? S23 Sb5 S26 66.18(7) 7_556 7_566 ? S6 Sb5 S26 130.14(6) 1_545 7_566 ? S6 Sb5 S26 89.03(5) 1_565 7_566 ? S35 Sb5 S26 154.96(4) 3_455 7_566 ? Sb7 Sb6 S10 68.1(3) . . ? Sb7 Sb6 S4 129.05(11) . 1_565 ? S10 Sb6 S4 94.53(13) . 1_565 ? Sb7 Sb6 S4 129.05(11) . . ? S10 Sb6 S4 94.53(13) . . ? S4 Sb6 S4 98.61(17) 1_565 . ? Sb7 Sb6 S8 43.57(9) . . ? S10 Sb6 S8 81.78(12) . . ? S4 Sb6 S8 172.58(13) 1_565 . ? S4 Sb6 S8 88.13(9) . . ? Sb7 Sb6 S8 43.57(9) . 1_565 ? S10 Sb6 S8 81.78(12) . 1_565 ? S4 Sb6 S8 88.13(9) 1_565 1_565 ? S4 Sb6 S8 172.58(13) . 1_565 ? S8 Sb6 S8 84.98(14) . 1_565 ? Sb7 Sb6 Pb1 137.6(3) . . ? S10 Sb6 Pb1 154.25(15) . . ? S4 Sb6 Pb1 69.37(11) 1_565 . ? S4 Sb6 Pb1 69.37(11) . . ? S8 Sb6 Pb1 116.30(10) . . ? S8 Sb6 Pb1 116.30(10) 1_565 . ? Sb7 Sb6 S3 96.4(3) . . ? S10 Sb6 S3 144.40(7) . . ? S4 Sb6 S3 118.85(13) 1_565 . ? S4 Sb6 S3 69.99(11) . . ? S8 Sb6 S3 66.34(10) . . ? S8 Sb6 S3 109.48(12) 1_565 . ? Pb1 Sb6 S3 50.05(7) . . ? Sb7 Sb6 S3 96.4(3) . 1_565 ? S10 Sb6 S3 144.40(7) . 1_565 ? S4 Sb6 S3 69.99(11) 1_565 1_565 ? S4 Sb6 S3 118.85(13) . 1_565 ? S8 Sb6 S3 109.48(12) . 1_565 ? S8 Sb6 S3 66.34(10) 1_565 1_565 ? Pb1 Sb6 S3 50.04(7) . 1_565 ? S3 Sb6 S3 65.90(7) . 1_565 ? Sb7 Sb6 S5 136.8(3) . . ? S10 Sb6 S5 68.65(12) . . ? S4 Sb6 S5 54.96(9) 1_565 . ? S4 Sb6 S5 54.96(9) . . ? S8 Sb6 S5 128.44(9) . . ? S8 Sb6 S5 128.44(9) 1_565 . ? Pb1 Sb6 S5 85.60(8) . . ? S3 Sb6 S5 119.30(9) . . ? S3 Sb6 S5 119.29(9) 1_565 . ? Sb7 Sb6 S10 78.80(15) . 1_565 ? S10 Sb6 S10 58.62(5) . 1_565 ? S4 Sb6 S10 52.69(10) 1_565 1_565 ? S4 Sb6 S10 133.50(12) . 1_565 ? S8 Sb6 S10 120.15(11) . 1_565 ? S8 Sb6 S10 49.37(9) 1_565 1_565 ? Pb1 Sb6 S10 117.97(6) . 1_565 ? S3 Sb6 S10 152.59(7) . 1_565 ? S3 Sb6 S10 87.66(5) 1_565 1_565 ? S5 Sb6 S10 79.07(6) . 1_565 ? Sb7 Sb6 S10 78.80(15) . 1_545 ? S10 Sb6 S10 58.62(5) . 1_545 ? S4 Sb6 S10 133.50(12) 1_565 1_545 ? S4 Sb6 S10 52.69(10) . 1_545 ? S8 Sb6 S10 49.37(9) . 1_545 ? S8 Sb6 S10 120.15(11) 1_565 1_545 ? Pb1 Sb6 S10 117.97(6) . 1_545 ? S3 Sb6 S10 87.66(5) . 1_545 ? S3 Sb6 S10 152.59(7) 1_565 1_545 ? S5 Sb6 S10 79.07(6) . 1_545 ? S10 Sb6 S10 117.23(10) 1_565 1_545 ? Sb6 Sb7 S10 95.1(3) . . ? Sb6 Sb7 S8 125.16(12) . . ? S10 Sb7 S8 96.36(14) . . ? Sb6 Sb7 S8 125.16(12) . 1_565 ? S10 Sb7 S8 96.35(14) . 1_565 ? S8 Sb7 S8 106.5(2) . 1_565 ? Sb6 Sb7 S4 40.85(9) . 1_565 ? S10 Sb7 S4 85.78(13) . 1_565 ? S8 Sb7 S4 165.99(13) . 1_565 ? S8 Sb7 S4 86.97(10) 1_565 1_565 ? Sb6 Sb7 S4 40.85(9) . . ? S10 Sb7 S4 85.78(13) . . ? S8 Sb7 S4 86.97(10) . . ? S8 Sb7 S4 165.99(13) 1_565 . ? S4 Sb7 S4 79.37(12) 1_565 . ? Sb6 Sb7 Pb3 109.4(3) . . ? S10 Sb7 Pb3 155.49(16) . . ? S8 Sb7 Pb3 69.84(11) . . ? S8 Sb7 Pb3 69.84(11) 1_565 . ? S4 Sb7 Pb3 112.63(10) 1_565 . ? S4 Sb7 Pb3 112.63(10) . . ? Sb6 Sb7 S3 73.0(3) . . ? S10 Sb7 S3 145.43(7) . . ? S8 Sb7 S3 67.56(12) . . ? S8 Sb7 S3 117.20(13) 1_565 . ? S4 Sb7 S3 103.12(11) 1_565 . ? S4 Sb7 S3 63.80(10) . . ? Pb3 Sb7 S3 48.83(6) . . ? Sb6 Sb7 S3 73.0(3) . 1_565 ? S10 Sb7 S3 145.43(7) . 1_565 ? S8 Sb7 S3 117.20(13) . 1_565 ? S8 Sb7 S3 67.57(12) 1_565 1_565 ? S4 Sb7 S3 63.80(10) 1_565 1_565 ? S4 Sb7 S3 103.12(11) . 1_565 ? Pb3 Sb7 S3 48.83(6) . 1_565 ? S3 Sb7 S3 63.13(7) . 1_565 ? Sb6 Sb7 S13 170.5(3) . . ? S10 Sb7 S13 75.43(14) . . ? S8 Sb7 S13 57.22(11) . . ? S8 Sb7 S13 57.22(11) 1_565 . ? S4 Sb7 S13 136.30(8) 1_565 . ? S4 Sb7 S13 136.30(8) . . ? Pb3 Sb7 S13 80.05(8) . . ? S3 Sb7 S13 114.78(9) . . ? S3 Sb7 S13 114.78(9) 1_565 . ? Sb6 Sb7 S10 92.53(16) . 1_565 ? S10 Sb7 S10 60.39(5) . 1_565 ? S8 Sb7 S10 138.70(14) . 1_565 ? S8 Sb7 S10 50.07(10) 1_565 1_565 ? S4 Sb7 S10 53.74(8) 1_565 1_565 ? S4 Sb7 S10 121.25(10) . 1_565 ? Pb3 Sb7 S10 116.71(5) . 1_565 ? S3 Sb7 S10 149.53(8) . 1_565 ? S3 Sb7 S10 87.23(5) 1_565 1_565 ? S13 Sb7 S10 82.86(7) . 1_565 ? Sb6 Sb7 S10 92.53(16) . 1_545 ? S10 Sb7 S10 60.39(5) . 1_545 ? S8 Sb7 S10 50.07(10) . 1_545 ? S8 Sb7 S10 138.69(14) 1_565 1_545 ? S4 Sb7 S10 121.25(10) 1_565 1_545 ? S4 Sb7 S10 53.74(8) . 1_545 ? Pb3 Sb7 S10 116.71(5) . 1_545 ? S3 Sb7 S10 87.23(5) . 1_545 ? S3 Sb7 S10 149.53(8) 1_565 1_545 ? S13 Sb7 S10 82.86(7) . 1_545 ? S10 Sb7 S10 120.78(10) 1_565 1_545 ? S9 Sb8 S12 91.80(12) . . ? S9 Sb8 S12 91.80(12) . 1_565 ? S12 Sb8 S12 106.06(17) . 1_565 ? S9 Sb8 S20 92.54(12) . 7_566 ? S12 Sb8 S20 170.29(13) . 7_566 ? S12 Sb8 S20 82.49(10) 1_565 7_566 ? S9 Sb8 S20 92.54(12) . 7_556 ? S12 Sb8 S20 82.49(10) . 7_556 ? S12 Sb8 S20 170.29(13) 1_565 7_556 ? S20 Sb8 S20 88.64(13) 7_566 7_556 ? S9 Sb8 S16 139.69(15) . . ? S12 Sb8 S16 65.64(11) . . ? S12 Sb8 S16 65.64(11) 1_565 . ? S20 Sb8 S16 115.35(12) 7_566 . ? S20 Sb8 S16 115.35(12) 7_556 . ? S9 Sb8 S18 157.49(13) . . ? S12 Sb8 S18 101.59(12) . . ? S12 Sb8 S18 101.59(12) 1_565 . ? S20 Sb8 S18 71.68(11) 7_566 . ? S20 Sb8 S18 71.68(11) 7_556 . ? S16 Sb8 S18 62.82(13) . . ? S9 Sb8 S10 73.26(12) . . ? S12 Sb8 S10 55.52(9) . . ? S12 Sb8 S10 55.52(9) 1_565 . ? S20 Sb8 S10 134.15(7) 7_566 . ? S20 Sb8 S10 134.15(7) 7_556 . ? S16 Sb8 S10 66.43(12) . . ? S18 Sb8 S10 129.25(10) . . ? S9 Sb8 S23 64.14(11) . 7_556 ? S12 Sb8 S23 123.65(9) . 7_556 ? S12 Sb8 S23 123.65(9) 1_565 7_556 ? S20 Sb8 S23 51.44(8) 7_566 7_556 ? S20 Sb8 S23 51.44(8) 7_556 7_556 ? S16 Sb8 S23 156.17(12) . 7_556 ? S18 Sb8 S23 93.35(9) . 7_556 ? S10 Sb8 S23 137.40(9) . 7_556 ? S9 Sb8 S9 60.44(4) . 1_545 ? S12 Sb8 S9 47.20(10) . 1_545 ? S12 Sb8 S9 135.27(11) 1_565 1_545 ? S20 Sb8 S9 129.02(10) 7_566 1_545 ? S20 Sb8 S9 54.13(9) 7_556 1_545 ? S16 Sb8 S9 112.10(6) . 1_545 ? S18 Sb8 S9 117.11(5) . 1_545 ? S10 Sb8 S9 81.83(6) . 1_545 ? S23 Sb8 S9 77.58(5) 7_556 1_545 ? S9 Sb8 S9 60.44(4) . 1_565 ? S12 Sb8 S9 135.27(11) . 1_565 ? S12 Sb8 S9 47.20(10) 1_565 1_565 ? S20 Sb8 S9 54.13(9) 7_566 1_565 ? S20 Sb8 S9 129.02(10) 7_556 1_565 ? S16 Sb8 S9 112.10(6) . 1_565 ? S18 Sb8 S9 117.11(5) . 1_565 ? S10 Sb8 S9 81.83(6) . 1_565 ? S23 Sb8 S9 77.58(5) 7_556 1_565 ? S9 Sb8 S9 120.88(9) 1_545 1_565 ? S9 Sb8 S5 20.26(10) . . ? S12 Sb8 S5 79.72(11) . . ? S12 Sb8 S5 79.72(11) 1_565 . ? S20 Sb8 S5 106.78(10) 7_566 . ? S20 Sb8 S5 106.78(10) 7_556 . ? S16 Sb8 S5 119.43(12) . . ? S18 Sb8 S5 177.75(9) . . ? S10 Sb8 S5 53.00(7) . . ? S23 Sb8 S5 84.40(7) 7_556 . ? S9 Sb8 S5 62.43(5) 1_545 . ? S9 Sb8 S5 62.43(5) 1_565 . ? S11 Sb9 S15 87.69(12) . 1_565 ? S11 Sb9 S15 87.69(12) . . ? S15 Sb9 S15 91.32(15) 1_565 . ? S11 Sb9 S14 88.77(13) . 1_565 ? S15 Sb9 S14 88.71(10) 1_565 1_565 ? S15 Sb9 S14 176.45(15) . 1_565 ? S11 Sb9 S14 88.77(13) . . ? S15 Sb9 S14 176.46(15) 1_565 . ? S15 Sb9 S14 88.71(10) . . ? S14 Sb9 S14 91.04(16) 1_565 . ? S11 Sb9 S21 152.10(15) . . ? S15 Sb9 S21 73.09(11) 1_565 . ? S15 Sb9 S21 73.09(11) . . ? S14 Sb9 S21 110.29(11) 1_565 . ? S14 Sb9 S21 110.28(11) . . ? S11 Sb9 S14 146.94(14) . 7 ? S15 Sb9 S14 114.49(11) 1_565 7 ? S15 Sb9 S14 114.49(11) . 7 ? S14 Sb9 S14 68.65(12) 1_565 7 ? S14 Sb9 S14 68.65(12) . 7 ? S21 Sb9 S14 60.96(11) . 7 ? S11 Sb9 S11 59.50(4) . 1_545 ? S15 Sb9 S11 126.57(11) 1_565 1_545 ? S15 Sb9 S11 50.46(9) . 1_545 ? S14 Sb9 S11 127.14(11) 1_565 1_545 ? S14 Sb9 S11 51.27(10) . 1_545 ? S21 Sb9 S11 116.65(5) . 1_545 ? S14 Sb9 S11 115.18(6) 7 1_545 ? S11 Sb9 S11 59.50(4) . 1_565 ? S15 Sb9 S11 50.46(9) 1_565 1_565 ? S15 Sb9 S11 126.57(11) . 1_565 ? S14 Sb9 S11 51.27(10) 1_565 1_565 ? S14 Sb9 S11 127.15(11) . 1_565 ? S21 Sb9 S11 116.65(5) . 1_565 ? S14 Sb9 S11 115.18(6) 7 1_565 ? S11 Sb9 S11 118.99(9) 1_545 1_565 ? S11 Sb9 S24 60.83(11) . 7 ? S15 Sb9 S24 126.13(9) 1_565 7 ? S15 Sb9 S24 126.13(9) . 7 ? S14 Sb9 S24 51.54(9) 1_565 7 ? S14 Sb9 S24 51.54(9) . 7 ? S21 Sb9 S24 147.07(10) . 7 ? S14 Sb9 S24 86.10(9) 7 7 ? S11 Sb9 S24 75.68(6) 1_545 7 ? S11 Sb9 S24 75.68(6) 1_565 7 ? S11 Sb9 S13 58.74(12) . . ? S15 Sb9 S13 51.87(9) 1_565 . ? S15 Sb9 S13 51.87(9) . . ? S14 Sb9 S13 125.98(9) 1_565 . ? S14 Sb9 S13 125.98(9) . . ? S21 Sb9 S13 93.36(11) . . ? S14 Sb9 S13 154.32(10) 7 . ? S11 Sb9 S13 74.73(6) 1_545 . ? S11 Sb9 S13 74.73(6) 1_565 . ? S24 Sb9 S13 119.57(8) 7 . ? S11 Sb9 S21 126.29(6) . 1_565 ? S15 Sb9 S21 43.45(11) 1_565 1_565 ? S15 Sb9 S21 109.65(10) . 1_565 ? S14 Sb9 S21 72.68(10) 1_565 1_565 ? S14 Sb9 S21 139.64(12) . 1_565 ? S21 Sb9 S21 47.96(4) . 1_565 ? S14 Sb9 S21 71.03(7) 7 1_565 ? S11 Sb9 S21 160.10(8) 1_545 1_565 ? S11 Sb9 S21 70.16(6) 1_565 1_565 ? S24 Sb9 S21 124.20(6) 7 1_565 ? S13 Sb9 S21 92.25(7) . 1_565 ? S13 Sb10 S17 87.35(15) . 1_565 ? S13 Sb10 S17 87.36(15) . . ? S17 Sb10 S17 102.66(19) 1_565 . ? S13 Sb10 S15 90.68(12) . . ? S17 Sb10 S15 172.24(12) 1_565 . ? S17 Sb10 S15 84.73(11) . . ? S13 Sb10 S15 90.68(12) . 1_565 ? S17 Sb10 S15 84.73(11) 1_565 1_565 ? S17 Sb10 S15 172.24(12) . 1_565 ? S15 Sb10 S15 87.79(14) . 1_565 ? S13 Sb10 O 163.7(6) . 1_565 ? S17 Sb10 O 82.5(4) 1_565 1_565 ? S17 Sb10 O 82.5(4) . 1_565 ? S15 Sb10 O 101.0(4) . 1_565 ? S15 Sb10 O 101.0(4) 1_565 1_565 ? S13 Sb10 S21 146.04(13) . . ? S17 Sb10 S21 112.73(13) 1_565 . ? S17 Sb10 S21 112.72(13) . . ? S15 Sb10 S21 65.65(11) . . ? S15 Sb10 S21 65.65(11) 1_565 . ? O Sb10 S21 50.3(6) 1_565 . ? S13 Sb10 S16 70.37(14) . . ? S17 Sb10 S16 52.96(11) 1_565 . ? S17 Sb10 S16 52.96(11) . . ? S15 Sb10 S16 133.05(9) . . ? S15 Sb10 S16 133.05(9) 1_565 . ? O Sb10 S16 93.3(6) 1_565 . ? S21 Sb10 S16 143.59(12) . . ? S13 Sb10 S11 62.23(11) . . ? S17 Sb10 S11 121.99(10) 1_565 . ? S17 Sb10 S11 122.00(10) . . ? S15 Sb10 S11 50.80(8) . . ? S15 Sb10 S11 50.80(8) 1_565 . ? O Sb10 S11 134.1(6) 1_565 . ? S21 Sb10 S11 83.81(9) . . ? S16 Sb10 S11 132.60(11) . . ? S13 Sb10 S22 134.96(11) . . ? S17 Sb10 S22 91.04(12) 1_565 . ? S17 Sb10 S22 49.21(13) . . ? S15 Sb10 S22 95.65(9) . . ? S15 Sb10 S22 134.00(12) 1_565 . ? O Sb10 S22 33.3(4) 1_565 . ? S21 Sb10 S22 74.20(9) . . ? S16 Sb10 S22 73.03(10) . . ? S11 Sb10 S22 145.74(7) . . ? S13 Sb10 S22 134.96(11) . 1_565 ? S17 Sb10 S22 49.21(13) 1_565 1_565 ? S17 Sb10 S22 91.04(12) . 1_565 ? S15 Sb10 S22 134.00(12) . 1_565 ? S15 Sb10 S22 95.65(9) 1_565 1_565 ? O Sb10 S22 33.3(4) 1_565 1_565 ? S21 Sb10 S22 74.20(9) . 1_565 ? S16 Sb10 S22 73.03(10) . 1_565 ? S11 Sb10 S22 145.74(7) . 1_565 ? S22 Sb10 S22 50.93(5) . 1_565 ? S13 Sb10 S13 59.05(5) . 1_545 ? S17 Sb10 S13 130.23(14) 1_565 1_545 ? S17 Sb10 S13 46.11(11) . 1_545 ? S15 Sb10 S13 53.95(9) . 1_545 ? S15 Sb10 S13 126.92(10) 1_565 1_545 ? O Sb10 S13 119.58(12) 1_565 1_545 ? S21 Sb10 S13 115.25(6) . 1_545 ? S16 Sb10 S13 80.05(7) . 1_545 ? S11 Sb10 S13 76.13(6) . 1_545 ? S22 Sb10 S13 89.70(6) . 1_545 ? S22 Sb10 S13 137.07(7) 1_565 1_545 ? S19 Sb11 S16 89.44(15) . . ? S19 Sb11 S16 89.45(15) . 1_545 ? S16 Sb11 S16 99.9(2) . 1_545 ? S19 Sb11 S18 83.98(12) . . ? S16 Sb11 S18 86.95(12) . . ? S16 Sb11 S18 170.48(16) 1_545 . ? S19 Sb11 S18 83.98(12) . 1_545 ? S16 Sb11 S18 170.48(16) . 1_545 ? S16 Sb11 S18 86.95(12) 1_545 1_545 ? S18 Sb11 S18 85.53(13) . 1_545 ? S19 Sb11 S12 158.69(14) . . ? S16 Sb11 S12 77.01(15) . . ? S16 Sb11 S12 77.01(15) 1_545 . ? S18 Sb11 S12 111.21(11) . . ? S18 Sb11 S12 111.21(11) 1_545 . ? S19 Sb11 S20 140.83(13) . 7_556 ? S16 Sb11 S20 114.45(12) . 7_556 ? S16 Sb11 S20 114.45(12) 1_545 7_556 ? S18 Sb11 S20 67.81(10) . 7_556 ? S18 Sb11 S20 67.81(10) 1_545 7_556 ? S12 Sb11 S20 60.48(11) . 7_556 ? S19 Sb11 S17 66.64(11) . . ? S16 Sb11 S17 53.53(9) . . ? S16 Sb11 S17 53.53(9) 1_545 . ? S18 Sb11 S17 128.71(8) . . ? S18 Sb11 S17 128.71(8) 1_545 . ? S12 Sb11 S17 92.05(12) . . ? S20 Sb11 S17 152.53(11) 7_556 . ? S19 Sb11 S19 58.41(4) . 1_565 ? S16 Sb11 S19 48.92(14) . 1_565 ? S16 Sb11 S19 130.31(11) 1_545 1_565 ? S18 Sb11 S19 50.71(9) . 1_565 ? S18 Sb11 S19 121.56(10) 1_545 1_565 ? S12 Sb11 S19 119.21(5) . 1_565 ? S20 Sb11 S19 113.96(5) 7_556 1_565 ? S17 Sb11 S19 78.01(6) . 1_565 ? S19 Sb11 S19 58.41(4) . 1_545 ? S16 Sb11 S19 130.31(11) . 1_545 ? S16 Sb11 S19 48.92(14) 1_545 1_545 ? S18 Sb11 S19 121.56(10) . 1_545 ? S18 Sb11 S19 50.71(9) 1_545 1_545 ? S12 Sb11 S19 119.21(5) . 1_545 ? S20 Sb11 S19 113.96(5) 7_556 1_545 ? S17 Sb11 S19 78.01(6) . 1_545 ? S19 Sb11 S19 116.82(9) 1_565 1_545 ? S19 Sb11 S23 56.60(10) . . ? S16 Sb11 S23 122.13(14) . . ? S16 Sb11 S23 122.13(14) 1_545 . ? S18 Sb11 S23 48.37(8) . . ? S18 Sb11 S23 48.36(8) 1_545 . ? S12 Sb11 S23 144.71(10) . . ? S20 Sb11 S23 84.23(9) 7_556 . ? S17 Sb11 S23 123.24(9) . . ? S19 Sb11 S23 73.24(5) 1_565 . ? S19 Sb11 S23 73.24(5) 1_545 . ? S19 Sb11 S12 123.58(5) . 1_545 ? S16 Sb11 S12 118.85(15) . 1_545 ? S16 Sb11 S12 41.46(12) 1_545 1_545 ? S18 Sb11 S12 139.57(10) . 1_545 ? S18 Sb11 S12 70.63(8) 1_545 1_545 ? S12 Sb11 S12 53.59(4) . 1_545 ? S20 Sb11 S12 72.99(6) 7_556 1_545 ? S17 Sb11 S12 91.22(7) . 1_545 ? S19 Sb11 S12 167.21(8) 1_565 1_545 ? S19 Sb11 S12 66.68(6) 1_545 1_545 ? S23 Sb11 S12 118.98(5) . 1_545 ? S23 Sb12 S20 88.25(13) . 1_545 ? S23 Sb12 S20 88.26(13) . . ? S20 Sb12 S20 96.42(16) 1_545 . ? S23 Sb12 S18 89.63(12) . 1_545 ? S20 Sb12 S18 85.43(10) 1_545 1_545 ? S20 Sb12 S18 177.15(13) . 1_545 ? S23 Sb12 S18 89.63(12) . . ? S20 Sb12 S18 177.14(13) 1_545 . ? S20 Sb12 S18 85.43(10) . . ? S18 Sb12 S18 92.64(15) 1_545 . ? S23 Sb12 S20 154.14(14) . 7_556 ? S20 Sb12 S20 108.53(11) 1_545 7_556 ? S20 Sb12 S20 108.53(11) . 7_556 ? S18 Sb12 S20 72.82(11) 1_545 7_556 ? S18 Sb12 S20 72.82(11) . 7_556 ? S23 Sb12 S18 147.33(14) . 7_556 ? S20 Sb12 S18 70.51(11) 1_545 7_556 ? S20 Sb12 S18 70.50(11) . 7_556 ? S18 Sb12 S18 112.22(9) 1_545 7_556 ? S18 Sb12 S18 112.22(9) . 7_556 ? S20 Sb12 S18 58.53(10) 7_556 7_556 ? S23 Sb12 S19 61.58(11) . . ? S20 Sb12 S19 124.82(9) 1_545 . ? S20 Sb12 S19 124.82(9) . . ? S18 Sb12 S19 52.38(8) 1_545 . ? S18 Sb12 S19 52.38(8) . . ? S20 Sb12 S19 92.56(9) 7_556 . ? S18 Sb12 S19 151.09(10) 7_556 . ? S23 Sb12 S23 59.51(5) . 1_565 ? S20 Sb12 S23 128.83(12) 1_545 1_565 ? S20 Sb12 S23 48.86(10) . 1_565 ? S18 Sb12 S23 128.31(10) 1_545 1_565 ? S18 Sb12 S23 51.21(9) . 1_565 ? S20 Sb12 S23 117.17(5) 7_556 1_565 ? S18 Sb12 S23 115.29(5) 7_556 1_565 ? S19 Sb12 S23 76.03(5) . 1_565 ? S23 Sb12 S23 59.51(5) . 1_545 ? S20 Sb12 S23 48.86(10) 1_545 1_545 ? S20 Sb12 S23 128.83(11) . 1_545 ? S18 Sb12 S23 51.21(9) 1_545 1_545 ? S18 Sb12 S23 128.31(10) . 1_545 ? S20 Sb12 S23 117.17(5) 7_556 1_545 ? S18 Sb12 S23 115.29(5) 7_556 1_545 ? S19 Sb12 S23 76.03(5) . 1_545 ? S23 Sb12 S23 119.01(9) 1_565 1_545 ? S23 Sb12 S9 60.82(11) . 7_556 ? S20 Sb12 S9 53.41(9) 1_545 7_556 ? S20 Sb12 S9 53.41(9) . 7_556 ? S18 Sb12 S9 126.86(9) 1_545 7_556 ? S18 Sb12 S9 126.86(9) . 7_556 ? S20 Sb12 S9 145.04(9) 7_556 7_556 ? S18 Sb12 S9 86.51(9) 7_556 7_556 ? S19 Sb12 S9 122.40(7) . 7_556 ? S23 Sb12 S9 75.68(5) 1_565 7_556 ? S23 Sb12 S9 75.68(5) 1_545 7_556 ? S23 Sb12 S20 127.59(6) . 7_546 ? S20 Sb12 S20 70.57(13) 1_545 7_546 ? S20 Sb12 S20 139.78(7) . 7_546 ? S18 Sb12 S20 42.95(10) 1_545 7_546 ? S18 Sb12 S20 109.36(10) . 7_546 ? S20 Sb12 S20 47.32(4) 7_556 7_546 ? S18 Sb12 S20 69.27(7) 7_556 7_546 ? S19 Sb12 S20 91.74(6) . 7_546 ? S23 Sb12 S20 160.57(7) 1_565 7_546 ? S23 Sb12 S20 71.09(6) 1_545 7_546 ? S9 Sb12 S20 123.74(5) 7_556 7_546 ? S24 Sb13 S21 90.78(13) . 1_545 ? S24 Sb13 S21 90.78(13) . . ? S21 Sb13 S21 99.03(17) 1_545 . ? S24 Sb13 S14 87.00(12) . 7_545 ? S21 Sb13 S14 87.56(10) 1_545 7_545 ? S21 Sb13 S14 173.08(12) . 7_545 ? S24 Sb13 S14 87.00(12) . 7 ? S21 Sb13 S14 173.08(12) 1_545 7 ? S21 Sb13 S14 87.56(10) . 7 ? S14 Sb13 S14 85.78(14) 7_545 7 ? S24 Sb13 S14 148.54(13) . . ? S21 Sb13 S14 109.10(12) 1_545 . ? S21 Sb13 S14 109.10(12) . . ? S14 Sb13 S14 70.32(12) 7_545 . ? S14 Sb13 S14 70.32(12) 7 . ? S24 Sb13 S15 149.96(13) . . ? S21 Sb13 S15 70.32(11) 1_545 . ? S21 Sb13 S15 70.32(11) . . ? S14 Sb13 S15 114.28(10) 7_545 . ? S14 Sb13 S15 114.28(10) 7 . ? S14 Sb13 S15 61.50(10) . . ? S24 Sb13 S25 63.61(11) . . ? S21 Sb13 S25 54.87(10) 1_545 . ? S21 Sb13 S25 54.87(10) . . ? S14 Sb13 S25 129.15(9) 7_545 . ? S14 Sb13 S25 129.15(9) 7 . ? S14 Sb13 S25 147.85(10) . . ? S15 Sb13 S25 86.35(9) . . ? S24 Sb13 S24 59.59(4) . 1_565 ? S21 Sb13 S24 131.52(12) 1_545 1_565 ? S21 Sb13 S24 49.53(10) . 1_565 ? S14 Sb13 S24 124.09(10) 7_545 1_565 ? S14 Sb13 S24 52.16(9) 7 1_565 ? S14 Sb13 S24 115.58(5) . 1_565 ? S15 Sb13 S24 115.99(5) . 1_565 ? S25 Sb13 S24 77.00(6) . 1_565 ? S24 Sb13 S24 59.59(4) . 1_545 ? S21 Sb13 S24 49.53(10) 1_545 1_545 ? S21 Sb13 S24 131.51(12) . 1_545 ? S14 Sb13 S24 52.16(9) 7_545 1_545 ? S14 Sb13 S24 124.09(10) 7 1_545 ? S14 Sb13 S24 115.58(5) . 1_545 ? S15 Sb13 S24 115.99(5) . 1_545 ? S25 Sb13 S24 77.00(6) . 1_545 ? S24 Sb13 S24 119.18(9) 1_565 1_545 ? S24 Sb13 S11 58.80(11) . 7 ? S21 Sb13 S11 124.21(10) 1_545 7 ? S21 Sb13 S11 124.21(10) . 7 ? S14 Sb13 S11 49.29(8) 7_545 7 ? S14 Sb13 S11 49.29(8) 7 7 ? S14 Sb13 S11 89.75(9) . 7 ? S15 Sb13 S11 151.25(9) . 7 ? S25 Sb13 S11 122.40(7) . 7 ? S24 Sb13 S11 74.80(5) 1_565 7 ? S24 Sb13 S11 74.80(5) 1_545 7 ? S24 Sb13 O 94.8(4) . . ? S21 Sb13 O 27.21(16) 1_545 . ? S21 Sb13 O 72.10(16) . . ? S14 Sb13 O 114.61(15) 7_545 . ? S14 Sb13 O 159.58(15) 7 . ? S14 Sb13 O 114.1(4) . . ? S15 Sb13 O 57.8(4) . . ? S25 Sb13 O 38.1(3) . . ? S24 Sb13 O 111.9(2) 1_565 . ? S24 Sb13 O 73.3(2) 1_545 . ? S11 Sb13 O 146.1(3) 7 . ? O Sb14 O 143.4(17) . 1_565 ? O Sb14 S25 94.4(9) . . ? O Sb14 S25 94.4(9) 1_565 . ? O Sb14 S22 72.6(8) . . ? O Sb14 S22 72.6(8) 1_565 . ? S25 Sb14 S22 85.86(15) . . ? O Sb14 S21 147.2(8) . . ? O Sb14 S21 69.3(8) 1_565 . ? S25 Sb14 S21 82.85(12) . . ? S22 Sb14 S21 139.11(7) . . ? O Sb14 S21 69.3(8) . 1_545 ? O Sb14 S21 147.2(8) 1_565 1_545 ? S25 Sb14 S21 82.85(12) . 1_545 ? S22 Sb14 S21 139.12(7) . 1_545 ? S21 Sb14 S21 78.01(12) . 1_545 ? O Sb14 S17 79.3(9) . . ? O Sb14 S17 79.3(9) 1_565 . ? S25 Sb14 S17 158.03(14) . . ? S22 Sb14 S17 72.17(14) . . ? S21 Sb14 S17 113.73(11) . . ? S21 Sb14 S17 113.73(11) 1_545 . ? O Sb14 S15 97.6(9) . . ? O Sb14 S15 97.7(9) 1_565 . ? S25 Sb14 S15 140.78(14) . . ? S22 Sb14 S15 133.36(14) . . ? S21 Sb14 S15 67.14(11) . . ? S21 Sb14 S15 67.14(11) 1_545 . ? S17 Sb14 S15 61.19(11) . . ? O Sb14 S25 149.3(9) . 1_565 ? O Sb14 S25 38.5(9) 1_565 1_565 ? S25 Sb14 S25 59.90(5) . 1_565 ? S22 Sb14 S25 87.92(8) . 1_565 ? S21 Sb14 S25 52.63(9) . 1_565 ? S21 Sb14 S25 118.82(9) 1_545 1_565 ? S17 Sb14 S25 117.72(5) . 1_565 ? S15 Sb14 S25 112.86(6) . 1_565 ? O Sb14 S25 38.5(9) . 1_545 ? O Sb14 S25 149.3(9) 1_565 1_545 ? S25 Sb14 S25 59.90(5) . 1_545 ? S22 Sb14 S25 87.92(8) . 1_545 ? S21 Sb14 S25 118.82(9) . 1_545 ? S21 Sb14 S25 52.63(9) 1_545 1_545 ? S17 Sb14 S25 117.72(5) . 1_545 ? S15 Sb14 S25 112.86(6) . 1_545 ? S25 Sb14 S25 119.80(9) 1_565 1_545 ? O Sb14 S22 131.1(8) . 1_565 ? O Sb14 S22 14.9(9) 1_565 1_565 ? S25 Sb14 S22 87.85(8) . 1_565 ? S22 Sb14 S22 58.74(5) . 1_565 ? S21 Sb14 S22 81.62(8) . 1_565 ? S21 Sb14 S22 158.49(9) 1_545 1_565 ? S17 Sb14 S22 80.86(7) . 1_565 ? S15 Sb14 S22 110.87(7) . 1_565 ? S25 Sb14 S22 40.68(7) 1_565 1_565 ? S25 Sb14 S22 136.12(8) 1_545 1_565 ? O Sb14 S22 14.9(9) . 1_545 ? O Sb14 S22 131.1(8) 1_565 1_545 ? S25 Sb14 S22 87.85(8) . 1_545 ? S22 Sb14 S22 58.74(5) . 1_545 ? S21 Sb14 S22 158.49(9) . 1_545 ? S21 Sb14 S22 81.62(8) 1_545 1_545 ? S17 Sb14 S22 80.86(7) . 1_545 ? S15 Sb14 S22 110.87(7) . 1_545 ? S25 Sb14 S22 136.12(8) 1_565 1_545 ? S25 Sb14 S22 40.68(7) 1_545 1_545 ? S22 Sb14 S22 117.49(11) 1_565 1_545 ? S29 Sb15 S26 87.35(11) . . ? S29 Sb15 S26 87.35(11) . 1_545 ? S26 Sb15 S26 98.66(15) . 1_545 ? S29 Sb15 S32 85.35(11) . 1_545 ? S26 Sb15 S32 170.23(12) . 1_545 ? S26 Sb15 S32 87.48(9) 1_545 1_545 ? S29 Sb15 S32 85.35(11) . . ? S26 Sb15 S32 87.48(9) . . ? S26 Sb15 S32 170.24(12) 1_545 . ? S32 Sb15 S32 85.47(12) 1_545 . ? S29 Sb15 S7 145.68(4) . 7_556 ? S26 Sb15 S7 70.87(10) . 7_556 ? S26 Sb15 S7 121.15(11) 1_545 7_556 ? S32 Sb15 S7 112.42(10) 1_545 7_556 ? S32 Sb15 S7 67.99(10) . 7_556 ? S29 Sb15 S7 145.68(4) . 7_546 ? S26 Sb15 S7 121.16(11) . 7_546 ? S26 Sb15 S7 70.87(10) 1_545 7_546 ? S32 Sb15 S7 67.99(10) 1_545 7_546 ? S32 Sb15 S7 112.42(10) . 7_546 ? S7 Sb15 S7 67.71(7) 7_556 7_546 ? S29 Sb15 S22 62.49(11) . . ? S26 Sb15 S22 53.28(8) . . ? S26 Sb15 S22 53.28(8) 1_545 . ? S32 Sb15 S22 127.59(8) 1_545 . ? S32 Sb15 S22 127.59(8) . . ? S7 Sb15 S22 117.30(8) 7_556 . ? S7 Sb15 S22 117.30(8) 7_546 . ? S29 Sb15 S29 58.98(4) . 1_545 ? S26 Sb15 S29 128.77(10) . 1_545 ? S26 Sb15 S29 47.64(9) 1_545 1_545 ? S32 Sb15 S29 51.44(8) 1_545 1_545 ? S32 Sb15 S29 122.67(9) . 1_545 ? S7 Sb15 S29 154.55(6) 7_556 1_545 ? S7 Sb15 S29 87.02(5) 7_546 1_545 ? S22 Sb15 S29 76.23(6) . 1_545 ? S29 Sb15 S29 58.98(4) . 1_565 ? S26 Sb15 S29 47.63(9) . 1_565 ? S26 Sb15 S29 128.77(10) 1_545 1_565 ? S32 Sb15 S29 122.67(9) 1_545 1_565 ? S32 Sb15 S29 51.44(8) . 1_565 ? S7 Sb15 S29 87.02(5) 7_556 1_565 ? S7 Sb15 S29 154.55(6) 7_546 1_565 ? S22 Sb15 S29 76.23(6) . 1_565 ? S29 Sb15 S29 117.97(8) 1_545 1_565 ? S29 Sb15 S19 108.83(11) . . ? S26 Sb15 S19 53.11(8) . . ? S26 Sb15 S19 53.10(8) 1_545 . ? S32 Sb15 S19 135.82(7) 1_545 . ? S32 Sb15 S19 135.82(7) . . ? S7 Sb15 S19 79.39(8) 7_556 . ? S7 Sb15 S19 79.39(8) 7_546 . ? S22 Sb15 S19 46.34(8) . . ? S29 Sb15 S19 99.57(5) 1_545 . ? S29 Sb15 S19 99.57(5) 1_565 . ? S29 Sb15 S35 57.19(10) . . ? S26 Sb15 S35 121.42(9) . . ? S26 Sb15 S35 121.42(9) 1_545 . ? S32 Sb15 S35 48.89(7) 1_545 . ? S32 Sb15 S35 48.89(7) . . ? S7 Sb15 S35 111.98(8) 7_556 . ? S7 Sb15 S35 111.98(8) 7_546 . ? S22 Sb15 S35 119.68(8) . . ? S29 Sb15 S35 73.79(5) 1_545 . ? S29 Sb15 S35 73.79(5) 1_565 . ? S19 Sb15 S35 166.02(7) . . ? Sb61 Sb16 S27 90.8(14) 6_565 . ? Sb61 Sb16 S28 71(3) 6_565 1_565 ? S27 Sb16 S28 92.6(3) . 1_565 ? Sb61 Sb16 S28 175(3) 6_565 . ? S27 Sb16 S28 92.6(3) . . ? S28 Sb16 S28 105.7(6) 1_565 . ? Sb61 Sb16 S2 17(3) 6_565 7_565 ? S27 Sb16 S2 83.7(3) . 7_565 ? S28 Sb16 S2 86.16(15) 1_565 7_565 ? S28 Sb16 S2 167.8(5) . 7_565 ? Sb61 Sb16 S2 98(4) 6_565 7 ? S27 Sb16 S2 83.7(3) . 7 ? S28 Sb16 S2 167.8(5) 1_565 7 ? S28 Sb16 S2 86.16(15) . 7 ? S2 Sb16 S2 81.9(4) 7_565 7 ? Sb61 Sb16 Pb15 105.3(18) 6_565 . ? S27 Sb16 Pb15 149.9(7) . . ? S28 Sb16 Pb15 70.0(3) 1_565 . ? S28 Sb16 Pb15 70.0(3) . . ? S2 Sb16 Pb15 118.1(2) 7_565 . ? S2 Sb16 Pb15 118.1(2) 7 . ? Sb61 Sb16 Pb14 67(3) 6_565 3 ? S27 Sb16 Pb14 135.4(6) . 3 ? S28 Sb16 Pb14 113.0(2) 1_565 3 ? S28 Sb16 Pb14 113.0(2) . 3 ? S2 Sb16 Pb14 63.5(3) 7_565 3 ? S2 Sb16 Pb14 63.5(3) 7 3 ? Pb15 Sb16 Pb14 74.7(2) . 3 ? Sb61 Sb16 S33 56.3(14) 6_565 1_565 ? S27 Sb16 S33 145.45(19) . 1_565 ? S28 Sb16 S33 68.24(16) 1_565 1_565 ? S28 Sb16 S33 119.6(3) . 1_565 ? S2 Sb16 S33 67.18(19) 7_565 1_565 ? S2 Sb16 S33 108.9(4) 7 1_565 ? Pb15 Sb16 S33 50.97(11) . 1_565 ? Pb14 Sb16 S33 45.38(15) 3 1_565 ? Sb61 Sb16 S33 110(2) 6_565 . ? S27 Sb16 S33 145.45(19) . . ? S28 Sb16 S33 119.6(3) 1_565 . ? S28 Sb16 S33 68.24(16) . . ? S2 Sb16 S33 108.9(4) 7_565 . ? S2 Sb16 S33 67.18(19) 7 . ? Pb15 Sb16 S33 50.97(11) . . ? Pb14 Sb16 S33 45.38(15) 3 . ? S33 Sb16 S33 65.72(13) 1_565 . ? Sb61 Sb16 S27 136(3) 6_565 1_545 ? S27 Sb16 S27 59.37(8) . 1_545 ? S28 Sb16 S27 135.2(5) 1_565 1_545 ? S28 Sb16 S27 48.51(14) . 1_545 ? S2 Sb16 S27 120.5(3) 7_565 1_545 ? S2 Sb16 S27 51.69(9) 7 1_545 ? Pb15 Sb16 S27 116.2(2) . 1_545 ? Pb14 Sb16 S27 111.3(2) 3 1_545 ? S33 Sb16 S27 152.4(2) 1_565 1_545 ? S33 Sb16 S27 87.30(6) . 1_545 ? Sb61 Sb16 S27 45(2) 6_565 1_565 ? S27 Sb16 S27 59.37(8) . 1_565 ? S28 Sb16 S27 48.50(14) 1_565 1_565 ? S28 Sb16 S27 135.1(5) . 1_565 ? S2 Sb16 S27 51.69(9) 7_565 1_565 ? S2 Sb16 S27 120.5(3) 7 1_565 ? Pb15 Sb16 S27 116.2(2) . 1_565 ? Pb14 Sb16 S27 111.3(2) 3 1_565 ? S33 Sb16 S27 87.30(6) 1_565 1_565 ? S33 Sb16 S27 152.4(2) . 1_565 ? S27 Sb16 S27 118.73(15) 1_545 1_565 ? Sb61 Sb61 S28 132.3(3) 6_565 . ? Sb61 Sb61 S27 80.8(4) 6_565 . ? S28 Sb61 S27 94.2(4) . . ? Sb61 Sb61 S2 128.1(3) 6_565 7 ? S28 Sb61 S2 99.4(5) . 7 ? S27 Sb61 S2 93.0(3) . 7 ? Sb61 Sb61 S28 36.6(3) 6_565 1_565 ? S28 Sb61 S28 95.7(3) . 1_565 ? S27 Sb61 S28 81.0(3) . 1_565 ? S2 Sb61 S28 164.1(6) 7 1_565 ? Sb61 Sb61 S2 40.70(17) 6_565 7_565 ? S28 Sb61 S2 171.8(4) . 7_565 ? S27 Sb61 S2 80.8(4) . 7_565 ? S2 Sb61 S2 87.4(3) 7 7_565 ? S28 Sb61 S2 77.1(4) 1_565 7_565 ? Sb61 Sb61 Sb61 180.0 6_565 6 ? S28 Sb61 Sb61 47.7(3) . 6 ? S27 Sb61 Sb61 99.2(4) . 6 ? S2 Sb61 Sb61 51.9(3) 7 6 ? S28 Sb61 Sb61 143.4(3) 1_565 6 ? S2 Sb61 Sb61 139.30(17) 7_565 6 ? Sb61 Sb61 Pb14 83.2(3) 6_565 3 ? S28 Sb61 Pb14 122.1(4) . 3 ? S27 Sb61 Pb14 141.4(5) . 3 ? S2 Sb61 Pb14 70.3(2) 7 3 ? S28 Sb61 Pb14 105.5(4) 1_565 3 ? S2 Sb61 Pb14 64.4(3) 7_565 3 ? Sb61 Sb61 Pb14 96.8(3) 6 3 ? Sb61 Sb61 Pb15 83.3(3) 6_565 . ? S28 Sb61 Pb15 68.4(2) . . ? S27 Sb61 Pb15 136.9(3) . . ? S2 Sb61 Pb15 127.7(3) 7 . ? S28 Sb61 Pb15 62.97(18) 1_565 . ? S2 Sb61 Pb15 111.0(4) 7_565 . ? Sb61 Sb61 Pb15 96.7(3) 6 . ? Pb14 Sb61 Pb15 74.8(2) 3 . ? Sb61 Sb61 S33 117.9(2) 6_565 . ? S28 Sb61 S33 73.8(3) . . ? S27 Sb61 S33 161.3(6) . . ? S2 Sb61 S33 75.4(2) 7 . ? S28 Sb61 S33 113.8(2) 1_565 . ? S2 Sb61 S33 112.6(3) 7_565 . ? Sb61 Sb61 S33 62.1(2) 6 . ? Pb14 Sb61 S33 48.31(14) 3 . ? Pb15 Sb61 S33 52.31(13) . . ? Sb61 Sb61 S33 51.94(19) 6_565 1_565 ? S28 Sb61 S33 116.5(3) . 1_565 ? S27 Sb61 S33 132.7(5) . 1_565 ? S2 Sb61 S33 114.4(3) 7 1_565 ? S28 Sb61 S33 62.0(2) 1_565 1_565 ? S2 Sb61 S33 63.9(3) 7_565 1_565 ? Sb61 Sb61 S33 128.06(19) 6 1_565 ? Pb14 Sb61 S33 44.33(17) 3 1_565 ? Pb15 Sb61 S33 48.29(14) . 1_565 ? S33 Sb61 S33 65.92(14) . 1_565 ? Sb61 Sb61 S27 146.52(13) 6_565 1_545 ? S28 Sb61 S27 54.5(3) . 1_545 ? S27 Sb61 S27 65.7(3) . 1_545 ? S2 Sb61 S27 57.2(3) 7 1_545 ? S28 Sb61 S27 130.9(3) 1_565 1_545 ? S2 Sb61 S27 127.6(2) 7_565 1_545 ? Sb61 Sb61 S27 33.48(13) 6 1_545 ? Pb14 Sb61 S27 123.1(3) 3 1_545 ? Pb15 Sb61 S27 121.1(4) . 1_545 ? S33 Sb61 S27 95.6(3) . 1_545 ? S33 Sb61 S27 161.5(3) 1_565 1_545 ? S34 Pb15 S30 84.37(13) . 1_565 ? S34 Pb15 S30 84.36(13) . . ? S30 Pb15 S30 93.50(16) 1_565 . ? S34 Pb15 S33 78.26(13) . 1_565 ? S30 Pb15 S33 88.60(9) 1_565 1_565 ? S30 Pb15 S33 162.21(17) . 1_565 ? S34 Pb15 S33 78.25(13) . . ? S30 Pb15 S33 162.21(17) 1_565 . ? S30 Pb15 S33 88.60(9) . . ? S33 Pb15 S33 84.21(15) 1_565 . ? S34 Pb15 Sb16 141.9(3) . . ? S30 Pb15 Sb16 119.74(18) 1_565 . ? S30 Pb15 Sb16 119.74(18) . . ? S33 Pb15 Sb16 73.7(2) 1_565 . ? S33 Pb15 Sb16 73.7(2) . . ? S34 Pb15 S28 141.58(8) . 1_565 ? S30 Pb15 S28 74.04(12) 1_565 1_565 ? S30 Pb15 S28 127.54(18) . 1_565 ? S33 Pb15 S28 69.98(12) 1_565 1_565 ? S33 Pb15 S28 118.13(15) . 1_565 ? Sb16 Pb15 S28 45.70(17) . 1_565 ? S34 Pb15 S28 141.58(8) . . ? S30 Pb15 S28 127.53(18) 1_565 . ? S30 Pb15 S28 74.04(12) . . ? S33 Pb15 S28 118.13(15) 1_565 . ? S33 Pb15 S28 69.98(12) . . ? Sb16 Pb15 S28 45.71(17) . . ? S28 Pb15 S28 74.74(13) 1_565 . ? S34 Pb15 Sb61 137.5(2) . . ? S30 Pb15 Sb61 127.5(2) 1_565 . ? S30 Pb15 Sb61 116.0(3) . . ? S33 Pb15 Sb61 75.7(3) 1_565 . ? S33 Pb15 Sb61 66.22(19) . . ? Sb16 Pb15 Sb61 7.78(13) . . ? S28 Pb15 Sb61 53.5(2) 1_565 . ? S28 Pb15 Sb61 42.5(3) . . ? S34 Pb15 Sb61 137.5(2) . 6_565 ? S30 Pb15 Sb61 116.0(3) 1_565 6_565 ? S30 Pb15 Sb61 127.5(2) . 6_565 ? S33 Pb15 Sb61 66.22(19) 1_565 6_565 ? S33 Pb15 Sb61 75.7(3) . 6_565 ? Sb16 Pb15 Sb61 7.78(13) . 6_565 ? S28 Pb15 Sb61 42.5(3) 1_565 6_565 ? S28 Pb15 Sb61 53.5(2) . 6_565 ? Sb61 Pb15 Sb61 13.4(5) . 6_565 ? S34 Pb15 S31 60.46(12) . . ? S30 Pb15 S31 50.33(9) 1_565 . ? S30 Pb15 S31 50.32(9) . . ? S33 Pb15 S31 121.36(10) 1_565 . ? S33 Pb15 S31 121.36(10) . . ? Sb16 Pb15 S31 157.7(3) . . ? S28 Pb15 S31 120.13(13) 1_565 . ? S28 Pb15 S31 120.13(13) . . ? Sb61 Pb15 S31 160.5(2) . . ? Sb61 Pb15 S31 160.5(2) 6_565 . ? S34 Pb15 S24 132.82(12) . . ? S30 Pb15 S24 88.03(12) 1_565 . ? S30 Pb15 S24 49.67(11) . . ? S33 Pb15 S24 148.12(12) 1_565 . ? S33 Pb15 S24 106.57(8) . . ? Sb16 Pb15 S24 80.6(3) . . ? S28 Pb15 S24 78.63(11) 1_565 . ? S28 Pb15 S24 44.94(12) . . ? Sb61 Pb15 S24 81.4(2) . . ? Sb61 Pb15 S24 87.03(16) 6_565 . ? S31 Pb15 S24 79.17(9) . . ? S34 Sb17 S30 92.6(2) . 1_565 ? S34 Sb17 S30 92.6(2) . . ? S30 Sb17 S30 100.1(3) 1_565 . ? S34 Sb17 S33 80.2(3) . 1_565 ? S30 Sb17 S33 89.11(10) 1_565 1_565 ? S30 Sb17 S33 168.6(3) . 1_565 ? S34 Sb17 S33 80.2(3) . . ? S30 Sb17 S33 168.6(3) 1_565 . ? S30 Sb17 S33 89.11(10) . . ? S33 Sb17 S33 81.0(3) 1_565 . ? S34 Sb17 S28 142.08(19) . 1_565 ? S30 Sb17 S28 71.49(17) 1_565 1_565 ? S30 Sb17 S28 123.4(3) . 1_565 ? S33 Sb17 S28 65.78(14) 1_565 1_565 ? S33 Sb17 S28 109.0(2) . 1_565 ? S34 Sb17 S28 142.08(19) . . ? S30 Sb17 S28 123.4(3) 1_565 . ? S30 Sb17 S28 71.49(17) . . ? S33 Sb17 S28 109.0(2) 1_565 . ? S33 Sb17 S28 65.79(14) . . ? S28 Sb17 S28 69.02(16) 1_565 . ? S34 Sb17 S31 66.65(19) . . ? S30 Sb17 S31 55.24(15) 1_565 . ? S30 Sb17 S31 55.24(15) . . ? S33 Sb17 S31 127.79(16) 1_565 . ? S33 Sb17 S31 127.79(16) . . ? S28 Sb17 S31 122.1(2) 1_565 . ? S28 Sb17 S31 122.1(2) . . ? S34 Sb17 S34 58.72(10) . 1_565 ? S30 Sb17 S34 50.84(13) 1_565 1_565 ? S30 Sb17 S34 132.7(2) . 1_565 ? S33 Sb17 S34 49.94(10) 1_565 1_565 ? S33 Sb17 S34 117.8(3) . 1_565 ? S28 Sb17 S34 85.72(7) 1_565 1_565 ? S28 Sb17 S34 153.35(15) . 1_565 ? S31 Sb17 S34 78.13(10) . 1_565 ? S34 Sb17 S34 58.72(10) . 1_545 ? S30 Sb17 S34 132.7(2) 1_565 1_545 ? S30 Sb17 S34 50.84(13) . 1_545 ? S33 Sb17 S34 117.8(3) 1_565 1_545 ? S33 Sb17 S34 49.94(10) . 1_545 ? S28 Sb17 S34 153.35(15) 1_565 1_545 ? S28 Sb17 S34 85.72(7) . 1_545 ? S31 Sb17 S34 78.13(10) . 1_545 ? S34 Sb17 S34 117.45(19) 1_565 1_545 ? S34 Sb17 S24 139.7(2) . . ? S30 Sb17 S24 88.0(3) 1_565 . ? S30 Sb17 S24 47.95(18) . . ? S33 Sb17 S24 140.0(2) 1_565 . ? S33 Sb17 S24 103.21(13) . . ? S28 Sb17 S24 75.57(18) 1_565 . ? S28 Sb17 S24 44.06(14) . . ? S31 Sb17 S24 81.20(17) . . ? S34 Sb17 S24 138.61(19) 1_565 . ? S34 Sb17 S24 92.42(9) 1_545 . ? S34 Sb17 S24 139.7(2) . 1_565 ? S30 Sb17 S24 47.94(18) 1_565 1_565 ? S30 Sb17 S24 88.0(3) . 1_565 ? S33 Sb17 S24 103.20(13) 1_565 1_565 ? S33 Sb17 S24 140.0(2) . 1_565 ? S28 Sb17 S24 44.07(14) 1_565 1_565 ? S28 Sb17 S24 75.56(18) . 1_565 ? S31 Sb17 S24 81.20(17) . 1_565 ? S34 Sb17 S24 92.42(9) 1_565 1_565 ? S34 Sb17 S24 138.61(19) 1_545 1_565 ? S24 Sb17 S24 48.93(11) . 1_565 ? S35 Sb18 S36 89.76(12) . . ? S35 Sb18 S36 89.76(12) . 1_545 ? S36 Sb18 S36 95.85(16) . 1_545 ? S35 Sb18 S32 87.54(11) . . ? S36 Sb18 S32 87.18(10) . . ? S36 Sb18 S32 175.93(13) 1_545 . ? S35 Sb18 S32 87.54(11) . 1_545 ? S36 Sb18 S32 175.93(13) . 1_545 ? S36 Sb18 S32 87.18(10) 1_545 1_545 ? S32 Sb18 S32 89.67(13) . 1_545 ? S35 Sb18 S36 148.55(4) . 5_666 ? S36 Sb18 S36 69.87(15) . 5_666 ? S36 Sb18 S36 115.21(9) 1_545 5_666 ? S32 Sb18 S36 68.38(10) . 5_666 ? S32 Sb18 S36 111.28(11) 1_545 5_666 ? S35 Sb18 S36 148.55(4) . 5_656 ? S36 Sb18 S36 115.21(9) . 5_656 ? S36 Sb18 S36 69.87(15) 1_545 5_656 ? S32 Sb18 S36 111.28(11) . 5_656 ? S32 Sb18 S36 68.38(10) 1_545 5_656 ? S36 Sb18 S36 62.50(8) 5_666 5_656 ? S35 Sb18 S6 61.76(11) . 3_545 ? S36 Sb18 S6 53.68(9) . 3_545 ? S36 Sb18 S6 53.68(9) 1_545 3_545 ? S32 Sb18 S6 127.11(8) . 3_545 ? S32 Sb18 S6 127.11(8) 1_545 3_545 ? S36 Sb18 S6 116.92(8) 5_666 3_545 ? S36 Sb18 S6 116.92(8) 5_656 3_545 ? S35 Sb18 S35 59.35(4) . 1_545 ? S36 Sb18 S35 129.53(11) . 1_545 ? S36 Sb18 S35 50.16(10) 1_545 1_545 ? S32 Sb18 S35 125.78(10) . 1_545 ? S32 Sb18 S35 51.06(9) 1_545 1_545 ? S36 Sb18 S35 151.79(6) 5_666 1_545 ? S36 Sb18 S35 89.35(6) 5_656 1_545 ? S6 Sb18 S35 76.04(5) 3_545 1_545 ? S35 Sb18 S35 59.35(4) . 1_565 ? S36 Sb18 S35 50.15(10) . 1_565 ? S36 Sb18 S35 129.53(11) 1_545 1_565 ? S32 Sb18 S35 51.06(9) . 1_565 ? S32 Sb18 S35 125.78(10) 1_545 1_565 ? S36 Sb18 S35 89.35(6) 5_666 1_565 ? S36 Sb18 S35 151.79(6) 5_656 1_565 ? S6 Sb18 S35 76.04(5) 3_545 1_565 ? S35 Sb18 S35 118.70(9) 1_545 1_565 ? S35 Sb18 S29 59.18(11) . . ? S36 Sb18 S29 124.98(9) . . ? S36 Sb18 S29 124.98(9) 1_545 . ? S32 Sb18 S29 50.96(8) . . ? S32 Sb18 S29 50.96(8) 1_545 . ? S36 Sb18 S29 112.91(8) 5_666 . ? S36 Sb18 S29 112.91(8) 5_656 . ? S6 Sb18 S29 120.94(7) 3_545 . ? S35 Sb18 S29 74.86(5) 1_545 . ? S35 Sb18 S29 74.86(5) 1_565 . ? S35 Sb18 S32 129.54(10) . 5_666 ? S36 Sb18 S32 43.36(11) . 5_666 ? S36 Sb18 S32 80.16(10) 1_545 5_666 ? S32 Sb18 S32 103.91(9) . 5_666 ? S32 Sb18 S32 140.23(7) 1_545 5_666 ? S36 Sb18 S32 45.58(8) 5_666 5_666 ? S36 Sb18 S32 71.86(7) 5_656 5_666 ? S6 Sb18 S32 72.99(7) 3_545 5_666 ? S35 Sb18 S32 130.30(6) 1_545 5_666 ? S35 Sb18 S32 90.13(5) 1_565 5_666 ? S29 Sb18 S32 154.83(4) . 5_666 ? S30 Sb20 S31 86.66(13) . 1_545 ? S30 Sb20 S31 86.66(13) . . ? S31 Sb20 S31 100.74(15) 1_545 . ? S30 Sb20 S34 79.23(11) . . ? S31 Sb20 S34 162.80(12) 1_545 . ? S31 Sb20 S34 88.31(9) . . ? S30 Sb20 S34 79.23(11) . 1_545 ? S31 Sb20 S34 88.31(9) 1_545 1_545 ? S31 Sb20 S34 162.80(12) . 1_545 ? S34 Sb20 S34 79.48(10) . 1_545 ? S30 Sb20 S1 141.40(6) . 3 ? S31 Sb20 S1 130.59(12) 1_545 3 ? S31 Sb20 S1 77.63(11) . 3 ? S34 Sb20 S1 65.43(9) . 3 ? S34 Sb20 S1 107.59(10) 1_545 3 ? S30 Sb20 S1 141.40(6) . 3_545 ? S31 Sb20 S1 77.63(11) 1_545 3_545 ? S31 Sb20 S1 130.59(12) . 3_545 ? S34 Sb20 S1 107.59(10) . 3_545 ? S34 Sb20 S1 65.43(9) 1_545 3_545 ? S1 Sb20 S1 68.32(8) 3 3_545 ? S30 Sb20 S29 116.36(11) . . ? S31 Sb20 S29 57.10(9) 1_545 . ? S31 Sb20 S29 57.10(9) . . ? S34 Sb20 S29 138.70(6) . . ? S34 Sb20 S29 138.70(6) 1_545 . ? S1 Sb20 S29 84.07(8) 3 . ? S1 Sb20 S29 84.07(8) 3_545 . ? S30 Sb20 S25 59.13(11) . . ? S31 Sb20 S25 54.90(9) 1_545 . ? S31 Sb20 S25 54.90(9) . . ? S34 Sb20 S25 122.98(8) . . ? S34 Sb20 S25 122.98(8) 1_545 . ? S1 Sb20 S25 129.37(7) 3 . ? S1 Sb20 S25 129.37(7) 3_545 . ? S29 Sb20 S25 57.22(7) . . ? S30 Sb20 S30 57.53(4) . 1_545 ? S31 Sb20 S30 47.07(10) 1_545 1_545 ? S31 Sb20 S30 128.21(11) . 1_545 ? S34 Sb20 S30 116.05(8) . 1_545 ? S34 Sb20 S30 50.23(8) 1_545 1_545 ? S1 Sb20 S30 153.29(7) 3 1_545 ? S1 Sb20 S30 86.89(6) 3_545 1_545 ? S29 Sb20 S30 103.79(6) . 1_545 ? S25 Sb20 S30 74.01(6) . 1_545 ? S30 Sb20 S30 57.53(4) . 1_565 ? S31 Sb20 S30 128.21(11) 1_545 1_565 ? S31 Sb20 S30 47.07(10) . 1_565 ? S34 Sb20 S30 50.23(8) . 1_565 ? S34 Sb20 S30 116.05(8) 1_545 1_565 ? S1 Sb20 S30 86.89(6) 3 1_565 ? S1 Sb20 S30 153.29(7) 3_545 1_565 ? S29 Sb20 S30 103.79(6) . 1_565 ? S25 Sb20 S30 74.01(6) . 1_565 ? S30 Sb20 S30 115.07(8) 1_545 1_565 ? S30 Sb20 S35 167.79(11) . . ? S31 Sb20 S35 85.56(11) 1_545 . ? S31 Sb20 S35 85.56(11) . . ? S34 Sb20 S35 109.90(9) . . ? S34 Sb20 S35 109.90(9) 1_545 . ? S1 Sb20 S35 45.06(6) 3 . ? S1 Sb20 S35 45.06(6) 3_545 . ? S29 Sb20 S35 51.43(7) . . ? S25 Sb20 S35 108.66(7) . . ? S30 Sb20 S35 121.64(4) 1_545 . ? S30 Sb20 S35 121.64(4) 1_565 . ? As4 S1 Sb4 0.00(10) 1_545 1_545 ? As4 S1 Sb4 100.81(16) 1_545 . ? Sb4 S1 Sb4 100.81(16) 1_545 . ? As4 S1 Pb2 95.95(11) 1_545 . ? Sb4 S1 Pb2 95.95(11) 1_545 . ? Sb4 S1 Pb2 95.95(11) . . ? As4 S1 Pb13 129.47(8) 1_545 3_445 ? Sb4 S1 Pb13 129.47(8) 1_545 3_445 ? Sb4 S1 Pb13 129.47(8) . 3_445 ? Pb2 S1 Pb13 84.84(11) . 3_445 ? As4 S1 S35 148.49(15) 1_545 3_455 ? Sb4 S1 S35 148.49(15) 1_545 3_455 ? Sb4 S1 S35 88.39(7) . 3_455 ? Pb2 S1 S35 52.88(8) . 3_455 ? Pb13 S1 S35 52.55(8) 3_445 3_455 ? As4 S1 S35 88.38(7) 1_545 3_445 ? Sb4 S1 S35 88.38(7) 1_545 3_445 ? Sb4 S1 S35 148.49(15) . 3_445 ? Pb2 S1 S35 52.88(8) . 3_445 ? Pb13 S1 S35 52.55(8) 3_445 3_445 ? S35 S1 S35 69.71(11) 3_455 3_445 ? As4 S1 S5 41.04(8) 1_545 1_545 ? Sb4 S1 S5 41.04(8) 1_545 1_545 ? Sb4 S1 S5 97.13(13) . 1_545 ? Pb2 S1 S5 55.44(8) . 1_545 ? Pb13 S1 S5 122.76(11) 3_445 1_545 ? S35 S1 S5 108.30(13) 3_455 1_545 ? S35 S1 S5 70.28(10) 3_445 1_545 ? As4 S1 S5 97.13(13) 1_545 . ? Sb4 S1 S5 97.13(13) 1_545 . ? Sb4 S1 S5 41.04(8) . . ? Pb2 S1 S5 55.44(8) . . ? Pb13 S1 S5 122.76(11) 3_445 . ? S35 S1 S5 70.28(10) 3_455 . ? S35 S1 S5 108.30(13) 3_445 . ? S5 S1 S5 69.49(10) 1_545 . ? As4 S1 Pb16 70.99(7) 1_545 3_445 ? Sb4 S1 Pb16 70.99(7) 1_545 3_445 ? Sb4 S1 Pb16 122.66(14) . 3_445 ? Pb2 S1 Pb16 140.56(8) . 3_445 ? Pb13 S1 Pb16 76.90(9) 3_445 3_445 ? S35 S1 Pb16 128.44(14) 3_455 3_445 ? S35 S1 Pb16 88.85(8) 3_445 3_445 ? S5 S1 Pb16 107.14(5) 1_545 3_445 ? S5 S1 Pb16 159.19(14) . 3_445 ? As4 S1 Sb20 70.99(7) 1_545 3_445 ? Sb4 S1 Sb20 70.99(7) 1_545 3_445 ? Sb4 S1 Sb20 122.66(14) . 3_445 ? Pb2 S1 Sb20 140.56(8) . 3_445 ? Pb13 S1 Sb20 76.90(9) 3_445 3_445 ? S35 S1 Sb20 128.44(14) 3_455 3_445 ? S35 S1 Sb20 88.85(8) 3_445 3_445 ? S5 S1 Sb20 107.14(5) 1_545 3_445 ? S5 S1 Sb20 159.19(14) . 3_445 ? Pb16 S1 Sb20 0.00(6) 3_445 3_445 ? Sb61 S2 Sb61 76.3(7) 4 7 ? Sb61 S2 Pb3 89.90(19) 4 . ? Sb61 S2 Pb3 89.90(19) 7 . ? Sb61 S2 Sb3 170.1(3) 4 . ? Sb61 S2 Sb3 95.0(4) 7 . ? Pb3 S2 Sb3 94.74(13) . . ? Sb61 S2 Sb3 95.0(4) 4 1_565 ? Sb61 S2 Sb3 170.1(3) 7 1_565 ? Pb3 S2 Sb3 94.74(13) . 1_565 ? Sb3 S2 Sb3 93.37(17) . 1_565 ? Sb61 S2 Pb14 95.6(4) 4 1_565 ? Sb61 S2 Pb14 165.3(3) 7 1_565 ? Pb3 S2 Pb14 102.50(16) . 1_565 ? Sb3 S2 Pb14 91.89(15) . 1_565 ? Sb3 S2 Pb14 7.80(9) 1_565 1_565 ? Sb61 S2 Pb14 165.3(3) 4 . ? Sb61 S2 Pb14 95.7(4) 7 . ? Pb3 S2 Pb14 102.50(15) . . ? Sb3 S2 Pb14 7.80(9) . . ? Sb3 S2 Pb14 91.89(15) 1_565 . ? Pb14 S2 Pb14 89.4(3) 1_565 . ? Sb61 S2 Sb16 3.0(5) 4 7_565 ? Sb61 S2 Sb16 79.1(2) 7 7_565 ? Pb3 S2 Sb16 88.97(16) . 7_565 ? Sb3 S2 Sb16 173.0(2) . 7_565 ? Sb3 S2 Sb16 92.2(2) 1_565 7_565 ? Pb14 S2 Sb16 93.1(2) 1_565 7_565 ? Pb14 S2 Sb16 167.4(2) . 7_565 ? Sb61 S2 Sb16 79.1(2) 4 7 ? Sb61 S2 Sb16 3.0(5) 7 7 ? Pb3 S2 Sb16 88.97(16) . 7 ? Sb3 S2 Sb16 92.2(2) . 7 ? Sb3 S2 Sb16 173.0(2) 1_565 7 ? Pb14 S2 Sb16 167.4(2) 1_565 7 ? Pb14 S2 Sb16 93.1(2) . 7 ? Sb16 S2 Sb16 81.9(4) 7_565 7 ? Sb61 S2 Sb61 11.2(4) 4 7_565 ? Sb61 S2 Sb61 87.4(3) 7 7_565 ? Pb3 S2 Sb61 89.91(15) . 7_565 ? Sb3 S2 Sb61 174.8(2) . 7_565 ? Sb3 S2 Sb61 83.83(17) 1_565 7_565 ? Pb14 S2 Sb61 84.7(2) 1_565 7_565 ? Pb14 S2 Sb61 167.2(2) . 7_565 ? Sb16 S2 Sb61 8.41(18) 7_565 7_565 ? Sb16 S2 Sb61 90.2(3) 7 7_565 ? Sb61 S2 Sb61 87.4(3) 4 4_545 ? Sb61 S2 Sb61 11.2(4) 7 4_545 ? Pb3 S2 Sb61 89.91(15) . 4_545 ? Sb3 S2 Sb61 83.83(17) . 4_545 ? Sb3 S2 Sb61 174.8(2) 1_565 4_545 ? Pb14 S2 Sb61 167.2(2) 1_565 4_545 ? Pb14 S2 Sb61 84.7(2) . 4_545 ? Sb16 S2 Sb61 90.2(3) 7_565 4_545 ? Sb16 S2 Sb61 8.41(18) 7 4_545 ? Sb61 S2 Sb61 98.6(3) 7_565 4_545 ? Sb61 S2 Pb14 106.3(3) 4 5 ? Sb61 S2 Pb14 63.7(3) 7 5 ? Pb3 S2 Pb14 143.50(8) . 5 ? Sb3 S2 Pb14 65.10(12) . 5 ? Sb3 S2 Pb14 115.53(18) 1_565 5 ? Pb14 S2 Pb14 107.99(16) 1_565 5 ? Pb14 S2 Pb14 59.0(2) . 5 ? Sb16 S2 Pb14 108.6(2) 7_565 5 ? Sb16 S2 Pb14 63.4(2) 7 5 ? Sb61 S2 Pb14 112.1(2) 7_565 5 ? Sb61 S2 Pb14 59.27(17) 4_545 5 ? Sb3 S3 Pb14 2.0(3) . . ? Sb3 S3 Pb1 102.58(14) . 1_545 ? Pb14 S3 Pb1 101.18(17) . 1_545 ? Sb3 S3 Pb1 102.58(14) . . ? Pb14 S3 Pb1 101.18(17) . . ? Pb1 S3 Pb1 87.13(12) 1_545 . ? Sb3 S3 Sb1 93.01(15) . . ? Pb14 S3 Sb1 91.56(18) . . ? Pb1 S3 Sb1 87.16(11) 1_545 . ? Pb1 S3 Sb1 9.80(6) . . ? Sb3 S3 Sb1 93.00(15) . 1_545 ? Pb14 S3 Sb1 91.56(18) . 1_545 ? Pb1 S3 Sb1 9.80(6) 1_545 1_545 ? Pb1 S3 Sb1 87.16(11) . 1_545 ? Sb1 S3 Sb1 85.52(15) . 1_545 ? Sb3 S3 Pb3 97.60(13) . 1_545 ? Pb14 S3 Pb3 99.04(17) . 1_545 ? Pb1 S3 Pb3 90.63(4) 1_545 1_545 ? Pb1 S3 Pb3 159.70(16) . 1_545 ? Sb1 S3 Pb3 169.40(17) . 1_545 ? Sb1 S3 Pb3 94.00(6) 1_545 1_545 ? Sb3 S3 Pb3 97.60(13) . . ? Pb14 S3 Pb3 99.05(17) . . ? Pb1 S3 Pb3 159.70(16) 1_545 . ? Pb1 S3 Pb3 90.63(4) . . ? Sb1 S3 Pb3 94.00(6) . . ? Sb1 S3 Pb3 169.40(17) 1_545 . ? Pb3 S3 Pb3 84.52(11) 1_545 . ? Sb3 S3 S33 51.44(11) . 3_445 ? Pb14 S3 S33 50.09(14) . 3_445 ? Pb1 S3 S33 51.16(9) 1_545 3_445 ? Pb1 S3 S33 98.70(13) . 3_445 ? Sb1 S3 S33 91.15(13) . 3_445 ? Sb1 S3 S33 41.68(11) 1_545 3_445 ? Pb3 S3 S33 95.53(6) 1_545 3_445 ? Pb3 S3 S33 148.88(14) . 3_445 ? Sb3 S3 S33 51.44(11) . 3_455 ? Pb14 S3 S33 50.09(14) . 3_455 ? Pb1 S3 S33 98.70(13) 1_545 3_455 ? Pb1 S3 S33 51.15(9) . 3_455 ? Sb1 S3 S33 41.68(11) . 3_455 ? Sb1 S3 S33 91.15(13) 1_545 3_455 ? Pb3 S3 S33 148.88(14) 1_545 3_455 ? Pb3 S3 S33 95.53(6) . 3_455 ? S33 S3 S33 68.77(10) 3_445 3_455 ? Sb3 S3 S2 50.30(10) . 1_545 ? Pb14 S3 S2 51.67(15) . 1_545 ? Pb1 S3 S2 96.78(7) 1_545 1_545 ? Pb1 S3 S2 152.83(15) . 1_545 ? Sb1 S3 S2 143.14(16) . 1_545 ? Sb1 S3 S2 92.28(9) 1_545 1_545 ? Pb3 S3 S2 47.44(8) 1_545 1_545 ? Pb3 S3 S2 94.40(12) . 1_545 ? S33 S3 S2 64.60(10) 3_445 1_545 ? S33 S3 S2 101.74(12) 3_455 1_545 ? Sb3 S3 S2 50.30(10) . . ? Pb14 S3 S2 51.66(15) . . ? Pb1 S3 S2 152.83(15) 1_545 . ? Pb1 S3 S2 96.78(7) . . ? Sb1 S3 S2 92.28(9) . . ? Sb1 S3 S2 143.13(16) 1_545 . ? Pb3 S3 S2 94.40(12) 1_545 . ? Pb3 S3 S2 47.44(8) . . ? S33 S3 S2 101.74(13) 3_445 . ? S33 S3 S2 64.60(10) 3_455 . ? S2 S3 S2 68.09(10) 1_545 . ? Sb6 S4 Sb6 98.61(17) 1_545 . ? Sb6 S4 Pb4 92.28(12) 1_545 . ? Sb6 S4 Pb4 92.28(12) . . ? Sb6 S4 Sb4 172.90(15) 1_545 . ? Sb6 S4 Sb4 87.71(5) . . ? Pb4 S4 Sb4 90.69(11) . . ? Sb6 S4 As4 87.71(5) 1_545 1_545 ? Sb6 S4 As4 172.90(15) . 1_545 ? Pb4 S4 As4 90.69(11) . 1_545 ? Sb4 S4 As4 85.80(13) . 1_545 ? Sb6 S4 Sb4 87.71(5) 1_545 1_545 ? Sb6 S4 Sb4 172.90(15) . 1_545 ? Pb4 S4 Sb4 90.69(11) . 1_545 ? Sb4 S4 Sb4 85.80(13) . 1_545 ? As4 S4 Sb4 0.00(8) 1_545 1_545 ? Sb6 S4 Sb7 89.07(14) 1_545 . ? Sb6 S4 Sb7 10.10(5) . . ? Pb4 S4 Sb7 89.35(11) . . ? Sb4 S4 Sb7 97.42(4) . . ? As4 S4 Sb7 176.78(12) 1_545 . ? Sb4 S4 Sb7 176.78(12) 1_545 . ? Sb6 S4 Sb7 10.10(5) 1_545 1_545 ? Sb6 S4 Sb7 89.07(14) . 1_545 ? Pb4 S4 Sb7 89.35(11) . 1_545 ? Sb4 S4 Sb7 176.78(12) . 1_545 ? As4 S4 Sb7 97.42(4) 1_545 1_545 ? Sb4 S4 Sb7 97.42(4) 1_545 1_545 ? Sb7 S4 Sb7 79.37(12) . 1_545 ? Sb6 S4 Pb1 61.30(8) 1_545 1_545 ? Sb6 S4 Pb1 116.84(15) . 1_545 ? Pb4 S4 Pb1 142.05(6) . 1_545 ? Sb4 S4 Pb1 112.93(15) . 1_545 ? As4 S4 Pb1 63.46(7) 1_545 1_545 ? Sb4 S4 Pb1 63.46(7) 1_545 1_545 ? Sb7 S4 Pb1 114.92(14) . 1_545 ? Sb7 S4 Pb1 68.70(8) 1_545 1_545 ? Sb6 S4 Pb1 116.84(15) 1_545 . ? Sb6 S4 Pb1 61.31(8) . . ? Pb4 S4 Pb1 142.05(6) . . ? Sb4 S4 Pb1 63.46(7) . . ? As4 S4 Pb1 112.93(15) 1_545 . ? Sb4 S4 Pb1 112.93(15) 1_545 . ? Sb7 S4 Pb1 68.70(8) . . ? Sb7 S4 Pb1 114.92(14) 1_545 . ? Pb1 S4 Pb1 75.81(11) 1_545 . ? Sb6 S4 Sb1 115.07(15) 1_545 . ? Sb6 S4 Sb1 65.99(9) . . ? Pb4 S4 Sb1 146.53(6) . . ? Sb4 S4 Sb1 64.55(9) . . ? As4 S4 Sb1 108.42(14) 1_545 . ? Sb4 S4 Sb1 108.42(14) 1_545 . ? Sb7 S4 Sb1 73.07(9) . . ? Sb7 S4 Sb1 114.10(14) 1_545 . ? Pb1 S4 Sb1 71.16(10) 1_545 . ? Pb1 S4 Sb1 5.11(4) . . ? Sb4 S5 Pb4 103.65(11) . 1_565 ? Sb4 S5 Pb4 103.65(11) . . ? Pb4 S5 Pb4 84.16(9) 1_565 . ? Sb4 S5 Pb2 100.22(11) . 1_565 ? Pb4 S5 Pb2 91.99(3) 1_565 1_565 ? Pb4 S5 Pb2 156.07(13) . 1_565 ? Sb4 S5 Pb2 100.22(11) . . ? Pb4 S5 Pb2 156.07(13) 1_565 . ? Pb4 S5 Pb2 91.99(3) . . ? Pb2 S5 Pb2 81.99(9) 1_565 . ? Sb4 S5 S9 154.44(17) . . ? Pb4 S5 S9 58.90(7) 1_565 . ? Pb4 S5 S9 58.90(7) . . ? Pb2 S5 S9 99.00(10) 1_565 . ? Pb2 S5 S9 99.01(10) . . ? Sb4 S5 S6 146.05(17) . . ? Pb4 S5 S6 101.38(10) 1_565 . ? Pb4 S5 S6 101.38(10) . . ? Pb2 S5 S6 56.16(7) 1_565 . ? Pb2 S5 S6 56.16(7) . . ? S9 S5 S6 59.51(11) . . ? Sb4 S5 S1 47.69(8) . . ? Pb4 S5 S1 150.73(14) 1_565 . ? Pb4 S5 S1 96.22(6) . . ? Pb2 S5 S1 98.49(11) 1_565 . ? Pb2 S5 S1 53.12(7) . . ? S9 S5 S1 144.16(6) . . ? S6 S5 S1 107.18(12) . . ? Sb4 S5 S1 47.68(8) . 1_565 ? Pb4 S5 S1 96.22(6) 1_565 1_565 ? Pb4 S5 S1 150.73(14) . 1_565 ? Pb2 S5 S1 53.12(7) 1_565 1_565 ? Pb2 S5 S1 98.49(11) . 1_565 ? S9 S5 S1 144.16(6) . 1_565 ? S6 S5 S1 107.18(12) . 1_565 ? S1 S5 S1 69.49(10) . 1_565 ? Sb4 S5 S4 52.77(10) . . ? Pb4 S5 S4 95.50(11) 1_565 . ? Pb4 S5 S4 50.88(8) . . ? Pb2 S5 S4 152.97(13) 1_565 . ? Pb2 S5 S4 100.34(6) . . ? S9 S5 S4 107.11(12) . . ? S6 S5 S4 145.85(6) . . ? S1 S5 S4 63.79(10) . . ? S1 S5 S4 100.16(12) 1_565 . ? Sb4 S5 S4 52.77(10) . 1_565 ? Pb4 S5 S4 50.88(8) 1_565 1_565 ? Pb4 S5 S4 95.50(11) . 1_565 ? Pb2 S5 S4 100.34(6) 1_565 1_565 ? Pb2 S5 S4 152.97(13) . 1_565 ? S9 S5 S4 107.11(12) . 1_565 ? S6 S5 S4 145.85(6) . 1_565 ? S1 S5 S4 100.16(12) . 1_565 ? S1 S5 S4 63.80(10) 1_565 1_565 ? S4 S5 S4 65.66(9) . 1_565 ? Sb5 S6 Pb5 99.56(10) . . ? Sb5 S6 Pb5 99.56(10) . 1_565 ? Pb5 S6 Pb5 84.02(10) . 1_565 ? Sb5 S6 Pb2 107.39(11) . 1_565 ? Pb5 S6 Pb2 153.03(13) . 1_565 ? Pb5 S6 Pb2 90.45(4) 1_565 1_565 ? Sb5 S6 Pb2 107.38(11) . . ? Pb5 S6 Pb2 90.45(4) . . ? Pb5 S6 Pb2 153.04(13) 1_565 . ? Pb2 S6 Pb2 82.59(9) 1_565 . ? Sb5 S6 S9 145.74(16) . . ? Pb5 S6 S9 56.97(7) . . ? Pb5 S6 S9 56.97(7) 1_565 . ? Pb2 S6 S9 98.11(10) 1_565 . ? Pb2 S6 S9 98.12(10) . . ? Sb5 S6 S5 156.45(17) . . ? Pb5 S6 S5 97.88(10) . . ? Pb5 S6 S5 97.88(10) 1_565 . ? Pb2 S6 S5 56.68(7) 1_565 . ? Pb2 S6 S5 56.68(7) . . ? S9 S6 S5 57.81(11) . . ? Sb5 S6 S7 46.69(8) . 1_565 ? Pb5 S6 S7 99.05(11) . 1_565 ? Pb5 S6 S7 53.37(7) 1_565 1_565 ? Pb2 S6 S7 98.67(6) 1_565 1_565 ? Pb2 S6 S7 153.41(14) . 1_565 ? S9 S6 S7 107.92(12) . 1_565 ? S5 S6 S7 144.38(6) . 1_565 ? Sb5 S6 S7 46.68(8) . . ? Pb5 S6 S7 53.38(7) . . ? Pb5 S6 S7 99.05(11) 1_565 . ? Pb2 S6 S7 153.41(14) 1_565 . ? Pb2 S6 S7 98.67(6) . . ? S9 S6 S7 107.92(12) . . ? S5 S6 S7 144.38(6) . . ? S7 S6 S7 68.56(10) 1_565 . ? Sb5 S6 S36 53.14(9) . 3_445 ? Pb5 S6 S36 99.50(6) . 3_445 ? Pb5 S6 S36 152.70(13) 1_565 3_445 ? Pb2 S6 S36 97.43(11) 1_565 3_445 ? Pb2 S6 S36 54.26(8) . 3_445 ? S9 S6 S36 145.88(6) . 3_445 ? S5 S6 S36 108.32(12) . 3_445 ? S7 S6 S36 99.47(12) 1_565 3_445 ? S7 S6 S36 63.62(10) . 3_445 ? Sb5 S6 S36 53.14(9) . 3_455 ? Pb5 S6 S36 152.70(13) . 3_455 ? Pb5 S6 S36 99.50(6) 1_565 3_455 ? Pb2 S6 S36 54.26(8) 1_565 3_455 ? Pb2 S6 S36 97.43(11) . 3_455 ? S9 S6 S36 145.88(6) . 3_455 ? S5 S6 S36 108.32(12) . 3_455 ? S7 S6 S36 63.62(10) 1_565 3_455 ? S7 S6 S36 99.47(12) . 3_455 ? S36 S6 S36 65.44(10) 3_445 3_455 ? Sb5 S6 S6 90.0 . 1_565 ? Pb5 S6 S6 132.01(5) . 1_565 ? Pb5 S6 S6 47.99(5) 1_565 1_565 ? Pb2 S6 S6 48.70(5) 1_565 1_565 ? Pb2 S6 S6 131.29(5) . 1_565 ? S9 S6 S6 90.0 . 1_565 ? S5 S6 S6 90.0 . 1_565 ? S7 S6 S6 55.72(5) 1_565 1_565 ? S7 S6 S6 124.28(5) . 1_565 ? S36 S6 S6 122.72(5) 3_445 1_565 ? S36 S6 S6 57.28(5) 3_455 1_565 ? Sb5 S7 Sb5 101.37(15) 1_545 . ? Sb5 S7 Pb5 94.45(11) 1_545 . ? Sb5 S7 Pb5 94.45(11) . . ? Sb5 S7 Pb9 129.30(7) 1_545 7_556 ? Sb5 S7 Pb9 129.30(7) . 7_556 ? Pb5 S7 Pb9 84.18(11) . 7_556 ? Sb5 S7 S23 147.75(15) 1_545 7_556 ? Sb5 S7 S23 87.96(7) . 7_556 ? Pb5 S7 S23 53.78(8) . 7_556 ? Pb9 S7 S23 51.08(8) 7_556 7_556 ? Sb5 S7 S23 87.96(7) 1_545 7_546 ? Sb5 S7 S23 147.75(15) . 7_546 ? Pb5 S7 S23 53.78(8) . 7_546 ? Pb9 S7 S23 51.08(8) 7_556 7_546 ? S23 S7 S23 69.44(11) 7_556 7_546 ? Sb5 S7 S6 96.90(12) 1_545 . ? Sb5 S7 S6 41.29(7) . . ? Pb5 S7 S6 53.60(8) . . ? Pb9 S7 S6 120.79(12) 7_556 . ? S23 S7 S6 69.94(10) 7_556 . ? S23 S7 S6 107.38(13) 7_546 . ? Sb5 S7 S6 41.29(7) 1_545 1_545 ? Sb5 S7 S6 96.90(12) . 1_545 ? Pb5 S7 S6 53.61(8) . 1_545 ? Pb9 S7 S6 120.79(12) 7_556 1_545 ? S23 S7 S6 107.38(13) 7_556 1_545 ? S23 S7 S6 69.94(10) 7_546 1_545 ? S6 S7 S6 68.56(10) . 1_545 ? Sb5 S7 Sb15 119.97(14) 1_545 7_556 ? Sb5 S7 Sb15 68.75(7) . 7_556 ? Pb5 S7 Sb15 143.51(6) . 7_556 ? Pb9 S7 Sb15 82.79(9) 7_556 7_556 ? S23 S7 Sb15 92.23(8) 7_556 7_556 ? S23 S7 Sb15 132.34(13) 7_546 7_556 ? S6 S7 Sb15 106.43(6) . 7_556 ? S6 S7 Sb15 155.57(15) 1_545 7_556 ? Sb5 S7 Sb15 68.74(7) 1_545 7_546 ? Sb5 S7 Sb15 119.97(14) . 7_546 ? Pb5 S7 Sb15 143.51(6) . 7_546 ? Pb9 S7 Sb15 82.79(9) 7_556 7_546 ? S23 S7 Sb15 132.34(13) 7_556 7_546 ? S23 S7 Sb15 92.23(8) 7_546 7_546 ? S6 S7 Sb15 155.57(15) . 7_546 ? S6 S7 Sb15 106.43(6) 1_545 7_546 ? Sb15 S7 Sb15 67.71(7) 7_556 7_546 ? Sb5 S7 S26 111.17(11) 1_545 7_556 ? Sb5 S7 S26 111.17(11) . 7_556 ? Pb5 S7 S26 138.22(15) . 7_556 ? Pb9 S7 S26 54.04(9) 7_556 7_556 ? S23 S7 S26 93.44(12) 7_556 7_556 ? S23 S7 S26 93.44(12) 7_546 7_556 ? S6 S7 S26 145.65(5) . 7_556 ? S6 S7 S26 145.65(5) 1_545 7_556 ? Sb15 S7 S26 42.43(6) 7_556 7_556 ? Sb15 S7 S26 42.43(6) 7_546 7_556 ? Sb5 S7 S32 72.46(10) 1_545 7_556 ? Sb5 S7 S32 72.46(10) . 7_556 ? Pb5 S7 S32 158.63(15) . 7_556 ? Pb9 S7 S32 117.19(13) 7_556 7_556 ? S23 S7 S32 139.33(9) 7_556 7_556 ? S23 S7 S32 139.33(9) 7_546 7_556 ? S6 S7 S32 110.06(12) . 7_556 ? S6 S7 S32 110.06(12) 1_545 7_556 ? Sb15 S7 S32 47.71(7) 7_556 7_556 ? Sb15 S7 S32 47.71(7) 7_546 7_556 ? S26 S7 S32 63.15(11) 7_556 7_556 ? Sb7 S8 Sb7 106.5(2) 1_545 . ? Sb7 S8 Pb7A 91.64(13) 1_545 . ? Sb7 S8 Pb7A 91.64(13) . . ? Sb7 S8 Sb6 95.83(16) 1_545 . ? Sb7 S8 Sb6 11.26(5) . . ? Pb7A S8 Sb6 95.74(13) . . ? Sb7 S8 Sb6 11.27(5) 1_545 1_545 ? Sb7 S8 Sb6 95.83(16) . 1_545 ? Pb7A S8 Sb6 95.74(13) . 1_545 ? Sb6 S8 Sb6 84.98(14) . 1_545 ? Sb7 S8 Pb6 126.75(10) 1_545 . ? Sb7 S8 Pb6 126.75(10) . . ? Pb7A S8 Pb6 88.03(14) . . ? Sb6 S8 Pb6 137.18(7) . . ? Sb6 S8 Pb6 137.19(7) 1_545 . ? Sb7 S8 Pb7B 93.81(15) 1_545 . ? Sb7 S8 Pb7B 93.81(15) . . ? Pb7A S8 Pb7B 3.62(15) . . ? Sb6 S8 Pb7B 98.40(15) . . ? Sb6 S8 Pb7B 98.40(15) 1_545 . ? Pb6 S8 Pb7B 84.40(17) . . ? Sb7 S8 Pb3 123.10(17) 1_545 . ? Sb7 S8 Pb3 65.98(8) . . ? Pb7A S8 Pb3 142.09(6) . . ? Sb6 S8 Pb3 68.40(7) . . ? Sb6 S8 Pb3 115.81(14) 1_545 . ? Pb6 S8 Pb3 82.71(10) . . ? Pb7B S8 Pb3 141.04(8) . . ? Sb7 S8 Pb3 65.98(8) 1_545 1_545 ? Sb7 S8 Pb3 123.10(17) . 1_545 ? Pb7A S8 Pb3 142.09(6) . 1_545 ? Sb6 S8 Pb3 115.81(14) . 1_545 ? Sb6 S8 Pb3 68.40(7) 1_545 1_545 ? Pb6 S8 Pb3 82.71(10) . 1_545 ? Pb7B S8 Pb3 141.04(8) . 1_545 ? Pb3 S8 Pb3 73.00(9) . 1_545 ? Sb7 S8 S13 85.92(9) 1_545 1_545 ? Sb7 S8 S13 147.64(17) . 1_545 ? Pb7A S8 S13 57.59(11) . 1_545 ? Sb6 S8 S13 153.33(17) . 1_545 ? Sb6 S8 S13 96.98(7) 1_545 1_545 ? Pb6 S8 S13 50.25(9) . 1_545 ? Pb7B S8 S13 54.96(13) . 1_545 ? Pb3 S8 S13 131.84(15) . 1_545 ? Pb3 S8 S13 89.26(9) 1_545 1_545 ? Sb7 S8 S13 147.64(17) 1_545 . ? Sb7 S8 S13 85.92(9) . . ? Pb7A S8 S13 57.59(11) . . ? Sb6 S8 S13 96.97(7) . . ? Sb6 S8 S13 153.33(17) 1_545 . ? Pb6 S8 S13 50.25(9) . . ? Pb7B S8 S13 54.96(13) . . ? Pb3 S8 S13 89.26(9) . . ? Pb3 S8 S13 131.84(15) 1_545 . ? S13 S8 S13 69.72(12) 1_545 . ? Sb7 S8 S10 39.43(10) 1_545 1_545 ? Sb7 S8 S10 97.38(15) . 1_545 ? Pb7A S8 S10 53.02(10) . 1_545 ? Sb6 S8 S10 91.45(13) . 1_545 ? Sb6 S8 S10 42.76(9) 1_545 1_545 ? Pb6 S8 S10 123.13(12) . 1_545 ? Pb7B S8 S10 55.64(13) . 1_545 ? Pb3 S8 S10 153.69(16) . 1_545 ? Pb3 S8 S10 103.16(6) 1_545 1_545 ? S13 S8 S10 73.08(10) 1_545 1_545 ? S13 S8 S10 110.59(15) . 1_545 ? Sb8 S9 Pb5 104.02(11) . . ? Sb8 S9 Pb5 104.02(11) . 1_565 ? Pb5 S9 Pb5 83.95(9) . 1_565 ? Sb8 S9 Pb4 98.88(11) . 1_565 ? Pb5 S9 Pb4 157.02(14) . 1_565 ? Pb5 S9 Pb4 92.46(3) 1_565 1_565 ? Sb8 S9 Pb4 98.88(11) . . ? Pb5 S9 Pb4 92.46(3) . . ? Pb5 S9 Pb4 157.02(14) 1_565 . ? Pb4 S9 Pb4 82.01(9) 1_565 . ? Sb8 S9 S5 145.55(17) . . ? Pb5 S9 S5 101.41(10) . . ? Pb5 S9 S5 101.41(10) 1_565 . ? Pb4 S9 S5 56.97(7) 1_565 . ? Pb4 S9 S5 56.97(7) . . ? Sb8 S9 S6 151.77(17) . . ? Pb5 S9 S6 56.91(7) . . ? Pb5 S9 S6 56.92(7) 1_565 . ? Pb4 S9 S6 102.32(10) 1_565 . ? Pb4 S9 S6 102.32(10) . . ? S5 S9 S6 62.68(11) . . ? Sb8 S9 S12 46.83(9) . 1_565 ? Pb5 S9 S12 149.73(14) . 1_565 ? Pb5 S9 S12 94.81(6) 1_565 1_565 ? Pb4 S9 S12 53.08(8) 1_565 1_565 ? Pb4 S9 S12 99.46(11) . 1_565 ? S5 S9 S12 108.44(12) . 1_565 ? S6 S9 S12 144.10(6) . 1_565 ? Sb8 S9 S12 46.83(9) . . ? Pb5 S9 S12 94.81(6) . . ? Pb5 S9 S12 149.73(14) 1_565 . ? Pb4 S9 S12 99.46(11) 1_565 . ? Pb4 S9 S12 53.08(8) . . ? S5 S9 S12 108.44(12) . . ? S6 S9 S12 144.10(6) . . ? S12 S9 S12 71.32(11) 1_565 . ? Sb8 S9 S20 50.05(9) . 7_566 ? Pb5 S9 S20 97.41(11) . 7_566 ? Pb5 S9 S20 53.97(8) 1_565 7_566 ? Pb4 S9 S20 98.75(6) 1_565 7_566 ? Pb4 S9 S20 148.83(13) . 7_566 ? S5 S9 S20 147.08(6) . 7_566 ? S6 S9 S20 107.85(12) . 7_566 ? S12 S9 S20 59.22(11) 1_565 7_566 ? S12 S9 S20 96.51(13) . 7_566 ? Sb8 S9 S20 50.05(9) . 7_556 ? Pb5 S9 S20 53.97(8) . 7_556 ? Pb5 S9 S20 97.41(11) 1_565 7_556 ? Pb4 S9 S20 148.83(14) 1_565 7_556 ? Pb4 S9 S20 98.75(6) . 7_556 ? S5 S9 S20 147.08(6) . 7_556 ? S6 S9 S20 107.85(12) . 7_556 ? S12 S9 S20 96.51(13) 1_565 7_556 ? S12 S9 S20 59.22(11) . 7_556 ? S20 S9 S20 64.84(10) 7_566 7_556 ? Sb7 S10 Sb6 16.78(8) . . ? Sb7 S10 Pb7A 93.22(14) . 1_565 ? Sb6 S10 Pb7A 105.26(14) . 1_565 ? Sb7 S10 Pb7A 93.22(14) . . ? Sb6 S10 Pb7A 105.26(14) . . ? Pb7A S10 Pb7A 86.64(15) 1_565 . ? Sb7 S10 Pb4 106.91(13) . . ? Sb6 S10 Pb4 94.56(12) . . ? Pb7A S10 Pb4 159.86(17) 1_565 . ? Pb7A S10 Pb4 91.60(5) . . ? Sb7 S10 Pb4 106.91(13) . 1_565 ? Sb6 S10 Pb4 94.56(12) . 1_565 ? Pb7A S10 Pb4 91.60(5) 1_565 1_565 ? Pb7A S10 Pb4 159.86(17) . 1_565 ? Pb4 S10 Pb4 83.19(10) . 1_565 ? Sb7 S10 Pb7B 98.36(18) . 1_565 ? Sb6 S10 Pb7B 110.99(18) . 1_565 ? Pb7A S10 Pb7B 6.19(9) 1_565 1_565 ? Pb7A S10 Pb7B 82.95(16) . 1_565 ? Pb4 S10 Pb7B 154.4(2) . 1_565 ? Pb4 S10 Pb7B 93.37(10) 1_565 1_565 ? Sb7 S10 Pb7B 98.36(18) . . ? Sb6 S10 Pb7B 110.99(18) . . ? Pb7A S10 Pb7B 82.95(16) 1_565 . ? Pb7A S10 Pb7B 6.19(9) . . ? Pb4 S10 Pb7B 93.37(10) . . ? Pb4 S10 Pb7B 154.4(2) 1_565 . ? Pb7B S10 Pb7B 78.9(2) 1_565 . ? Sb7 S10 S12 142.79(6) . 1_565 ? Sb6 S10 S12 141.53(8) . 1_565 ? Pb7A S10 S12 59.45(10) 1_565 1_565 ? Pb7A S10 S12 108.41(16) . 1_565 ? Pb4 S10 S12 102.47(13) . 1_565 ? Pb4 S10 S12 54.44(9) 1_565 1_565 ? Pb7B S10 S12 56.57(15) 1_565 1_565 ? Pb7B S10 S12 102.23(19) . 1_565 ? Sb7 S10 S12 142.79(6) . . ? Sb6 S10 S12 141.53(8) . . ? Pb7A S10 S12 108.41(16) 1_565 . ? Pb7A S10 S12 59.45(10) . . ? Pb4 S10 S12 54.44(9) . . ? Pb4 S10 S12 102.47(13) 1_565 . ? Pb7B S10 S12 102.23(19) 1_565 . ? Pb7B S10 S12 56.57(15) . . ? S12 S10 S12 73.83(12) 1_565 . ? Sb7 S10 S8 44.22(9) . . ? Sb6 S10 S8 55.46(10) . . ? Pb7A S10 S8 97.28(13) 1_565 . ? Pb7A S10 S8 49.85(11) . . ? Pb4 S10 S8 96.86(7) . . ? Pb4 S10 S8 150.00(15) 1_565 . ? Pb7B S10 S8 98.52(16) 1_565 . ? Pb7B S10 S8 55.53(16) . . ? S12 S10 S8 151.54(17) 1_565 . ? S12 S10 S8 101.76(8) . . ? Sb7 S10 S8 44.22(9) . 1_565 ? Sb6 S10 S8 55.46(10) . 1_565 ? Pb7A S10 S8 49.85(11) 1_565 1_565 ? Pb7A S10 S8 97.27(13) . 1_565 ? Pb4 S10 S8 150.00(15) . 1_565 ? Pb4 S10 S8 96.87(7) 1_565 1_565 ? Pb7B S10 S8 55.53(16) 1_565 1_565 ? Pb7B S10 S8 98.52(16) . 1_565 ? S12 S10 S8 101.76(8) 1_565 1_565 ? S12 S10 S8 151.54(17) . 1_565 ? S8 S10 S8 68.42(11) . 1_565 ? Sb9 S11 Pb10 100.78(12) . 7 ? Sb9 S11 Pb10 100.78(12) . 7_565 ? Pb10 S11 Pb10 86.66(11) 7 7_565 ? Sb9 S11 Pb6 100.80(11) . . ? Pb10 S11 Pb6 90.48(3) 7 . ? Pb10 S11 Pb6 158.38(15) 7_565 . ? Sb9 S11 Pb6 100.80(11) . 1_565 ? Pb10 S11 Pb6 158.38(15) 7 1_565 ? Pb10 S11 Pb6 90.48(3) 7_565 1_565 ? Pb6 S11 Pb6 84.34(10) . 1_565 ? Sb9 S11 S15 51.23(10) . 1_565 ? Pb10 S11 S15 151.99(15) 7 1_565 ? Pb10 S11 S15 96.71(6) 7_565 1_565 ? Pb6 S11 S15 95.83(12) . 1_565 ? Pb6 S11 S15 49.63(8) 1_565 1_565 ? Sb9 S11 S15 51.23(10) . . ? Pb10 S11 S15 96.71(6) 7 . ? Pb10 S11 S15 151.99(15) 7_565 . ? Pb6 S11 S15 49.63(8) . . ? Pb6 S11 S15 95.83(12) 1_565 . ? S15 S11 S15 67.85(11) 1_565 . ? Sb9 S11 S14 50.67(10) . 1_565 ? Pb10 S11 S14 96.69(12) 7 1_565 ? Pb10 S11 S14 50.12(8) 7_565 1_565 ? Pb6 S11 S14 151.39(15) . 1_565 ? Pb6 S11 S14 97.86(7) 1_565 1_565 ? S15 S11 S14 65.80(11) 1_565 1_565 ? S15 S11 S14 101.90(14) . 1_565 ? Sb9 S11 S14 50.67(10) . . ? Pb10 S11 S14 50.13(9) 7 . ? Pb10 S11 S14 96.69(12) 7_565 . ? Pb6 S11 S14 97.86(7) . . ? Pb6 S11 S14 151.39(15) 1_565 . ? S15 S11 S14 101.90(14) 1_565 . ? S15 S11 S14 65.80(11) . . ? S14 S11 S14 67.01(11) 1_565 . ? Sb9 S11 S27 146.39(5) . 7 ? Pb10 S11 S27 61.74(8) 7 7 ? Pb10 S11 S27 106.13(12) 7_565 7 ? Pb6 S11 S27 54.36(8) . 7 ? Pb6 S11 S27 98.76(12) 1_565 7 ? S15 S11 S27 141.45(15) 1_565 7 ? S15 S11 S27 99.85(9) . 7 ? S14 S11 S27 151.00(15) 1_565 7 ? S14 S11 S27 105.68(8) . 7 ? Sb9 S11 S27 146.39(5) . 7_565 ? Pb10 S11 S27 106.13(12) 7 7_565 ? Pb10 S11 S27 61.74(8) 7_565 7_565 ? Pb6 S11 S27 98.76(12) . 7_565 ? Pb6 S11 S27 54.37(8) 1_565 7_565 ? S15 S11 S27 99.85(9) 1_565 7_565 ? S15 S11 S27 141.45(15) . 7_565 ? S14 S11 S27 105.68(8) 1_565 7_565 ? S14 S11 S27 151.00(15) . 7_565 ? S27 S11 S27 66.38(10) 7 7_565 ? Sb9 S11 S28 138.45(18) . 7 ? Pb10 S11 S28 52.68(8) 7 7 ? Pb10 S11 S28 52.68(8) 7_565 7 ? Pb6 S11 S28 109.59(11) . 7 ? Pb6 S11 S28 109.59(11) 1_565 7 ? S15 S11 S28 146.07(5) 1_565 7 ? S15 S11 S28 146.07(5) . 7 ? S14 S11 S28 96.60(13) 1_565 7 ? S14 S11 S28 96.60(13) . 7 ? S27 S11 S28 55.34(10) 7 7 ? S27 S11 S28 55.34(10) 7_565 7 ? As8 S12 Sb8 0.00(8) 1_545 1_545 ? As8 S12 Sb8 106.06(17) 1_545 . ? Sb8 S12 Sb8 106.06(17) 1_545 . ? As8 S12 Pb4 97.11(12) 1_545 . ? Sb8 S12 Pb4 97.11(12) 1_545 . ? Sb8 S12 Pb4 97.11(12) . . ? As8 S12 Sb11 82.19(12) 1_545 . ? Sb8 S12 Sb11 82.19(12) 1_545 . ? Sb8 S12 Sb11 82.18(12) . . ? Pb4 S12 Sb11 178.81(17) . . ? As8 S12 Pb7B 124.70(10) 1_545 . ? Sb8 S12 Pb7B 124.70(10) 1_545 . ? Sb8 S12 Pb7B 124.70(10) . . ? Pb4 S12 Pb7B 96.9(2) . . ? Sb11 S12 Pb7B 84.27(19) . . ? As8 S12 Pb7A 126.12(9) 1_545 . ? Sb8 S12 Pb7A 126.12(9) 1_545 . ? Sb8 S12 Pb7A 126.12(9) . . ? Pb4 S12 Pb7A 89.52(14) . . ? Sb11 S12 Pb7A 91.67(15) . . ? Pb7B S12 Pb7A 7.40(10) . . ? As8 S12 S10 86.18(7) 1_545 1_545 ? Sb8 S12 S10 86.18(7) 1_545 1_545 ? Sb8 S12 S10 153.27(17) . 1_545 ? Pb4 S12 S10 57.22(10) . 1_545 ? Sb11 S12 S10 123.60(13) . 1_545 ? Pb7B S12 S10 58.75(15) . 1_545 ? Pb7A S12 S10 53.64(10) . 1_545 ? As8 S12 S10 153.27(17) 1_545 . ? Sb8 S12 S10 153.27(17) 1_545 . ? Sb8 S12 S10 86.18(7) . . ? Pb4 S12 S10 57.22(10) . . ? Sb11 S12 S10 123.61(13) . . ? Pb7B S12 S10 58.75(15) . . ? Pb7A S12 S10 53.64(10) . . ? S10 S12 S10 73.83(12) 1_545 . ? As8 S12 S9 100.44(14) 1_545 . ? Sb8 S12 S9 100.44(14) 1_545 . ? Sb8 S12 S9 41.37(8) . . ? Pb4 S12 S9 56.72(9) . . ? Sb11 S12 S9 122.43(12) . . ? Pb7B S12 S9 131.37(15) . . ? Pb7A S12 S9 126.48(13) . . ? S10 S12 S9 113.93(15) 1_545 . ? S10 S12 S9 72.86(10) . . ? As8 S12 S9 41.37(8) 1_545 1_545 ? Sb8 S12 S9 41.37(8) 1_545 1_545 ? Sb8 S12 S9 100.44(14) . 1_545 ? Pb4 S12 S9 56.72(9) . 1_545 ? Sb11 S12 S9 122.43(12) . 1_545 ? Pb7B S12 S9 131.37(15) . 1_545 ? Pb7A S12 S9 126.48(13) . 1_545 ? S10 S12 S9 72.86(10) 1_545 1_545 ? S10 S12 S9 113.93(15) . 1_545 ? S9 S12 S9 71.32(11) . 1_545 ? Sb10 S13 Pb6 97.57(12) . 1_565 ? Sb10 S13 Pb6 97.57(12) . . ? Pb6 S13 Pb6 89.81(12) 1_565 . ? Sb10 S13 Pb7B 103.9(2) . 1_565 ? Pb6 S13 Pb7B 90.71(10) 1_565 1_565 ? Pb6 S13 Pb7B 158.2(2) . 1_565 ? Sb10 S13 Pb7B 103.9(2) . . ? Pb6 S13 Pb7B 158.2(2) 1_565 . ? Pb6 S13 Pb7B 90.71(10) . . ? Pb7B S13 Pb7B 80.9(2) 1_565 . ? Sb10 S13 Pb7A 111.15(15) . . ? Pb6 S13 Pb7A 151.24(19) 1_565 . ? Pb6 S13 Pb7A 87.91(6) . . ? Pb7B S13 Pb7A 81.26(12) 1_565 . ? Pb7B S13 Pb7A 7.47(10) . . ? Sb10 S13 Pb7A 111.15(15) . 1_565 ? Pb6 S13 Pb7A 87.90(6) 1_565 1_565 ? Pb6 S13 Pb7A 151.24(19) . 1_565 ? Pb7B S13 Pb7A 7.47(10) 1_565 1_565 ? Pb7B S13 Pb7A 81.26(12) . 1_565 ? Pb7A S13 Pb7A 80.60(11) . 1_565 ? Sb10 S13 S17 48.29(11) . 1_565 ? Pb6 S13 S17 89.99(8) 1_565 1_565 ? Pb6 S13 S17 145.45(18) . 1_565 ? Pb7B S13 S17 56.31(18) 1_565 1_565 ? Pb7B S13 S17 101.7(2) . 1_565 ? Pb7A S13 S17 107.73(16) . 1_565 ? Pb7A S13 S17 63.24(13) 1_565 1_565 ? Sb10 S13 S17 48.29(11) . . ? Pb6 S13 S17 145.45(18) 1_565 . ? Pb6 S13 S17 89.99(8) . . ? Pb7B S13 S17 101.7(2) 1_565 . ? Pb7B S13 S17 56.31(18) . . ? Pb7A S13 S17 63.24(13) . . ? Pb7A S13 S17 107.73(16) 1_565 . ? S17 S13 S17 71.39(13) 1_565 . ? Sb10 S13 S8 145.10(6) . 1_565 ? Pb6 S13 S8 58.02(9) 1_565 1_565 ? Pb6 S13 S8 106.10(15) . 1_565 ? Pb7B S13 S8 56.67(17) 1_565 1_565 ? Pb7B S13 S8 101.10(19) . 1_565 ? Pb7A S13 S8 95.24(14) . 1_565 ? Pb7A S13 S8 49.60(12) 1_565 1_565 ? S17 S13 S8 102.96(9) 1_565 1_565 ? S17 S13 S8 153.04(18) . 1_565 ? Sb10 S13 S8 145.10(6) . . ? Pb6 S13 S8 106.10(15) 1_565 . ? Pb6 S13 S8 58.02(9) . . ? Pb7B S13 S8 101.09(19) 1_565 . ? Pb7B S13 S8 56.67(17) . . ? Pb7A S13 S8 49.60(12) . . ? Pb7A S13 S8 95.23(14) 1_565 . ? S17 S13 S8 153.04(18) 1_565 . ? S17 S13 S8 102.96(9) . . ? S8 S13 S8 69.72(12) 1_565 . ? Sb9 S14 Sb9 91.04(16) . 1_545 ? Sb9 S14 Pb10 92.44(12) . 7 ? Sb9 S14 Pb10 92.44(12) 1_545 7 ? Sb9 S14 Sb13 175.46(18) . 7_545 ? Sb9 S14 Sb13 91.47(4) 1_545 7_545 ? Pb10 S14 Sb13 91.23(12) 7 7_545 ? Sb9 S14 Sb13 91.47(4) . 7 ? Sb9 S14 Sb13 175.46(18) 1_545 7 ? Pb10 S14 Sb13 91.23(12) 7 7 ? Sb13 S14 Sb13 85.78(14) 7_545 7 ? Sb9 S14 S11 91.61(14) . 1_545 ? Sb9 S14 S11 40.56(8) 1_545 1_545 ? Pb10 S14 S11 51.89(9) 7 1_545 ? Sb13 S14 S11 92.76(8) 7_545 1_545 ? Sb13 S14 S11 143.09(17) 7 1_545 ? Sb9 S14 S11 40.56(8) . . ? Sb9 S14 S11 91.61(14) 1_545 . ? Pb10 S14 S11 51.89(9) 7 . ? Sb13 S14 S11 143.09(17) 7_545 . ? Sb13 S14 S11 92.76(8) 7 . ? S11 S14 S11 67.01(11) 1_545 . ? Sb9 S14 S24 143.89(17) . 7_545 ? Sb9 S14 S24 91.67(8) 1_545 7_545 ? Pb10 S14 S24 51.47(9) 7 7_545 ? Sb13 S14 S24 39.78(8) 7_545 7_545 ? Sb13 S14 S24 88.53(13) 7 7_545 ? S11 S14 S24 68.19(10) 1_545 7_545 ? S11 S14 S24 103.36(14) . 7_545 ? Sb9 S14 S24 91.66(8) . 7 ? Sb9 S14 S24 143.90(17) 1_545 7 ? Pb10 S14 S24 51.47(9) 7 7 ? Sb13 S14 S24 88.53(13) 7_545 7 ? Sb13 S14 S24 39.78(8) 7 7 ? S11 S14 S24 103.36(14) 1_545 7 ? S11 S14 S24 68.19(10) . 7 ? S24 S14 S24 66.16(11) 7_545 7 ? Sb9 S14 Sb13 67.86(10) . . ? Sb9 S14 Sb13 67.86(10) 1_545 . ? Pb10 S14 Sb13 150.95(17) 7 . ? Sb13 S14 Sb13 109.68(12) 7_545 . ? Sb13 S14 Sb13 109.68(12) 7 . ? S11 S14 Sb13 105.50(12) 1_545 . ? S11 S14 Sb13 105.50(12) . . ? S24 S14 Sb13 144.75(7) 7_545 . ? S24 S14 Sb13 144.75(7) 7 . ? Sb9 S14 S21 134.35(8) . 7 ? Sb9 S14 S21 134.35(8) 1_545 7 ? Pb10 S14 S21 90.40(14) 7 7 ? Sb13 S14 S21 42.91(7) 7_545 7 ? Sb13 S14 S21 42.91(7) 7 7 ? S11 S14 S21 124.40(13) 1_545 7 ? S11 S14 S21 124.40(13) . 7 ? S24 S14 S21 56.22(10) 7_545 7 ? S24 S14 S21 56.22(10) 7 7 ? Sb13 S14 S21 118.64(15) . 7 ? Sb9 S14 S15 45.57(8) . . ? Sb9 S14 S15 45.57(8) 1_545 . ? Pb10 S14 S15 90.96(14) 7 . ? Sb13 S14 S15 137.04(7) 7_545 . ? Sb13 S14 S15 137.04(7) 7 . ? S11 S14 S15 56.61(10) 1_545 . ? S11 S14 S15 56.61(10) . . ? S24 S14 S15 124.80(13) 7_545 . ? S24 S14 S15 124.80(13) 7 . ? Sb13 S14 S15 59.99(10) . . ? S21 S14 S15 178.64(17) 7 . ? Sb9 S15 Sb9 91.32(15) 1_545 . ? Sb9 S15 Pb6 94.95(12) 1_545 . ? Sb9 S15 Pb6 94.94(12) . . ? Sb9 S15 Sb10 176.68(18) 1_545 . ? Sb9 S15 Sb10 90.38(4) . . ? Pb6 S15 Sb10 87.75(12) . . ? Sb9 S15 As10 90.38(4) 1_545 1_545 ? Sb9 S15 As10 176.68(18) . 1_545 ? Pb6 S15 As10 87.75(12) . 1_545 ? Sb10 S15 As10 87.79(14) . 1_545 ? Sb9 S15 Sb10 90.38(4) 1_545 1_545 ? Sb9 S15 Sb10 176.68(18) . 1_545 ? Pb6 S15 Sb10 87.75(12) . 1_545 ? Sb10 S15 Sb10 87.79(14) . 1_545 ? As10 S15 Sb10 0.00(10) 1_545 1_545 ? Sb9 S15 S11 41.08(8) 1_545 1_545 ? Sb9 S15 S11 92.55(13) . 1_545 ? Pb6 S15 S11 53.92(9) . 1_545 ? Sb10 S15 S11 141.67(17) . 1_545 ? As10 S15 S11 90.61(8) 1_545 1_545 ? Sb10 S15 S11 90.61(8) 1_545 1_545 ? Sb9 S15 S11 92.55(13) 1_545 . ? Sb9 S15 S11 41.08(8) . . ? Pb6 S15 S11 53.92(9) . . ? Sb10 S15 S11 90.61(8) . . ? As10 S15 S11 141.67(17) 1_545 . ? Sb10 S15 S11 141.67(17) 1_545 . ? S11 S15 S11 67.85(11) 1_545 . ? Sb9 S15 S17 134.29(8) 1_545 . ? Sb9 S15 S17 134.29(8) . . ? Pb6 S15 S17 85.45(14) . . ? Sb10 S15 S17 43.91(7) . . ? As10 S15 S17 43.91(7) 1_545 . ? Sb10 S15 S17 43.91(7) 1_545 . ? S11 S15 S17 122.41(14) 1_545 . ? S11 S15 S17 122.41(14) . . ? Sb9 S15 Sb14 111.96(12) 1_545 . ? Sb9 S15 Sb14 111.97(12) . . ? Pb6 S15 Sb14 140.56(16) . . ? Sb10 S15 Sb14 64.73(9) . . ? As10 S15 Sb14 64.73(9) 1_545 . ? Sb10 S15 Sb14 64.73(9) 1_545 . ? S11 S15 Sb14 145.71(6) 1_545 . ? S11 S15 Sb14 145.71(6) . . ? S17 S15 Sb14 55.11(11) . . ? Sb11 S16 Sb11 99.9(2) 1_565 . ? Sb11 S16 Pb8 94.61(18) 1_565 . ? Sb11 S16 Pb8 94.61(18) . . ? Sb11 S16 Pb7B 153.4(3) 1_565 . ? Sb11 S16 Pb7B 86.91(11) . . ? Pb8 S16 Pb7B 110.56(18) . . ? Sb11 S16 Pb7B 86.91(11) 1_565 1_565 ? Sb11 S16 Pb7B 153.4(3) . 1_565 ? Pb8 S16 Pb7B 110.56(18) . 1_565 ? Pb7B S16 Pb7B 76.5(2) . 1_565 ? Sb11 S16 S12 108.68(17) 1_565 . ? Sb11 S16 S12 55.86(10) . . ? Pb8 S16 S12 144.39(8) . . ? Pb7B S16 S12 54.45(16) . . ? Pb7B S16 S12 97.6(2) 1_565 . ? Sb11 S16 S12 55.86(10) 1_565 1_565 ? Sb11 S16 S12 108.68(17) . 1_565 ? Pb8 S16 S12 144.39(8) . 1_565 ? Pb7B S16 S12 97.6(2) . 1_565 ? Pb7B S16 S12 54.45(16) 1_565 1_565 ? S12 S16 S12 70.31(14) . 1_565 ? Sb11 S16 S17 89.67(8) 1_565 1_565 ? Sb11 S16 S17 150.2(2) . 1_565 ? Pb8 S16 S17 56.24(11) . 1_565 ? Pb7B S16 S17 97.10(19) . 1_565 ? Pb7B S16 S17 54.35(17) 1_565 1_565 ? S12 S16 S17 146.4(2) . 1_565 ? S12 S16 S17 100.12(11) 1_565 1_565 ? Sb11 S16 S17 150.2(2) 1_565 . ? Sb11 S16 S17 89.67(8) . . ? Pb8 S16 S17 56.24(11) . . ? Pb7B S16 S17 54.35(17) . . ? Pb7B S16 S17 97.10(19) 1_565 . ? S12 S16 S17 100.13(11) . . ? S12 S16 S17 146.4(2) 1_565 . ? S17 S16 S17 69.54(14) 1_565 . ? Sb11 S16 Pb7A 148.8(2) 1_565 . ? Sb11 S16 Pb7A 89.18(9) . . ? Pb8 S16 Pb7A 114.50(14) . . ? Pb7B S16 Pb7A 4.70(9) . . ? Pb7B S16 Pb7A 72.96(18) 1_565 . ? S12 S16 Pb7A 52.94(11) . . ? S12 S16 Pb7A 92.94(18) 1_565 . ? S17 S16 Pb7A 97.14(16) 1_565 . ? S17 S16 Pb7A 58.43(12) . . ? Sb11 S16 Pb7A 89.18(9) 1_565 1_565 ? Sb11 S16 Pb7A 148.8(2) . 1_565 ? Pb8 S16 Pb7A 114.50(14) . 1_565 ? Pb7B S16 Pb7A 72.96(18) . 1_565 ? Pb7B S16 Pb7A 4.70(9) 1_565 1_565 ? S12 S16 Pb7A 92.94(18) . 1_565 ? S12 S16 Pb7A 52.93(11) 1_565 1_565 ? S17 S16 Pb7A 58.43(12) 1_565 1_565 ? S17 S16 Pb7A 97.14(16) . 1_565 ? Pb7A S16 Pb7A 69.22(15) . 1_565 ? Sb11 S16 S19 43.53(11) 1_565 1_565 ? Sb11 S16 S19 97.6(2) . 1_565 ? Pb8 S16 S19 51.25(11) . 1_565 ? Pb7B S16 S19 161.4(2) . 1_565 ? Pb7B S16 S19 104.72(11) 1_565 1_565 ? S12 S16 S19 141.67(19) . 1_565 ? S12 S16 S19 98.02(10) 1_565 1_565 ? S17 S16 S19 70.19(12) 1_565 1_565 ? S17 S16 S19 107.45(18) . 1_565 ? Pb7A S16 S19 164.47(17) . 1_565 ? Pb7A S16 S19 109.10(7) 1_565 1_565 ? As10 S17 Sb10 0.00(6) 1_545 1_545 ? As10 S17 Sb10 102.66(19) 1_545 . ? Sb10 S17 Sb10 102.66(19) 1_545 . ? As10 S17 Pb8 151.4(2) 1_545 . ? Sb10 S17 Pb8 151.4(2) 1_545 . ? Sb10 S17 Pb8 81.11(6) . . ? As10 S17 Pb8 81.11(6) 1_545 1_545 ? Sb10 S17 Pb8 81.11(6) 1_545 1_545 ? Sb10 S17 Pb8 151.4(2) . 1_545 ? Pb8 S17 Pb8 82.76(13) . 1_545 ? As10 S17 Pb7B 99.90(17) 1_545 . ? Sb10 S17 Pb7B 99.90(17) 1_545 . ? Sb10 S17 Pb7B 99.90(17) . . ? Pb8 S17 Pb7B 107.46(17) . . ? Pb8 S17 Pb7B 107.46(17) 1_545 . ? As10 S17 S13 101.31(16) 1_545 . ? Sb10 S17 S13 101.31(16) 1_545 . ? Sb10 S17 S13 44.35(10) . . ? Pb8 S17 S13 100.84(6) . . ? Pb8 S17 S13 163.6(2) 1_545 . ? Pb7B S17 S13 56.17(14) . . ? As10 S17 S13 44.36(10) 1_545 1_545 ? Sb10 S17 S13 44.36(10) 1_545 1_545 ? Sb10 S17 S13 101.31(16) . 1_545 ? Pb8 S17 S13 163.6(2) . 1_545 ? Pb8 S17 S13 100.84(6) 1_545 1_545 ? Pb7B S17 S13 56.17(14) . 1_545 ? S13 S17 S13 71.39(13) . 1_545 ? As10 S17 Pb7A 97.65(14) 1_545 . ? Sb10 S17 Pb7A 97.65(14) 1_545 . ? Sb10 S17 Pb7A 97.65(14) . . ? Pb8 S17 Pb7A 110.09(14) . . ? Pb8 S17 Pb7A 110.09(14) 1_545 . ? Pb7B S17 Pb7A 3.67(15) . . ? S13 S17 Pb7A 53.60(10) . . ? S13 S17 Pb7A 53.60(10) 1_545 . ? As10 S17 Sb14 72.85(13) 1_545 . ? Sb10 S17 Sb14 72.85(13) 1_545 . ? Sb10 S17 Sb14 72.85(13) . . ? Pb8 S17 Sb14 81.48(12) . . ? Pb8 S17 Sb14 81.48(12) 1_545 . ? Pb7B S17 Sb14 167.8(2) . . ? S13 S17 Sb14 114.79(15) . . ? S13 S17 Sb14 114.79(15) 1_545 . ? Pb7A S17 Sb14 164.14(18) . . ? Sb12 S18 As12 92.64(15) . 1_565 ? Sb12 S18 Sb12 92.64(15) . 1_565 ? As12 S18 Sb12 0.00(6) 1_565 1_565 ? Sb12 S18 Pb9 91.61(12) . . ? As12 S18 Pb9 91.61(12) 1_565 . ? Sb12 S18 Pb9 91.61(12) 1_565 . ? Sb12 S18 Sb11 90.61(4) . . ? As12 S18 Sb11 173.07(17) 1_565 . ? Sb12 S18 Sb11 173.07(17) 1_565 . ? Pb9 S18 Sb11 94.42(11) . . ? Sb12 S18 Sb11 173.07(17) . 1_565 ? As12 S18 Sb11 90.61(4) 1_565 1_565 ? Sb12 S18 Sb11 90.61(4) 1_565 1_565 ? Pb9 S18 Sb11 94.41(11) . 1_565 ? Sb11 S18 Sb11 85.53(13) . 1_565 ? Sb12 S18 S23 92.26(13) . 1_565 ? As12 S18 S23 40.58(8) 1_565 1_565 ? Sb12 S18 S23 40.58(8) 1_565 1_565 ? Pb9 S18 S23 51.05(9) . 1_565 ? Sb11 S18 S23 145.40(16) . 1_565 ? Sb11 S18 S23 94.19(7) 1_565 1_565 ? Sb12 S18 S23 40.58(8) . . ? As12 S18 S23 92.26(13) 1_565 . ? Sb12 S18 S23 92.26(13) 1_565 . ? Pb9 S18 S23 51.05(9) . . ? Sb11 S18 S23 94.19(7) . . ? Sb11 S18 S23 145.39(16) 1_565 . ? S23 S18 S23 67.05(10) 1_565 . ? Sb12 S18 S19 143.68(16) . 1_565 ? As12 S18 S19 90.56(7) 1_565 1_565 ? Sb12 S18 S19 90.56(7) 1_565 1_565 ? Pb9 S18 S19 52.12(8) . 1_565 ? Sb11 S18 S19 90.45(12) . 1_565 ? Sb11 S18 S19 42.31(8) 1_565 1_565 ? S23 S18 S19 67.66(10) 1_565 1_565 ? S23 S18 S19 103.16(14) . 1_565 ? Sb12 S18 S19 90.56(7) . . ? As12 S18 S19 143.68(16) 1_565 . ? Sb12 S18 S19 143.68(16) 1_565 . ? Pb9 S18 S19 52.12(8) . . ? Sb11 S18 S19 42.31(8) . . ? Sb11 S18 S19 90.45(12) 1_565 . ? S23 S18 S19 103.16(14) 1_565 . ? S23 S18 S19 67.65(10) . . ? S19 S18 S19 66.78(10) 1_565 . ? Sb12 S18 S20 46.34(7) . . ? As12 S18 S20 46.34(7) 1_565 . ? Sb12 S18 S20 46.34(7) 1_565 . ? Pb9 S18 S20 90.81(14) . . ? Sb11 S18 S20 136.80(7) . . ? Sb11 S18 S20 136.80(7) 1_565 . ? S23 S18 S20 57.42(10) 1_565 . ? S23 S18 S20 57.42(10) . . ? S19 S18 S20 125.07(13) 1_565 . ? S19 S18 S20 125.06(13) . . ? Sb11 S19 Pb8 96.20(10) . 1_545 ? Sb11 S19 Pb8 96.20(10) . . ? Pb8 S19 Pb8 89.79(11) 1_545 . ? Sb11 S19 Pb9 102.66(11) . 1_545 ? Pb8 S19 Pb9 88.88(3) 1_545 1_545 ? Pb8 S19 Pb9 161.13(15) . 1_545 ? Sb11 S19 Pb9 102.66(11) . . ? Pb8 S19 Pb9 161.12(15) 1_545 . ? Pb8 S19 Pb9 88.88(3) . . ? Pb9 S19 Pb9 86.35(10) 1_545 . ? Sb11 S19 S22 134.79(16) . . ? Pb8 S19 S22 55.04(8) 1_545 . ? Pb8 S19 S22 55.04(8) . . ? Pb9 S19 S22 109.83(11) 1_545 . ? Pb9 S19 S22 109.83(11) . . ? Sb11 S19 S16 47.02(9) . . ? Pb8 S19 S16 98.01(12) 1_545 . ? Pb8 S19 S16 49.37(9) . . ? Pb9 S19 S16 149.31(15) 1_545 . ? Pb9 S19 S16 95.37(8) . . ? S22 S19 S16 98.41(13) . . ? Sb11 S19 S16 47.02(9) . 1_545 ? Pb8 S19 S16 49.37(9) 1_545 1_545 ? Pb8 S19 S16 98.01(12) . 1_545 ? Pb9 S19 S16 95.37(8) 1_545 1_545 ? Pb9 S19 S16 149.32(15) . 1_545 ? S22 S19 S16 98.41(13) . 1_545 ? S16 S19 S16 68.12(14) . 1_545 ? Sb11 S19 S18 53.71(9) . . ? Pb8 S19 S18 149.85(14) 1_545 . ? Pb8 S19 S18 95.04(6) . . ? Pb9 S19 S18 95.54(12) 1_545 . ? Pb9 S19 S18 48.97(8) . . ? S22 S19 S18 146.61(5) . . ? S16 S19 S18 64.25(11) . . ? S16 S19 S18 100.48(13) 1_545 . ? Sb11 S19 S18 53.71(10) . 1_545 ? Pb8 S19 S18 95.04(6) 1_545 1_545 ? Pb8 S19 S18 149.85(14) . 1_545 ? Pb9 S19 S18 48.97(8) 1_545 1_545 ? Pb9 S19 S18 95.54(12) . 1_545 ? S22 S19 S18 146.61(5) . 1_545 ? S16 S19 S18 100.48(13) . 1_545 ? S16 S19 S18 64.25(11) 1_545 1_545 ? S18 S19 S18 66.78(10) . 1_545 ? Sb11 S19 S26 147.55(5) . 1_545 ? Pb8 S19 S26 64.39(8) 1_545 1_545 ? Pb8 S19 S26 108.77(13) . 1_545 ? Pb9 S19 S26 54.12(7) 1_545 1_545 ? Pb9 S19 S26 98.33(11) . 1_545 ? S22 S19 S26 56.07(10) . 1_545 ? S16 S19 S26 153.97(15) . 1_545 ? S16 S19 S26 107.47(8) 1_545 1_545 ? S18 S19 S26 139.75(14) . 1_545 ? S18 S19 S26 100.09(9) 1_545 1_545 ? Sb11 S19 S26 147.55(5) . . ? Pb8 S19 S26 108.77(13) 1_545 . ? Pb8 S19 S26 64.39(8) . . ? Pb9 S19 S26 98.33(11) 1_545 . ? Pb9 S19 S26 54.12(7) . . ? S22 S19 S26 56.07(10) . . ? S16 S19 S26 107.48(8) . . ? S16 S19 S26 153.97(15) 1_545 . ? S18 S19 S26 100.10(9) . . ? S18 S19 S26 139.75(14) 1_545 . ? S26 S19 S26 64.57(9) 1_545 . ? As12 S20 Sb12 0.00(13) 1_565 1_565 ? As12 S20 Sb12 96.42(16) 1_565 . ? Sb12 S20 Sb12 96.42(16) 1_565 . ? As12 S20 As8 87.38(4) 1_565 7_566 ? Sb12 S20 As8 87.38(4) 1_565 7_566 ? Sb12 S20 As8 174.93(17) . 7_566 ? As12 S20 Sb8 87.38(4) 1_565 7_566 ? Sb12 S20 Sb8 87.38(4) 1_565 7_566 ? Sb12 S20 Sb8 174.93(17) . 7_566 ? As8 S20 Sb8 0.00(5) 7_566 7_566 ? As12 S20 As8 174.93(17) 1_565 7_556 ? Sb12 S20 As8 174.93(17) 1_565 7_556 ? Sb12 S20 As8 87.38(4) . 7_556 ? As8 S20 As8 88.64(13) 7_566 7_556 ? Sb8 S20 As8 88.64(13) 7_566 7_556 ? As12 S20 Sb8 174.93(17) 1_565 7_556 ? Sb12 S20 Sb8 174.93(17) 1_565 7_556 ? Sb12 S20 Sb8 87.38(4) . 7_556 ? As8 S20 Sb8 88.64(13) 7_566 7_556 ? Sb8 S20 Sb8 88.64(13) 7_566 7_556 ? As8 S20 Sb8 0.0 7_556 7_556 ? As12 S20 Pb5 94.79(12) 1_565 7_556 ? Sb12 S20 Pb5 94.79(12) 1_565 7_556 ? Sb12 S20 Pb5 94.79(12) . 7_556 ? As8 S20 Pb5 88.22(12) 7_566 7_556 ? Sb8 S20 Pb5 88.22(12) 7_566 7_556 ? As8 S20 Pb5 88.22(12) 7_556 7_556 ? Sb8 S20 Pb5 88.22(12) 7_556 7_556 ? As12 S20 S23 42.04(8) 1_565 1_565 ? Sb12 S20 S23 42.04(8) 1_565 1_565 ? Sb12 S20 S23 96.06(14) . 1_565 ? As8 S20 S23 89.00(8) 7_566 1_565 ? Sb8 S20 S23 89.00(8) 7_566 1_565 ? As8 S20 S23 141.03(18) 7_556 1_565 ? Sb8 S20 S23 141.03(18) 7_556 1_565 ? Pb5 S20 S23 52.83(9) 7_556 1_565 ? As12 S20 S23 96.06(14) 1_565 . ? Sb12 S20 S23 96.06(14) 1_565 . ? Sb12 S20 S23 42.04(8) . . ? As8 S20 S23 141.03(18) 7_566 . ? Sb8 S20 S23 141.03(18) 7_566 . ? As8 S20 S23 89.00(8) 7_556 . ? Sb8 S20 S23 89.00(8) 7_556 . ? Pb5 S20 S23 52.83(9) 7_556 . ? S23 S20 S23 69.34(12) 1_565 . ? As12 S20 S12 131.36(8) 1_565 7_556 ? Sb12 S20 S12 131.36(8) 1_565 7_556 ? Sb12 S20 S12 131.36(8) . 7_556 ? As8 S20 S12 44.39(7) 7_566 7_556 ? Sb8 S20 S12 44.39(7) 7_566 7_556 ? As8 S20 S12 44.39(7) 7_556 7_556 ? Sb8 S20 S12 44.39(7) 7_556 7_556 ? Pb5 S20 S12 90.28(14) 7_556 7_556 ? S23 S20 S12 124.12(13) 1_565 7_556 ? S23 S20 S12 124.12(13) . 7_556 ? Sb13 S21 Sb13 99.03(17) . 1_565 ? Sb13 S21 Pb11 96.64(13) . . ? Sb13 S21 Pb11 96.64(13) 1_565 . ? Sb13 S21 O 130.20(10) . 1_565 ? Sb13 S21 O 130.20(10) 1_565 1_565 ? Pb11 S21 O 85.9(6) . 1_565 ? Sb13 S21 As14 168.87(15) . 1_565 ? Sb13 S21 As14 91.36(4) 1_565 1_565 ? Pb11 S21 As14 86.03(12) . 1_565 ? O S21 As14 39.02(6) 1_565 1_565 ? Sb13 S21 Sb14 168.87(15) . 1_565 ? Sb13 S21 Sb14 91.36(4) 1_565 1_565 ? Pb11 S21 Sb14 86.03(12) . 1_565 ? O S21 Sb14 39.02(6) 1_565 1_565 ? As14 S21 Sb14 0.00(5) 1_565 1_565 ? Sb13 S21 Sb14 91.36(4) . . ? Sb13 S21 Sb14 168.87(15) 1_565 . ? Pb11 S21 Sb14 86.03(12) . . ? O S21 Sb14 39.02(6) 1_565 . ? As14 S21 Sb14 78.01(12) 1_565 . ? Sb14 S21 Sb14 78.01(12) 1_565 . ? Sb13 S21 S24 96.16(15) . 1_565 ? Sb13 S21 S24 41.41(9) 1_565 1_565 ? Pb11 S21 S24 55.76(10) . 1_565 ? O S21 S24 124.3(5) 1_565 1_565 ? As14 S21 S24 94.27(8) 1_565 1_565 ? Sb14 S21 S24 94.27(8) 1_565 1_565 ? Sb14 S21 S24 141.62(18) . 1_565 ? Sb13 S21 S24 41.41(9) . . ? Sb13 S21 S24 96.16(15) 1_565 . ? Pb11 S21 S24 55.76(10) . . ? O S21 S24 124.3(5) 1_565 . ? As14 S21 S24 141.62(18) 1_565 . ? Sb14 S21 S24 141.62(18) 1_565 . ? Sb14 S21 S24 94.27(8) . . ? S24 S21 S24 68.60(11) 1_565 . ? Sb13 S21 Sb9 72.63(11) . . ? Sb13 S21 Sb9 72.63(11) 1_565 . ? Pb11 S21 Sb9 162.88(18) . . ? O S21 Sb9 111.2(6) 1_565 . ? As14 S21 Sb9 107.10(12) 1_565 . ? Sb14 S21 Sb9 107.10(12) 1_565 . ? Sb14 S21 Sb9 107.10(12) . . ? S24 S21 Sb9 111.08(13) 1_565 . ? S24 S21 Sb9 111.08(13) . . ? Sb13 S21 S25 144.61(18) . 1_565 ? Sb13 S21 S25 89.51(8) 1_565 1_565 ? Pb11 S21 S25 48.09(9) . 1_565 ? O S21 S25 56.2(5) 1_565 1_565 ? As14 S21 S25 38.54(8) 1_565 1_565 ? Sb14 S21 S25 38.54(8) 1_565 1_565 ? Sb14 S21 S25 84.23(12) . 1_565 ? S24 S21 S25 68.14(11) 1_565 1_565 ? S24 S21 S25 103.78(15) . 1_565 ? Sb9 S21 S25 142.05(9) . 1_565 ? Sb14 S22 Sb12b 98.50(17) . . ? Sb14 S22 Sb12b 98.50(17) . 1_545 ? Sb12b S22 Sb12b 97.6(2) . 1_545 ? Sb14 S22 O 48.2(5) . 1_565 ? Sb12b S22 O 65.8(6) . 1_565 ? Sb12b S22 O 134.9(7) 1_545 1_565 ? Sb14 S22 O 48.2(5) . . ? Sb12b S22 O 134.9(7) . . ? Sb12b S22 O 65.8(6) 1_545 . ? O S22 O 95.7(10) 1_565 . ? Sb14 S22 Pb12a 91.61(13) . 1_545 ? Sb12b S22 Pb12a 93.86(17) . 1_545 ? Sb12b S22 Pb12a 8.45(10) 1_545 1_545 ? O S22 Pb12a 126.4(7) 1_565 1_545 ? O S22 Pb12a 63.5(6) . 1_545 ? Sb14 S22 Pb12a 91.61(13) . . ? Sb12b S22 Pb12a 8.45(10) . . ? Sb12b S22 Pb12a 93.86(17) 1_545 . ? O S22 Pb12a 63.5(6) 1_565 . ? O S22 Pb12a 126.4(7) . . ? Pb12a S22 Pb12a 89.20(15) 1_545 . ? Sb14 S22 Pb8 101.64(14) . 1_545 ? Sb12b S22 Pb8 158.7(2) . 1_545 ? Sb12b S22 Pb8 86.15(11) 1_545 1_545 ? O S22 Pb8 124.8(7) 1_565 1_545 ? O S22 Pb8 65.6(6) . 1_545 ? Pb12a S22 Pb8 92.32(5) 1_545 1_545 ? Pb12a S22 Pb8 166.61(19) . 1_545 ? Sb14 S22 Pb8 101.64(14) . . ? Sb12b S22 Pb8 86.15(11) . . ? Sb12b S22 Pb8 158.7(2) 1_545 . ? O S22 Pb8 65.6(6) 1_565 . ? O S22 Pb8 124.8(7) . . ? Pb12a S22 Pb8 166.61(19) 1_545 . ? Pb12a S22 Pb8 92.32(5) . . ? Pb8 S22 Pb8 83.20(12) 1_545 . ? Sb14 S22 S25 45.66(11) . . ? Sb12b S22 S25 69.16(16) . . ? Sb12b S22 S25 69.16(16) 1_545 . ? O S22 S25 65.7(7) 1_565 . ? O S22 S25 65.7(7) . . ? Pb12a S22 S25 60.71(11) 1_545 . ? Pb12a S22 S25 60.71(11) . . ? Pb8 S22 S25 130.99(11) 1_545 . ? Pb8 S22 S25 130.99(11) . . ? Sb14 S22 S26 141.40(9) . 1_545 ? Sb12b S22 S26 100.43(18) . 1_545 ? Sb12b S22 S26 45.85(15) 1_545 1_545 ? O S22 S26 166.0(6) 1_565 1_545 ? O S22 S26 96.1(5) . 1_545 ? Pb12a S22 S26 53.91(10) 1_545 1_545 ? Pb12a S22 S26 103.28(16) . 1_545 ? Pb8 S22 S26 67.34(9) 1_545 1_545 ? Pb8 S22 S26 112.90(15) . 1_545 ? S25 S22 S26 112.82(14) . 1_545 ? Sb12 S23 Pb9 99.14(11) . . ? Sb12 S23 Pb9 99.13(11) . 1_545 ? Pb9 S23 Pb9 88.62(11) . 1_545 ? Sb12 S23 Pb5 106.34(12) . 7_556 ? Pb9 S23 Pb5 87.88(4) . 7_556 ? Pb9 S23 Pb5 154.52(16) 1_545 7_556 ? Sb12 S23 Pb5 106.34(12) . 7_546 ? Pb9 S23 Pb5 154.52(16) . 7_546 ? Pb9 S23 Pb5 87.88(4) 1_545 7_546 ? Pb5 S23 Pb5 84.54(10) 7_556 7_546 ? Sb12 S23 S7 145.19(6) . 7_556 ? Pb9 S23 S7 56.35(8) . 7_556 ? Pb9 S23 S7 103.99(13) 1_545 7_556 ? Pb5 S23 S7 53.94(8) 7_556 7_556 ? Pb5 S23 S7 100.23(12) 7_546 7_556 ? Sb12 S23 S7 145.19(5) . 7_546 ? Pb9 S23 S7 103.98(13) . 7_546 ? Pb9 S23 S7 56.35(8) 1_545 7_546 ? Pb5 S23 S7 100.23(12) 7_556 7_546 ? Pb5 S23 S7 53.94(8) 7_546 7_546 ? S7 S23 S7 69.45(11) 7_556 7_546 ? Sb12 S23 S20 49.70(10) . 1_545 ? Pb9 S23 S20 148.71(15) . 1_545 ? Pb9 S23 S20 93.42(7) 1_545 1_545 ? Pb5 S23 S20 102.53(12) 7_556 1_545 ? Pb5 S23 S20 56.74(9) 7_546 1_545 ? S7 S23 S20 150.92(15) 7_556 1_545 ? S7 S23 S20 103.05(8) 7_546 1_545 ? Sb12 S23 S20 49.70(10) . . ? Pb9 S23 S20 93.42(7) . . ? Pb9 S23 S20 148.70(15) 1_545 . ? Pb5 S23 S20 56.74(9) 7_556 . ? Pb5 S23 S20 102.52(12) 7_546 . ? S7 S23 S20 103.05(8) 7_556 . ? S7 S23 S20 150.92(15) 7_546 . ? S20 S23 S20 69.34(12) 1_545 . ? Sb12 S23 S18 49.79(9) . 1_545 ? Pb9 S23 S18 96.91(11) . 1_545 ? Pb9 S23 S18 49.36(8) 1_545 1_545 ? Pb5 S23 S18 156.07(15) 7_556 1_545 ? Pb5 S23 S18 99.85(6) 7_546 1_545 ? S7 S23 S18 145.60(15) 7_556 1_545 ? S7 S23 S18 101.30(8) 7_546 1_545 ? S20 S23 S18 62.36(11) 1_545 1_545 ? S20 S23 S18 99.47(14) . 1_545 ? Sb12 S23 S18 49.79(9) . . ? Pb9 S23 S18 49.36(8) . . ? Pb9 S23 S18 96.91(11) 1_545 . ? Pb5 S23 S18 99.85(6) 7_556 . ? Pb5 S23 S18 156.07(15) 7_546 . ? S7 S23 S18 101.30(8) 7_556 . ? S7 S23 S18 145.60(15) 7_546 . ? S20 S23 S18 99.47(14) 1_545 . ? S20 S23 S18 62.36(11) . . ? S18 S23 S18 67.05(10) 1_545 . ? Sb13 S24 Pb10 102.78(12) . 1_545 ? Sb13 S24 Pb10 102.78(12) . . ? Pb10 S24 Pb10 86.43(10) 1_545 . ? Sb13 S24 Pb11 97.88(11) . . ? Pb10 S24 Pb11 159.08(15) 1_545 . ? Pb10 S24 Pb11 92.20(3) . . ? Sb13 S24 Pb11 97.88(11) . 1_545 ? Pb10 S24 Pb11 92.20(3) 1_545 1_545 ? Pb10 S24 Pb11 159.08(15) . 1_545 ? Pb11 S24 Pb11 81.69(10) . 1_545 ? Sb13 S24 S28 154.53(19) . . ? Pb10 S24 S28 60.11(9) 1_545 . ? Pb10 S24 S28 60.11(9) . . ? Pb11 S24 S28 101.31(12) . . ? Pb11 S24 S28 101.31(12) 1_545 . ? Sb13 S24 S21 47.81(9) . 1_545 ? Pb10 S24 S21 95.55(7) 1_545 1_545 ? Pb10 S24 S21 150.28(15) . 1_545 ? Pb11 S24 S21 95.91(12) . 1_545 ? Pb11 S24 S21 50.63(9) 1_545 1_545 ? S28 S24 S21 144.41(7) . 1_545 ? Sb13 S24 S21 47.81(9) . . ? Pb10 S24 S21 150.28(15) 1_545 . ? Pb10 S24 S21 95.55(7) . . ? Pb11 S24 S21 50.63(9) . . ? Pb11 S24 S21 95.90(12) 1_545 . ? S28 S24 S21 144.41(7) . . ? S21 S24 S21 68.60(11) 1_545 . ? Sb13 S24 S30 142.49(16) . . ? Pb10 S24 S30 104.32(10) 1_545 . ? Pb10 S24 S30 104.32(10) . . ? Pb11 S24 S30 55.82(8) . . ? Pb11 S24 S30 55.82(8) 1_545 . ? S28 S24 S30 62.98(13) . . ? S21 S24 S30 103.88(13) 1_545 . ? S21 S24 S30 103.88(13) . . ? Sb13 S24 S14 53.22(10) . 7_545 ? Pb10 S24 S14 49.59(8) 1_545 7_545 ? Pb10 S24 S14 95.70(12) . 7_545 ? Pb11 S24 S14 151.06(14) . 7_545 ? Pb11 S24 S14 99.28(7) 1_545 7_545 ? S28 S24 S14 106.77(14) . 7_545 ? S21 S24 S14 64.67(11) 1_545 7_545 ? S21 S24 S14 100.80(14) . 7_545 ? S30 S24 S14 146.29(6) . 7_545 ? Sb13 S24 S14 53.22(10) . 7 ? Pb10 S24 S14 95.70(12) 1_545 7 ? Pb10 S24 S14 49.59(8) . 7 ? Pb11 S24 S14 99.28(7) . 7 ? Pb11 S24 S14 151.06(14) 1_545 7 ? S28 S24 S14 106.77(14) . 7 ? S21 S24 S14 100.80(14) 1_545 7 ? S21 S24 S14 64.67(11) . 7 ? S30 S24 S14 146.29(6) . 7 ? S14 S24 S14 66.16(11) 7_545 7 ? Sb13 S24 S24 89.999(1) . 1_565 ? Pb10 S24 S24 133.22(5) 1_545 1_565 ? Pb10 S24 S24 46.79(5) . 1_565 ? Pb11 S24 S24 49.16(5) . 1_565 ? Pb11 S24 S24 130.84(5) 1_545 1_565 ? S28 S24 S24 90.0 . 1_565 ? S21 S24 S24 124.30(6) 1_545 1_565 ? S21 S24 S24 55.70(6) . 1_565 ? S30 S24 S24 90.0 . 1_565 ? S14 S24 S24 123.08(5) 7_545 1_565 ? S14 S24 S24 56.92(5) 7 1_565 ? Sb14 S25 Pb11 107.78(12) . 1_545 ? Sb14 S25 Pb11 107.78(12) . . ? Pb11 S25 Pb11 92.17(12) 1_545 . ? Sb14 S25 Pb12a 87.85(11) . 1_545 ? Pb11 S25 Pb12a 91.14(5) 1_545 1_545 ? Pb11 S25 Pb12a 162.14(16) . 1_545 ? Sb14 S25 Pb12a 87.85(11) . . ? Pb11 S25 Pb12a 162.14(16) 1_545 . ? Pb11 S25 Pb12a 91.14(5) . . ? Pb12a S25 Pb12a 80.61(11) 1_545 . ? Sb14 S25 S22 48.49(12) . . ? Pb11 S25 S22 131.97(7) 1_545 . ? Pb11 S25 S22 131.97(7) . . ? Pb12a S25 S22 53.47(9) 1_545 . ? Pb12a S25 S22 53.47(9) . . ? Sb14 S25 O 40.3(4) . 1_565 ? Pb11 S25 O 143.1(5) 1_545 1_565 ? Pb11 S25 O 85.0(4) . 1_565 ? Pb12a S25 O 102.6(5) 1_545 1_565 ? Pb12a S25 O 54.8(5) . 1_565 ? S22 S25 O 49.2(5) . 1_565 ? Sb14 S25 O 40.3(4) . . ? Pb11 S25 O 85.0(4) 1_545 . ? Pb11 S25 O 143.1(5) . . ? Pb12a S25 O 54.8(5) 1_545 . ? Pb12a S25 O 102.6(5) . . ? S22 S25 O 49.2(5) . . ? O S25 O 75.9(7) 1_565 . ? Sb14 S25 Sb12b 82.98(14) . . ? Pb11 S25 Sb12b 163.73(16) 1_545 . ? Pb11 S25 Sb12b 96.13(7) . . ? Pb12a S25 Sb12b 76.81(12) 1_545 . ? Pb12a S25 Sb12b 6.12(7) . . ? S22 S25 Sb12b 47.35(11) . . ? O S25 Sb12b 52.1(6) 1_565 . ? O S25 Sb12b 96.5(5) . . ? Sb14 S25 Sb12b 82.98(14) . 1_545 ? Pb11 S25 Sb12b 96.13(7) 1_545 1_545 ? Pb11 S25 Sb12b 163.72(16) . 1_545 ? Pb12a S25 Sb12b 6.11(7) 1_545 1_545 ? Pb12a S25 Sb12b 76.81(12) . 1_545 ? S22 S25 Sb12b 47.35(11) . 1_545 ? O S25 Sb12b 96.5(5) 1_565 1_545 ? O S25 Sb12b 52.1(6) . 1_545 ? Sb12b S25 Sb12b 72.62(14) . 1_545 ? Sb14 S25 S31 138.91(10) . 1_545 ? Pb11 S25 S31 64.35(9) 1_545 1_545 ? Pb11 S25 S31 112.65(14) . 1_545 ? Pb12a S25 S31 53.76(10) 1_545 1_545 ? Pb12a S25 S31 98.24(13) . 1_545 ? S22 S25 S31 104.57(14) . 1_545 ? O S25 S31 149.2(6) 1_565 1_545 ? O S25 S31 99.2(4) . 1_545 ? Sb12b S25 S31 99.47(15) . 1_545 ? Sb12b S25 S31 59.48(13) 1_545 1_545 ? Sb12b S26 Sb15 99.10(14) . . ? Sb12b S26 Sb15 99.10(14) . 1_565 ? Sb15 S26 Sb15 98.66(15) . 1_565 ? Sb12b S26 Pb12a 3.50(15) . . ? Sb15 S26 Pb12a 96.85(11) . . ? Sb15 S26 Pb12a 96.85(11) 1_565 . ? Sb12b S26 Pb9 150.7(2) . . ? Sb15 S26 Pb9 99.88(11) . . ? Sb15 S26 Pb9 99.88(11) 1_565 . ? Pb12a S26 Pb9 154.18(16) . . ? Sb12b S26 S22 50.40(12) . 1_565 ? Sb15 S26 S22 149.49(16) . 1_565 ? Sb15 S26 S22 88.67(8) 1_565 1_565 ? Pb12a S26 S22 52.73(10) . 1_565 ? Pb9 S26 S22 108.02(13) . 1_565 ? Sb12b S26 S22 50.40(13) . . ? Sb15 S26 S22 88.67(8) . . ? Sb15 S26 S22 149.49(16) 1_565 . ? Pb12a S26 S22 52.73(10) . . ? Pb9 S26 S22 108.01(13) . . ? S22 S26 S22 71.35(13) 1_565 . ? Sb12b S26 S29 55.95(13) . . ? Sb15 S26 S29 43.57(8) . . ? Sb15 S26 S29 98.39(13) 1_565 . ? Pb12a S26 S29 53.47(9) . . ? Pb9 S26 S29 141.34(8) . . ? S22 S26 S29 106.19(14) 1_565 . ? S22 S26 S29 67.02(10) . . ? Sb12b S26 S29 55.95(13) . 1_565 ? Sb15 S26 S29 98.39(13) . 1_565 ? Sb15 S26 S29 43.57(8) 1_565 1_565 ? Pb12a S26 S29 53.47(9) . 1_565 ? Pb9 S26 S29 141.34(8) . 1_565 ? S22 S26 S29 67.02(11) 1_565 1_565 ? S22 S26 S29 106.19(14) . 1_565 ? S29 S26 S29 70.03(10) . 1_565 ? Sb12b S26 Pb8 77.19(17) . . ? Sb15 S26 Pb8 130.66(8) . . ? Sb15 S26 Pb8 130.66(8) 1_565 . ? Pb12a S26 Pb8 80.69(11) . . ? Pb9 S26 Pb8 73.49(9) . . ? S22 S26 Pb8 50.78(9) 1_565 . ? S22 S26 Pb8 50.78(9) . . ? S29 S26 Pb8 117.31(11) . . ? S29 S26 Pb8 117.31(11) 1_565 . ? Sb12b S26 S7 156.7(2) . 7_556 ? Sb15 S26 S7 66.71(10) . 7_556 ? Sb15 S26 S7 66.71(10) 1_565 7_556 ? Pb12a S26 S7 153.19(16) . 7_556 ? Pb9 S26 S7 52.62(9) . 7_556 ? S22 S26 S7 141.69(8) 1_565 7_556 ? S22 S26 S7 141.69(8) . 7_556 ? S29 S26 S7 106.12(12) . 7_556 ? S29 S26 S7 106.12(12) 1_565 7_556 ? Pb8 S26 S7 126.12(13) . 7_556 ? Sb12b S26 S19 107.67(17) . . ? Sb15 S26 S19 92.62(7) . . ? Sb15 S26 S19 148.86(15) 1_565 . ? Pb12a S26 S19 110.56(13) . . ? Pb9 S26 S19 49.38(8) . . ? S22 S26 S19 96.18(13) 1_565 . ? S22 S26 S19 58.98(10) . . ? S29 S26 S19 109.58(6) . . ? S29 S26 S19 161.46(16) 1_565 . ? Pb8 S26 S19 45.40(7) . . ? S7 S26 S19 91.92(11) 7_556 . ? Sb16 S27 Sb61 11.07(16) . 6_565 ? Sb16 S27 Sb61 11.07(16) . . ? Sb61 S27 Sb61 18.4(7) 6_565 . ? Sb16 S27 Pb3 102.9(3) . 7 ? Sb61 S27 Pb3 105.3(4) 6_565 7 ? Sb61 S27 Pb3 91.9(2) . 7 ? Sb16 S27 Pb3 102.9(3) . 7_565 ? Sb61 S27 Pb3 91.9(2) 6_565 7_565 ? Sb61 S27 Pb3 105.3(4) . 7_565 ? Pb3 S27 Pb3 92.11(12) 7 7_565 ? Sb16 S27 Pb6 155.7(4) . 7 ? Sb61 S27 Pb6 159.8(3) 6_565 7 ? Sb61 S27 Pb6 159.7(3) . 7 ? Pb3 S27 Pb6 93.84(10) 7 7 ? Pb3 S27 Pb6 93.84(10) 7_565 7 ? Sb16 S27 Pb10 76.0(4) . . ? Sb61 S27 Pb10 82.3(2) 6_565 . ? Sb61 S27 Pb10 82.3(2) . . ? Pb3 S27 Pb10 133.76(6) 7 . ? Pb3 S27 Pb10 133.76(6) 7_565 . ? Pb6 S27 Pb10 79.71(9) 7 . ? Sb16 S27 S28 45.3(3) . 1_565 ? Sb61 S27 S28 42.6(4) 6_565 1_565 ? Sb61 S27 S28 56.3(3) . 1_565 ? Pb3 S27 S28 147.82(16) 7 1_565 ? Pb3 S27 S28 91.73(8) 7_565 1_565 ? Pb6 S27 S28 117.74(13) 7 1_565 ? Pb10 S27 S28 54.15(10) . 1_565 ? Sb16 S27 S28 45.3(3) . . ? Sb61 S27 S28 56.3(3) 6_565 . ? Sb61 S27 S28 42.6(4) . . ? Pb3 S27 S28 91.73(8) 7 . ? Pb3 S27 S28 147.83(16) 7_565 . ? Pb6 S27 S28 117.74(13) 7 . ? Pb10 S27 S28 54.15(10) . . ? S28 S27 S28 69.06(13) 1_565 . ? Sb16 S27 S2 56.2(3) . 7_565 ? Sb61 S27 S2 45.6(2) 6_565 7_565 ? Sb61 S27 S2 58.4(4) . 7_565 ? Pb3 S27 S2 96.18(12) 7 7_565 ? Pb3 S27 S2 47.08(8) 7_565 7_565 ? Pb6 S27 S2 139.83(9) 7 7_565 ? Pb10 S27 S2 118.15(11) . 7_565 ? S28 S27 S2 64.25(12) 1_565 7_565 ? S28 S27 S2 100.75(14) . 7_565 ? Sb16 S27 S2 56.2(3) . 7 ? Sb61 S27 S2 58.4(4) 6_565 7 ? Sb61 S27 S2 45.6(2) . 7 ? Pb3 S27 S2 47.08(8) 7 7 ? Pb3 S27 S2 96.18(12) 7_565 7 ? Pb6 S27 S2 139.83(9) 7 7 ? Pb10 S27 S2 118.15(11) . 7 ? S28 S27 S2 100.74(14) 1_565 7 ? S28 S27 S2 64.25(12) . 7 ? S2 S27 S2 66.42(10) 7_565 7 ? Sb16 S27 S11 109.6(4) . 7 ? Sb61 S27 S11 119.9(2) 6_565 7 ? Sb61 S27 S11 108.8(4) . 7 ? Pb3 S27 S11 92.01(7) 7 7 ? Pb3 S27 S11 145.42(15) 7_565 7 ? Pb6 S27 S11 51.62(8) 7 7 ? Pb10 S27 S11 48.47(7) . 7 ? S28 S27 S11 102.58(14) 1_565 7 ? S28 S27 S11 66.25(11) . 7 ? S2 S27 S11 164.90(15) 7_565 7 ? S2 S27 S11 111.46(6) 7 7 ? Sb61 S28 Sb61 84.6(5) . 6 ? Sb61 S28 Sb16 10.5(2) . . ? Sb61 S28 Sb16 95.2(5) 6 . ? Sb61 S28 Sb16 95.2(5) . 1_545 ? Sb61 S28 Sb16 10.5(2) 6 1_545 ? Sb16 S28 Sb16 105.7(6) . 1_545 ? Sb61 S28 Sb61 11.1(4) . 6_565 ? Sb61 S28 Sb61 95.7(3) 6 6_565 ? Sb16 S28 Sb61 0.8(5) . 6_565 ? Sb16 S28 Sb61 106.3(2) 1_545 6_565 ? Sb61 S28 Sb61 95.7(3) . 1_545 ? Sb61 S28 Sb61 11.1(4) 6 1_545 ? Sb16 S28 Sb61 106.3(2) . 1_545 ? Sb16 S28 Sb61 0.8(5) 1_545 1_545 ? Sb61 S28 Sb61 106.9(6) 6_565 1_545 ? Sb61 S28 Pb10 88.5(2) . . ? Sb61 S28 Pb10 145.6(3) 6 . ? Sb16 S28 Pb10 79.5(3) . . ? Sb16 S28 Pb10 145.6(3) 1_545 . ? Sb61 S28 Pb10 79.3(3) 6_565 . ? Sb61 S28 Pb10 146.0(2) 1_545 . ? Sb61 S28 Pb10 145.6(3) . 1_545 ? Sb61 S28 Pb10 88.6(2) 6 1_545 ? Sb16 S28 Pb10 145.6(3) . 1_545 ? Sb16 S28 Pb10 79.5(3) 1_545 1_545 ? Sb61 S28 Pb10 146.0(2) 6_565 1_545 ? Sb61 S28 Pb10 79.3(3) 1_545 1_545 ? Pb10 S28 Pb10 78.30(13) . 1_545 ? Sb61 S28 Pb15 117.4(3) . 1_545 ? Sb61 S28 Pb15 69.1(2) 6 1_545 ? Sb16 S28 Pb15 122.2(3) . 1_545 ? Sb16 S28 Pb15 64.27(18) 1_545 1_545 ? Sb61 S28 Pb15 122.0(2) 6_565 1_545 ? Sb61 S28 Pb15 63.55(18) 1_545 1_545 ? Pb10 S28 Pb15 141.8(2) . 1_545 ? Pb10 S28 Pb15 91.08(9) 1_545 1_545 ? Sb61 S28 Pb15 69.1(2) . . ? Sb61 S28 Pb15 117.4(3) 6 . ? Sb16 S28 Pb15 64.27(18) . . ? Sb16 S28 Pb15 122.2(3) 1_545 . ? Sb61 S28 Pb15 63.55(18) 6_565 . ? Sb61 S28 Pb15 122.0(2) 1_545 . ? Pb10 S28 Pb15 91.09(9) . . ? Pb10 S28 Pb15 141.8(2) 1_545 . ? Pb15 S28 Pb15 74.74(13) 1_545 . ? Sb61 S28 S24 137.3(2) . . ? Sb61 S28 S24 137.3(3) 6 . ? Sb16 S28 S24 126.8(3) . . ? Sb16 S28 S24 126.8(3) 1_545 . ? Sb61 S28 S24 126.3(3) 6_565 . ? Sb61 S28 S24 126.3(3) 1_545 . ? Pb10 S28 S24 53.07(10) . . ? Pb10 S28 S24 53.07(10) 1_545 . ? Pb15 S28 S24 91.20(16) 1_545 . ? Pb15 S28 S24 91.20(16) . . ? Sb61 S28 S27 91.9(3) . 1_545 ? Sb61 S28 S27 43.17(18) 6 1_545 ? Sb16 S28 S27 99.3(3) . 1_545 ? Sb16 S28 S27 42.12(16) 1_545 1_545 ? Sb61 S28 S27 100.1(3) 6_565 1_545 ? Sb61 S28 S27 42.66(15) 1_545 1_545 ? Pb10 S28 S27 103.64(15) . 1_545 ? Pb10 S28 S27 61.33(9) 1_545 1_545 ? Pb15 S28 S27 102.98(8) 1_545 1_545 ? Pb15 S28 S27 155.9(2) . 1_545 ? S24 S28 S27 112.92(15) . 1_545 ? Sb15 S29 Pb13 102.70(11) . . ? Sb15 S29 Pb13 102.70(11) . 1_545 ? Pb13 S29 Pb13 88.80(11) . 1_545 ? Sb15 S29 Pb12a 101.68(12) . . ? Pb13 S29 Pb12a 87.21(4) . . ? Pb13 S29 Pb12a 155.58(15) 1_545 . ? Sb15 S29 Pb12a 101.68(12) . 1_545 ? Pb13 S29 Pb12a 155.58(15) . 1_545 ? Pb13 S29 Pb12a 87.21(4) 1_545 1_545 ? Pb12a S29 Pb12a 86.55(11) . 1_545 ? Sb15 S29 Sb12b 93.02(16) . 1_545 ? Pb13 S29 Sb12b 164.03(18) . 1_545 ? Pb13 S29 Sb12b 90.46(8) 1_545 1_545 ? Pb12a S29 Sb12b 86.89(11) . 1_545 ? Pb12a S29 Sb12b 8.77(9) 1_545 1_545 ? Sb15 S29 Sb12b 93.02(16) . . ? Pb13 S29 Sb12b 90.46(8) . . ? Pb13 S29 Sb12b 164.03(18) 1_545 . ? Pb12a S29 Sb12b 8.77(9) . . ? Pb12a S29 Sb12b 86.89(11) 1_545 . ? Sb12b S29 Sb12b 85.90(17) 1_545 . ? Sb15 S29 S26 49.08(9) . . ? Pb13 S29 S26 94.40(6) . . ? Pb13 S29 S26 151.61(14) 1_545 . ? Pb12a S29 S26 52.80(10) . . ? Pb12a S29 S26 100.49(13) 1_545 . ? Sb12b S29 S26 93.81(15) 1_545 . ? Sb12b S29 S26 44.32(14) . . ? Sb15 S29 S26 49.08(9) . 1_545 ? Pb13 S29 S26 151.61(14) . 1_545 ? Pb13 S29 S26 94.41(6) 1_545 1_545 ? Pb12a S29 S26 100.49(13) . 1_545 ? Pb12a S29 S26 52.80(10) 1_545 1_545 ? Sb12b S29 S26 44.33(14) 1_545 1_545 ? Sb12b S29 S26 93.81(15) . 1_545 ? S26 S29 S26 70.03(10) . 1_545 ? Sb15 S29 S31 145.78(5) . . ? Pb13 S29 S31 57.14(8) . . ? Pb13 S29 S31 103.98(12) 1_545 . ? Pb12a S29 S31 54.29(10) . . ? Pb12a S29 S31 100.64(13) 1_545 . ? Sb12b S29 S31 107.74(16) 1_545 . ? Sb12b S29 S31 62.68(14) . . ? S26 S29 S31 101.39(8) . . ? S26 S29 S31 147.20(15) 1_545 . ? Sb15 S29 S31 145.78(5) . 1_545 ? Pb13 S29 S31 103.98(12) . 1_545 ? Pb13 S29 S31 57.13(8) 1_545 1_545 ? Pb12a S29 S31 100.64(13) . 1_545 ? Pb12a S29 S31 54.29(10) 1_545 1_545 ? Sb12b S29 S31 62.67(14) 1_545 1_545 ? Sb12b S29 S31 107.74(16) . 1_545 ? S26 S29 S31 147.20(15) . 1_545 ? S26 S29 S31 101.39(8) 1_545 1_545 ? S31 S29 S31 68.17(11) . 1_545 ? Sb15 S29 S32 53.60(9) . 1_545 ? Pb13 S29 S32 96.50(11) . 1_545 ? Pb13 S29 S32 49.18(8) 1_545 1_545 ? Pb12a S29 S32 155.24(15) . 1_545 ? Pb12a S29 S32 99.02(6) 1_545 1_545 ? Sb12b S29 S32 95.06(10) 1_545 1_545 ? Sb12b S29 S32 146.62(18) . 1_545 ? S26 S29 S32 102.45(13) . 1_545 ? S26 S29 S32 65.59(10) 1_545 1_545 ? S31 S29 S32 145.58(15) . 1_545 ? S31 S29 S32 102.17(9) 1_545 1_545 ? Sb20 S30 Sb17 98.1(2) . 1_545 ? Sb20 S30 Sb17 98.1(2) . . ? Sb17 S30 Sb17 100.1(3) 1_545 . ? Sb20 S30 Pb15 103.91(13) . 1_545 ? Sb17 S30 Pb15 6.18(15) 1_545 1_545 ? Sb17 S30 Pb15 97.03(18) . 1_545 ? Sb20 S30 Pb15 103.91(13) . . ? Sb17 S30 Pb15 97.03(18) 1_545 . ? Sb17 S30 Pb15 6.18(15) . . ? Pb15 S30 Pb15 93.50(16) 1_545 . ? Sb20 S30 Pb11 107.64(11) . . ? Sb17 S30 Pb11 152.7(2) 1_545 . ? Sb17 S30 Pb11 85.59(19) . . ? Pb15 S30 Pb11 147.64(16) 1_545 . ? Pb15 S30 Pb11 85.85(8) . . ? Sb20 S30 Pb11 107.64(11) . 1_545 ? Sb17 S30 Pb11 85.59(19) 1_545 1_545 ? Sb17 S30 Pb11 152.7(2) . 1_545 ? Pb15 S30 Pb11 85.85(8) 1_545 1_545 ? Pb15 S30 Pb11 147.64(16) . 1_545 ? Pb11 S30 Pb11 78.03(10) . 1_545 ? Sb20 S30 S31 47.28(9) . 1_545 ? Sb17 S30 S31 87.35(14) 1_545 1_545 ? Sb17 S30 S31 145.4(2) . 1_545 ? Pb15 S30 S31 92.87(8) 1_545 1_545 ? Pb15 S30 S31 151.15(17) . 1_545 ? Pb11 S30 S31 103.18(13) . 1_545 ? Pb11 S30 S31 60.94(9) 1_545 1_545 ? Sb20 S30 S31 47.28(9) . . ? Sb17 S30 S31 145.4(2) 1_545 . ? Sb17 S30 S31 87.35(14) . . ? Pb15 S30 S31 151.15(17) 1_545 . ? Pb15 S30 S31 92.88(8) . . ? Pb11 S30 S31 60.94(9) . . ? Pb11 S30 S31 103.18(13) 1_545 . ? S31 S30 S31 69.06(11) 1_545 . ? Sb20 S30 S24 151.83(17) . . ? Sb17 S30 S24 99.9(2) 1_545 . ? Sb17 S30 S24 99.9(2) . . ? Pb15 S30 S24 95.22(13) 1_545 . ? Pb15 S30 S24 95.22(13) . . ? Pb11 S30 S24 52.78(7) . . ? Pb11 S30 S24 52.78(7) 1_545 . ? S31 S30 S24 112.17(13) 1_545 . ? S31 S30 S24 112.17(13) . . ? Sb20 S30 S34 57.47(9) . . ? Sb17 S30 S34 95.5(2) 1_545 . ? Sb17 S30 S34 41.75(19) . . ? Pb15 S30 S34 96.79(14) 1_545 . ? Pb15 S30 S34 47.07(10) . . ? Pb11 S30 S34 105.99(5) . . ? Pb11 S30 S34 165.09(14) 1_545 . ? S31 S30 S34 104.21(14) 1_545 . ? S31 S30 S34 67.87(10) . . ? S24 S30 S34 140.92(9) . . ? Sb20 S31 Pb16 100.74(15) . 1_565 ? Sb20 S31 Sb20 100.74(15) . 1_565 ? Pb16 S31 Sb20 0.00(5) 1_565 1_565 ? Sb20 S31 Pb12a 129.27(8) . . ? Pb16 S31 Pb12a 129.28(8) 1_565 . ? Sb20 S31 Pb12a 129.28(8) 1_565 . ? Sb20 S31 Pb13 91.46(12) . . ? Pb16 S31 Pb13 91.46(12) 1_565 . ? Sb20 S31 Pb13 91.46(12) 1_565 . ? Pb12a S31 Pb13 80.70(12) . . ? Sb20 S31 Pb11 99.98(12) . . ? Pb16 S31 Pb11 99.98(12) 1_565 . ? Sb20 S31 Pb11 99.98(12) 1_565 . ? Pb12a S31 Pb11 81.24(11) . . ? Pb13 S31 Pb11 161.94(15) . . ? Sb20 S31 Sb12b 128.88(8) . . ? Pb16 S31 Sb12b 128.88(8) 1_565 . ? Sb20 S31 Sb12b 128.88(8) 1_565 . ? Pb12a S31 Sb12b 3.20(11) . . ? Pb13 S31 Sb12b 77.50(13) . . ? Pb11 S31 Sb12b 84.44(13) . . ? Sb20 S31 S25 88.02(8) . . ? Pb16 S31 S25 147.13(18) 1_565 . ? Sb20 S31 S25 147.13(18) 1_565 . ? Pb12a S31 S25 55.79(9) . . ? Pb13 S31 S25 120.18(12) . . ? Pb11 S31 S25 47.16(8) . . ? Sb12b S31 S25 58.15(11) . . ? Sb20 S31 S25 147.13(18) . 1_565 ? Pb16 S31 S25 88.02(8) 1_565 1_565 ? Sb20 S31 S25 88.02(8) 1_565 1_565 ? Pb12a S31 S25 55.79(9) . 1_565 ? Pb13 S31 S25 120.17(12) . 1_565 ? Pb11 S31 S25 47.16(8) . 1_565 ? Sb12b S31 S25 58.15(11) . 1_565 ? S25 S31 S25 69.18(12) . 1_565 ? Sb20 S31 S30 46.06(9) . . ? Pb16 S31 S30 100.32(14) 1_565 . ? Sb20 S31 S30 100.32(14) 1_565 . ? Pb12a S31 S30 119.22(14) . . ? Pb13 S31 S30 137.21(11) . . ? Pb11 S31 S30 54.44(9) . . ? Sb12b S31 S30 121.62(14) . . ? S25 S31 S30 63.48(11) . . ? S25 S31 S30 101.37(15) 1_565 . ? Sb20 S31 S30 100.33(14) . 1_565 ? Pb16 S31 S30 46.06(9) 1_565 1_565 ? Sb20 S31 S30 46.06(9) 1_565 1_565 ? Pb12a S31 S30 119.21(14) . 1_565 ? Pb13 S31 S30 137.21(11) . 1_565 ? Pb11 S31 S30 54.44(9) . 1_565 ? Sb12b S31 S30 121.62(14) . 1_565 ? S25 S31 S30 101.36(15) . 1_565 ? S25 S31 S30 63.48(11) 1_565 1_565 ? S30 S31 S30 69.06(11) . 1_565 ? Pb13 S32 Sb18 93.18(11) . . ? Pb13 S32 Sb18 93.18(11) . 1_565 ? Sb18 S32 Sb18 89.67(13) . 1_565 ? Pb13 S32 Sb15 91.52(11) . 1_565 ? Sb18 S32 Sb15 174.82(16) . 1_565 ? Sb18 S32 Sb15 92.24(3) 1_565 1_565 ? Pb13 S32 Sb15 91.52(11) . . ? Sb18 S32 Sb15 92.24(3) . . ? Sb18 S32 Sb15 174.82(16) 1_565 . ? Sb15 S32 Sb15 85.47(12) 1_565 . ? Pb13 S32 S35 52.30(8) . 1_565 ? Sb18 S32 S35 91.35(12) . 1_565 ? Sb18 S32 S35 40.89(8) 1_565 1_565 ? Sb15 S32 S35 93.24(7) 1_565 1_565 ? Sb15 S32 S35 143.79(15) . 1_565 ? Pb13 S32 S35 52.30(8) . . ? Sb18 S32 S35 40.89(8) . . ? Sb18 S32 S35 91.35(12) 1_565 . ? Sb15 S32 S35 143.79(15) 1_565 . ? Sb15 S32 S35 93.24(7) . . ? S35 S32 S35 67.12(10) 1_565 . ? Pb13 S32 S29 50.53(8) . 1_565 ? Sb18 S32 S29 143.71(15) . 1_565 ? Sb18 S32 S29 91.91(7) 1_565 1_565 ? Sb15 S32 S29 41.05(7) 1_565 1_565 ? Sb15 S32 S29 89.40(12) . 1_565 ? S35 S32 S29 67.42(10) 1_565 1_565 ? S35 S32 S29 102.82(13) . 1_565 ? Pb13 S32 S29 50.53(8) . . ? Sb18 S32 S29 91.91(7) . . ? Sb18 S32 S29 143.71(15) 1_565 . ? Sb15 S32 S29 89.40(12) 1_565 . ? Sb15 S32 S29 41.05(7) . . ? S35 S32 S29 102.82(13) 1_565 . ? S35 S32 S29 67.42(10) . . ? S29 S32 S29 66.46(10) 1_565 . ? Pb13 S32 S7 145.88(16) . 7_556 ? Sb18 S32 S7 110.53(11) . 7_556 ? Sb18 S32 S7 110.53(11) 1_565 7_556 ? Sb15 S32 S7 64.30(9) 1_565 7_556 ? Sb15 S32 S7 64.30(9) . 7_556 ? S35 S32 S7 145.46(6) 1_565 7_556 ? S35 S32 S7 145.47(6) . 7_556 ? S29 S32 S7 102.78(12) 1_565 7_556 ? S29 S32 S7 102.78(12) . 7_556 ? Pb13 S32 S36 92.68(13) . . ? Sb18 S32 S36 44.86(7) . . ? Sb18 S32 S36 44.86(7) 1_565 . ? Sb15 S32 S36 137.05(6) 1_565 . ? Sb15 S32 S36 137.05(6) . . ? S35 S32 S36 57.53(10) 1_565 . ? S35 S32 S36 57.53(10) . . ? S29 S32 S36 124.95(12) 1_565 . ? S29 S32 S36 124.95(12) . . ? S7 S32 S36 121.45(15) 7_556 . ? Pb13 S32 Sb5 147.55(5) . 7_566 ? Sb18 S32 Sb5 113.86(13) . 7_566 ? Sb18 S32 Sb5 70.47(7) 1_565 7_566 ? Sb15 S32 Sb5 62.42(7) 1_565 7_566 ? Sb15 S32 Sb5 104.36(12) . 7_566 ? S35 S32 Sb5 106.98(6) 1_565 7_566 ? S35 S32 Sb5 150.61(14) . 7_566 ? S29 S32 Sb5 100.74(7) 1_565 7_566 ? S29 S32 Sb5 139.51(14) . 7_566 ? S7 S32 Sb5 40.22(6) 7_556 7_566 ? S36 S32 Sb5 94.38(11) . 7_566 ? Sb1 S33 Pb14 104.10(17) 3_545 3_545 ? Sb1 S33 Pb14 104.10(17) 3_545 3 ? Pb14 S33 Pb14 93.3(3) 3_545 3 ? Sb1 S33 Sb3 96.23(15) 3_545 3 ? Pb14 S33 Sb3 93.45(15) 3_545 3 ? Pb14 S33 Sb3 8.13(10) 3 3 ? Sb1 S33 Sb3 96.23(15) 3_545 3_545 ? Pb14 S33 Sb3 8.13(10) 3_545 3_545 ? Pb14 S33 Sb3 93.45(15) 3 3_545 ? Sb3 S33 Sb3 92.39(17) 3 3_545 ? Sb1 S33 Pb1 4.03(12) 3_545 3_545 ? Pb14 S33 Pb1 101.42(16) 3_545 3_545 ? Pb14 S33 Pb1 101.42(16) 3 3_545 ? Sb3 S33 Pb1 93.45(13) 3 3_545 ? Sb3 S33 Pb1 93.45(13) 3_545 3_545 ? Sb1 S33 Pb15 94.32(14) 3_545 . ? Pb14 S33 Pb15 160.5(2) 3_545 . ? Pb14 S33 Pb15 88.13(14) 3 . ? Sb3 S33 Pb15 90.72(8) 3 . ? Sb3 S33 Pb15 168.61(18) 3_545 . ? Pb1 S33 Pb15 97.29(12) 3_545 . ? Sb1 S33 Pb15 94.32(14) 3_545 1_545 ? Pb14 S33 Pb15 88.13(14) 3_545 1_545 ? Pb14 S33 Pb15 160.5(2) 3 1_545 ? Sb3 S33 Pb15 168.61(18) 3 1_545 ? Sb3 S33 Pb15 90.72(8) 3_545 1_545 ? Pb1 S33 Pb15 97.29(12) 3_545 1_545 ? Pb15 S33 Pb15 84.20(15) . 1_545 ? Sb1 S33 Sb17 88.81(18) 3_545 . ? Pb14 S33 Sb17 164.8(2) 3_545 . ? Pb14 S33 Sb17 91.14(17) 3 . ? Sb3 S33 Sb17 93.04(13) 3 . ? Sb3 S33 Sb17 172.1(2) 3_545 . ? Pb1 S33 Sb17 91.88(17) 3_545 . ? Pb15 S33 Sb17 5.77(13) . . ? Pb15 S33 Sb17 82.88(14) 1_545 . ? Sb1 S33 Sb17 88.82(18) 3_545 1_545 ? Pb14 S33 Sb17 91.14(17) 3_545 1_545 ? Pb14 S33 Sb17 164.8(2) 3 1_545 ? Sb3 S33 Sb17 172.1(2) 3 1_545 ? Sb3 S33 Sb17 93.04(13) 3_545 1_545 ? Pb1 S33 Sb17 91.88(17) 3_545 1_545 ? Pb15 S33 Sb17 82.88(14) . 1_545 ? Pb15 S33 Sb17 5.76(13) 1_545 1_545 ? Sb17 S33 Sb17 81.0(3) . 1_545 ? Sb1 S33 Sb61 150.9(2) 3_545 . ? Pb14 S33 Sb61 102.3(2) 3_545 . ? Pb14 S33 Sb61 62.1(3) 3 . ? Sb3 S33 Sb61 70.1(3) 3 . ? Sb3 S33 Sb61 109.50(19) 3_545 . ? Pb1 S33 Sb61 151.8(2) 3_545 . ? Pb15 S33 Sb61 61.47(15) . . ? Pb15 S33 Sb61 98.6(3) 1_545 . ? Sb17 S33 Sb61 67.23(18) . . ? Sb17 S33 Sb61 102.7(3) 1_545 . ? Sb1 S33 Sb61 150.9(2) 3_545 6 ? Pb14 S33 Sb61 62.1(3) 3_545 6 ? Pb14 S33 Sb61 102.3(2) 3 6 ? Sb3 S33 Sb61 109.50(19) 3 6 ? Sb3 S33 Sb61 70.1(3) 3_545 6 ? Pb1 S33 Sb61 151.8(2) 3_545 6 ? Pb15 S33 Sb61 98.6(3) . 6 ? Pb15 S33 Sb61 61.47(15) 1_545 6 ? Sb17 S33 Sb61 102.7(3) . 6 ? Sb17 S33 Sb61 67.23(19) 1_545 6 ? Sb61 S33 Sb61 55.7(5) . 6 ? Sb17 S34 Sb1 98.5(2) . 3 ? Sb17 S34 Sb1 98.5(2) . 3_545 ? Sb1 S34 Sb1 98.22(18) 3 3_545 ? Sb17 S34 Pb15 4.4(3) . . ? Sb1 S34 Pb15 95.69(15) 3 . ? Sb1 S34 Pb15 95.69(15) 3_545 . ? Sb17 S34 Pb1 108.41(19) . 3 ? Sb1 S34 Pb1 9.95(7) 3 3 ? Sb1 S34 Pb1 95.20(14) 3_545 3 ? Pb15 S34 Pb1 105.47(13) . 3 ? Sb17 S34 Pb1 108.41(19) . 3_545 ? Sb1 S34 Pb1 95.20(14) 3 3_545 ? Sb1 S34 Pb1 9.95(7) 3_545 3_545 ? Pb15 S34 Pb1 105.47(13) . 3_545 ? Pb1 S34 Pb1 90.70(13) 3 3_545 ? Sb17 S34 Pb16 87.97(19) . 1_565 ? Sb1 S34 Pb16 90.66(7) 3 1_565 ? Sb1 S34 Pb16 168.04(16) 3_545 1_565 ? Pb15 S34 Pb16 91.35(12) . 1_565 ? Pb1 S34 Pb16 92.21(5) 3 1_565 ? Pb1 S34 Pb16 161.48(16) 3_545 1_565 ? Sb17 S34 Sb20 87.97(19) . 1_565 ? Sb1 S34 Sb20 90.66(7) 3 1_565 ? Sb1 S34 Sb20 168.04(16) 3_545 1_565 ? Pb15 S34 Sb20 91.35(12) . 1_565 ? Pb1 S34 Sb20 92.21(5) 3 1_565 ? Pb1 S34 Sb20 161.48(16) 3_545 1_565 ? Pb16 S34 Sb20 0.00(4) 1_565 1_565 ? Sb17 S34 Sb20 87.97(19) . . ? Sb1 S34 Sb20 168.04(16) 3 . ? Sb1 S34 Sb20 90.67(7) 3_545 . ? Pb15 S34 Sb20 91.35(12) . . ? Pb1 S34 Sb20 161.48(16) 3 . ? Pb1 S34 Sb20 92.21(5) 3_545 . ? Pb16 S34 Sb20 79.49(10) 1_565 . ? Sb20 S34 Sb20 79.49(10) 1_565 . ? Sb17 S34 S33 57.87(19) . . ? Sb1 S34 S33 95.45(15) 3 . ? Sb1 S34 S33 41.49(12) 3_545 . ? Pb15 S34 S33 54.61(10) . . ? Pb1 S34 S33 99.52(13) 3 . ? Pb1 S34 S33 51.03(9) 3_545 . ? Pb16 S34 S33 145.81(15) 1_565 . ? Sb20 S34 S33 145.81(15) 1_565 . ? Sb20 S34 S33 96.51(7) . . ? Sb17 S34 S33 57.87(19) . 1_565 ? Sb1 S34 S33 41.50(12) 3 1_565 ? Sb1 S34 S33 95.45(15) 3_545 1_565 ? Pb15 S34 S33 54.61(10) . 1_565 ? Pb1 S34 S33 51.03(9) 3 1_565 ? Pb1 S34 S33 99.52(13) 3_545 1_565 ? Pb16 S34 S33 96.51(7) 1_565 1_565 ? Sb20 S34 S33 96.51(7) 1_565 1_565 ? Sb20 S34 S33 145.81(15) . 1_565 ? S33 S34 S33 67.87(10) . 1_565 ? Sb18 S35 Pb2 105.16(11) . 3 ? Sb18 S35 Pb2 105.16(11) . 3_545 ? Pb2 S35 Pb2 86.58(11) 3 3_545 ? Sb18 S35 Pb13 100.91(11) . 1_545 ? Pb2 S35 Pb13 153.91(15) 3 1_545 ? Pb2 S35 Pb13 87.68(4) 3_545 1_545 ? Sb18 S35 Pb13 100.91(11) . . ? Pb2 S35 Pb13 87.68(4) 3 . ? Pb2 S35 Pb13 153.91(15) 3_545 . ? Pb13 S35 Pb13 86.37(10) 1_545 . ? Sb18 S35 S1 145.10(5) . 3_545 ? Pb2 S35 S1 101.35(12) 3 3_545 ? Pb2 S35 S1 54.05(8) 3_545 3_545 ? Pb13 S35 S1 55.50(8) 1_545 3_545 ? Pb13 S35 S1 102.47(12) . 3_545 ? Sb18 S35 S1 145.10(5) . 3 ? Pb2 S35 S1 54.05(8) 3 3 ? Pb2 S35 S1 101.35(12) 3_545 3 ? Pb13 S35 S1 102.47(12) 1_545 3 ? Pb13 S35 S1 55.51(8) . 3 ? S1 S35 S1 69.71(11) 3_545 3 ? Sb18 S35 S36 48.80(9) . . ? Pb2 S35 S36 56.42(9) 3 . ? Pb2 S35 S36 102.28(12) 3_545 . ? Pb13 S35 S36 149.53(15) 1_545 . ? Pb13 S35 S36 95.59(7) . . ? S1 S35 S36 150.89(16) 3_545 . ? S1 S35 S36 103.61(8) 3 . ? Sb18 S35 S36 48.80(9) . 1_545 ? Pb2 S35 S36 102.28(12) 3 1_545 ? Pb2 S35 S36 56.42(9) 3_545 1_545 ? Pb13 S35 S36 95.59(7) 1_545 1_545 ? Pb13 S35 S36 149.53(15) . 1_545 ? S1 S35 S36 103.61(8) 3_545 1_545 ? S1 S35 S36 150.89(16) 3 1_545 ? S36 S35 S36 67.90(11) . 1_545 ? Sb18 S35 S32 51.57(9) . . ? Pb2 S35 S32 99.23(6) 3 . ? Pb2 S35 S32 156.73(14) 3_545 . ? Pb13 S35 S32 96.04(12) 1_545 . ? Pb13 S35 S32 49.34(8) . . ? S1 S35 S32 144.09(15) 3_545 . ? S1 S35 S32 100.26(8) 3 . ? S36 S35 S32 64.00(11) . . ? S36 S35 S32 100.32(13) 1_545 . ? Sb18 S35 S32 51.57(9) . 1_545 ? Pb2 S35 S32 156.73(14) 3 1_545 ? Pb2 S35 S32 99.23(6) 3_545 1_545 ? Pb13 S35 S32 49.34(8) 1_545 1_545 ? Pb13 S35 S32 96.03(12) . 1_545 ? S1 S35 S32 100.25(8) 3_545 1_545 ? S1 S35 S32 144.09(15) 3 1_545 ? S36 S35 S32 100.32(13) . 1_545 ? S36 S35 S32 64.00(11) 1_545 1_545 ? S32 S35 S32 67.12(10) . 1_545 ? Sb18 S35 S35 90.0 . 1_565 ? Pb2 S35 S35 46.71(5) 3 1_565 ? Pb2 S35 S35 133.29(5) 3_545 1_565 ? Pb13 S35 S35 133.19(5) 1_545 1_565 ? Pb13 S35 S35 46.81(5) . 1_565 ? S1 S35 S35 124.86(5) 3_545 1_565 ? S1 S35 S35 55.15(5) 3 1_565 ? S36 S35 S35 56.05(5) . 1_565 ? S36 S35 S35 123.95(5) 1_545 1_565 ? S32 S35 S35 56.44(5) . 1_565 ? S32 S35 S35 123.56(5) 1_545 1_565 ? Sb18 S36 Sb18 95.86(16) 1_565 . ? Sb18 S36 Sb5 89.51(4) 1_565 3 ? Sb18 S36 Sb5 173.44(16) . 3 ? Sb18 S36 Sb5 173.44(16) 1_565 3_545 ? Sb18 S36 Sb5 89.51(4) . 3_545 ? Sb5 S36 Sb5 84.90(13) 3 3_545 ? Sb18 S36 Pb2 92.40(12) 1_565 3 ? Sb18 S36 Pb2 92.40(12) . 3 ? Sb5 S36 Pb2 91.15(12) 3 3 ? Sb5 S36 Pb2 91.15(12) 3_545 3 ? Sb18 S36 S35 41.45(8) 1_565 1_565 ? Sb18 S36 S35 94.56(14) . 1_565 ? Sb5 S36 S35 91.96(8) 3 1_565 ? Sb5 S36 S35 142.01(17) 3_545 1_565 ? Pb2 S36 S35 51.00(9) 3 1_565 ? Sb18 S36 S35 94.56(14) 1_565 . ? Sb18 S36 S35 41.45(8) . . ? Sb5 S36 S35 142.01(17) 3 . ? Sb5 S36 S35 91.96(8) 3_545 . ? Pb2 S36 S35 51.00(9) 3 . ? S35 S36 S35 67.90(11) 1_565 . ? Sb18 S36 S6 90.40(8) 1_565 3 ? Sb18 S36 S6 144.04(17) . 3 ? Sb5 S36 S6 39.28(7) 3 3 ? Sb5 S36 S6 87.45(13) 3_545 3 ? Pb2 S36 S6 51.88(8) 3 3 ? S35 S36 S6 67.58(10) 1_565 3 ? S35 S36 S6 102.84(14) . 3 ? Sb18 S36 S6 144.04(17) 1_565 3_545 ? Sb18 S36 S6 90.40(8) . 3_545 ? Sb5 S36 S6 87.45(13) 3 3_545 ? Sb5 S36 S6 39.28(7) 3_545 3_545 ? Pb2 S36 S6 51.88(8) 3 3_545 ? S35 S36 S6 102.85(14) 1_565 3_545 ? S35 S36 S6 67.57(10) . 3_545 ? S6 S36 S6 65.44(10) 3 3_545 ? Sb18 S36 S32 47.96(8) 1_565 . ? Sb18 S36 S32 47.96(8) . . ? Sb5 S36 S32 137.46(7) 3 . ? Sb5 S36 S32 137.46(7) 3_545 . ? Pb2 S36 S32 91.57(13) 3 . ? S35 S36 S32 58.47(10) 1_565 . ? S35 S36 S32 58.47(10) . . ? S6 S36 S32 126.04(12) 3 . ? S6 S36 S32 126.04(12) 3_545 . ? Sb18 S36 S7 131.87(8) 1_565 3 ? Sb18 S36 S7 131.87(8) . 3 ? Sb5 S36 S7 42.45(6) 3 3 ? Sb5 S36 S7 42.45(6) 3_545 3 ? Pb2 S36 S7 91.52(13) 3 3 ? S35 S36 S7 123.84(13) 1_565 3 ? S35 S36 S7 123.84(13) . 3 ? S6 S36 S7 56.29(9) 3 3 ? S6 S36 S7 56.29(9) 3_545 3 ? S32 S36 S7 176.91(17) . 3 ? Sb18 S36 S32 107.95(13) 1_565 5_666 ? Sb18 S36 S32 107.95(13) . 5_666 ? Sb5 S36 S32 66.63(10) 3 5_666 ? Sb5 S36 S32 66.63(10) 3_545 5_666 ? Pb2 S36 S32 149.04(17) 3 5_666 ? S35 S36 S32 144.85(7) 1_565 5_666 ? S35 S36 S32 144.85(7) . 5_666 ? S6 S36 S32 103.61(13) 3 5_666 ? S6 S36 S32 103.61(13) 3_545 5_666 ? S32 S36 S32 119.40(14) . 5_666 ? S7 S36 S32 57.51(11) 3 5_666 ? Sb14 O As14 143.4(17) . 1_545 ? Sb14 O Sb14 143.4(17) . 1_545 ? As14 O Sb14 0.00(10) 1_545 1_545 ? Sb14 O S22 59.2(3) . . ? As14 O S22 153.5(14) 1_545 . ? Sb14 O S22 153.5(14) 1_545 . ? Sb14 O S22 153.5(14) . 1_545 ? As14 O S22 59.2(3) 1_545 1_545 ? Sb14 O S22 59.2(3) 1_545 1_545 ? S22 O S22 95.7(10) . 1_545 ? Sb14 O Sb12b 99.2(9) . 1_545 ? As14 O Sb12b 99.2(9) 1_545 1_545 ? Sb14 O Sb12b 99.2(9) 1_545 1_545 ? S22 O Sb12b 56.4(6) . 1_545 ? S22 O Sb12b 56.4(6) 1_545 1_545 ? Sb14 O Pb12a 96.7(9) . 1_545 ? As14 O Pb12a 96.7(9) 1_545 1_545 ? Sb14 O Pb12a 96.7(9) 1_545 1_545 ? S22 O Pb12a 60.8(6) . 1_545 ? S22 O Pb12a 60.8(6) 1_545 1_545 ? Sb12b O Pb12a 8.81(13) 1_545 1_545 ? Sb14 O As10 88.7(9) . 1_545 ? As14 O As10 88.7(9) 1_545 1_545 ? Sb14 O As10 88.7(9) 1_545 1_545 ? S22 O As10 109.0(9) . 1_545 ? S22 O As10 109.0(9) 1_545 1_545 ? Sb12b O As10 153.6(12) 1_545 1_545 ? Pb12a O As10 162.4(12) 1_545 1_545 ? Sb14 O Sb10 88.7(9) . 1_545 ? As14 O Sb10 88.7(9) 1_545 1_545 ? Sb14 O Sb10 88.7(9) 1_545 1_545 ? S22 O Sb10 109.0(9) . 1_545 ? S22 O Sb10 109.0(9) 1_545 1_545 ? Sb12b O Sb10 153.6(12) 1_545 1_545 ? Pb12a O Sb10 162.4(12) 1_545 1_545 ? As10 O Sb10 0.00(7) 1_545 1_545 ? Sb14 O Pb8 107.1(9) . 1_545 ? As14 O Pb8 107.1(9) 1_545 1_545 ? Sb14 O Pb8 107.1(9) 1_545 1_545 ? S22 O Pb8 62.1(6) . 1_545 ? S22 O Pb8 62.1(6) 1_545 1_545 ? Sb12b O Pb8 80.3(8) 1_545 1_545 ? Pb12a O Pb8 89.1(9) 1_545 1_545 ? As10 O Pb8 73.3(7) 1_545 1_545 ? Sb10 O Pb8 73.3(7) 1_545 1_545 ? Sb14 O S21 71.7(8) . 1_545 ? As14 O S21 71.7(8) 1_545 1_545 ? Sb14 O S21 71.7(8) 1_545 1_545 ? S22 O S21 128.8(6) . 1_545 ? S22 O S21 128.8(6) 1_545 1_545 ? Sb12b O S21 124.5(11) 1_545 1_545 ? Pb12a O S21 115.7(11) 1_545 1_545 ? As10 O S21 82.0(8) 1_545 1_545 ? Sb10 O S21 82.0(8) 1_545 1_545 ? Pb8 O S21 155.2(12) 1_545 1_545 ? _refine_diff_density_max 5.231 _refine_diff_density_min -4.905 _refine_diff_density_rms 0.462