# # h,k,l, Fc-squared, Fo-squared, sigma(Fo-squared) and status flag # data_shelxl _shelx_title ' xx1 in P -1' _shelx_refln_list_code 4 _shelx_F_calc_maximum 1005.62 _exptl_crystal_F_000 2128.00 _reflns_d_resolution_high 0.7143 loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' _cell_length_a 8.9200 _cell_length_b 9.4290 _cell_length_c 20.0620 _cell_angle_alpha 79.660 _cell_angle_beta 88.840 _cell_angle_gamma 62.720 _shelx_F_squared_multiplier 1.000 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_calc _refln_F_squared_meas _refln_F_squared_sigma _refln_observed_status 2 0 0 94727.63 138515.27 3115.99 o 3 0 0 654582.13 852293.25 37283.71 o 4 0 0 12940.05 25331.12 2418.51 o 5 0 0 41399.67 46546.21 2327.00 o 6 0 0 86469.04 113541.76 12766.27 o 7 0 0 6749.03 7744.38 1793.75 o 8 0 0 52893.07 56973.45 5385.17 o 9 0 0 2059.21 1679.00 2614.71 o 10 0 0 9433.38 6913.08 4709.17 o 11 0 0 286.18 3582.83 5358.12 o -10 1 0 2308.15 6414.94 5309.89 o -9 1 0 13470.66 16913.53 4487.55 o -8 1 0 7886.03 6966.28 2594.58 o -7 1 0 24771.69 25112.55 3320.60 o -6 1 0 52063.82 52281.09 6355.95 o -5 1 0 17504.56 22178.25 1953.47 o -4 1 0 187774.08 217713.98 4797.18 o -3 1 0 185370.45 214048.73 7196.11 o -1 1 0 4721.64 7468.95 1366.46 o 2 1 0 58512.35 68198.02 1859.88 o 3 1 0 40291.58 41722.26 1627.17 o 4 1 0 29973.82 35449.65 4052.14 o 5 1 0 113078.45 128646.78 7885.38 o 6 1 0 2803.48 7091.48 2265.77 o 7 1 0 47606.21 49714.27 3427.26 o 8 1 0 33888.03 37021.05 3034.86 o 9 1 0 1039.70 833.01 2440.06 o 10 1 0 18498.49 19116.21 7586.64 o 11 1 0 907.87 2024.82 5724.92 o -10 2 0 12270.16 7410.22 8918.53 o -9 2 0 1567.35 3299.67 3666.56 o -8 2 0 312.37 3413.37 2986.79 o -7 2 0 25851.66 21096.21 3421.55 o -6 2 0 12101.01 13268.36 3426.82 o -5 2 0 6850.70 6317.01 1741.17 o -4 2 0 24835.44 23732.97 1876.13 o -3 2 0 975.35 1494.94 1091.11 o -2 2 0 58385.53 66049.30 2896.64 o -1 2 0 260138.47 269059.25 5084.73 o 0 2 0 48653.97 44445.45 2219.64 o 1 2 0 10809.71 5120.90 830.71 o 2 2 0 187784.67 193838.39 1931.75 o 3 2 0 33679.43 37745.47 1968.32 o 4 2 0 980.51 1657.80 772.68 o 5 2 0 75802.41 98004.38 7394.41 o 6 2 0 68087.74 79651.06 5989.50 o 7 2 0 21768.84 26360.72 2884.43 o 8 2 0 3663.08 4193.95 1844.65 o 9 2 0 446.33 1338.91 3934.46 o 10 2 0 198.11 2169.47 3462.38 o 11 2 0 4514.69 2559.27 4850.83 o -9 3 0 8.25 3394.17 3170.92 o -8 3 0 11402.01 9927.22 3726.75 o -7 3 0 1654.44 2860.27 2650.11 o -6 3 0 5459.95 3474.64 2229.48 o -5 3 0 132917.55 142865.52 6203.46 o -4 3 0 3401.09 3787.03 1892.40 o -3 3 0 23942.12 25226.81 2654.22 o -2 3 0 71627.34 73634.09 3576.92 o -1 3 0 54994.25 63642.12 3433.75 o 0 3 0 495327.84 428889.91 5956.88 o 1 3 0 183488.27 127081.85 6067.07 o 2 3 0 10727.06 9272.36 1322.28 o 3 3 0 777296.31 726452.00 29058.79 o 4 3 0 50012.43 50419.08 3585.51 o 5 3 0 126019.36 150061.61 6535.15 o 6 3 0 116615.26 158481.25 9038.74 o 7 3 0 269.77 1431.26 1163.62 o 8 3 0 53525.57 59565.61 4314.33 o 9 3 0 23956.90 28080.82 5352.57 o 10 3 0 5748.32 4645.44 4834.60 o 11 3 0 14052.31 12124.63 7436.76 o 12 3 0 24.91 2167.57 5438.62 o -8 4 0 23157.24 17057.67 5375.66 o -7 4 0 0.36 2744.45 2719.99 o -6 4 0 14091.83 10993.00 2578.36 o -5 4 0 13439.38 13205.29 2486.33 o -4 4 0 2457.31 1718.19 1442.71 o -3 4 0 55846.24 61109.01 3521.14 o -2 4 0 48.21 495.61 1014.85 o -1 4 0 37247.43 29839.74 3274.94 o 0 4 0 278557.16 237782.13 5242.23 o 1 4 0 139622.38 93509.36 8088.03 o 2 4 0 21613.83 17509.75 1635.19 o 3 4 0 38470.08 34505.96 7899.15 o 4 4 0 105797.94 90100.25 1648.28 o 5 4 0 29778.31 32614.83 4773.92 o 6 4 0 6751.96 9516.59 2620.52 o 7 4 0 5436.35 6109.91 2179.20 o 8 4 0 51856.19 55354.55 5020.71 o 9 4 0 38.11 2979.18 2628.78 o 10 4 0 20202.57 15908.97 4866.93 o 11 4 0 1172.21 2573.23 4746.19 o 12 4 0 70.36 3249.61 5159.06 o -7 5 0 16942.77 14867.83 3805.41 o -6 5 0 11661.19 8380.75 3005.61 o -5 5 0 227.18 2102.49 2414.02 o -4 5 0 5911.40 7672.42 2734.97 o -3 5 0 66659.82 71173.34 3845.10 o -2 5 0 595.83 959.37 1375.99 o -1 5 0 8953.60 9015.59 2349.51 o 0 5 0 27248.19 19656.29 3161.97 o 1 5 0 3324.23 2870.39 1226.29 o 2 5 0 133196.92 95323.84 2523.63 o 3 5 0 34201.87 22212.01 1817.12 o 4 5 0 112366.34 76038.59 15982.34 o 5 5 0 61114.19 66107.91 6057.22 o 6 5 0 54066.07 50508.89 5075.89 o 7 5 0 38139.95 42668.50 6125.86 o 8 5 0 21372.95 22749.69 3713.80 o 9 5 0 22390.26 23811.84 4150.53 o 10 5 0 18180.13 8275.32 3586.54 o 11 5 0 3848.89 7055.35 5474.77 o 12 5 0 60.05 2431.61 7126.96 o -7 6 0 80.26 1563.97 4779.05 o -6 6 0 956.64 1555.97 3647.44 o -5 6 0 3733.75 3873.19 3165.10 o -4 6 0 429.16 991.52 2669.32 o -3 6 0 1473.38 2337.54 2761.04 o -2 6 0 29761.48 38925.18 6251.34 o -1 6 0 34065.22 37070.79 5775.14 o 0 6 0 168940.50 200818.66 6697.41 o 1 6 0 15336.11 11928.23 2306.09 o 2 6 0 1540.38 1470.91 1305.87 o 3 6 0 105852.59 85747.11 2580.65 o 4 6 0 1165.00 1778.62 2127.98 o 5 6 0 16354.49 11337.18 4861.10 o 6 6 0 101177.72 104052.32 6335.15 o 7 6 0 14065.21 13500.58 5086.45 o 8 6 0 16465.22 13778.31 3043.37 o 9 6 0 2093.00 2761.19 2211.05 o 10 6 0 1517.49 1284.60 2449.05 o 11 6 0 165.89 2182.44 2787.60 o 12 6 0 1012.07 4178.57 6964.76 o -6 7 0 1783.33 2416.91 4927.97 o -5 7 0 40452.30 36714.88 12241.37 o -4 7 0 5790.95 5458.64 3490.66 o -3 7 0 14320.58 15641.13 5272.34 o -2 7 0 31922.33 41317.13 6457.04 o -1 7 0 2589.87 3147.30 3749.92 o 0 7 0 17489.19 20550.45 5646.70 o 1 7 0 19297.34 24173.61 4451.01 o 2 7 0 464.12 1426.26 1313.06 o 3 7 0 55682.72 48310.86 2825.74 o 4 7 0 13797.02 12898.47 4936.14 o 5 7 0 17834.82 18615.94 4916.61 o 6 7 0 4670.34 2065.21 2490.73 o 7 7 0 1229.12 2151.01 2529.33 o 8 7 0 46347.41 47462.98 4469.23 o 9 7 0 483.71 2798.36 2654.19 o 10 7 0 3592.87 3719.71 3579.38 o 11 7 0 13412.53 8498.43 4147.62 o 12 7 0 1150.20 2453.46 4124.56 o -5 8 0 1993.27 4466.68 7663.40 o -4 8 0 8.72 3917.85 4788.65 o -3 8 0 15489.76 21136.72 7697.45 o -2 8 0 206.87 2368.48 3208.70 o -1 8 0 3336.60 2389.58 3172.92 o 0 8 0 42773.60 52425.20 7181.05 o 1 8 0 1024.43 3592.13 3958.13 o 2 8 0 32289.05 35996.98 6952.33 o 3 8 0 24331.35 21921.52 3923.88 o 4 8 0 625.43 2269.37 1995.72 o 5 8 0 84061.70 72399.94 14833.37 o 6 8 0 10059.09 8834.15 4538.75 o 7 8 0 17612.91 17370.15 4322.08 o 8 8 0 20611.14 17932.49 4069.75 o 9 8 0 2752.64 2218.03 2917.65 o 10 8 0 7906.06 4405.97 2882.33 o 11 8 0 1498.69 4053.93 3431.42 o 12 8 0 2319.46 2204.10 5464.78 o -3 9 0 869.57 4260.87 4394.24 o -2 9 0 5973.48 5462.39 4754.15 o -1 9 0 1661.68 2779.64 4714.00 o 0 9 0 385.97 1998.38 4051.17 o 1 9 0 25505.02 29948.36 6227.71 o 2 9 0 16707.40 12183.08 5892.66 o 3 9 0 32752.60 32559.97 4296.39 o 4 9 0 4012.99 3259.34 2560.15 o 5 9 0 1313.28 2647.15 2280.78 o 6 9 0 9142.87 5871.11 4750.26 o 7 9 0 4301.96 4359.56 4243.03 o 8 9 0 87.02 1118.10 3051.40 o 9 9 0 5670.67 4741.06 4837.55 o 10 9 0 16797.27 15540.58 7152.94 o 11 9 0 1799.82 1787.14 4561.65 o -2 10 0 7729.07 12053.02 7430.93 o -1 10 0 4083.91 3220.82 4892.49 o 0 10 0 15642.25 16567.77 8135.23 o 1 10 0 519.61 1092.67 3693.30 o 2 10 0 4.36 3449.75 4697.41 o 3 10 0 17553.07 21198.64 6635.26 o 4 10 0 47.09 2658.43 2564.66 o 5 10 0 562.99 1493.59 2793.24 o 6 10 0 13863.81 10013.75 4943.55 o 7 10 0 105.97 3687.12 4789.49 o 8 10 0 7132.19 8864.28 5803.08 o 9 10 0 1745.32 4613.79 4727.46 o 10 10 0 2943.37 2657.00 5287.17 o 11 10 0 2253.94 3295.00 4891.77 o 0 11 0 6500.01 25855.27 9834.81 o 1 11 0 656.21 4289.91 6614.65 o 2 11 0 1524.89 1468.73 4830.24 o 3 11 0 8469.63 10699.01 5742.78 o 4 11 0 1457.90 2545.56 4711.97 o 5 11 0 5990.78 6505.52 3879.74 o 6 11 0 1169.42 6798.53 6343.38 o 7 11 0 503.26 4255.60 5087.89 o 8 11 0 10092.24 8039.66 5201.75 o 9 11 0 1979.98 1074.52 5070.60 o 10 11 0 5750.73 3736.93 5291.99 o 2 12 0 2528.40 3306.97 5230.33 o 3 12 0 280.88 3077.73 5810.02 o 4 12 0 3219.16 5211.26 6172.45 o 5 12 0 14069.75 27626.46 9025.58 o 6 12 0 8377.17 9043.00 6857.65 o 7 12 0 1420.87 3924.74 6432.24 o 8 12 0 2539.51 4357.60 5242.68 o 9 12 0 1501.06 518.54 6447.02 o -9 -12 1 460.36 2879.90 6188.57 o -8 -12 1 655.83 6161.53 7008.99 o -7 -12 1 3.02 1527.06 6486.66 o -6 -12 1 935.47 1970.69 4881.64 o -5 -12 1 129.86 6240.59 10385.39 o -4 -12 1 0.34 3960.85 4641.32 o -3 -12 1 399.88 831.45 4331.86 o -2 -12 1 276.18 3301.12 5027.70 o -10 -11 1 409.06 3245.82 4769.58 o -9 -11 1 369.09 3660.77 5560.48 o -8 -11 1 1137.44 2889.85 4666.29 o -7 -11 1 876.16 3504.93 5767.36 o -6 -11 1 29.02 1650.99 5981.52 o -5 -11 1 2925.75 3002.34 3212.35 o -4 -11 1 311.37 2025.52 3620.68 o -3 -11 1 132.16 7120.97 6395.17 o -2 -11 1 3003.13 9283.30 5998.26 o -1 -11 1 1100.73 4775.15 6268.75 o 0 -11 1 111.89 6230.17 5536.62 o -11 -10 1 1251.43 3686.56 5419.51 o -10 -10 1 274.68 2431.97 5917.30 o -9 -10 1 118.41 2695.74 4596.32 o -8 -10 1 2485.23 4882.06 4548.93 o -7 -10 1 53.05 1554.72 4331.96 o -6 -10 1 2489.93 1814.08 4069.21 o -5 -10 1 255.83 1637.91 2764.45 o -4 -10 1 567.73 2255.54 2709.37 o -3 -10 1 1442.84 2189.63 3768.06 o -2 -10 1 241.26 106.91 4319.02 o -1 -10 1 1236.97 5209.93 5449.67 o 0 -10 1 4263.60 4072.85 5128.96 o 1 -10 1 483.91 2355.89 5904.59 o 2 -10 1 463.00 2076.14 4662.83 o -11 -9 1 1425.98 1369.31 5489.96 o -10 -9 1 1916.01 1668.75 3956.89 o -9 -9 1 560.83 1558.21 3558.59 o -8 -9 1 1826.96 2296.15 4674.42 o -7 -9 1 48.52 1118.75 3793.14 o -6 -9 1 3566.13 1265.59 3118.64 o -5 -9 1 845.49 1652.38 2387.22 o -4 -9 1 2301.29 5071.26 2950.08 o -3 -9 1 4620.14 4867.81 3048.37 o -2 -9 1 3097.53 3840.21 4198.15 o -1 -9 1 237.26 1734.15 3575.48 o 0 -9 1 1815.17 1285.41 3169.08 o 1 -9 1 315.75 2067.21 4309.04 o 2 -9 1 1501.51 656.39 4067.50 o 3 -9 1 1268.31 2058.77 4641.08 o -12 -8 1 2735.50 8498.10 7460.66 o -11 -8 1 277.62 2875.56 3399.46 o -10 -8 1 17.65 1891.28 2874.74 o -9 -8 1 2636.78 3895.91 5412.52 o -8 -8 1 523.25 3179.57 4193.62 o -7 -8 1 71.35 1134.24 2829.81 o -6 -8 1 109.18 2042.83 3766.05 o -5 -8 1 278.29 6956.53 5168.62 o -4 -8 1 118.39 1335.74 2508.94 o -3 -8 1 22.71 3293.27 3565.08 o -2 -8 1 40.42 1315.56 2305.71 o -1 -8 1 4415.53 4117.65 3728.71 o 0 -8 1 157.36 1111.70 2772.95 o 1 -8 1 450.68 -356.70 2982.17 o 2 -8 1 23.01 2578.93 3521.76 o 3 -8 1 1255.00 4314.82 6153.19 o 4 -8 1 3263.26 3430.52 4051.21 o 5 -8 1 180.42 4707.89 7068.06 o -12 -7 1 72.45 1588.04 4802.92 o -11 -7 1 6191.40 3191.58 3363.98 o -10 -7 1 3844.16 3756.96 3162.66 o -9 -7 1 855.40 2295.37 2572.36 o -8 -7 1 288.31 1794.43 2155.21 o -7 -7 1 4184.79 4096.23 3693.01 o -6 -7 1 1801.27 1411.97 2370.90 o -5 -7 1 7811.77 4147.96 4246.60 o -4 -7 1 27.19 723.82 2070.89 o -3 -7 1 1754.25 1734.42 1491.94 o -2 -7 1 2648.94 2137.18 1678.43 o -1 -7 1 1758.90 4452.69 3510.54 o 0 -7 1 164.12 3028.04 2428.40 o 1 -7 1 6419.94 6908.27 4657.20 o 2 -7 1 6.29 1185.83 3201.55 o 3 -7 1 1209.01 372.10 3490.21 o 4 -7 1 82.81 4903.84 4662.56 o 5 -7 1 187.36 3601.87 3636.72 o 6 -7 1 1137.48 1986.94 5132.93 o -12 -6 1 276.89 1691.37 5865.90 o -11 -6 1 1627.89 2984.54 3985.64 o -10 -6 1 195.99 2035.92 3080.78 o -9 -6 1 329.00 749.19 1900.57 o -8 -6 1 4865.48 3079.54 2161.64 o -7 -6 1 11645.57 10667.15 5330.75 o -6 -6 1 3345.82 4129.94 3846.73 o -5 -6 1 10715.06 9716.28 3873.61 o -4 -6 1 14587.67 15796.73 5182.19 o -3 -6 1 9098.26 6676.72 1728.27 o -2 -6 1 462.95 604.59 1414.24 o -1 -6 1 3438.35 1587.81 1158.13 o 0 -6 1 16365.03 21511.96 5335.56 o 1 -6 1 3045.64 3261.56 3304.49 o 2 -6 1 3875.95 3697.24 2683.43 o 3 -6 1 18443.59 20530.12 6044.90 o 4 -6 1 69.74 -25.73 3324.08 o 5 -6 1 4.28 3433.22 3675.92 o 6 -6 1 8289.45 5428.30 4255.66 o 7 -6 1 19.53 2492.79 5672.90 o -12 -5 1 1634.74 787.24 5018.07 o -11 -5 1 5377.98 2673.36 3053.97 o -10 -5 1 24.77 2080.75 2812.15 o -9 -5 1 16573.54 17930.41 4280.72 o -8 -5 1 392.59 486.08 1800.59 o -7 -5 1 276.12 359.34 2133.43 o -6 -5 1 28386.23 34804.82 6210.07 o -5 -5 1 185.65 361.87 2106.91 o -4 -5 1 18387.62 15899.88 1918.50 o -3 -5 1 25162.52 19087.06 1980.18 o -2 -5 1 162.99 1032.05 1533.93 o -1 -5 1 6228.31 5008.45 1914.96 o 0 -5 1 1436.10 1870.47 1477.18 o 1 -5 1 3946.60 3424.70 1847.71 o 2 -5 1 861.38 2263.21 1713.71 o 3 -5 1 9379.07 10158.01 2760.23 o 4 -5 1 4976.43 4764.59 2519.10 o 5 -5 1 1207.89 2933.04 2346.16 o 6 -5 1 1329.06 862.55 2326.62 o 7 -5 1 820.50 1724.66 2605.20 o -12 -4 1 692.51 608.95 5359.67 o -11 -4 1 13564.86 11160.37 6392.60 o -10 -4 1 14515.34 16861.62 5228.57 o -9 -4 1 16.79 684.79 1952.47 o -8 -4 1 18911.53 18673.96 4091.60 o -7 -4 1 3004.65 3038.20 1715.42 o -6 -4 1 20800.49 22885.30 2841.58 o -5 -4 1 1637.72 1242.33 1545.83 o -4 -4 1 21485.02 19663.70 1667.32 o -3 -4 1 17163.43 10564.60 2290.69 o -2 -4 1 1235.50 1385.36 1039.85 o -1 -4 1 8323.33 6157.84 1959.37 o 0 -4 1 19529.64 15051.62 2606.24 o 1 -4 1 1014.10 1246.22 1438.88 o 2 -4 1 5882.72 4322.49 2364.99 o 3 -4 1 66.91 1834.45 2023.09 o 4 -4 1 8175.88 7444.78 3112.17 o 5 -4 1 2143.65 1547.03 1792.48 o 6 -4 1 8088.99 10468.66 3561.10 o 7 -4 1 1787.84 2197.75 2850.12 o 8 -4 1 387.33 3608.12 3035.62 o -12 -3 1 50.17 8153.65 7442.07 o -11 -3 1 1569.67 2006.07 4524.61 o -10 -3 1 478.55 2745.24 3279.41 o -9 -3 1 3631.68 4174.48 2392.64 o -8 -3 1 1586.09 2467.23 1651.43 o -7 -3 1 9464.76 9601.95 2964.57 o -6 -3 1 431.30 1536.25 1604.97 o -5 -3 1 39699.72 45777.03 2946.84 o -4 -3 1 1698.37 5537.52 1919.04 o -3 -3 1 31422.91 26833.89 1974.12 o -2 -3 1 30824.27 17714.75 4282.03 o -1 -3 1 1594.63 2524.84 1398.85 o 0 -3 1 92.26 624.12 1220.09 o 1 -3 1 17897.83 16827.52 1712.16 o 2 -3 1 41.11 1308.64 1229.47 o 3 -3 1 40699.94 44571.71 2911.25 o 4 -3 1 3885.48 4170.18 1525.99 o 5 -3 1 175.22 866.14 1384.34 o 6 -3 1 19765.77 21889.86 4135.81 o 7 -3 1 608.93 2337.65 2535.06 o 8 -3 1 392.48 2589.59 2666.37 o 9 -3 1 7005.25 4608.46 3814.96 o -11 -2 1 3929.11 4647.85 4957.15 o -10 -2 1 2041.86 3296.64 4879.23 o -9 -2 1 5417.10 4007.74 2637.38 o -8 -2 1 13271.68 12799.82 3394.82 o -7 -2 1 453.07 1487.18 1585.41 o -6 -2 1 22609.38 25402.94 2083.13 o -5 -2 1 22187.23 23274.41 1832.65 o -4 -2 1 31649.32 34209.20 4238.97 o -3 -2 1 97221.29 106634.99 10774.43 o -1 -2 1 3832.51 3301.27 1119.75 o 0 -2 1 3605.43 3700.71 1524.44 o 1 -2 1 44.48 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