#======================================================================= data_global #======================================================================= _audit_creation_method 'Jana2000 Version : 08/11/2007' # 1. PROCESSING SUMMARY (IUCr Office Use Only) _journal_date_recd_electronic ? _journal_date_to_coeditor ? _journal_date_from_coeditor ? _journal_date_accepted ? _journal_date_printers_first ? _journal_date_printers_final ? _journal_date_proofs_out ? _journal_date_proofs_in ? _journal_coeditor_name ? _journal_coeditor_code ? _journal_coeditor_notes ; ? ; _journal_techeditor_code ? _journal_paper_category ? _journal_techeditor_notes ; ? ; _journal_coden_ASTM ? _journal_name_full 'Acta Crystallographica Section C' _journal_year ? _journal_volume ? _journal_issue ? _journal_page_first ? _journal_page_last ? _journal_suppl_publ_number ? _journal_suppl_publ_pages ? #======================================================================= # 2. SUBMISSION DETAILS _publ_contact_author_name ? _publ_contact_author_address ; ? ; _publ_contact_author_email ? _publ_contact_author_fax ? _publ_contact_author_phone ? _publ_requested_journal 'Acta Crystallographica Section C' _publ_requested_category ? _publ_contact_letter ; ? ; #======================================================================= # 3. TITLE AND AUTHOR LIST _publ_section_title ; ? ; _publ_section_title_footnote ; ? ; loop_ _publ_author_name _publ_author_footnote _publ_author_address ? # name ; ? # footnote ; ; ? # address ; #======================================================================= # 4. TEXT _publ_section_synopsis ; ? ; _publ_section_abstract ; ? ; _publ_section_comment ; ? ; _publ_section_introduction ; ? ; _publ_section_experimental ; ? ; _publ_section_exptl_prep ; ? ; _publ_section_exptl_refinement ; ? ; _publ_section_exptl_solution ; ? ; _publ_section_discussion ; ? ; _publ_section_acknowledgements ; ? ; _publ_section_references ; Becker, P. J. & Coppens, P. (1974). Acta Cryst. A30, 129-153. Petricek, V., Dusek, M. & Palatinus L. (2000). Jana2000. Structure Determination Software Programs. Institute of Physics, Praha, Czech Republic. # enable this reference if Diamond ver. 2 was used for visualization #Brandenburg, K. (1999). DIAMOND. Version. 2.1c. #Crystal Impact GbR, Bonn, Germany. # enable this reference if Diamond ver. 3 was used for visualization #Brandenburg, K. & Putz, H. (2005). DIAMOND Version 3. #Crystal Impact GbR, Postfach 1251, D-53002 Bonn, Germany. # enable this reference if SIR97 was used for solving of the structure #Altomare, A., Burla, M. C., Camalli, M., Cascarano, G., Giacovazzo, C., #Guagliardi, A., Moliterni, A. G. G., Polidori, G., Spagna, R. (1997). #SIR97. A Package for Crystal Structure Solution by Direct Methods #and Refinement, Bari, Rome, Italy. # use this reference if SIR2002 was used for solving of the structure #Burla, M.C., Camalli, M., Carrozzini, B., Cascarano, G., Giacovazzo, C., #Polidori, G., Spagna, R. #SIR2002: the program, J. Appl. Cryst, (2003). 36, 1103 # enable this reference if bond valences were calculated #Brown, I. D. (1996). J. Appl. Cryst. 29, 479-480. # enable this reference if Xshape wase used for crystal shape refinement #Stoe & Cie (1998). X-SHAPE. Stoe & Cie, Darmstadt, Germany. # enable this reference if Flack coefficient was refined #Flack, H. D. (1983). Acta Cryst. A39, 876-881. ; _publ_section_figure_captions ; ? ; _publ_section_table_legends ; ? ; #======================================================================= data_(I) #======================================================================= # 5. CHEMICAL DATA _chemical_name_systematic ; ? ; _chemical_name_common ? _chemical_formula_moiety ? _chemical_formula_structural ? _chemical_formula_analytical ? _chemical_formula_iupac ? _chemical_formula_sum 'Cs0.125 Fe0.375 O5.25 Pb0.375 W1.375' _chemical_formula_weight 452 _chemical_melting_point ? _chemical_compound_source ? _chemical_absolute_configuration . #======================================================================= # 6. CRYSTAL DATA _symmetry_cell_setting orthorhombic _symmetry_space_group_name_H-M 'C m c m' _symmetry_space_group_name_Hall '-C -2x;-2yc;-2zc' loop_ _symmetry_equiv_pos_site_id _symmetry_equiv_pos_as_xyz 1 x,y,z 2 -x,y,z 3 x,-y,1/2+z 4 x,y,1/2-z 5 -x,-y,-z 6 x,-y,-z 7 -x,y,1/2-z 8 -x,-y,1/2+z 9 1/2+x,1/2+y,z 10 1/2-x,1/2+y,z 11 1/2+x,1/2-y,1/2+z 12 1/2+x,1/2+y,1/2-z 13 1/2-x,1/2-y,-z 14 1/2+x,1/2-y,-z 15 1/2-x,1/2+y,1/2-z 16 1/2-x,1/2-y,1/2+z _cell_length_a 7.298 _cell_length_b 12.6405 _cell_length_c 19.582 _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_volume 1806.447 _cell_formula_units_Z 16 _cell_measurement_reflns_used ? _cell_measurement_theta_min ? _cell_measurement_theta_max ? _cell_measurement_temperature ? _cell_special_details ; ? ; _exptl_crystal_density_diffrn 6.6463 _exptl_crystal_density_meas ? _exptl_crystal_density_method ? _exptl_crystal_F_000 2904 _exptl_absorpt_coefficient_mu 51.052 _exptl_crystal_description ? _exptl_crystal_size_max ? _exptl_crystal_size_mid ? _exptl_crystal_size_min ? _exptl_crystal_size_rad ? _exptl_crystal_colour ? _exptl_absorpt_correction_type None _exptl_absorpt_process_details ? _exptl_absorpt_correction_T_min 1.000 _exptl_absorpt_correction_T_max 1.000 #======================================================================= # 7. EXPERIMENTAL DATA _exptl_special_details ? _diffrn_ambient_temperature 293 _diffrn_radiation_type 'Mo K\a' _diffrn_radiation_wavelength 0.71073 _diffrn_radiation_source ? _diffrn_radiation_monochromator ? _diffrn_measurement_device_type ? _diffrn_detector_area_resol_mean ? _diffrn_measurement_method ? _diffrn_reflns_number 15562 _diffrn_reflns_theta_min 2.08 _diffrn_reflns_theta_max 30.21 _diffrn_reflns_theta_full 0.00 _diffrn_measured_fraction_theta_max ? _diffrn_measured_fraction_theta_full 0.00 _diffrn_reflns_av_R_equivalents 0.0675 _diffrn_reflns_av_sigmaI/netI 0.0389 _diffrn_reflns_limit_h_min -9 _diffrn_reflns_limit_h_max 9 _diffrn_reflns_limit_k_min -17 _diffrn_reflns_limit_k_max 17 _diffrn_reflns_limit_l_min -27 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_reduction_process ? _diffrn_standards_number ? _diffrn_standards_interval_count ? _diffrn_standards_interval_time ? _diffrn_standards_decay_% ? #======================================================================= # 8. REFINEMENT DATA _refine_special_details ; ? ; _reflns_number_total 1375 _reflns_number_gt 1223 _reflns_threshold_expression 'I>3\s(I)' _refine_ls_structure_factor_coef F _refine_ls_R_factor_gt 0.0588 _refine_ls_wR_factor_gt 0.0922 _refine_ls_R_factor_all 0.0645 _refine_ls_wR_factor_ref 0.0970 _refine_ls_goodness_of_fit_ref 1.23 _refine_ls_goodness_of_fit_gt 1.24 _refine_ls_restrained_S_gt ? _refine_ls_restrained_S_all ? _refine_ls_number_reflns 1375 _refine_ls_number_parameters 72 _refine_ls_number_restraints ? _refine_ls_number_constraints ? _refine_ls_weighting_scheme sigma _refine_ls_weighting_details 'w=1/(\s^2^(F)+0.0049F^2^)' _refine_ls_hydrogen_treatment ? _refine_ls_shift/su_max 0.0398 _refine_ls_shift/su_mean 0.0114 _refine_diff_density_max 2.29 _refine_diff_density_min -2.57 _refine_ls_extinction_method 'B-C type 1 Gaussian isotropic (Becker & Coppens, 1974)' _refine_ls_extinction_coef 2085(**) loop_ _atom_type_symbol _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source _atom_type_scat_Cromer_Mann_a1 _atom_type_scat_Cromer_Mann_b1 _atom_type_scat_Cromer_Mann_a2 _atom_type_scat_Cromer_Mann_b2 _atom_type_scat_Cromer_Mann_a3 _atom_type_scat_Cromer_Mann_b3 _atom_type_scat_Cromer_Mann_a4 _atom_type_scat_Cromer_Mann_b4 _atom_type_scat_Cromer_Mann_c O 0.011 0.006 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.867 32.908901 0.2508 Fe 0.346 0.844 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 11.7695 4.7611 7.3573 0.3072 3.5222 15.3535 2.3045 76.880501 1.0369 W -0.849 6.872 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 29.0818 1.72029 15.43 9.2259 14.4327 0.321703 5.11982 57.056 9.8875 Pb -3.394 10.111 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 31.061701 0.6902 13.0637 2.3576 18.441999 8.618 5.9696 47.2579 13.4118 Cs -0.368 2.119 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' 20.3892 3.569 19.106199 0.3107 10.662 24.387899 1.4953 213.904007 3.3352 _computing_data_collection ? _computing_cell_refinement ? _computing_data_reduction ? _computing_structure_solution ? _computing_structure_refinement 'Jana2000 (Petricek, Dusek & Palatinus, 2000)' _computing_molecular_graphics ? _computing_publication_material 'Jana2000 (Petricek, Dusek & Palatinus, 2000)' #======================================================================= # 9. ATOMIC COORDINATES AND DISPLACEMENT PARAMETERS loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_adp_type _atom_site_U_iso_or_equiv _atom_site_symmetry_multiplicity _atom_site_occupancy _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group W1 W 0 0 0 Uani 0.0357(7) 4 0.88(3) d . . . Fe1 Fe 0 0 0 Uani 0.0357(7) 4 0.12(3) d . . . W2a W 0 -0.16917(11) 0.15677(7) Uani 0.0267(6) 8 0.80(3) d . . . Fe2a Fe 0 -0.169171 0.156772 Uani 0.0267(6) 8 0.20(3) d . . . W2b W 0.25054(9) 0.08208(9) 0.15477(7) Uani 0.0294(5) 16 0.70(2) d . . . Fe2b Fe 0.250542 0.082076 0.154772 Uani 0.0294(5) 16 0.30(2) d . . . Pb1b Pb 0.25 0.25 0 Uani 0.0346(18) 8 0.228(9) d . . . Pb2 Pb 0 0.3379(2) 0.14436(16) Uani 0.0306(11) 8 0.345(10) d . . . Cs1 Cs 0 0.3470(15) 0.25 Uiso 0.062(4) 4 0.214(10) d . . . O1a O 0 -0.1306(10) 0.0595(6) Uiso 0.006(2) 8 1 d . . . O1b O 0.1825(16) 0.0617(9) 0.0564(5) Uiso 0.023(2) 16 1 d . . . O2a O 0 -0.4557(11) 0.1289(8) Uiso 0.017(3) 8 1 d . . . O2b O 0.6876(15) 0.2238(11) 0.1389(5) Uiso 0.021(2) 16 1 d . . . O3a O 0 -0.877(2) 0.1660(12) Uiso 0.042(6) 8 1 d . . . O3b O 0.8119(14) -0.0666(9) 0.1709(4) Uiso 0.0114(17) 16 1 d . . . O4a O 0 0.8079(17) 0.25 Uiso 0.013(4) 4 1 d . . . O4b O 0.683(2) 0.0969(10) 0.25 Uiso 0.016(3) 8 1 d . . . O5 O 0 0.316(3) 0.0395(12) Uiso 0.067(6) 8 1 d . . . loop_ _atom_site_aniso_label _atom_site_aniso_type_symbol _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_12 _atom_site_aniso_U_13 _atom_site_aniso_U_23 W1 W 0.0428(13) 0.0384(13) 0.0259(6) 0 0 0.0057(7) Fe1 Fe 0.0428(13) 0.0384(13) 0.0259(6) 0 0 0.0057(7) W2a W 0.0245(13) 0.0197(12) 0.0359(7) 0 0 -0.0001(4) Fe2a Fe 0.0245(13) 0.0197(12) 0.0359(7) 0 0 -0.0001(4) W2b W 0.0128(9) 0.0160(9) 0.0596(10) -0.0011(4) 0.0005(3) 0.0016(4) Fe2b Fe 0.0128(9) 0.0160(9) 0.0596(10) -0.0011(4) 0.0005(3) 0.0016(4) Pb1b Pb 0.054(4) 0.019(3) 0.031(2) 0.0038(15) 0.0019(13) -0.0011(16) Pb2 Pb 0.019(2) 0.035(2) 0.0382(14) 0 0 0.0039(11) #======================================================================= # 10. MOLECULAR GEOMETRY loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_site_symmetry_1 _geom_bond_site_symmetry_2 _geom_bond_distance _geom_bond_publ_flag W1 Fe1 . . 0 yes W1 W2a . . 3.7413(13) yes W1 W2a . 5_555 3.7413(13) yes W1 Fe2a . . 3.7413 yes W1 Fe2a . 5_555 3.7413 yes W1 W2b . . 3.6885(12) yes W1 W2b . 5_555 3.6885(12) yes W1 W2b . 2_555 3.6885(12) yes W1 W2b . 6_555 3.6885(12) yes W1 Fe2b . . 3.6885 yes W1 Fe2b . 5_555 3.6885 yes W1 Fe2b . 2_555 3.6885 yes W1 Fe2b . 6_555 3.6885 yes W1 Pb1b . . 3.649 yes W1 Pb1b . 9_445 3.649 yes W1 Pb1b . 2_555 3.649 yes W1 Pb1b . 10_545 3.649 yes W1 O1a . . 2.020(12) yes W1 O1a . 5_555 2.020(12) yes W1 O1b . . 1.897(11) yes W1 O1b . 5_555 1.897(11) yes W1 O1b . 2_555 1.897(11) yes W1 O1b . 6_555 1.897(11) yes W1 O3a . 1_565 3.60(3) yes W1 O3a . 5_545 3.60(3) yes W1 O3b . 1_455 3.714(9) yes W1 O3b . 5_655 3.714(9) yes W1 O3b . 2_655 3.714(9) yes W1 O3b . 6_455 3.714(9) yes W1 O5 . . 4.07(3) yes W1 O5 . 5_555 4.07(3) yes Fe1 W2a . . 3.7413(13) yes Fe1 W2a . 5_555 3.7413(13) yes Fe1 Fe2a . . 3.7413 yes Fe1 Fe2a . 5_555 3.7413 yes Fe1 W2b . . 3.6885(12) yes Fe1 W2b . 5_555 3.6885(12) yes Fe1 W2b . 2_555 3.6885(12) yes Fe1 W2b . 6_555 3.6885(12) yes Fe1 Fe2b . . 3.6885 yes Fe1 Fe2b . 5_555 3.6885 yes Fe1 Fe2b . 2_555 3.6885 yes Fe1 Fe2b . 6_555 3.6885 yes Fe1 Pb1b . . 3.649 yes Fe1 Pb1b . 9_445 3.649 yes Fe1 Pb1b . 2_555 3.649 yes Fe1 Pb1b . 10_545 3.649 yes Fe1 O1a . . 2.020(12) yes Fe1 O1a . 5_555 2.020(12) yes Fe1 O1b . . 1.897(11) yes Fe1 O1b . 5_555 1.897(11) yes Fe1 O1b . 2_555 1.897(11) yes Fe1 O1b . 6_555 1.897(11) yes Fe1 O3a . 1_565 3.60(3) yes Fe1 O3a . 5_545 3.60(3) yes Fe1 O3b . 1_455 3.714(9) yes Fe1 O3b . 5_655 3.714(9) yes Fe1 O3b . 2_655 3.714(9) yes Fe1 O3b . 6_455 3.714(9) yes Fe1 O5 . . 4.07(3) yes Fe1 O5 . 5_555 4.07(3) yes W2a W2a . 7_555 3.6512(18) yes W2a Fe2a . . 0 yes W2a Fe2a . 7_555 3.6512(13) yes W2a W2b . . 3.6648(16) yes W2a W2b . 9_445 3.6336(16) yes W2a W2b . 2_555 3.6648(16) yes W2a W2b . 10_545 3.6336(16) yes W2a Fe2b . . 3.6648(12) yes W2a Fe2b . 9_445 3.6336(12) yes W2a Fe2b . 2_555 3.6648(12) yes W2a Fe2b . 10_545 3.6336(12) yes W2a Pb1b . 9_445 3.7144(11) yes W2a Pb1b . 10_545 3.7144(11) yes W2a Pb2 . 9_445 3.6582(2) yes W2a Pb2 . 9_545 3.6582(2) yes W2a Cs1 . 9_445 4.0853(11) yes W2a Cs1 . 9_545 4.0853(11) yes W2a O1a . . 1.966(12) yes W2a O1b . . 3.763(11) yes W2a O1b . 2_555 3.763(11) yes W2a O2a . . 3.663(14) yes W2a O2b . 9_445 1.956(12) yes W2a O2b . 10_545 1.956(12) yes W2a O3a . 1_565 3.70(3) yes W2a O3b . 1_455 1.909(11) yes W2a O3b . 2_655 1.909(11) yes W2a O3b . 7_655 3.866(9) yes W2a O3b . 4_455 3.866(9) yes W2a O4a . 1_545 1.849(4) yes W2a O4b . 9_445 3.724(12) yes W2a O4b . 10_545 3.724(12) yes Fe2a Fe2a . 7_555 3.6512 yes Fe2a W2b . . 3.6648(11) yes Fe2a W2b . 9_445 3.6336(11) yes Fe2a W2b . 2_555 3.6648(11) yes Fe2a W2b . 10_545 3.6336(11) yes Fe2a Fe2b . . 3.6648 yes Fe2a Fe2b . 9_445 3.6336 yes Fe2a Fe2b . 2_555 3.6648 yes Fe2a Fe2b . 10_545 3.6336 yes Fe2a Pb1b . 9_445 3.7144 yes Fe2a Pb1b . 10_545 3.7144 yes Fe2a Pb2 . 9_445 3.6582(2) yes Fe2a Pb2 . 9_545 3.6582(2) yes Fe2a Cs1 . 9_445 4.0853(9) yes Fe2a Cs1 . 9_545 4.0853(9) yes Fe2a O1a . . 1.966(12) yes Fe2a O1b . . 3.763(11) yes Fe2a O1b . 2_555 3.763(11) yes Fe2a O2a . . 3.663(14) yes Fe2a O2b . 9_445 1.956(12) yes Fe2a O2b . 10_545 1.956(12) yes Fe2a O3a . 1_565 3.70(3) yes Fe2a O3b . 1_455 1.909(11) yes Fe2a O3b . 2_655 1.909(11) yes Fe2a O3b . 7_655 3.866(9) yes Fe2a O3b . 4_455 3.866(9) yes Fe2a O4a . 1_545 1.849(3) yes Fe2a O4b . 9_445 3.724(12) yes Fe2a O4b . 10_545 3.724(12) yes W2b W2b . 2_555 3.6569(9) yes W2b W2b . 2_655 3.6411(9) yes W2b W2b . 4_555 3.7295(19) yes W2b Fe2b . . 0 yes W2b Fe2b . 2_555 3.6569(7) yes W2b Fe2b . 2_655 3.6411(7) yes W2b Fe2b . 4_555 3.7295(14) yes W2b Pb1b . . 3.7001(13) yes W2b Pb2 . . 3.720(3) yes W2b Pb2 . 9_545 3.590(3) yes W2b Cs1 . 9_545 3.952(14) yes W2b O1a . . 3.748(11) yes W2b O1b . . 2.007(10) yes W2b O1b . 2_555 3.710(11) yes W2b O2a . 9_555 1.949(5) yes W2b O2b . . 3.672(12) yes W2b O2b . 2_655 1.874(13) yes W2b O3a . 1_565 1.913(9) yes W2b O3a . 7_565 3.99(2) yes W2b O3b . 1_455 3.725(10) yes W2b O3b . 2_655 1.959(11) yes W2b O3b . 7_655 3.922(9) yes W2b O4a . 9_545 3.865(16) yes W2b O4b . . 3.674(12) yes W2b O4b . 2_655 1.935(4) yes W2b O5 . . 4.15(3) yes Fe2b Fe2b . 2_555 3.6569 yes Fe2b Fe2b . 2_655 3.6411 yes Fe2b Fe2b . 4_555 3.7295 yes Fe2b Pb1b . . 3.7001 yes Fe2b Pb2 . . 3.720(3) yes Fe2b Pb2 . 9_545 3.590(3) yes Fe2b Cs1 . 9_545 3.952(14) yes Fe2b O1a . . 3.748(11) yes Fe2b O1b . . 2.007(10) yes Fe2b O1b . 2_555 3.710(11) yes Fe2b O2a . 9_555 1.949(5) yes Fe2b O2b . . 3.672(12) yes Fe2b O2b . 2_655 1.874(13) yes Fe2b O3a . 1_565 1.913(9) yes Fe2b O3a . 7_565 3.99(2) yes Fe2b O3b . 1_455 3.725(10) yes Fe2b O3b . 2_655 1.959(11) yes Fe2b O3b . 7_655 3.922(9) yes Fe2b O4a . 9_545 3.865(16) yes Fe2b O4b . . 3.674(12) yes Fe2b O4b . 2_655 1.935(4) yes Fe2b O5 . . 4.15(3) yes Pb1b Pb1b . 2_555 3.649 yes Pb1b Pb1b . 2_655 3.649 yes Pb1b Pb2 . . 3.543(3) yes Pb1b Pb2 . 13_555 3.543(3) yes Pb1b O1a . 9_555 2.639(9) yes Pb1b O1a . 5_555 2.639(9) yes Pb1b O1b . . 2.669(12) yes Pb1b O1b . 13_555 2.669(12) yes Pb1b O1b . 2_555 4.104(12) yes Pb1b O1b . 10_555 4.122(12) yes Pb1b O1b . 6_555 4.122(12) yes Pb1b O1b . 14_555 4.104(12) yes Pb1b O2a . 9_555 4.057(13) yes Pb1b O2a . 5_555 4.057(13) yes Pb1b O2b . 2_655 2.778(9) yes Pb1b O2b . 14_455 2.778(9) yes Pb1b O3a . 1_565 4.06(2) yes Pb1b O3a . 13_545 4.06(2) yes Pb1b O3b . 9_455 4.097(9) yes Pb1b O3b . 5_655 4.097(9) yes Pb1b O5 . . 2.153(16) yes Pb1b O5 . 13_555 2.153(16) yes Pb2 Pb2 . 7_555 4.137(5) yes Pb2 Cs1 . . 2.072(3) yes Pb2 O1a . 9_455 4.029(5) yes Pb2 O1a . 9_555 4.029(5) yes Pb2 O1b . . 4.114(12) yes Pb2 O1b . 9_455 4.043(12) yes Pb2 O1b . 2_555 4.114(12) yes Pb2 O1b . 10_555 4.043(12) yes Pb2 O2a . 1_565 2.627(14) yes Pb2 O2b . 1_455 2.699(12) yes Pb2 O2b . 2_655 2.699(12) yes Pb2 O3a . 1_565 2.75(3) yes Pb2 O3b . 9_455 2.629(10) yes Pb2 O3b . 10_555 2.629(10) yes Pb2 O4b . 9_455 4.098(12) yes Pb2 O4b . 10_555 4.098(12) yes Pb2 O5 . . 2.07(2) yes Cs1 O2a . 1_565 3.44(2) yes Cs1 O2a . 7_565 3.44(2) yes Cs1 O2b . 1_455 3.515(14) yes Cs1 O2b . 2_655 3.515(14) yes Cs1 O2b . 7_655 3.515(14) yes Cs1 O2b . 4_455 3.515(14) yes Cs1 O3a . 1_565 3.27(3) yes Cs1 O3a . 7_565 3.27(3) yes Cs1 O3b . 9_455 2.962(12) yes Cs1 O3b . 10_555 2.962(12) yes Cs1 O3b . 15_555 2.962(12) yes Cs1 O3b . 12_455 2.962(12) yes Cs1 O4a . 9_445 3.682(4) yes Cs1 O4a . 9_545 3.682(4) yes Cs1 O4b . 1_455 3.92(2) yes Cs1 O4b . 9_455 3.43(2) yes Cs1 O4b . 2_655 3.92(2) yes Cs1 O4b . 10_555 3.43(2) yes Cs1 O5 . . 4.14(2) yes Cs1 O5 . 7_555 4.14(2) yes O1a O1a . 5_555 4.041(18) yes O1a O1b . . 2.772(16) yes O1a O1b . 5_555 2.771(15) yes O1a O1b . 2_555 2.772(16) yes O1a O1b . 6_555 2.771(15) yes O1a O2b . 9_445 2.771(16) yes O1a O2b . 10_545 2.771(16) yes O1a O3a . 1_565 3.82(3) yes O1a O3b . 1_455 2.702(14) yes O1a O3b . 2_655 2.702(14) yes O1a O4a . 1_545 3.810(13) yes O1a O5 . 9_445 3.731(7) yes O1a O5 . 9_545 3.731(7) yes O1a O5 . 5_555 3.05(3) yes O1b O1b . 5_555 3.795(16) yes O1b O1b . 2_555 2.663(17) yes O1b O1b . 6_555 2.703(15) yes O1b O2a . 9_555 2.727(14) yes O1b O2b . 2_655 2.777(16) yes O1b O3a . 1_565 2.64(2) yes O1b O3b . 1_455 3.870(15) yes O1b O3b . 2_655 2.769(14) yes O1b O4b . 2_655 3.941(11) yes O1b O5 . . 3.50(3) yes O1b O5 . 9_545 3.88(3) yes O1b O5 . 13_555 3.36(2) yes O2a O2b . 9_445 2.658(18) yes O2a O2b . 10_545 2.658(18) yes O2a O3a . 9_455 3.852(10) yes O2a O3a . 9_555 3.852(10) yes O2a O3b . 9_445 2.797(13) yes O2a O3b . 10_545 2.797(13) yes O2a O4a . 1_545 4.09(2) yes O2a O4b . 9_445 2.804(16) yes O2a O4b . 10_545 2.804(16) yes O2a O5 . 1_545 3.37(3) yes O2a O5 . 5_555 3.74(3) yes O2b O2b . 2_655 2.738(16) yes O2b O3a . 1_665 2.665(19) yes O2b O3b . . 3.833(17) yes O2b O3b . 9_455 3.864(16) yes O2b O3b . 10_655 2.723(17) yes O2b O4a . 9_545 2.781(13) yes O2b O4b . . 2.703(13) yes O2b O4b . 2_655 3.826(16) yes O2b O5 . 1_655 3.22(2) yes O2b O5 . 13_555 3.79(2) yes O3a O3a . 7_555 3.29(3) yes O3a O3b . 1_445 2.76(3) yes O3a O3b . 2_645 2.76(3) yes O3a O4b . 1_445 2.854(19) yes O3a O4b . 2_645 2.854(19) yes O3a O5 . 1_545 3.48(4) yes O3b O3b . 2_755 2.745(14) yes O3b O3b . 7_755 4.138(13) yes O3b O3b . 4_555 3.096(12) yes O3b O4a . 1_645 2.608(16) yes O3b O4b . . 2.747(15) yes O3b O5 . 9_545 3.74(2) yes O4a O4b . 9_455 2.98(2) yes O4a O4b . 10_555 2.98(2) yes O4b O4b . 2_655 2.68(2) yes #======================================================================= # 11. STRUCTURE-FACTOR LIST loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma _refln_observed_status 2 0 0 23.46 24.67 1.77 o 6 0 0 56.50 42.04 4.44 o 1 1 0 167.76 158.15 12.66 o 3 1 0 83.24 91.35 6.00 o 5 1 0 119.55 110.98 8.65 o 7 1 0 71.63 67.75 5.32 o 0 2 0 162.53 157.92 12.26 o 2 2 0 185.54 192.50 13.75 o 4 2 0 113.89 112.98 8.21 o 6 2 0 145.45 122.08 11.34 o 8 2 0 58.47 50.76 5.06 o 1 3 0 20.31 24.56 1.50 o 3 3 0 82.69 89.11 6.13 o 5 3 0 23.49 24.72 1.84 o 7 3 0 43.87 51.86 3.28 o 9 3 0 47.22 45.10 3.75 o 0 4 0 194.31 192.42 14.40 o 2 4 0 81.04 91.15 5.86 o 4 4 0 200.05 173.45 15.09 o 6 4 0 72.62 74.90 5.48 o 8 4 0 173.06 108.53 14.74 o 1 5 0 81.92 91.54 5.91 o 3 5 0 108.05 113.27 8.01 o 5 5 0 59.48 61.23 4.42 o 7 5 0 48.43 47.99 3.81 o 9 5 0 44.29 38.77 3.85 o 0 6 0 87.52 89.28 6.49 o 4 6 0 25.53 24.83 1.97 o 6 6 0 349.49 355.91 25.92 o 8 6 0 15.40 16.70 1.90 o 1 7 0 106.83 113.06 7.70 o 3 7 0 115.77 110.95 8.35 o 5 7 0 73.68 74.95 5.47 o 7 7 0 55.12 48.25 4.10 o 0 8 0 182.14 173.60 13.50 o 2 8 0 113.82 110.92 8.21 o 4 8 0 132.96 122.10 10.37 o 6 8 0 49.30 47.92 3.74 o 8 8 0 128.81 70.82 10.99 o 1 9 0 24.15 24.75 1.78 o 3 9 0 55.21 42.08 4.02 o 5 9 0 42.37 51.89 3.16 o 7 9 0 15.86 16.61 1.65 o 0 10 0 63.37 61.03 4.71 o 2 10 0 136.69 121.91 9.90 o 4 10 0 64.95 67.68 4.82 o 6 10 0 176.65 108.45 13.32 o 8 10 0 53.70 44.71 4.61 o 1 11 0 72.10 75.22 5.20 o 3 11 0 68.02 67.99 4.93 o 5 11 0 55.04 50.89 4.09 o 7 11 0 44.50 38.83 3.39 o 0 12 0 367.47 355.91 27.22 o 2 12 0 46.26 52.11 3.36 o 4 12 0 275.75 300.81 20.44 o 6 12 0 45.68 45.27 3.41 o 1 13 0 47.51 47.88 3.43 o 3 13 0 56.35 50.68 4.14 o 5 13 0 32.86 29.22 2.55 o 7 13 0 38.95 30.74 3.00 o 0 14 0 49.68 48.37 4.28 o 2 14 0 154.98 108.58 11.49 o 4 14 0 34.22 29.32 2.77 o 6 14 0 122.79 69.63 9.58 o 1 15 0 14.94 16.62 1.29 o 3 15 0 45.88 45.11 3.35 o 5 15 0 13.56 13.75 2.11 o 0 16 0 111.69 70.61 8.43 o 2 16 0 47.85 38.70 3.50 o 4 16 0 117.30 69.47 9.15 o 1 17 0 55.16 44.89 4.03 o 3 17 0 41.41 30.86 3.84 o 1 1 1 96.14 102.37 6.84 o 3 1 1 24.23 22.97 1.73 o 5 1 1 92.27 85.90 6.56 o 7 1 1 39.27 36.60 2.88 o 0 2 1 95.40 102.22 6.91 o 4 2 1 79.51 74.39 5.66 o 6 2 1 281.18 267.60 20.21 o 8 2 1 52.59 45.37 3.98 o 3 3 1 28.12 26.47 2.05 o 5 3 1 28.18 23.78 2.10 o 7 3 1 29.45 20.86 2.21 o 9 3 1 23.91 19.18 2.71 o 2 4 1 25.07 22.91 1.80 o 4 4 1 357.44 332.71 26.95 o 6 4 1 50.52 49.72 3.67 o 8 4 1 200.97 201.37 14.62 o 1 5 1 24.40 22.98 1.75 o 3 5 1 74.79 74.46 5.33 o 5 5 1 20.83 16.91 1.64 o 7 5 1 46.88 43.07 3.51 o 9 5 1 25.33 26.32 2.37 o 0 6 1 31.87 26.40 2.33 o 4 6 1 28.21 23.79 2.08 o 6 6 1 87.00 11.29 6.57 o 8 6 1 18.05 15.53 1.63 o 1 7 1 75.04 74.59 5.33 o 3 7 1 87.51 85.97 6.22 o 5 7 1 49.88 49.75 3.62 o 7 7 1 53.94 46.88 3.94 o 9 7 1 44.83 38.03 3.44 o 0 8 1 367.96 332.66 26.97 o 2 8 1 87.53 85.81 6.22 o 4 8 1 265.90 267.55 19.24 o 6 8 1 45.76 43.08 3.31 o 8 8 1 155.92 151.02 11.56 o 1 9 1 25.56 23.95 1.85 o 5 9 1 27.91 20.96 2.11 o 7 9 1 20.89 15.53 1.73 o 0 10 1 22.26 17.00 1.67 o 2 10 1 266.48 267.59 18.93 o 4 10 1 39.59 36.68 2.90 o 6 10 1 195.44 201.35 14.15 o 8 10 1 44.07 38.14 3.38 o 1 11 1 49.70 49.67 3.54 o 3 11 1 36.67 36.57 2.62 o 5 11 1 50.20 45.33 3.64 o 7 11 1 26.03 26.31 2.16 o 0 12 1 89.22 11.34 6.55 o 2 12 1 26.00 20.83 1.90 o 6 12 1 25.89 19.20 2.07 o 1 13 1 44.13 43.17 3.14 o 3 13 1 52.20 45.43 3.73 o 5 13 1 33.27 32.02 2.45 o 7 13 1 35.78 33.62 2.71 o 0 14 1 52.08 46.92 3.87 o 2 14 1 201.76 201.22 14.39 o 4 14 1 33.43 32.05 2.45 o 6 14 1 143.05 134.17 10.60 o 1 15 1 15.34 15.61 1.22 o 3 15 1 24.76 19.31 1.87 o 0 16 1 160.35 151.02 11.75 o 2 16 1 27.54 26.47 2.01 o 4 16 1 135.19 134.24 9.91 o 1 17 1 43.52 37.98 3.17 o 3 17 1 37.71 33.57 2.76 o 0 0 2 84.46 107.65 6.26 o 2 0 2 143.58 147.27 10.35 o 4 0 2 82.97 85.77 5.98 o 6 0 2 73.95 71.39 5.49 o 1 1 2 79.17 88.95 5.63 o 3 1 2 33.84 34.30 2.41 o 5 1 2 59.61 58.98 4.24 o 7 1 2 17.06 14.70 1.35 o 0 2 2 77.14 88.69 5.56 o 2 2 2 257.30 242.39 18.62 o 4 2 2 49.38 51.02 3.51 o 6 2 2 166.61 150.94 11.97 o 8 2 2 16.73 15.88 1.76 o 1 3 2 142.47 147.52 10.13 o 3 3 2 118.77 124.67 8.50 o 5 3 2 88.69 86.36 6.40 o 7 3 2 53.10 55.94 3.96 o 9 3 2 36.50 36.00 3.23 o 0 4 2 262.88 242.44 19.47 o 2 4 2 31.53 34.18 2.25 o 4 4 2 200.96 188.47 14.55 o 6 4 2 24.48 22.67 1.82 o 8 4 2 103.08 86.03 7.78 o 1 5 2 33.75 34.23 2.40 o 3 5 2 48.33 51.08 3.44 o 5 5 2 13.25 12.89 1.24 o 7 5 2 24.26 21.14 1.98 o 9 5 2 10.56 6.14 3.17 < 0 6 2 119.21 124.42 8.63 o 2 6 2 80.61 85.76 5.73 o 4 6 2 84.88 86.22 6.15 o 6 6 2 66.75 64.31 4.81 o 8 6 2 38.08 39.18 2.82 o 1 7 2 50.48 51.29 3.59 o 3 7 2 58.62 59.09 4.17 o 5 7 2 22.12 22.80 1.70 o 7 7 2 27.24 25.27 2.03 o 9 7 2 12.76 8.47 3.32 < 0 8 2 192.86 188.55 13.96 o 2 8 2 58.02 58.82 4.13 o 4 8 2 156.41 150.99 11.38 o 6 8 2 23.33 21.14 1.78 o 8 8 2 109.10 76.95 8.24 o 1 9 2 88.61 86.43 6.30 o 3 9 2 76.12 71.52 5.42 o 5 9 2 57.20 55.99 4.13 o 7 9 2 40.07 39.22 2.91 o 0 10 2 13.83 12.87 1.25 o 2 10 2 157.56 150.96 11.22 o 4 10 2 17.42 14.61 1.36 o 6 10 2 107.97 86.03 7.93 o 8 10 2 19.29 8.42 1.76 o 1 11 2 22.88 22.65 1.65 o 3 11 2 16.98 14.61 1.30 o 5 11 2 19.05 15.88 1.57 o 7 11 2 10.61 6.14 1.86 o 0 12 2 71.15 64.29 5.15 o 2 12 2 56.00 55.84 3.98 o 4 12 2 69.39 57.33 4.99 o 6 12 2 34.24 35.97 2.53 o 1 13 2 25.07 21.29 1.81 o 3 13 2 19.86 16.00 1.48 o 5 13 2 19.09 15.46 1.54 o 7 13 2 17.75 6.68 2.04 o 0 14 2 26.59 25.19 2.01 o 2 14 2 101.63 86.18 7.25 o 4 14 2 19.43 15.39 1.53 o 6 14 2 75.77 58.86 5.92 o 1 15 2 40.81 39.25 2.91 o 3 15 2 36.01 36.09 2.60 o 5 15 2 25.67 28.22 2.03 o 0 16 2 104.33 76.96 7.73 o 2 16 2 9.28 6.18 1.41 o 4 16 2 80.88 58.80 6.13 o 1 17 2 14.83 8.42 1.27 o 3 17 2 11.53 6.64 2.36 < 1 1 3 17.63 17.68 1.28 o 3 1 3 19.43 16.29 1.41 o 5 1 3 11.29 10.26 0.99 o 7 1 3 12.58 12.73 1.21 o 0 2 3 18.27 17.78 1.36 o 2 2 3 141.86 143.57 10.08 o 4 2 3 6.14 6.92 1.06 o 6 2 3 82.91 74.02 5.93 o 8 2 3 0.00 3.70 30.37 < 3 3 3 78.00 80.00 5.54 o 5 3 3 27.94 21.17 2.07 o 7 3 3 23.02 19.02 1.80 o 9 3 3 17.87 10.25 2.23 o 0 4 3 137.68 143.63 9.92 o 2 4 3 19.12 16.27 1.39 o 4 4 3 97.81 97.30 7.05 o 6 4 3 3.94 3.51 3.35 < 8 4 3 58.89 48.48 4.33 o 1 5 3 19.23 16.30 1.40 o 3 5 3 7.12 6.91 0.98 o 5 5 3 15.75 15.79 1.30 o 7 5 3 10.14 7.73 1.62 o 9 5 3 6.76 8.25 3.66 < 0 6 3 78.54 79.97 5.66 o 4 6 3 28.52 21.18 2.11 o 6 6 3 31.35 25.63 2.46 o 8 6 3 13.85 4.41 1.54 o 1 7 3 6.24 6.89 1.14 < 3 7 3 12.23 10.26 1.02 o 5 7 3 7.28 3.49 1.62 < 7 7 3 7.16 2.27 1.93 < 9 7 3 7.80 8.85 2.66 < 0 8 3 95.66 97.21 6.89 o 2 8 3 10.97 10.32 1.00 o 4 8 3 81.35 73.99 5.83 o 6 8 3 10.27 7.78 1.41 o 8 8 3 55.00 42.75 4.10 o 1 9 3 25.90 21.21 1.86 o 5 9 3 23.34 19.04 1.81 o 7 9 3 15.90 4.42 1.45 o 0 10 3 16.56 15.83 1.34 o 2 10 3 78.70 74.00 5.60 o 4 10 3 14.74 12.78 1.24 o 6 10 3 59.42 48.45 4.37 o 8 10 3 8.26 8.91 3.17 < 1 11 3 4.98 3.49 1.59 < 3 11 3 12.77 12.75 1.10 o 5 11 3 5.94 3.69 2.11 < 7 11 3 1.67 8.25 7.32 < 0 12 3 28.59 25.65 2.14 o 2 12 3 21.02 19.07 1.55 o 6 12 3 17.69 10.22 1.65 o 1 13 3 7.69 7.73 1.10 o 3 13 3 4.92 3.69 1.98 < 5 13 3 8.87 6.94 1.78 < 0 14 3 7.32 2.28 1.85 < 2 14 3 56.12 48.41 4.01 o 4 14 3 7.62 6.98 1.83 < 6 14 3 43.27 37.59 3.17 o 1 15 3 10.26 4.42 1.09 o 3 15 3 14.68 10.24 1.41 o 0 16 3 50.58 42.73 3.66 o 2 16 3 3.71 8.31 2.65 < 4 16 3 42.52 37.58 3.11 o 1 17 3 4.74 8.85 2.58 < 3 17 3 5.56 5.02 3.92 < 2 0 4 170.77 170.31 12.36 o 4 0 4 239.18 242.40 17.24 o 6 0 4 78.39 74.10 5.71 o 8 0 4 160.16 151.00 12.09 o 1 1 4 60.58 66.48 4.31 o 3 1 4 67.24 68.22 4.78 o 5 1 4 36.86 37.98 2.63 o 7 1 4 18.98 18.61 1.48 o 0 2 4 60.94 66.26 4.40 o 2 2 4 295.88 273.02 21.20 o 4 2 4 24.80 26.81 1.79 o 6 2 4 214.04 206.05 15.23 o 8 2 4 19.37 19.73 1.81 o 1 3 4 169.50 170.54 12.05 o 3 3 4 152.67 154.54 10.85 o 5 3 4 102.69 100.75 7.35 o 7 3 4 69.41 65.19 5.06 o 9 3 4 50.04 46.90 3.83 o 0 4 4 294.36 273.01 21.42 o 2 4 4 63.66 68.04 4.52 o 4 4 4 255.07 257.04 18.12 o 6 4 4 16.26 15.21 1.43 o 8 4 4 151.16 144.53 11.01 o 1 5 4 64.49 68.18 4.58 o 3 5 4 23.44 26.79 1.69 o 5 5 4 42.28 41.51 3.16 o 7 5 4 20.08 18.38 1.65 o 9 5 4 3.90 4.87 6.20 < 0 6 4 148.63 154.31 10.71 o 2 6 4 234.95 242.31 16.69 o 4 6 4 98.44 100.69 7.03 o 6 6 4 159.44 172.10 11.49 o 8 6 4 47.39 49.51 3.47 o 1 7 4 25.47 26.95 1.85 o 3 7 4 36.40 38.04 2.59 o 5 7 4 17.50 15.24 1.49 o 7 7 4 19.07 27.25 1.57 o 9 7 4 13.26 7.77 1.78 o 0 8 4 250.52 257.16 18.06 o 2 8 4 38.06 37.89 2.71 o 4 8 4 207.22 206.10 14.74 o 6 8 4 20.47 18.40 1.66 o 8 8 4 105.06 107.49 7.71 o 1 9 4 102.65 100.79 7.29 o 3 9 4 77.18 74.14 5.49 o 5 9 4 69.16 65.21 5.04 o 7 9 4 49.20 49.45 3.57 o 0 10 4 41.41 41.40 3.00 o 2 10 4 205.17 206.02 14.58 o 4 10 4 19.43 18.52 1.46 o 6 10 4 142.87 144.52 10.47 o 8 10 4 11.79 7.77 1.83 o 1 11 4 12.65 15.19 1.10 o 3 11 4 18.54 18.55 1.38 o 5 11 4 21.45 19.69 1.78 o 7 11 4 5.12 4.87 2.67 < 0 12 4 163.92 171.96 11.86 o 2 12 4 69.39 65.14 4.96 o 4 12 4 155.83 150.90 11.24 o 6 12 4 48.27 46.98 3.51 o 1 13 4 22.10 18.46 1.62 o 3 13 4 19.74 19.66 1.52 o 5 13 4 15.88 20.90 1.45 o 0 14 4 22.96 27.31 1.96 o 2 14 4 145.73 144.68 10.38 o 4 14 4 19.59 20.89 1.58 o 6 14 4 82.09 88.85 5.95 o 1 15 4 51.15 49.52 3.65 o 3 15 4 50.05 46.96 3.59 o 5 15 4 33.73 37.74 2.47 o 0 16 4 110.82 107.43 8.03 o 2 16 4 0.00 4.90 21.51 < 4 16 4 83.97 88.77 6.08 o 1 17 4 10.63 7.79 1.26 o 1 1 5 106.53 111.62 7.58 o 3 1 5 32.64 30.21 2.33 o 5 1 5 85.16 82.40 6.06 o 7 1 5 37.95 37.38 2.71 o 9 1 5 23.51 25.91 3.09 o 0 2 5 107.34 111.47 7.77 o 2 2 5 344.17 313.74 25.04 o 4 2 5 113.41 116.46 8.06 o 6 2 5 294.48 283.25 20.95 o 8 2 5 76.61 78.08 5.69 o 3 3 5 33.64 27.52 2.40 o 5 3 5 21.38 20.16 1.58 o 7 3 5 17.49 18.73 1.52 o 9 3 5 12.37 13.35 3.10 < 0 4 5 347.64 313.72 27.10 o 2 4 5 32.79 30.16 2.34 o 4 4 5 355.71 335.66 25.32 o 6 4 5 82.39 84.41 5.97 o 8 4 5 216.79 228.39 15.63 o 1 5 5 31.11 30.15 2.22 o 3 5 5 109.48 116.43 7.78 o 5 5 5 10.86 9.08 1.32 o 7 5 5 52.46 50.94 3.81 o 9 5 5 22.73 27.83 1.91 o 0 6 5 34.55 27.42 2.51 o 4 6 5 23.03 20.16 1.69 o 6 6 5 22.84 19.19 1.91 o 8 6 5 13.95 13.50 1.46 o 1 7 5 110.81 116.58 7.87 o 3 7 5 80.43 82.43 5.74 o 5 7 5 78.88 84.36 5.69 o 7 7 5 50.61 46.13 3.68 o 9 7 5 41.99 42.94 3.24 o 0 8 5 354.50 335.58 25.55 o 2 8 5 81.00 82.34 5.79 o 4 8 5 281.20 283.20 20.00 o 6 8 5 52.72 51.02 3.81 o 8 8 5 166.83 172.50 12.07 o 1 9 5 22.36 20.31 1.64 o 5 9 5 19.03 18.80 1.54 o 7 9 5 14.21 13.51 1.51 o 0 10 5 13.86 9.12 1.42 o 2 10 5 276.72 283.22 19.70 o 4 10 5 38.63 37.49 2.76 o 6 10 5 215.39 228.38 15.67 o 8 10 5 38.82 43.08 2.88 o 1 11 5 82.27 84.27 5.85 o 3 11 5 36.77 37.35 2.63 o 5 11 5 79.31 77.98 5.74 o 7 11 5 23.71 27.83 1.87 o 0 12 5 18.61 19.21 1.56 o 2 12 5 20.58 18.69 1.54 o 6 12 5 12.78 13.37 1.47 o 1 13 5 53.76 51.06 3.83 o 3 13 5 78.30 78.14 5.59 o 5 13 5 27.91 25.96 2.17 o 0 14 5 52.82 46.09 3.89 o 2 14 5 222.28 228.26 15.81 o 4 14 5 29.52 25.95 2.18 o 6 14 5 141.02 150.66 10.64 o 1 15 5 10.37 13.56 1.22 o 3 15 5 9.15 13.43 1.46 o 0 16 5 171.07 172.52 12.33 o 2 16 5 25.03 27.98 1.87 o 4 16 5 136.22 150.72 9.98 o 1 17 5 40.11 42.92 2.88 o 2 0 6 38.24 42.14 2.77 o 4 0 6 498.05 407.13 42.42 o 6 0 6 33.54 32.85 2.45 o 8 0 6 266.03 254.64 19.51 o 1 1 6 138.87 151.31 9.87 o 3 1 6 98.60 107.20 7.01 o 5 1 6 91.23 93.02 6.48 o 7 1 6 60.94 58.96 4.35 o 9 1 6 29.01 27.62 2.70 o 0 2 6 138.87 150.95 10.01 o 2 2 6 76.80 87.58 5.46 o 4 2 6 104.89 115.84 7.45 o 6 2 6 79.52 84.86 5.66 o 8 2 6 55.14 56.10 4.01 o 1 3 6 35.16 42.00 2.51 o 3 3 6 40.86 44.32 2.91 o 5 3 6 33.71 37.46 2.43 o 7 3 6 31.58 32.20 2.34 o 9 3 6 32.00 31.20 2.62 o 0 4 6 79.42 87.45 5.73 o 2 4 6 96.40 107.00 6.86 o 4 4 6 87.67 98.11 6.24 o 6 4 6 73.40 78.01 5.26 o 8 4 6 78.46 76.81 5.76 o 1 5 6 96.56 107.30 6.87 o 3 5 6 105.77 116.12 7.51 o 5 5 6 61.85 64.06 4.44 o 7 5 6 49.31 50.97 3.57 o 9 5 6 31.53 36.32 2.47 o 0 6 6 42.45 44.47 3.07 o 2 6 6 475.56 407.14 35.85 o 4 6 6 34.15 37.59 2.48 o 6 6 6 303.06 302.90 21.85 o 8 6 6 34.33 33.71 2.55 o 1 7 6 105.76 115.91 7.52 o 3 7 6 89.26 92.97 6.36 o 5 7 6 73.51 78.01 5.28 o 7 7 6 43.15 39.60 3.13 o 9 7 6 36.08 37.51 2.66 o 0 8 6 89.99 98.24 6.49 o 2 8 6 89.85 92.85 6.38 o 4 8 6 76.58 84.87 5.45 o 6 8 6 51.44 50.89 3.72 o 8 8 6 60.73 58.73 4.41 o 1 9 6 35.24 37.48 2.52 o 3 9 6 30.08 32.77 2.16 o 5 9 6 31.77 32.23 2.32 o 7 9 6 34.27 33.63 2.59 o 0 10 6 61.40 63.88 4.48 o 2 10 6 80.92 84.66 5.76 o 4 10 6 61.36 58.90 4.36 o 6 10 6 82.14 76.75 6.41 o 8 10 6 36.27 37.52 2.69 o 1 11 6 75.85 78.24 5.40 o 3 11 6 59.75 59.08 4.25 o 5 11 6 57.82 56.22 4.22 o 7 11 6 31.48 36.35 2.36 o 0 12 6 306.68 302.94 22.10 o 2 12 6 34.36 32.32 2.46 o 4 12 6 272.06 254.68 19.47 o 6 12 6 34.84 31.30 2.62 o 1 13 6 52.82 50.91 3.76 o 3 13 6 56.26 56.05 4.02 o 5 13 6 27.87 27.65 2.13 o 0 14 6 44.78 39.63 3.28 o 2 14 6 76.94 76.88 5.52 o 4 14 6 28.09 27.64 2.09 o 1 15 6 34.81 33.67 2.49 o 3 15 6 32.98 31.24 2.39 o 5 15 6 30.67 32.47 2.94 o 0 16 6 59.75 58.56 4.39 o 2 16 6 33.46 36.21 2.41 o 1 17 6 37.52 37.63 2.71 o 1 1 7 48.23 54.33 3.43 o 3 1 7 62.20 66.80 4.43 o 5 1 7 37.57 40.26 2.68 o 7 1 7 36.26 32.83 2.61 o 9 1 7 24.74 26.33 2.31 o 0 2 7 49.17 54.15 3.55 o 2 2 7 170.91 185.37 12.14 o 4 2 7 59.72 63.90 4.25 o 6 2 7 130.53 138.62 9.27 o 8 2 7 46.40 44.04 3.39 o 3 3 7 11.85 11.64 1.07 o 5 3 7 3.73 5.78 2.43 < 7 3 7 6.28 6.66 2.24 < 9 3 7 3.87 4.06 6.95 < 0 4 7 175.44 185.39 12.64 o 2 4 7 61.86 66.67 4.40 o 4 4 7 147.68 157.70 10.49 o 6 4 7 50.78 50.59 3.62 o 8 4 7 92.61 94.89 6.75 o 1 5 7 61.01 66.90 4.34 o 3 5 7 59.06 64.05 4.20 o 5 5 7 41.37 42.81 2.95 o 7 5 7 40.53 40.37 2.95 o 9 5 7 19.48 18.99 1.90 o 0 6 7 11.40 11.68 1.27 o 4 6 7 3.82 5.81 2.32 < 6 6 7 9.64 7.79 2.16 < 8 6 7 0.00 3.56 29.03 < 1 7 7 58.08 63.96 4.13 o 3 7 7 36.37 40.22 2.60 o 5 7 7 51.13 50.59 3.65 o 7 7 7 28.65 26.85 2.17 o 9 7 7 20.48 22.18 1.94 o 0 8 7 145.11 157.60 10.46 o 2 8 7 37.57 40.15 2.68 o 4 8 7 131.42 138.58 9.34 o 6 8 7 41.26 40.34 3.00 o 8 8 7 83.16 86.64 6.10 o 1 9 7 5.63 5.79 1.47 < 5 9 7 5.56 6.65 2.03 < 7 9 7 7.66 3.56 2.13 < 0 10 7 42.40 42.68 3.07 o 2 10 7 129.36 138.60 9.21 o 4 10 7 35.15 32.80 2.52 o 6 10 7 96.42 94.89 6.95 o 8 10 7 22.23 22.25 1.83 o 1 11 7 51.27 50.65 3.65 o 3 11 7 35.17 32.84 2.52 o 5 11 7 48.53 44.06 3.53 o 7 11 7 21.51 18.97 1.83 o 0 12 7 9.99 7.79 1.36 o 2 12 7 8.99 6.63 1.17 o 6 12 7 6.95 4.06 2.44 < 1 13 7 41.42 40.34 2.95 o 3 13 7 47.29 44.05 3.38 o 5 13 7 25.74 26.32 2.00 o 0 14 7 30.90 26.84 2.28 o 2 14 7 94.17 94.80 6.70 o 4 14 7 25.50 26.34 1.93 o 1 15 7 0.00 3.59 24.08 < 3 15 7 3.97 4.07 3.76 < 0 16 7 86.76 86.63 6.32 o 2 16 7 21.64 18.95 1.67 o 1 17 7 23.77 22.17 1.79 o 0 0 8 208.86 195.52 15.47 o 2 0 8 109.38 119.69 7.88 o 4 0 8 155.37 149.37 11.20 o 6 0 8 54.64 54.81 3.95 o 8 0 8 70.08 66.25 5.16 o 1 1 8 13.13 9.69 1.09 o 3 1 8 70.07 74.52 4.98 o 5 1 8 17.90 18.73 1.34 o 7 1 8 20.68 23.81 1.63 o 9 1 8 8.20 6.69 4.11 < 0 2 8 11.82 9.73 1.47 o 2 2 8 134.05 143.92 9.53 o 4 2 8 44.30 45.68 3.15 o 6 2 8 32.73 31.98 2.36 o 8 2 8 32.24 32.44 2.42 o 1 3 8 110.85 119.93 7.88 o 3 3 8 94.60 103.76 6.72 o 5 3 8 65.55 71.46 4.68 o 7 3 8 46.39 46.95 3.32 o 9 3 8 24.73 27.09 2.20 o 0 4 8 135.97 143.87 9.84 o 2 4 8 66.37 74.37 4.72 o 4 4 8 81.40 86.85 5.78 o 6 4 8 40.39 42.97 2.89 o 8 4 8 30.90 30.95 2.39 o 1 5 8 69.14 74.59 4.91 o 3 5 8 44.42 45.75 3.16 o 5 5 8 43.88 45.78 3.13 o 7 5 8 17.64 20.07 1.64 o 9 5 8 10.25 13.45 2.37 < 0 6 8 93.99 103.49 6.78 o 2 6 8 152.53 149.36 10.84 o 4 6 8 64.83 71.29 4.61 o 6 6 8 88.82 86.09 6.41 o 8 6 8 27.80 25.85 2.26 o 1 7 8 43.87 45.72 3.12 o 3 7 8 16.96 18.75 1.28 o 5 7 8 41.59 43.02 2.98 o 7 7 8 2.26 3.19 8.66 < 9 7 8 9.07 9.29 5.70 < 0 8 8 82.56 86.90 5.97 o 2 8 8 18.89 18.74 1.40 o 4 8 8 35.40 32.00 2.55 o 6 8 8 20.31 20.04 1.62 o 8 8 8 12.88 9.97 1.85 o 1 9 8 66.74 71.50 4.74 o 3 9 8 55.98 54.93 3.98 o 5 9 8 45.38 46.96 3.24 o 7 9 8 28.57 25.93 2.20 o 0 10 8 45.17 45.66 3.27 o 2 10 8 35.17 32.02 2.52 o 4 10 8 23.26 23.79 1.72 o 6 10 8 35.62 30.99 2.78 o 8 10 8 0.00 9.30 42.81 < 1 11 8 43.28 43.12 3.09 o 3 11 8 22.98 23.95 1.69 o 5 11 8 33.40 32.48 2.43 o 7 11 8 14.74 13.51 1.80 o 0 12 8 91.06 86.10 6.57 o 2 12 8 46.23 46.80 3.29 o 4 12 8 70.81 66.25 5.05 o 6 12 8 26.54 27.00 2.13 o 1 13 8 20.11 20.03 1.51 o 3 13 8 32.16 32.43 2.32 o 5 13 8 8.66 6.67 2.51 < 0 14 8 4.54 3.21 2.96 < 2 14 8 31.57 30.99 2.28 o 4 14 8 3.85 6.67 4.23 < 1 15 8 30.57 25.90 2.23 o 3 15 8 28.23 27.09 2.06 o 0 16 8 11.77 9.95 1.73 o 2 16 8 15.04 13.43 1.45 o 1 17 8 11.03 9.29 1.88 o 1 1 9 35.23 29.05 2.51 o 3 1 9 18.06 17.48 1.36 o 5 1 9 36.51 35.47 2.61 o 7 1 9 7.30 11.37 2.28 < 9 1 9 6.44 11.74 6.86 < 0 2 9 35.18 29.11 2.56 o 2 2 9 275.53 269.81 19.57 o 4 2 9 17.25 14.46 1.31 o 6 2 9 160.98 163.12 11.51 o 8 2 9 8.23 10.97 2.18 < 3 3 9 24.05 20.38 1.75 o 5 3 9 18.41 19.01 1.45 o 7 3 9 11.64 14.68 1.41 o 9 3 9 12.46 14.73 2.73 < 0 4 9 278.04 269.83 20.04 o 2 4 9 18.68 17.44 1.39 o 4 4 9 213.87 221.45 15.23 o 6 4 9 9.35 8.21 1.30 o 8 4 9 121.29 122.09 8.79 o 1 5 9 17.48 17.46 1.32 o 3 5 9 16.08 14.44 1.25 o 5 5 9 13.98 12.03 1.27 o 7 5 9 8.58 12.66 2.00 < 9 5 9 0.00 13.06 50.40 < 0 6 9 27.89 20.52 2.14 o 4 6 9 21.62 19.01 1.61 o 6 6 9 10.06 11.91 1.45 o 8 6 9 12.53 13.06 1.72 o 1 7 9 15.97 14.53 1.25 o 3 7 9 35.74 35.53 2.56 o 5 7 9 9.51 8.22 1.27 o 7 7 9 15.86 19.28 2.07 o 0 8 9 208.56 221.41 15.03 o 2 8 9 36.34 35.51 2.60 o 4 8 9 161.64 163.10 11.49 o 6 8 9 11.09 12.67 1.46 o 8 8 9 86.49 86.35 6.78 o 1 9 9 19.09 19.07 1.48 o 5 9 9 13.61 14.73 1.34 o 7 9 9 13.41 13.09 1.66 o 0 10 9 15.80 11.99 1.40 o 2 10 9 160.60 163.17 11.51 o 4 10 9 11.85 11.42 1.29 o 6 10 9 130.05 122.08 9.41 o 1 11 9 9.61 8.20 1.08 o 3 11 9 10.65 11.39 1.28 o 5 11 9 7.86 10.96 1.86 < 7 11 9 5.70 13.06 3.58 < 0 12 9 5.68 12.00 2.49 < 2 12 9 16.23 14.72 1.30 o 6 12 9 14.98 14.73 1.86 o 1 13 9 10.60 12.73 1.11 o 3 13 9 8.84 11.02 1.31 o 5 13 9 7.82 11.77 2.18 < 0 14 9 19.98 19.32 1.64 o 2 14 9 124.62 121.99 8.89 o 4 14 9 9.17 11.78 2.00 < 1 15 9 7.91 13.13 1.69 < 3 15 9 12.36 14.83 1.46 o 0 16 9 83.62 86.39 6.14 o 2 16 9 7.71 13.15 1.76 < 2 0 10 130.01 132.44 9.37 o 4 0 10 275.88 277.16 19.89 o 6 0 10 47.76 48.34 3.46 o 8 0 10 148.74 151.12 11.22 o 1 1 10 35.81 36.38 2.56 o 3 1 10 40.36 43.09 2.88 o 5 1 10 25.55 26.13 1.86 o 7 1 10 5.43 7.08 2.40 < 9 1 10 14.45 18.97 4.21 < 0 2 10 36.78 36.30 2.67 o 2 2 10 317.35 306.23 22.55 o 4 2 10 29.56 27.96 2.12 o 6 2 10 185.82 189.99 13.25 o 8 2 10 13.02 13.85 1.64 o 1 3 10 133.86 132.72 9.51 o 3 3 10 130.93 138.28 9.31 o 5 3 10 88.41 86.86 6.29 o 7 3 10 66.42 68.49 4.74 o 9 3 10 48.00 49.03 3.63 o 0 4 10 320.63 306.20 23.11 o 2 4 10 39.57 43.08 2.82 o 4 4 10 243.87 250.79 17.36 o 6 4 10 13.02 14.28 1.32 o 8 4 10 124.16 131.60 9.04 o 1 5 10 40.38 43.04 2.88 o 3 5 10 27.62 27.95 1.99 o 5 5 10 16.34 16.08 1.34 o 7 5 10 15.83 18.92 1.49 o 9 5 10 14.31 9.36 2.07 o 0 6 10 130.39 137.99 9.44 o 2 6 10 273.68 277.15 19.44 o 4 6 10 85.41 86.72 6.08 o 6 6 10 172.48 175.87 12.27 o 8 6 10 35.61 38.80 2.62 o 1 7 10 29.35 28.10 2.10 o 3 7 10 25.25 26.20 1.86 o 5 7 10 13.99 14.33 1.31 o 7 7 10 13.09 23.00 1.79 o 0 8 10 239.06 250.89 17.71 o 2 8 10 28.23 26.12 2.05 o 4 8 10 180.80 190.01 12.86 o 6 8 10 19.06 18.93 1.60 o 8 8 10 90.98 95.69 6.68 o 1 9 10 85.04 86.99 6.07 o 3 9 10 48.49 48.48 3.45 o 5 9 10 66.23 68.55 4.72 o 7 9 10 36.14 38.83 2.74 o 0 10 10 16.71 16.04 1.40 o 2 10 10 181.39 189.93 12.93 o 4 10 10 5.05 7.05 2.29 < 6 10 10 123.92 131.56 8.94 o 1 11 10 11.39 14.26 1.16 o 3 11 10 4.80 7.07 2.16 < 5 11 10 7.66 13.86 2.09 < 7 11 10 0.00 9.37 30.62 < 0 12 10 172.35 175.78 12.42 o 2 12 10 67.52 68.42 4.80 o 4 12 10 146.08 151.03 10.40 o 6 12 10 45.92 49.04 3.35 o 1 13 10 19.92 19.05 1.51 o 3 13 10 12.84 13.94 1.20 o 5 13 10 12.86 19.02 1.59 o 0 14 10 18.92 23.06 1.55 o 2 14 10 122.22 131.71 8.70 o 4 14 10 17.17 19.01 1.63 o 1 15 10 38.06 38.86 2.74 o 3 15 10 46.44 49.09 3.33 o 0 16 10 89.03 95.62 6.45 o 2 16 10 10.25 9.42 1.95 < 1 1 11 88.63 90.15 6.30 o 3 1 11 68.41 67.86 4.86 o 5 1 11 67.44 68.98 4.80 o 7 1 11 37.33 40.24 2.69 o 9 1 11 36.69 35.00 3.12 o 0 2 11 84.01 89.86 6.06 o 2 2 11 313.01 306.61 22.24 o 4 2 11 67.43 67.16 4.79 o 6 2 11 203.47 206.96 14.53 o 8 2 11 38.15 37.95 2.77 o 3 3 11 19.59 22.11 1.46 o 5 3 11 12.59 15.69 1.33 o 7 3 11 12.93 15.73 1.49 o 9 3 11 10.07 11.43 3.63 < 0 4 11 312.69 306.57 22.54 o 2 4 11 68.58 67.72 4.87 o 4 4 11 243.32 252.33 17.29 o 6 4 11 45.91 44.83 3.28 o 8 4 11 140.05 144.50 10.00 o 1 5 11 68.73 67.88 4.88 o 3 5 11 68.25 67.33 4.85 o 5 5 11 46.21 46.02 3.30 o 7 5 11 44.22 45.85 3.17 o 9 5 11 18.68 23.65 2.51 o 0 6 11 20.87 22.04 1.61 o 4 6 11 13.21 15.69 1.30 o 6 6 11 1.14 12.09 11.23 < 8 6 11 0.00 9.02 32.86 < 1 7 11 65.70 67.40 4.67 o 3 7 11 67.46 69.03 4.80 o 5 7 11 46.84 44.92 3.34 o 7 7 11 40.17 39.70 2.95 o 0 8 11 244.71 252.35 17.64 o 2 8 11 67.88 68.78 4.82 o 4 8 11 202.54 206.94 14.41 o 6 8 11 44.90 45.77 3.24 o 8 8 11 112.82 121.42 8.22 o 1 9 11 14.09 15.81 1.21 o 5 9 11 14.10 15.78 1.44 o 7 9 11 2.02 9.03 11.11 < 0 10 11 45.74 45.97 3.31 o 2 10 11 195.43 206.91 13.91 o 4 10 11 37.50 40.22 2.68 o 6 10 11 136.22 144.48 9.82 o 1 11 11 46.55 44.83 3.32 o 3 11 11 38.99 40.18 2.79 o 5 11 11 39.08 37.97 2.81 o 7 11 11 19.11 23.62 3.45 o 0 12 11 0.00 12.11 25.35 < 2 12 11 14.53 15.69 1.27 o 6 12 11 0.00 11.44 33.02 < 1 13 11 44.85 45.95 3.20 o 3 13 11 38.97 38.08 2.79 o 5 13 11 34.20 35.05 2.53 o 0 14 11 40.82 39.66 2.97 o 2 14 11 138.07 144.40 9.84 o 4 14 11 32.79 34.99 2.40 o 1 15 11 3.85 9.07 3.18 < 3 15 11 0.00 11.51 26.36 < 0 16 11 114.78 121.41 8.31 o 2 16 11 18.35 23.68 1.98 o 0 0 12 343.56 321.28 25.45 o 2 0 12 28.60 25.77 2.11 o 4 0 12 264.70 261.65 19.08 o 6 0 12 24.21 22.36 1.95 o 8 0 12 135.43 136.28 9.94 o 1 1 12 113.14 125.84 8.04 o 3 1 12 94.41 106.72 6.71 o 5 1 12 72.67 73.82 5.18 o 7 1 12 53.60 57.14 3.82 o 9 1 12 22.89 25.31 2.63 o 0 2 12 106.48 125.51 7.71 o 2 2 12 29.03 31.42 2.08 o 4 2 12 73.70 73.36 5.26 o 6 2 12 13.09 15.97 1.36 o 8 2 12 23.59 27.07 1.90 o 1 3 12 28.34 25.84 2.04 o 3 3 12 28.67 25.65 2.06 o 5 3 12 26.91 24.32 1.98 o 7 3 12 25.47 23.72 1.91 o 9 3 12 22.32 19.92 2.45 o 0 4 12 29.59 31.40 2.17 o 2 4 12 97.60 106.47 6.94 o 4 4 12 19.68 16.43 1.52 o 6 4 12 44.36 48.28 3.17 o 8 4 12 12.81 16.10 2.26 o 1 5 12 95.30 106.81 6.81 o 3 5 12 75.78 73.61 5.40 o 5 5 12 72.65 75.07 5.17 o 7 5 12 34.81 37.48 2.54 o 0 6 12 29.44 25.60 2.17 o 2 6 12 260.21 261.71 18.49 o 4 6 12 27.14 24.26 1.98 o 6 6 12 170.25 168.44 12.10 o 8 6 12 19.89 19.18 1.82 o 1 7 12 74.15 73.47 5.28 o 3 7 12 75.09 73.75 5.34 o 5 7 12 46.73 48.33 3.33 o 7 7 12 29.56 29.68 2.34 o 0 8 12 18.82 16.43 1.54 o 2 8 12 72.76 73.62 5.18 o 4 8 12 15.04 15.96 1.33 o 6 8 12 34.07 37.35 2.47 o 8 8 12 15.80 16.31 1.84 o 1 9 12 27.31 24.35 1.98 o 3 9 12 24.19 22.43 1.80 o 5 9 12 24.80 23.75 1.85 o 7 9 12 21.06 19.23 1.86 o 0 10 12 70.45 74.87 5.08 o 2 10 12 15.61 15.91 1.30 o 4 10 12 54.00 57.05 3.86 o 6 10 12 17.32 16.06 1.76 o 1 11 12 46.97 48.49 3.35 o 3 11 12 54.91 57.24 3.91 o 5 11 12 24.95 27.20 1.89 o 0 12 12 162.38 168.56 11.71 o 2 12 12 26.95 23.70 1.95 o 4 12 12 129.95 136.36 9.25 o 6 12 12 21.14 19.89 2.04 o 1 13 12 37.03 37.39 2.65 o 3 13 12 25.76 27.08 1.90 o 5 13 12 27.13 25.27 2.21 o 0 14 12 28.27 29.59 2.09 o 2 14 12 17.59 16.13 1.38 o 4 14 12 24.29 25.23 1.88 o 1 15 12 22.24 19.21 1.71 o 3 15 12 21.63 19.95 1.67 o 0 16 12 13.84 16.25 1.62 o 1 1 13 32.15 34.49 2.30 o 3 1 13 27.29 27.78 1.98 o 5 1 13 27.79 27.97 2.05 o 7 1 13 15.48 16.03 1.39 o 9 1 13 16.80 15.08 2.94 o 0 2 13 31.96 34.37 2.34 o 2 2 13 19.29 16.76 1.44 o 4 2 13 47.84 45.61 3.41 o 6 2 13 11.97 12.32 1.41 o 8 2 13 31.99 33.12 2.37 o 3 3 13 69.11 74.62 4.91 o 5 3 13 25.04 25.25 1.85 o 7 3 13 26.69 26.32 2.02 o 0 4 13 19.59 16.73 1.55 o 2 4 13 27.68 27.70 1.99 o 4 4 13 5.70 7.22 2.13 < 6 4 13 33.92 34.16 2.45 o 8 4 13 11.05 14.09 2.29 < 1 5 13 28.09 27.82 2.03 o 3 5 13 47.90 45.77 3.41 o 5 5 13 16.93 19.16 1.46 o 7 5 13 21.64 24.51 1.77 o 0 6 13 68.30 74.59 4.93 o 4 6 13 26.26 25.24 1.94 o 6 6 13 27.57 30.97 2.09 o 8 6 13 3.36 4.68 6.33 < 1 7 13 46.96 45.68 3.34 o 3 7 13 28.29 27.96 2.09 o 5 7 13 34.79 34.22 2.51 o 7 7 13 19.26 21.92 1.86 o 0 8 13 8.17 7.19 1.84 < 2 8 13 28.08 27.88 2.04 o 4 8 13 13.45 12.30 1.37 o 6 8 13 22.56 24.45 1.83 o 1 9 13 25.90 25.29 1.89 o 5 9 13 26.57 26.35 1.98 o 7 9 13 7.91 4.70 4.34 < 0 10 13 18.09 19.15 1.54 o 2 10 13 11.40 12.36 1.24 o 4 10 13 15.77 15.97 1.39 o 6 10 13 11.56 14.13 2.05 o 1 11 13 35.33 34.27 2.53 o 3 11 13 16.35 15.99 1.34 o 5 11 13 30.17 33.20 2.26 o 0 12 13 28.75 30.96 2.16 o 2 12 13 26.66 26.35 1.94 o 1 13 13 22.90 24.50 1.69 o 3 13 13 30.28 33.14 2.19 o 5 13 13 18.21 15.09 2.38 o 0 14 13 21.20 21.90 1.70 o 2 14 13 13.15 14.09 1.31 o 4 14 13 14.41 15.05 1.85 o 1 15 13 5.39 4.67 2.02 < 0 0 14 261.03 248.92 19.34 o 2 0 14 50.77 52.88 3.79 o 4 0 14 206.03 198.97 14.86 o 6 0 14 26.55 27.33 2.04 o 8 0 14 104.61 107.82 7.68 o 1 1 14 47.34 52.82 3.38 o 3 1 14 42.95 46.41 3.08 o 5 1 14 29.06 28.13 2.14 o 7 1 14 19.59 18.31 1.58 o 0 2 14 46.39 52.65 3.40 o 2 2 14 37.23 43.05 2.66 o 4 2 14 53.13 51.57 3.79 o 6 2 14 9.74 9.80 1.60 o 8 2 14 28.45 29.42 2.17 o 1 3 14 51.47 53.01 3.68 o 3 3 14 50.44 44.47 3.60 o 5 3 14 34.13 33.48 2.46 o 7 3 14 23.13 23.46 1.81 o 0 4 14 36.62 43.05 2.67 o 2 4 14 48.03 46.25 3.44 o 4 4 14 8.48 12.83 1.77 < 6 4 14 37.34 36.16 2.69 o 8 4 14 11.26 16.11 2.34 < 1 5 14 46.02 46.41 3.28 o 3 5 14 54.80 51.67 3.92 o 5 5 14 25.15 21.75 1.88 o 7 5 14 23.63 22.74 1.88 o 0 6 14 50.62 44.35 3.67 o 2 6 14 208.68 198.95 14.83 o 4 6 14 34.43 33.38 2.49 o 6 6 14 129.56 130.52 9.22 o 8 6 14 13.98 11.96 2.00 o 1 7 14 53.12 51.64 3.78 o 3 7 14 28.79 28.10 2.12 o 5 7 14 35.84 36.22 2.59 o 7 7 14 13.47 14.62 1.86 o 0 8 14 12.63 12.93 1.43 o 2 8 14 28.42 28.11 2.07 o 4 8 14 13.25 9.74 1.34 o 6 8 14 21.23 22.78 1.77 o 1 9 14 35.27 33.49 2.53 o 3 9 14 28.32 27.41 2.05 o 5 9 14 22.43 23.47 1.76 o 7 9 14 12.37 12.00 1.82 o 0 10 14 27.46 21.67 2.06 o 2 10 14 12.32 9.74 1.24 o 4 10 14 20.78 18.25 1.60 o 6 10 14 15.89 16.04 1.92 o 1 11 14 37.98 36.25 2.72 o 3 11 14 21.66 18.31 1.63 o 5 11 14 29.95 29.43 2.23 o 0 12 14 130.16 130.47 9.38 o 2 12 14 23.17 23.38 1.70 o 4 12 14 103.89 107.79 7.38 o 1 13 14 20.10 22.71 1.53 o 3 13 14 29.62 29.39 2.16 o 0 14 14 10.30 14.66 1.70 o 2 14 14 16.28 16.03 1.39 o 1 15 14 8.82 11.98 1.47 o 1 1 15 33.70 35.30 2.41 o 3 1 15 26.98 26.93 1.97 o 5 1 15 25.36 25.15 1.89 o 7 1 15 16.83 17.38 1.48 o 0 2 15 32.75 35.19 2.40 o 2 2 15 189.58 184.47 13.47 o 4 2 15 39.47 37.97 2.83 o 6 2 15 138.41 138.96 9.84 o 8 2 15 27.70 29.83 2.16 o 3 3 15 20.60 6.47 1.61 o 5 3 15 15.52 15.11 1.38 o 7 3 15 10.50 11.88 1.70 o 0 4 15 186.28 184.45 13.43 o 2 4 15 28.43 26.88 2.07 o 4 4 15 170.06 164.06 12.09 o 6 4 15 31.28 31.23 2.29 o 8 4 15 100.45 102.96 7.15 o 1 5 15 27.96 26.98 2.04 o 3 5 15 38.76 38.04 2.78 o 5 5 15 14.30 14.43 1.46 o 7 5 15 21.30 22.02 1.78 o 0 6 15 22.02 6.50 1.76 o 4 6 15 18.11 15.07 1.52 o 6 6 15 0.00 8.58 29.71 < 1 7 15 39.38 38.03 2.82 o 3 7 15 27.65 25.16 2.02 o 5 7 15 30.63 31.23 2.22 o 7 7 15 14.20 16.62 2.10 o 0 8 15 167.48 164.02 12.07 o 2 8 15 26.44 25.11 1.93 o 4 8 15 140.27 138.94 9.98 o 6 8 15 20.45 22.01 1.84 o 1 9 15 16.00 15.13 1.33 o 5 9 15 10.50 11.91 1.88 o 0 10 15 14.75 14.38 1.50 o 2 10 15 137.81 138.99 9.81 o 4 10 15 17.30 17.39 1.46 o 6 10 15 100.84 102.98 7.21 o 1 11 15 32.05 31.24 2.31 o 3 11 15 15.53 17.43 1.33 o 5 11 15 28.85 29.83 2.14 o 0 12 15 8.13 8.62 2.04 < 2 12 15 11.57 11.93 1.24 o 1 13 15 21.55 22.08 1.63 o 3 13 15 28.58 29.90 2.08 o 0 14 15 14.02 16.60 1.49 o 2 14 15 100.95 102.89 7.18 o 0 0 16 132.88 111.56 9.85 o 2 0 16 114.45 108.53 8.25 o 4 0 16 133.58 121.39 9.63 o 6 0 16 85.97 89.48 6.20 o 8 0 16 91.22 94.63 6.69 o 1 1 16 24.79 23.32 1.83 o 3 1 16 10.22 9.40 1.39 o 5 1 16 15.28 15.12 1.42 o 7 1 16 1.67 3.44 8.73 < 0 2 16 25.95 23.39 2.01 o 2 2 16 192.56 188.52 13.68 o 4 2 16 10.62 13.45 1.48 o 6 2 16 119.48 121.84 8.49 o 8 2 16 3.26 9.13 7.47 < 1 3 16 111.74 108.80 7.94 o 3 3 16 92.48 84.84 6.59 o 5 3 16 82.90 78.72 5.89 o 7 3 16 46.34 47.74 3.31 o 0 4 16 182.41 188.46 13.15 o 2 4 16 9.66 9.42 1.48 o 4 4 16 153.78 148.19 10.93 o 6 4 16 6.41 8.15 2.60 < 8 4 16 75.47 79.87 5.40 o 1 5 16 11.04 9.39 1.39 o 3 5 16 10.96 13.43 1.44 o 5 5 16 0.00 2.19 27.20 < 7 5 16 8.07 7.22 2.48 < 0 6 16 90.01 84.57 6.49 o 2 6 16 134.18 121.37 9.53 o 4 6 16 80.43 78.57 5.72 o 6 6 16 108.70 107.44 7.72 o 1 7 16 15.28 13.50 1.36 o 3 7 16 17.70 15.18 1.47 o 5 7 16 5.42 8.17 2.62 < 7 7 16 0.00 8.97 41.83 < 0 8 16 150.94 148.27 10.88 o 2 8 16 15.39 15.11 1.36 o 4 8 16 119.78 121.86 8.51 o 6 8 16 8.81 7.22 2.60 < 1 9 16 83.40 78.81 5.93 o 3 9 16 87.81 89.63 6.24 o 5 9 16 46.56 47.80 3.34 o 0 10 16 1.73 2.20 10.28 < 2 10 16 121.51 121.75 8.64 o 4 10 16 4.82 3.46 3.12 < 6 10 16 74.07 79.85 5.28 o 1 11 16 5.43 8.18 1.98 < 3 11 16 0.00 3.45 24.85 < 5 11 16 8.56 9.18 2.25 < 0 12 16 110.53 107.40 8.00 o 2 12 16 45.11 47.61 3.22 o 4 12 16 91.57 94.63 6.51 o 1 13 16 10.90 7.25 1.31 o 3 13 16 8.40 9.13 1.72 < 0 14 16 8.40 8.94 2.07 < 2 14 16 73.42 79.98 5.23 o 1 1 17 57.31 52.51 4.08 o 3 1 17 59.71 59.30 4.25 o 5 1 17 36.19 37.20 2.61 o 7 1 17 28.78 29.50 2.12 o 0 2 17 57.97 52.31 4.19 o 2 2 17 116.77 109.47 8.30 o 4 2 17 55.85 52.80 3.98 o 6 2 17 89.64 88.83 6.37 o 8 2 17 33.33 37.73 2.44 o 3 3 17 18.46 18.95 1.55 o 5 3 17 8.42 8.84 1.72 < 7 3 17 5.27 9.16 3.33 < 0 4 17 114.31 109.49 8.28 o 2 4 17 62.40 59.12 4.44 o 4 4 17 101.08 93.59 7.18 o 6 4 17 42.57 42.51 3.05 o 1 5 17 60.11 59.29 4.28 o 3 5 17 56.96 52.92 4.05 o 5 5 17 40.24 40.88 2.89 o 7 5 17 33.48 35.83 2.47 o 0 6 17 20.06 19.02 1.72 o 4 6 17 7.78 8.89 1.85 < 6 6 17 8.26 12.72 2.29 < 1 7 17 56.65 52.98 4.03 o 3 7 17 38.07 37.24 2.73 o 5 7 17 43.26 42.62 3.09 o 7 7 17 23.71 25.19 2.12 o 0 8 17 101.30 93.57 7.33 o 2 8 17 36.76 37.08 2.64 o 4 8 17 91.13 88.82 6.48 o 6 8 17 34.17 35.76 2.51 o 1 9 17 7.78 8.83 1.60 < 5 9 17 10.21 9.14 1.84 o 0 10 17 43.64 40.75 3.19 o 2 10 17 90.94 88.82 6.46 o 4 10 17 30.49 29.41 2.22 o 1 11 17 43.38 42.58 3.10 o 3 11 17 28.46 29.47 2.07 o 5 11 17 34.81 37.77 2.63 o 0 12 17 6.81 12.69 2.56 < 2 12 17 5.51 9.18 2.29 < 1 13 17 33.16 35.89 2.38 o 3 13 17 34.76 37.82 2.54 o 0 14 17 23.74 25.10 1.86 o 0 0 18 125.95 116.13 9.34 o 2 0 18 12.81 17.01 1.57 o 4 0 18 89.05 84.03 6.42 o 6 0 18 9.01 7.90 2.21 < 1 1 18 100.71 95.81 7.16 o 3 1 18 54.41 50.06 3.87 o 5 1 18 73.40 74.08 5.22 o 7 1 18 31.86 32.16 2.33 o 0 2 18 100.53 95.60 7.25 o 2 2 18 39.09 39.30 2.80 o 4 2 18 55.03 51.35 3.93 o 6 2 18 34.17 39.29 2.47 o 1 3 18 12.18 17.05 1.33 o 3 3 18 15.59 17.48 1.47 o 5 3 18 12.77 13.20 1.43 o 7 3 18 15.07 13.16 1.66 o 0 4 18 39.72 39.33 2.90 o 2 4 18 55.08 49.95 3.92 o 4 4 18 30.29 30.28 2.20 o 6 4 18 25.99 24.84 1.96 o 1 5 18 53.69 50.10 3.82 o 3 5 18 55.42 51.48 3.95 o 5 5 18 30.83 30.54 2.25 o 7 5 18 24.03 25.60 1.96 o 0 6 18 18.01 17.41 1.73 o 2 6 18 91.07 84.06 6.48 o 4 6 18 13.71 13.14 1.42 o 6 6 18 47.21 48.38 3.40 o 1 7 18 55.11 51.49 3.92 o 3 7 18 74.76 74.12 5.32 o 5 7 18 26.69 24.90 1.98 o 0 8 18 30.43 30.26 2.29 o 2 8 18 74.75 73.89 5.31 o 4 8 18 35.35 39.29 2.54 o 6 8 18 24.40 25.54 1.98 o 1 9 18 14.05 13.16 1.32 o 3 9 18 8.58 7.90 1.62 < 5 9 18 16.07 13.14 1.53 o 0 10 18 32.02 30.43 2.38 o 2 10 18 35.42 39.33 2.54 o 4 10 18 32.85 32.09 2.38 o 1 11 18 25.57 24.91 1.87 o 3 11 18 31.63 32.16 2.29 o 0 12 18 48.47 48.45 3.51 o 2 12 18 13.86 13.11 1.33 o 1 13 18 24.23 25.66 1.79 o 1 1 19 16.08 15.01 1.41 o 3 1 19 19.75 20.65 1.56 o 5 1 19 7.47 7.35 2.21 < 7 1 19 3.52 8.53 4.83 < 0 2 19 20.13 14.96 1.69 o 2 2 19 75.91 75.29 5.40 o 4 2 19 19.12 16.23 1.61 o 6 2 19 35.60 40.30 2.57 o 3 3 19 14.38 3.79 1.43 o 5 3 19 10.01 8.71 1.70 o 7 3 19 6.36 4.69 2.80 < 0 4 19 75.03 75.25 5.41 o 2 4 19 21.13 20.58 1.64 o 4 4 19 56.43 56.73 4.02 o 6 4 19 13.40 13.39 1.64 o 1 5 19 20.29 20.65 1.60 o 3 5 19 17.30 16.29 1.52 o 5 5 19 13.20 13.64 1.46 o 0 6 19 15.36 3.80 1.73 o 4 6 19 12.05 8.67 1.49 o 6 6 19 6.64 9.21 3.37 < 1 7 19 15.44 16.22 1.39 o 3 7 19 9.50 7.31 1.56 o 5 7 19 12.80 13.40 1.56 o 0 8 19 55.80 56.81 4.05 o 2 8 19 7.86 7.32 1.76 < 4 8 19 37.03 40.33 2.66 o 1 9 19 9.78 8.69 1.45 o 5 9 19 8.89 4.70 1.93 < 0 10 19 12.43 13.59 1.56 o 2 10 19 36.77 40.32 2.64 o 4 10 19 7.56 8.49 1.89 < 1 11 19 12.70 13.46 1.36 o 3 11 19 7.73 8.50 1.80 < 0 12 19 5.97 9.27 2.80 < 2 12 19 8.54 4.71 1.59 < 0 0 20 211.76 198.30 15.69 o 2 0 20 21.68 23.08 1.78 o 4 0 20 162.50 157.60 11.71 o 6 0 20 4.25 8.30 4.99 < 1 1 20 53.79 45.96 3.83 o 3 1 20 51.89 49.06 3.70 o 5 1 20 26.90 23.25 1.99 o 7 1 20 21.88 26.13 1.76 o 0 2 20 53.72 45.80 3.89 o 2 2 20 10.68 7.93 1.57 o 4 2 20 34.55 32.42 2.51 o 6 2 20 10.52 12.79 1.63 o 1 3 20 22.63 23.07 1.71 o 3 3 20 16.53 18.03 1.46 o 5 3 20 10.09 11.35 1.63 o 0 4 20 12.33 7.91 1.82 o 2 4 20 49.94 48.91 3.56 o 4 4 20 7.40 8.24 2.05 < 6 4 20 22.12 24.80 1.79 o 1 5 20 49.72 49.09 3.54 o 3 5 20 38.22 32.54 2.75 o 5 5 20 32.84 35.99 2.39 o 0 6 20 17.55 18.05 1.71 o 2 6 20 163.98 157.63 11.65 o 4 6 20 11.38 11.37 1.47 o 6 6 20 89.80 103.43 6.38 o 1 7 20 35.52 32.49 2.55 o 3 7 20 27.63 23.20 2.03 o 5 7 20 22.93 24.86 1.80 o 0 8 20 6.83 8.21 2.69 < 2 8 20 27.60 23.18 2.02 o 4 8 20 10.04 12.73 1.62 o 1 9 20 9.84 11.32 1.44 o 3 9 20 9.41 8.26 1.60 o 0 10 20 34.56 35.88 2.55 o 2 10 20 14.01 12.72 1.36 o 4 10 20 24.25 26.07 1.94 o 1 11 20 23.48 24.90 1.76 o 3 11 20 23.46 26.17 1.90 o 0 12 20 89.54 103.43 6.46 o 1 1 21 46.14 40.31 3.30 o 3 1 21 49.09 45.70 3.50 o 5 1 21 26.68 28.75 1.98 o 0 2 21 45.10 40.16 3.28 o 2 2 21 132.89 126.81 9.45 o 4 2 21 26.13 27.05 1.95 o 6 2 21 71.29 77.01 5.07 o 3 3 21 9.25 5.55 1.68 < 5 3 21 6.39 9.19 2.38 < 0 4 21 133.14 126.83 9.60 o 2 4 21 47.75 45.58 3.40 o 4 4 21 87.26 89.48 6.21 o 6 4 21 14.62 17.47 1.62 o 1 5 21 48.39 45.75 3.45 o 3 5 21 27.75 27.15 2.05 o 5 5 21 36.87 39.74 2.67 o 0 6 21 6.62 5.58 3.09 < 4 6 21 8.92 9.18 1.75 < 1 7 21 26.40 27.13 1.95 o 3 7 21 27.30 28.76 2.01 o 5 7 21 17.04 17.51 1.58 o 0 8 21 82.59 89.47 5.96 o 2 8 21 26.53 28.65 1.95 o 4 8 21 71.08 77.00 5.07 o 1 9 21 4.07 9.22 3.46 < 0 10 21 36.70 39.62 2.69 o 2 10 21 72.68 77.05 5.17 o 1 11 21 15.60 17.52 1.39 o 0 0 22 38.25 33.85 3.01 o 2 0 22 83.40 80.07 6.02 o 4 0 22 37.20 35.65 2.74 o 6 0 22 46.68 52.14 3.42 o 1 1 22 5.25 8.47 2.81 < 3 1 22 0.00 7.52 26.27 < 5 1 22 6.79 5.88 2.30 < 0 2 22 5.05 8.53 3.70 < 2 2 22 110.25 104.09 7.83 o 4 2 22 11.22 11.66 1.60 o 6 2 22 52.19 57.13 3.73 o 1 3 22 86.29 80.33 6.13 o 3 3 22 71.86 68.37 5.11 o 5 3 22 53.18 55.79 3.80 o 0 4 22 111.95 104.10 8.07 o 2 4 22 5.18 7.55 2.86 < 4 4 22 73.88 74.58 5.26 o 1 5 22 5.32 7.52 2.76 < 3 5 22 8.43 11.62 1.92 < 5 5 22 10.38 9.68 1.96 < 0 6 22 71.75 68.13 5.18 o 2 6 22 35.69 35.64 2.57 o 4 6 22 53.39 55.61 3.80 o 1 7 22 9.30 11.63 1.63 o 3 7 22 7.16 5.88 2.04 < 0 8 22 71.20 74.60 5.14 o 2 8 22 4.52 5.92 2.95 < 4 8 22 52.63 57.16 3.79 o 1 9 22 53.00 55.79 3.78 o 3 9 22 48.34 52.29 3.46 o 0 10 22 9.78 9.65 2.07 < 2 10 22 52.96 57.13 3.79 o 1 1 23 35.75 31.06 2.56 o 3 1 23 28.16 24.78 2.07 o 5 1 23 26.41 26.62 1.98 o 0 2 23 36.90 30.94 2.71 o 2 2 23 24.12 19.53 1.80 o 4 2 23 34.06 30.71 2.46 o 3 3 23 27.42 26.37 2.01 o 5 3 23 9.32 11.36 1.81 < 0 4 23 23.61 19.57 1.91 o 2 4 23 28.67 24.67 2.10 o 4 4 23 23.89 22.41 1.82 o 1 5 23 28.24 24.73 2.07 o 3 5 23 31.41 30.77 2.28 o 0 6 23 28.87 26.40 2.21 o 4 6 23 12.47 11.35 1.55 o 1 7 23 33.24 30.85 2.40 o 3 7 23 25.42 26.66 1.90 o 0 8 23 23.44 22.39 1.88 o 2 8 23 25.54 26.53 1.91 o 1 9 23 11.29 11.33 1.47 o 0 10 23 7.89 14.17 7.92 < 0 0 24 42.19 33.43 3.18 o 2 0 24 8.43 11.22 2.39 < 4 0 24 26.82 20.48 2.20 o 1 1 24 42.10 32.40 3.01 o 3 1 24 37.99 32.57 2.73 o 5 1 24 24.50 21.87 1.88 o 0 2 24 41.73 32.35 3.04 o 2 2 24 47.81 48.55 3.41 o 4 2 24 28.61 24.03 2.11 o 1 3 24 10.27 11.21 1.48 o 3 3 24 0.00 7.02 27.29 < 0 4 24 48.72 48.57 3.53 o 2 4 24 39.05 32.56 2.81 o 4 4 24 34.91 40.40 2.53 o 1 5 24 39.25 32.62 2.81 o 3 5 24 28.93 24.09 2.13 o 0 6 24 5.06 7.01 4.03 < 2 6 24 27.71 20.50 2.04 o 1 7 24 29.11 24.08 2.12 o 3 7 24 24.82 21.91 2.04 o 0 8 24 33.66 40.33 2.50 o 2 8 24 23.85 21.80 1.98 o 1 1 25 6.46 5.02 1.99 < 3 1 25 8.86 10.62 1.84 < 0 2 25 7.46 5.03 2.56 < 2 2 25 36.18 43.43 2.60 o 4 2 25 8.43 5.60 1.99 < 3 3 25 6.84 4.96 2.34 < 0 4 25 36.71 43.40 2.69 o 2 4 25 10.16 10.61 1.72 o 1 5 25 12.00 10.61 1.48 o 3 5 25 7.14 5.59 2.40 < 0 6 25 10.12 4.94 2.31 < 1 7 25 0.00 5.63 28.33 < 0 0 26 63.61 62.04 4.74 o 2 0 26 9.20 12.65 2.73 < 1 1 26 30.66 27.90 2.22 o 3 1 26 34.32 35.26 2.48 o 0 2 26 29.42 27.80 2.25 o 2 2 26 13.82 11.78 1.38 o 1 3 26 7.61 12.57 2.12 < 3 3 26 12.93 17.15 2.05 o 0 4 26 12.13 11.80 1.86 o 2 4 26 32.89 35.17 2.39 o 1 5 26 33.84 35.28 2.45 o 0 6 26 0.00 17.24 59.90 < 1 1 27 19.38 20.16 1.57 o 0 2 27 18.87 20.08 1.89 o